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Grasso Ammonia Dryer

Removing Water Contamination from Ammonia Systems

Operating Manual (Translation of the original text)


O_661511_8
Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

COPYRIGHT
All Rights reserved.
No part of this publication may be copied or pub-
lished by means of printing, photocopying, microfilm
or otherwise without prior written consent of
• GEA Refrigeration Germany GmbH
herein after called manufacturer. This restriction
also applies to the corresponding drawings and dia-
grams.

LEGAL NOTICE
This documentation has been written in all con-
science. However, the manufacturer cannot be held
responsible, neither for any errors occurring in this
documentation nor for their consequences.

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Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

SYMBOLS USED IN THIS MANUAL


Danger!
Stands for an immediate danger which
leads to heavy physical injuries or to
the death.

Warning!
Stands for a possibly dangerous situa-
tion which leads to heavy physical
injuries or to the death.

Caution!
Stands for a possibly dangerous situa-
tion which could lead to light physical
injuries or to damages to property.

Hint!
Stands for an important tip whose
attention is important for the designa-
ted use and function of the device.

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Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

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Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

TABLE OF CONTENTS
1 TRANSPORT INSTRUCTIONS 7
1.1 Transport and storage 7
2 DESCRIPTION OF DESIGN AND FUNCTION 8
2.1 Grasso Ammonia Dryer GAD 150H with hotgas heating 8
2.1.1 Technical data 8
2.1.2 Function 8
2.1.3 Design 9
2.1.4 Customer parts list 11
2.2 Grasso Ammonia Dryer GAD 150E with electric heating element 13
2.2.1 Technical data 13
2.2.2 Function 13
2.2.3 Design 14
2.2.4 Customer parts list 16
3 OPERATING INSTRUCTIONS 18
3.1 Commissioning 18
3.2 Draining 19
3.3 Environment protection 20
3.4 Fault message 20
3.5 Switching off 20
3.6 Key assignment 21
4 MAINTENANCE INSTRUCTION 22
4.1 Maintenance work 22
4.2 Cleaning the vessel 22
5 ALARMS 24
5.1 Fault indications 24
6 TEST PROCEDURE 25
6.1 Procedure to determine the water content in ammonia refrigerating cycles (measurement) 25
6.2 Calculation of water concentration 26
6.3 Result of measuremen 27

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Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

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Operating Manual | Removing Water Contamination from Ammonia Systems Transport instructions
Grasso Ammonia Dryer

1 TRANSPORT INSTRUCTIONS

1.1 Transport and storage Hint!

Grasso Ammonia Dryer are high-quality products Grasso Ammonia Dryer are to be ade-
which must be handled with extreme care during quately protected from external influ-
transport. Protect the equipment from impacts and ences during transport and storage.
put it down carefully. This usually concerns lengthy stand-
When transported by crane, the Grasso Ammonia ing times outdoors before installation
Dryer must have the same position as in operation. and putting into service.
Do not use lifting points other than those provided for The manufacturer recommends the
this purpose. use of plastic sheeting to cover the
The lifting points are designated by the following whole product.
symbol: The Grasso Ammonia Dryer can also be transpor-
ted with a fork lift or lift truck.
The lifting points are clearly marked with the follow-
ing symbol:

fig.1: Designation of the lifting points

Warning!
It is forbidden to utilize fittings or fig.2: Marking of lifting points for fork lift or lift truck
pipes for attaching the Grasso Ammo-
nia Dryer.

The lifting points are arranged in one plane. The


ropes must be longer than 3 m.
A means of precluding damage to the surface must
be provided (timber or Armaflex supports).
Shackles must be used.
Position the Grasso Ammonia Dryer on the transport
vehicle such that it is prevented from sliding and tilt-
ing. The competent staff member or the company is
responsible for ensuring transport safety.
The storage area of Grasso Ammonia Dryer shall
be roofed, plain and paved and secured against
access of unauthorized persons. The Grasso
Ammonia Dryer must be protected against knocks
and impacts.

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Description of Design and Function Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

2 DESCRIPTION OF DESIGN AND FUNCTION

2.1 Grasso Ammonia Dryer GAD 150H 2.1.2 Function


with hotgas heating
Press the "New Cycle" button
2.1.1 Technical data
The type designation is mentioned on the machine
plate. to start the Grasso Ammonia Dryer.
The device is applicable for ammonia only. At the same time the solenoid filling valves (4010,
4015) and solenoid pilot valve for the extraction
Refrigerant charge 110 kg (4040) are opened.
The vessel is filled via connection A, solenoid valves
max. operating pressure 23.0 bar g.p. (4010, 4015) and the pilot valve (4040) until the
upper level is reached.
Operating limits The sensor (4050) closes the solenoid filling valves
(4010, 4015) and the pilot valve (4040) via the con-
Min. evaporating tem- troller and then opens the solenoid valve (4170) for
perature of plant to be - 43°C the hot gas supply.
dehumidfyied The ammonia evaporates and is extracted through
the main valve (4020), the isolating valve (4090) and
Max. evaporating tem- connection B.
perature of plant to be 5 °C The pressure inside the Grasso Ammonia Dryer is
dehumidfyied limited by the constant pressure valve (4030).
If the lower level is reached, the sensor (4060) ends
Dimensions, Weight the heating process via the controller.
The temperature sensor (4070) checks the sump
Length 2,200 mm temperature.
If this has not yet reached the preset difference
Width 750 mm between it and the saturation temperature, the ves-
sel is filled again via the solenoid valves (4010, 4015
Height 1000 mm and 4040).
A new evaporation cycle therefore begins automati-
Weight, empty 480 kg cally.
If the set difference between the sump temperature
Power supply and the saturation temperature has been exceeded
at the end of the heating process, the controller ends
Voltage 400 V, 3~, 50 Hz the evaporation process.
The water concentration in the sump is then approx
Rating 0.2 kW 60 to 70 %.
The "Cycle Finished - Drain" indicator light

lights up after the sump has been heated to the set


temperature.
The draining can now be carried out manually.

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Operating Manual | Removing Water Contamination from Ammonia Systems Description of Design and Function
Grasso Ammonia Dryer

Warning!
Note and follow the safety instruc-
tions!

2.1.3 Design
The layout of the Grasso Ammonia Dryer GAD 150 H is shown in the diagram below and consists of the follow-
ing components:

Item No. Designation

4010 1 Solenoid valve, MV 1.1

4015 1 Solenoid valve, MV 1.2

4020 1 Main valve

4030 1 Pilot valve CVP

4040 1 Pilot valve EVM, MV 2

4050, 4060 1 Level sensor

4070 1 Temperature sensor

4080 1 Overflow valve DN 15, 23 bar

4090 1 Stop valve

4100 1 Isolating valve with quick closing valve

4110 1 Stop valve

4130 1 Service valve, Pump down

4140 1 Pressure gauge, -1 / 25 bar

4145 1 Pressure gauge stop valve

4160 1 Vent valve

4170 1 Solenoid valve, hot gas

4180 1 Manual control valve

4190 1 Automatic steam trap

4210, 4211 1 Evaporation vessel

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Description of Design and Function Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

fig.3: Grasso Ammonia Dryer, hot gas heated, type GAD 150H

1 Low pressure surge drum


2 Existing refrigerating system
3 Suction side connection
4 Grasso Ammonia Dryer
5 Pump pressure side connection
6 Hot gas port
7 Condensate to the medium pressure
8 Valve mounted against the direction of flow
9 Following connection of the GAD 150H: Valve opened, blocked and sealed

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Operating Manual | Removing Water Contamination from Ammonia Systems Description of Design and Function
Grasso Ammonia Dryer

2.1.4 Customer parts list

Item No. Designation Order No: Manufacturer Ident

4010 1 Solenoid valve EVRAT 10 32F3056 503298430

4011 1 Coil 24 V, DC 20 W 18F6968 503298561

4015 1 Solenoid valve EVRAT 10 32F3056 503298430

4016 1 Coil 24 V, DC 20 W 18F6968 503298561

4020 1 Main valve ICS 25-15, 25 D 1 27H2090 503298728

4030 1 Pilot valve CVP 27B1164 503298180

4040 1 Pilot solenoid valve EVM-NC 27B1120 503298163

4041 1 Coil 24 V, DC 20 W 18F6968 503298561

4050 1 Optoelectronic level monitor MAX 634198174

4060 1 Optoelectronic level monitor MIN 634198173

Compact screw-in resistance thermometer GEA


4070 1 630498252E
Grasso-406-120 Pt100A

4080 1 Full-lift safety valve B15-23 44223c10a5a10011 500398535

4090 1 Stop valve DN 20 501698022C25

4100 1 Quick-acting valve/ stop valve 96564c1ca5a2e156 500298032

4110 1 Angle stop valve DN 20 501698002C25

4130 1 Stop valve DN 15 AVR 363 00 501298890

4140 1 Refrigeration gauge, -1 / 30 bar 631098327K

4145 1 Angle valve DN8 PS63 AG/AN4 501306632awp63

4160 1 Angle valve DN8 PS63 AC/A84 501299036awp63

4170 1 Solenoid valve EVRA 10 32F3069 503298430

4171 1 Coil 24 V, DC 20 W 18F6968 503298561

4180 1 Manual control valve DN15, shuttable 501598262

4190 1 High pressure float valve HR 1-H 355598026F3S

4200 1 Dryer

4205 1 Drip pan for condensation water B2385910

1 from serial number 0097

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Description of Design and Function Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

Item No. Designation Order No: Manufacturer Ident

4210 1 Plastic canister, 10 Liters 718598019

4211 1 Plastic canister, 20 Liters 718598020

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Operating Manual | Removing Water Contamination from Ammonia Systems Description of Design and Function
Grasso Ammonia Dryer

2.2 Grasso Ammonia Dryer GAD 150E 2.2.2 Function


with electric heating element
Press the "New Cycle" button
2.2.1 Technical data
The type designation is mentioned on the machine
plate. to start the Grasso Ammonia Dryer.
The device is applicable for ammonia only. At the same time the solenoid filling valves (4010,
4015) and the solenoid pilot valve for the extraction
Refrigerant charge 110 kg (4040) are opened.
The vessel is filled via connection A, solenoid valves
max. operating pressure 23.0 bar g.p. (4010, 4015) and the pilot valve (4040) until the
upper level is reached.
Operating limits The sensor (4050) closes the solenoid filling valves
(4010/4015) and the pilot valve (4040) via the con-
Min. evaporating tem- troller and then switches on the heater (4120).
perature of plant to be - 43°C The ammonia evaporates and is extracted through
dehumidfyied the main valve (4020), the isolating valve (4090) and
connection B.
Max. evaporating tem- The pressure inside the Grasso Ammonia Dryer is
perature of plant to be 5 °C limited by the constant pressure valve (4030).
dehumidfyied
If the lower level is reached, the sensor (4060) ends
the heating process via the controller.
Dimensions, Weight The temperature sensor (4070) checks the sump
temperature.
Length 2,200 mm
If this has not yet reached the preset difference
between it and the saturation temperature, the ves-
Width 750 mm sel is filled again via the solenoid valves (4010/4015
and 4040).
Height 1000 mm
With this a new evaporation cycle begins automati-
cally.
Weight, empty 500 kg
If the set difference between the sump temperature
and saturation temperature has been exceeded at
Power supply the end of the heating process, the controller stops
the evaporation process.
Voltage 400 V, 3~, 50 Hz The water concentration in the sump is then approx
60 to 70 %.
Rating 1.8 kW
The "Cycle Finished - Drain" indicator light

lights up after the sump has been heated to the set


temperature.
The draining can now be carried out manually.

Warning!
Note and follow the safety instruc-
tions!

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Description of Design and Function Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

2.2.3 Design
The layout of the Grasso Ammonia Dryer GAD 150 E is shown in the diagram below and consists of the follow-
ing main components:

Item No. Designation

4010 1 Solenoid valve, MV 1.1

4015 1 Solenoid valve, MV 1.2

4020 1 Main valve

4030 1 Pilot valve CVP

4040 1 Pilot valve EVM, MV 2

4050, 4060 1 Level sensor

4070 1 Temperature sensor

4080 1 Overflow valve DN 15, 23 bar

4090 1 Stop valve

4100 1 Isolating valve with quick closing valve

4110 1 Stop valve

4120 1 Electric heater

4130 1 Service valve, Pump down

4140 1 Pressure gauge, -1 / 25 bar

4145 1 Pressure gauge stop valve

4160 1 Vent valve

4210, 4211 1 Evaporation vessel

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Operating Manual | Removing Water Contamination from Ammonia Systems Description of Design and Function
Grasso Ammonia Dryer

fig.4: Grasso Ammonia Dryer, electrically heated, Type GAD 150E

1 Low pressure surge drum


2 Existing refrigerating system
3 Suction side connection
4 Grasso Ammonia Dryer
5 Pump pressure side connection
6 Valve mounted against the direction of flow
7 After connecting GAD 150E: Valve opened, blocked and sealed

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Description of Design and Function Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

2.2.4 Customer parts list

Manufacturer
Item No. Designation Order No:
Ident

4010 1 Solenoid valve EVRAT 10 32F3056 503298430

4011 1 Coil 24 V, DC 20 W 18F6968 503298561

4015 1 Solenoid valve EVRAT 10 32F3056 503298430

4016 1 Coil 24 V, DC 20 W 18F6968 503298561

4020 1 Main valve ICS 25 - 15, 25 D 2 27H2090 503298728

4030 1 Pilot valve CVP 27B1164 503298180

4040 1 Pilot solenoid valve EVM-NC 27B1120 503298163

4041 1 Coil 24 V, DC 20 W 18F6968 503298561

4050 1 Optoelectronic level monitor MAX 634198174

4060 1 Optoelectronic level monitor MIN 634198173

Compact screw-in resistance thermometer GEA


4070 1 630498252E
Grasso-406-120 Pt100A

4080 1 Full-lift safety valve B15-23 44223c10a5a10011 500398535

4090 1 Stop valve DN 20 501698022C25

4100 1 Quick acting valve/ stop valve 96564c1ca5a2e156 500298032

4110 1 Angle stop valve DN 20 501698002C25

4120 1 Electric heater EK 1500/400-465-40 380-400V-2Ph; 1350 - Type EK 1500/400-465-40


677398857
1500 W

Spare part: Temperature controller 716-RU/20°C...150°C/


677398558
1x16A-400V

Spare part: Temperature limiter type 602031/81 (-50°C –


677398861
150°C)

4130 1 Stop valve DN 15 501298890

4140 1 Refrigeration gauge, -1 / 30 bar 631098327K

4145 1 Angle valve DN8 PS63 AG/AN4 501306632awp63

4160 1 Angle valve DN8 PS63 AC/A84 501299036awp63

4200 1 Dryer

2 from serial number 0097

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Operating Manual | Removing Water Contamination from Ammonia Systems Description of Design and Function
Grasso Ammonia Dryer

Manufacturer
Item No. Designation Order No:
Ident

4205 1 Drip pan for condensation water B2385910

4210 1 Plastic canister, 10 Liters 718598019

4211 1 Plastic canister, 20 Liters 718598020

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Operating instructions Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

3 OPERATING INSTRUCTIONS

3.1 Commissioning Hint!

1. Connection A- connect to the discharge side of During operation of the GAD, the valve
the low-pressure surge drum (see functional plant valve at connection B must be
description). opened, blocked and sealed to ensure
that on activation of the pressure relief
2. Connection B - connect to the suction (intake) device (4080) the gauge pressure
side of the low-pressure surge drum (see func- inside the vessel can be discharged to
tional description). the suction side of the refrigeration
plant.
Hint!
This valve must not be closed again
The connections must be made care- until the GAD is to be disconnected.
fully and checked for leaks!
To shut down the GAD during normal
3. Evacuate the dryer (GAD). operation, close the plant valve
Valve position during evacuation: Valves upstream of connection A and initiate
(4090), (4110), (4130) open a new cycle by pressing the "START"
button.
Valve position during operation: Valves
(4090), (4110) open After 24 hours the GAD can be
switched off at the main switch.
4. Connect the equipment plug (400 V, 3~ , 50 Hz) Then close valve 4090.
5. Switch the main switch

switch to "I". The GAD is ready for operation.


6. Switching points for temperature sensor (4070)
at the controller's display (inside the connection
box) are permanently preset:
– Evaporating temperature 7 °C
– Temperature for ending the evaporation
process, sump temperature 15 °C
– End of reheating, sump temperature 35°C
– Fault, sump temperature 45 °C
7. Open the plant valve upstream of connection A.
8. Open the plant valve at connection B.

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Operating Manual | Removing Water Contamination from Ammonia Systems Operating instructions
Grasso Ammonia Dryer

9. Press the "New Cycle" button: 3.2 Draining


Caution!
Before draining the pressure inside
9.1 The solenoid filling valve MV 1 (4010/4015)
the vessel must be checked at the
and the extraction pilot valve MV 2 (4040)
pressure gauge (4140).
are opened.
9.2 The vessel is now filled until the upper If the pressure has risen to over 1 bar gauge pres-
level is reached. sure, press the button "Open Manually – MV 2"

9.3 The sensor (4050) closes the solenoid


valves MV 1 (4010/4015) and MV 2 (4040)
via the controller and then opens the hot
gas solenoid valve (4170) or starts up the
heater (4120). to lower it to 0.3 bar gauge pressure.
9.4 The ammonia evaporates and is extracted If the suction pressure in the low pressure surge
through the main valve (4020) by the low- drum is higher than 0.3 bar gauge pressure, the
pressure surge drum. dryer cannot be lowered to this gauge pressure
before draining.
9.5 The pressure inside the Grasso Ammonia
Dryer is adjusted to 4.5 bar gauge pres- In this case. particular caution is necessary when
sure (corresponds to 7°C) by the constant draining the vessel's sump!
pressure valve (4030) and is checked The drain valve (4100) is connected to a suitable
using the pressure gauge (4140). container.
In the event of differences, the constant
Danger!
pressure valve must be adjusted manually
during the initial heating process. Safety goggles and safety gloves must
be worn during the draining work!
9.6 If the lower level is reached, the sensor
(4060) ends the heating process via the 1. Ensure that the isolating valve is closed.
controller.
2. Open the quick closing valve with one hand,
9.7 If the sump temperature has not yet while carefully and slowly opening the upstream
reached the set value, the vessel is filled isolating valve with the other hand.
again via solenoid valves MV 1
(4010/4015) and MV 2 (4040). Caution!

9.8 If the set sump temperature has been In an emergency the quick closing
reached the "Cycle Finished - Drain" indi- valve can be closed again by releasing
cator light indicates it.

3. Completely drain the vessel.


Then close the manual isolating valve before the
quick closing valve (4100).
that the draining may be carried out man- 4. After draining, a new evaporation process cannot
ually. be started until the "New Cycle" button

is pressed.

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Operating instructions Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

3.3 Environment protection 3.4 Fault message


Danger! If the sump temperature exceeds the limit value, the
hot gas solenoid valve (4170) is closed or the heater
The drained mixture of water and (4120) is switched off.
ammonia may also contain oil. It must,
therefore, be disposed of in accord- The vessel must be drained in compliance with the
ance with local regulations! It must not aforementioned safety precautions.
be drained into the open air or public After the cause of the fault has been corrected, the
waters. evaporation process can be continued by pressing
The operator is responsible for its the "New cycle" button.
proper disposal!

The operator of the refrigeration application is


accountable for unloading and returning the refriger- A new cycle begins.
ant to the specialised trade and for the environmen-
tally friendly disposal of the refrigerant and polluted 3.5 Switching off
materials.
Switch the main switch
Therefore suitable and specially marked cans must
be supplied.

to "O".

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Operating Manual | Removing Water Contamination from Ammonia Systems Operating instructions
Grasso Ammonia Dryer

3.6 Key assignment

Function Key

"Drain"

"Sight glass lamp ON"

"New Cycle"

"Heat"

"Fault"

"Fill"

"Open manual extraction MV 2 –


note pressure gauge pressure"

"Lamp Test"

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Maintenance Instruction Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

4 MAINTENANCE INSTRUCTION
Perform all maintenance work carefully to keep the
4.1 Maintenance work Grasso Ammonia Dryer in good working order.
The Grasso Ammonia Dryer must only be serviced Guarantee claims will not be valid if the customer
by appropriately qualified personnel. failed to follow the Maintenance Instructions.
These maintenance instructions shall be adhered to
during all maintenance work.
Moreover, all health & safety and fire prevention reg-
ulations and the safety regulations for refrigeration
systems must also be observed.

Maintenance work

Check of Frequency Remarks

See maintenance instruction,


Tank at least twice-yearly Chapter "Cleaning the pressure
vessel"

4.2 Cleaning the vessel 8. Flush the pipes with compressed air, drain pres-
sure via item 4100
After 6 months of operation and on receiving the
Gaskets and accessories
"Cycle Finished - Drain" signal
Manufacturer
Gaskets / accessories
Ident

the vessel must be completely drained. for connection A and B, flange


763 000 045
More frequent cleaning may be necessary for the DN 20
specific system as solid dirt particles, oil and decom-
position products (silt) can accumulate in the vessel. 438 698 114 for sight glasses
Use the illuminated sight glass to evaluate whether
for the flange for heater / heating
cleaning is necessary or not. 763 000 052
coil, flange DN 100
Obvious malfunctions of level switches also indicate
an increased degree of soiling.
for temperature sensor (old style,
762 925 234
The following work must be carried out: with silver head)
1. Solenoid valves: Check/ Clean / Replace
for temperature sensor (new
2. Stop valves and quick acting valve: Check/ 762 998 212
style)
Clean / Replace
3. Heating coil: Check / Clean for level sensors item 4050 and
438 698 026
4060
4. Temperature sensor: Check / Clean the dip tube
5. Level sensor: Check / Clean the glass tube 718 598 019 10l canister
6. Illuminated sight glass: Check / Clean
718 598 020 20l canister
7. Sump pipe: Remove all residues, if necessary
using brush and cleaning agent 718 598 021 Sampling glass

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Operating Manual | Removing Water Contamination from Ammonia Systems Maintenance Instruction
Grasso Ammonia Dryer

The compressed air connection is provided via the


service valve (4160), the venting / draining connec-
tion via the drain valve (4100).
To connect the compressed air, all manual isolating
valves in connections A and B of the refrigerating
system must be closed.
The quick acting valve must be manually kept open
during the whole cleaning process.
Before starting-up again the vessel must be re-evac-
uated, see also Operation / start-up / Item 3.

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Alarms Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

5 ALARMS
Faults are acknowledged by pressing the
5.1 Fault indications

Display Meaning button.


If a fault occurs, check the level sensors are func-
Fault, sump temperature tioning properly.
Fault, continuous light
too high Hint!

Fault, minimum not If the fault recurs, completely clean the


Fault, flashing equipment at the start of any trouble-
reached
shooting.
Fault, flashing and Drain Fault, sump temperature
continuous light too low

Checking the level sensors are functioning properly

Max level Item 4050 switches on emerging LED on, if sensor is not in liquid
LED off, if sensor is in liquid

Min level Item 4060 switches on immersing LED on, if sensor is in liquid
LED off, if sensor is not in liquid

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Operating Manual | Removing Water Contamination from Ammonia Systems Test procedure
Grasso Ammonia Dryer

6 TEST PROCEDURE

6.1 Procedure to determine the water Even slight boiling can generate so much ammo-
nia vapour that even water can be absorbed
content in ammonia refrigerating
which would cause distorted measurement
cycles (measurement) results.
1. Where can the sample be taken? 8. The colour and turbidity of the drained ammonia
– On the discharge side of the refrigerant give an initial indication of its purity.
pump downstream of the low-pressure 9. At the end of the evaporation process the quan-
receiver or tity of water in the Grasso Ammonia Dryer test
– at the service valve, at the evaporator inlet (sample) bottle can be read off in "ml".

2. Under which conditions can the sample be


taken?
– The system is running in normal operating
mode
– No ice or condensate on the service valve
3. While taking the sample:

4. Drain 50 ml of liquid refrigerant into the Grasso


Ammonia Dryer sample bottle and then place the
bottle in a secure location to evaporate.

Danger!
Do not close the opening of the sam-
ple bottle and ensure that unauthor-
ised people do not have any access.

5. The evaporation can take up to four hours.


During this time ensure that the ambient air is as
dry as possible, as the moisture from humid air
can be absorbed and could distort the measure-
ment result.
6. Danger!
Do not attempt to speed up the evapo-
ration by additional heating (heating
element or holding in hand), as there
is a risk of the ammonia boiling vio-
lently and spilling out.

7. The evaporation should take place at normal


room temperature, but not at temperatures
above 30°C.

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Test procedure Operating Manual | Removing Water Contamination from Ammonia Systems
Grasso Ammonia Dryer

6.2 Calculation of water concentration

Quantity before evaporation (QB) 50 ml

Quantity after evaporation (QA) _____ ml

Appearance Ο clear
Ο cloudy

Colour Ο colourless
Ο yellow
Ο brown
Ο dark

Fixed values

Density water (DW) 1,00 g/cm³

Density ammonia (DA) 0,65 g/cm³

General calculation formula

QA DW

— x — x 100 % = _____ % Water concentration

QB DA

If "QB" is exactly 50 ml, following formula can be used:


QA x 0,03 x 100% = ______ % Water concentration

26 GEA Refrigeration Germany GmbH | O_661511_8 | Generated 04.08.2014


Operating Manual | Removing Water Contamination from Ammonia Systems Test procedure
Grasso Ammonia Dryer

6.3 Result of measuremen Date of measurement Humidity (in %)


A watercontent of ________ % in ammonia was
observed.
Interpretation of results

Value Interpretation

< 0,5 % Satisfactory

Rising power consumption.


0.5 % ... 2.0 % Further frequent measurements
are recommended.

Attention!
Maintenance/ repairing neces-
sary!
Water content in ammonia cycle
2.0 % ... 5.0 % is too high and leads to increased
wear, corrosion, oil aging. Shaft
seals can be damaged and the
whole ammonia cycle will be pol-
luted.

Critical!
> 5,0 %
Hint for serious leakages (e.g.
(up to 25 %)
heat exchanger).

The following table can be used for recording further


measurements.

Date of measurement Humidity (in %)

GEA Refrigeration Germany GmbH | O_661511_8 | Generated 04.08.2014 27

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