Topic:

Thermogravimetry TGA Spectra

Submitted by:

Akmal Javed Abid

Fa-2018/M.phill CHEM./02)

Akmaljaved226@gmail.com

Submitted to:

Dr Shabbir Hussain

dr.shabbirhussain@lgu.edu.pk

2019-20

Lahore Garrison University, Lahore.

 Sample ID ID55 Compound Temperature Range 53.628 °C - 800 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 97.9815 81.6195 18.36
2 Sn 118.71 1 118.71 Calculated original Mass 830.42
3 C 12 2 24 Calculated Evolve Mass 691.7475767
4 Phenyl 77 6 462 Calculated Residue Mass 155.6060195
5 CH2 14 2 28
6 NH 15 1 15
7 O 16 4 64
8
9 Result:
10 Practical Obtained 18.14864767
Total Caculated original Mass 830.42
Expected Evolve Compound Data Expected Residue Data
Sr # Evolve Components As a NO. Mass Total Mass Residue As No. Mass
1 Sn Sn 1 118.71 118.71 Sn SnO2 1 150.71
2 Phenyl C6H5 6 77 462
3 Carbon & Oxygen CO 2 28 56
4 Methylene C2H4 1 28 28 Total Residue Mass 150.71
5 N 1/2N2 1 14 14 Back Calulations:
6 H 1/2H2 1 1 1 Total Evolve Mass 679.71
Total Residual Mass 150.71
Total Mass 830.42
Impurity 0
Total Evolve Mass 679.71
 Sample ID ID66 Compound Temperature Range 45.151 °C - 731.177 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 97.8748 80.6924 17.1824
2 Sn 118.71 1 118.71 Calculated original Mass 747.32
3 Cl 35.45 2 70.9 Calculated Evolve Mass 616.1243177
4 Phenyl 77 4 308 Calculated Residue Mass 131.1956823
5 CH2 14 2 28
6 NH 15 1 15
7 O 16 4 64 Result:
8 C 12 2 24 Practical Obtained 18.02574533
9
10
Total Caculated original Mass 747.32
Expected Evolve Compound Data Expected Residue Data
Sr # Evolve Components As a NO. Mass Total Mass Residue As No. Mass
1 Sn & Chlorine SnCl2 1 189.61 189.61 Sn SnO 1 134.71
2 Carbon & Oxygen CO 1 28 28
3 Carbon & Oxygen CO2 1 44 44
4 Methylene C2H4 1 28 28 Total Residue Mass 134.71
5 Phenyl C6H5 4 77 308 Back Calulations:
6 N 1/2N2 1 14 14 Total Evolve Mass 612.61
7 H 1/2H2 1 1 1 Total Residual Mass 134.71
Total Mass 747.32
Impurity 0
Total Evolve Mass 612.61
 First Residue
Sample ID He1d Compound Temperature Range 51.609 °C - 379.202 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 100 57.0688 42.9312
2 Pd 106.42 1 106.42 Calculated original Mass 545.03
3 Cl 35.45 2 70.9 Calculated Evolve Mass 311.0420806
4 CH3 15 3 45 Calculated Residue Mass 233.9879194
5 CH2 14 6 84
6 S 32 2 64
7 N 14 2 28
8 C 12 1 12
9 O 16 1 16 Result:
10 Practical Obtained 43.58842633
Total Caculated original Mass 545.03
Expected Evolve Compound Data Expected Residue Data
Sr # Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
1 Tin 1/2SnCl4 1 130.2 130.2 Pd PdS2 1 170.42
2 Methyl CH3- 2 15 30 Sn 1/2MeSn 1 67.15
3 Carbon C 1 12 12
4 Methylene C2H4 3 28 84 Total Residue Mass 237.57
5 N N2 1 28 28 Back Calulations:
6 O 1/2O2 1 16 16 Total Evolve Mass 308
7 Methyl 1/2Me 1 7.8 7.8 Total Residual Mass 237.57
Total Mass 545.57
Impurity -0.54
Total Evolve Mass 308

Second Residue
Sample ID He1d Compound Temperature Range 338.392 °C - 800 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 46.46 15.2081 31.2563
2 Calculated original Mass 253.220938
3 Calculated Evolve Mass 82.88870743
4 Calculated Residue Mass 170.3562119
5
6
7
8
9 Result:
10 Practical Obtained 31.2680036
Total Caculated original Mass 0
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Sn 1/2MeSn 1 67.15 67.15 Pd PdS2 1 170.42
1 H2O H2O 1 18 18
2
3 Total Residue Mass 170.42
4 Back Calulations:
5 Total Evolve Mass 85.15
6 Total Residual Mass 170.42
7 Total Mass 255.57
Impurity -2.349062
Total Evolve Mass 85.15
 First Residue
Sample ID HE4d Compound Temperature Range 51.609 °C - 379.202 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 99.902 48.4947 51.4055
2 Pd 106.42 1 106.42 Calculated original Mass 649.48
3 Cl 35.45 3 106.35 Calculated Evolve Mass 315.2723445
4 Butyl 57 2 114 Calculated Residue Mass 334.1959534
5 CH2 14 6 84
6 S 32 2 64
7 N 14 2 28
8 C 12 1 12
9 O 16 1 16 Result:
10 Practical Obtained 50.5050194
Total Caculated original Mass 649.48
Expected Evolve Compound Data Expected Residue Data
ExpectedEvolve
EvolveCompound
Compound Data As a NO. Mass Total Mass Residue As No. Mass
Sr # Chlorine ClO 1 51.5 51.5 Pd PdS 1 138.42
1 Methylene C2H4 3 28 84 Sn SnCl2 1 189.6
2 Carbon & Sulfur CS 1 44 44
3 Methylene CH2 1 14 14 Total Residue Mass 328.02
4 Butyl C4H7 2 57 114 Back Calulations:
5 Total Evolve Mass 307.5
6 Total Residual Mass 328.02
7 Total Mass 635.52
Impurity 13.96
Total Evolve Mass 307.5

Second Residue
Sample ID HE5d Compound Temperature Range 338.392 °C - 800 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
 1 51.4055 29.9897 21.467
2 Calculated original Mass 328.02
3 Calculated Evolve Mass 191.3651534
4 Calculated Residue Mass 136.9815553
5
6
7
8
9 Result:
10 Practical Obtained 21.31243456
Total Caculated original Mass 0
Expected Evolve Compound Data Expected Residue Data
Sr # Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
1 SnCl2 SnCl2 1 189.6 189.6 Sn PdS 1 138.42
2
3
4 Total Residue Mass 138.42
5 Back Calulations:
6 Total Evolve Mass 189.6
7 Total Residual Mass 138.42
Total Mass 328.02
Impurity 0
Total Evolve Mass 189.6
 Sample ID HE5d Compound Temperature Range 106.106 °C - 850 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 99.902 78.395 21.5071
2 Pd 106.42 1 106.42 Calculated original Mass 731.03
3 Cl 35.45 2 70.9 Calculated Evolve Mass 573.6531486
4 Phenyl 77 3 231 Calculated Residue Mass 157.3775832
5 CH2 14 6 84
6 S 32 2 64
7 N 14 2 28
8 C 12 1 12
9 O 16 1 16 Result:
10 Practical Obtained 22.67622396
Total Caculated original Mass 731.03
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Sn 1/2SnCl4 1 130.25 130.25 Pd Pd 1 106.42
1 Methylene C2H4 3 28 84 Sn 1/2Sn 59.35
2 Carbon & Sulfur CS2 1 76 76
3 O 1/2O2 1 16 16 Total Residue Mass 165.77
4 Phenyl C6H5 3 77 231 Back Calulations:
5 N N2 1 28 28 Total Evolve Mass 565.25
6 Total Residual Mass 165.77
7 Total Mass 731.02
Impurity 0.01
Total Evolve Mass 565.25
 Sample ID HE6d Compound Temperature Range 55 °C - 700 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 98.6271 69.1793 29.4438
2 Pd 106.42 1 106.42 Calculated original Mass 689.48
3 Cl 35.45 3 106.35 Calculated Evolve Mass 483.6170156
4 Phenyl 77 2 154 Calculated Residue Mass 205.8350212
5 CH2 14 6 84
6 S 32 2 64
7 N 14 2 28
8 C 12 1 12
9 O 16 1 16 Result:
10 Practical Obtained 28.68393572
Total Caculated original Mass 689.48
Expected Evolve Compound Data Expected Residue Data
Sr # Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
1 Sn 1/2SnCl4 1 130.25 130.25 Pd PdS 1 138.42
2 Methylene C2H4 3 28 84 Sn 1/2Sn 1 59.35
3 Carbon & Sulfur CS 1 44 44
4 Phenyl C6H5 2 77 154 Total Residue Mass 197.77
5 N N2 1 28 28 Back Calulations:
6 O 1/2O2 1 16 16 Total Evolve Mass 491.7
7 Cl 1/2Cl2 1 35.45 35.45 Total Residual Mass 197.77
Total Mass 689.47
Impurity 0.01
Total Evolve Mass 491.7
 Sample ID HES Compound Temperature Range 73.156 °C - 300.602 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 H 1 2 2 100.0808 98.619 1.4519
2 CH2 14 6 84 Calculated original Mass 206
3 S 32 2 64 Calculated Evolve Mass 202.9911232
4 N 14 2 28 Calculated Residue Mass 2.988499293
5 C 12 1 12
6 O 16 1 16
7
8
9 Result:
10 Practical Obtained 0
Total Caculated original Mass 206
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # H&O H2O 1 18 18
1 Nitrogen N2 1 28 28
2 Methylene C2H4 3 28 84
3 Carbon& S CS2 1 76 76 Total Residue Mass 0
4 0 Back Calulations:
5 Total Evolve Mass 206
6 Total Residual Mass 0
7 Total Mass 206
Impurity 0
Total Evolve Mass 206
 Sample ID ID Compound Temperature Range 53.837 °C - 800 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 2 237.42 100.022 70.3631 29.65
2 Pd 106.42 1 106.42 Calculated original Mass 891.84
3 Methyl 15 6 90 Calculated Evolve Mass 627.3882456
4 Na 23 2 46 Calculated Residue Mass 264.3723981
5 CH2 14 4 56
6 C 12 6 72
7 O 16 8 128
8 S 32 4 128
9 N 14 2 28 Result:
10 Practical Obtained 30.20945461
Total Caculated original Mass 891.84
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Methyl CH3 6 15 90 Sn SnO 2 269.42
1 Carbon & Oxygen CO 4 28 112
2 Carbon & Sulfur CS2 2 76 152
3 Nitrogen N2 1 28 28 Total Residue Mass 269.42
4 NA & oxygen Na 2 23 46 Back Calulations:
5 Pd PdO2 1 138.4 138.4 Total Evolve Mass 622.4
6 Methylene C2H4 2 28 56 Total Residual Mass 269.42
7 Total Mass 891.82
 Impurity 0.02
Total Evolve Mass 622.4
 First Residue
Sample ID PC Compound Temperature Range 61.603 °C - 231.344 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 N 14 1 14 99.4656 13.0259 86.4397
2 C 12 1 12 Calculated original Mass 129
3 CH2 14 4 56 Calculated Evolve Mass 16.89369088
4 CH 13 1 13 Calculated Residue Mass 112.1063091
5 O 16 2 32
6 H 1 2 2
7
8
9 Result:
10 Practical Obtained 86.04651163
Total Caculated original Mass 129
Expected Evolve Compound Data Expected Residue Data
Sr # Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
1 H2O H2O 1 18 18 N(CH2)4CHCO 1 111
2
3
4 Total Residue Mass 111
5 Back Calulations:
6 Total Evolve Mass 18
7 Total Residual Mass 111
Total Mass 129
Impurity 0
Total Evolve Mass 18
Second Residue
Sample ID PC Compound Temperature Range 231.344 °C - 837.713 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 86.4397 79.0297 7.41
 2 Calculated original Mass 112.1063091
3 Calculated Evolve Mass 102.4960519
4 Calculated Residue Mass 9.610257215
5
6
7
8
9 Result:
10 Practical Obtained 10.70412548
Total Caculated original Mass
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Methylene CH2CH2 2 28 56 C 1 12
1 N 1/2N2 1 14 14
2 CO CO 1 28 28
3 H 1/2H2 1 1 1 Total Residue Mass 12
4 Back Calulations:
5 Total Evolve Mass 99
6 Total Residual Mass 12
7 Total Mass 111
Impurity 1.106309116
Total Evolve Mass 99
 Sample ID PC5D Compound Temperature Range 175.174 °C - 902.029 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 99.5277 68.0227 31.5051
2 Pd 106.42 1 106.42 Calculated original Mass 730.03
3 Phenyl 77 3 231 Calculated Evolve Mass 498.9426228
4 CH 13 1 13 Calculated Residue Mass 231.0881107
5 CH2 14 4 56
6 C 12 2 24
7 O 16 2 32
8 S 32 2 64
9 N 14 1 14 Result:
10 Cl 35.45 2 70.9 Practical Obtained 32.41921565
Total Caculated original Mass 730.03
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Phenyl C6H5 3 77 231 Sn 1/2Sn 1 59.35
1 Carbon & Oxygen CO 1 28 28 Pd PdCl2 1 177.32
2 Carbon & Sulfur CS2 1 76 76
3 Methylene C2H4 2 28 56 Total Residue Mass 236.67
4 Sn 1/2SnO2 1 75.35 75.35 Back Calulations:
5 N 1/2N2 1 14 14 Total Evolve Mass 493.35
6 H 1/2H2 1 1 1 Total Residual Mass 236.67
7 C C 1 12 12 Total Mass 730.02
Impurity 0.01
Total Evolve Mass 493.35
 First Residue
Sample ID PC11 Compound Temperature Range 93.196 °C - 326.231 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 99.2966 62.0908 37.1075
2 Sn 118.71 1 118.71 Calculated original Mass 530.42
3 Methyl 15 6 90 Calculated Evolve Mass 331.6750235
4 CH 13 1 13 Calculated Residue Mass 198.2198801
5 CH2 14 4 56
6 C 12 2 24
7 O 16 2 32
8 S 32 2 64
9 N 14 1 14 Result:
10 Practical Obtained 37.27235021
Total Caculated original Mass 530.42
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Methylene C2H4 2 28 56 Sn Me-Sn 1 133.7
1 Methyl CH3 5 15 75 S S2 1 64
2 Sn SnO 1 134.71 134.71
3 CO CO 1 28 28 Total Residue Mass 197.7
4 C&N CN 1 26 26 Back Calulations:
5 C C 1 12 12 Total Evolve Mass 332.71
6 H 1/2H2 1 1 1 Total Residual Mass 197.7
7 Total Mass 530.41
Impurity 0.01
Total Evolve Mass 332.71

Second Residue
Sample ID PC11 Compound Temperature Range 324.176 °C - 817.965 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 37.1075 13.2521 23.8554
2 Calculated original Mass 197.7
3 Calculated Evolve Mass 70.78972374
4 Calculated Residue Mass 127.4301564
5
6
7
8
9 Result:
10 Practical Obtained 25.20644018
Total Caculated original Mass 0
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # S S2 1 64 64 Sn Me-Sn 1 133.7
1
2
3 Total Residue Mass 133.7
4 Back Calulations:
5 Total Evolve Mass 64
6 Total Residual Mass 133.7
7 Total Mass 197.7
Impurity 0
Total Evolve Mass 64
 Sample ID PC55 Compound Temperature Range 220.162 °C - 753.360°C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 1 118.71 98.9203 82.6149 16.3053
2 Sn 118.71 1 118.71 Calculated original Mass 902.42
3 Phenyl 77 6 462 Calculated Evolve Mass 753.6707638
4 CH 13 1 13 Calculated Residue Mass 148.7483239
5 CH2 14 4 56
6 C 12 2 24
7 O 16 2 32
8 S 32 2 64
9 N 14 1 14 Result:
10 0 Practical Obtained 16.70064937
Total Caculated original Mass 902.42
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Phenyl C6H5 6 77 462 Sn SnS 1 150.71
1 Carbon & Oxygen CO 1 28 28
2 Carbon & Sulfur CS 1 44 44
3 Methylene C2H4 2 28 56 Total Residue Mass 150.71
4 Tin & Oxygen SnO 1 134.71 134.71 Back Calulations:
5 N 1/2N2 1 14 14 Total Evolve Mass 751.71
6 H 1/2H2 1 1 1 Total Residual Mass 150.71
7 C C 1 12 12 Total Mass 902.42
Impurity 0
Total Evolve Mass 751.71
 Sample ID SA3D Compound Temperature Range 50°C - 800 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 2 237.42 100.2325 63.2956 36.9369
2 Pd 106.42 1 106.42 Calculated original Mass 1011.84
3 Butyl 57 6 342 Calculated Evolve Mass 638.9646063
4 CH3 15 2 30 Calculated Residue Mass 372.8753937
5 CH2 14 2 28
6 C 12 4 48
7 O 16 4 64
8 S 32 4 128
9 N 14 2 28 Result:
10 0 Practical Obtained 37.14223593
Total Caculated original Mass 1011.84
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Butene C4H8 6 56 336 Sn Sn 2 237.4
1 H H2 3 2 6 Pd PdS 1 138.42
2 Carbon & Oxygen CO2 2 44 88
3 Crabon & Sulfur CS2 1 76 76 Total Residue Mass 375.82
4 Crabon & Sulfur CS 1 44 44 Back Calulations:
5 Methylene C2H4 1 28 28 Total Evolve Mass 636
6 Methyl CH3-CH3 1 30 30 Total Residual Mass 375.82
7 Nitrogen N2 1 28 28 Total Mass 1011.82
Impurity 0.02
Total Evolve Mass 636
 Sample ID SA4D Compound Temperature Range 36.892 °C - 820 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 2 237.42 100.1398 74.256 25.8839
2 Pd 106.42 1 106.42 Calculated original Mass 968.74
3 Butyl 57 4 228 Calculated Evolve Mass 718.3433304
4 CH3 15 2 30 Calculated Residue Mass 250.7476929
5 CH2 14 2 28
6 C 12 4 48
7 O 16 4 64
8 S 32 4 128 Result:
9 N 14 2 28 Practical Obtained 26.5427256
10 Cl 35.45 2 70.9
Total Caculated original Mass 968.74
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Butyl C4H8 4 56 224 Sn Sn 1 118.71
1 H H2 2 2 4 Pd PdS 1 138.42
2 Carbon & Oxygen CO2 2 44 88
3 Sn and Chlorine SnCl2 1 189.32 189.32 Total Residue Mass 257.13
4 Sulfur & Carbon CS2 1 76 76 Back Calulations:
5 Sulfur & Carbon CS 1 44 44 Total Evolve Mass 711.32
6 Methylene C2H4 1 28 28 Total Residual Mass 257.13
7 Methyl CH3-CH3 1 30 30 Total Mass 968.45
Nitrogen N2 1 28 28 Impurity 0.29
Total Evolve Mass 711.32
 Sample ID SA5D Compound Temperature Range 60 °C - 800 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Sn 118.71 2 237.42 99.9424 64.6962 35.2463
2 Pd 106.42 1 106.42 Calculated original Mass 1131.84
3 Phenyl 77 6 462 Calculated Evolve Mass 732.6794935
4 CH3 15 2 30 Calculated Residue Mass 399.161639
5 CH2 14 2 28
6 C 12 4 48
7 O 16 4 64
8 S 32 4 128 Result:
9 N 14 2 28 Practical Obtained 36.03159457
10 0
Total Caculated original Mass 1131.84
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Phenyl C6H5 6 77 462 Sn SnO 2 269.4
1 Carbon & Oxygen CO 2 28 56 Pd PdS 1 138.42
2 Carbon & Sulfur CS2 1 76 76
3 Carbon & Sulfur CS 1 44 44 Total Residue Mass 407.82
4 Methylene C2H4 2 14 28 Back Calulations:
5 Methyl CH3-CH3 1 30 30 Total Evolve Mass 724
6 Nitrogen N2 1 28 28 Total Residual Mass 407.82
7 Total Mass 1131.82
Impurity 0.02
Total Evolve Mass 724
 First Residue
Sample ID IDA Compound Temperature Range 120.929 °C - 351.543 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 Na 23 2 46 97.6554 12.6949 84.9605
2 CH2 14 2 28 Calculated original Mass 195
3 H 1 3 3 Calculated Evolve Mass 25.34939696
4 N 14 1 14 Calculated Residue Mass 169.650603
5 C 12 2 24
6 O 16 5 80
7
8
9 Result:
10 Practical Obtained 84.96520597
Total Caculated original Mass 195
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # water H2O 1 18 18 NaCH2-NH-CH2COONa 133
1 Carbon and oxygen 1/6CO2 1 7.33 7.33 5/6CO2 36.66
2
3 Total Residue Mass 169.66
4 Back Calulations:
5 Total Evolve Mass 25.33
6 Total Residual Mass 169.66
7 Total Mass 194.99
Impurity 0.01
Total Evolve Mass 25.33
 Second Residue
Sample ID IDA Compound Temperature Range 350.649 °C - 794 °C
Sr # Element Atomic mass No. Total mass Orginal %age Evovle %age Residue %age
1 84.9605 33.76 51.07
2 Calculated original Mass 169.65
3 Calculated Evolve Mass 67.41255476
4 Calculated Residue Mass 101.9774636
5
6
7
8
9 Result:
10 Practical Obtained 52.58386384
Total Caculated original Mass 0
Expected Evolve Compound Data Expected Residue Data
Evolve Compound As a NO. Mass Total Mass Residue As No. Mass
Sr # Carbon and oxygen CO 1 28 28
1 Carbon and oxygen 5/6CO2 1 36.66 36.66
NaCH2-NH-CH2ONa 105
2
3 Total Residue Mass 105
4 Back Calulations:
5 Total Evolve Mass 64.66
6 Total Residual Mass 105
7 Total Mass 169.66
Impurity -0.01
Total Evolve Mass 64.66