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Analytical
Chemistry

CHM 421

PM Dr. Zuraida Khusaimi

B302(A)
016-2128514
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Semester Sep 2019 – Jan 2020

n Credit hours: 4
n Lecture – 3 hours/week for 14
weeks
n Lab (10 experiments) –
3 hours/week for 9 weeks
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 Zuraida Khusaimi/CHM421/Sep2019

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CHM 421 Lesson Plan (Sep19 – Jan20)

Wk Date Contents

1 3/9 – 6/9 TOPIC 1: Units for Quantities and Concentration

ENTRANCE SURVEY

2 10/9 – TOPIC 1: Units for Quantities and Concentration

Briefing & Experiment 1: Calibration
13/9
3 17/9 – TOPIC 2: Apparatus and Techniques
Experiment 2: Analysis of an unknown Vinegar sample
20/9 QUIZ 1
4 23/9 – TOPIC 3: Sampling & Statistics
Experiment 3: Neutralisation Capacity of Commercial Antacid
27/9 Tablet
5 30/9 – TOPIC 3: Sampling & Statistics
Experiment 4: Solubility of Ionic Salts in Water
4/10 QUIZ 2
6 7/10 – TOPIC 3: Sampling & Statistics
Experiment 5: Distillation and Hardness of Water
11/10
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+ CHM 421 Lesson Plan (Sep19 – Jan20) 4

Wk Date Contents
7 14/10- TOPIC 4: Titrimetric Analysis – Acid-base titrations & Back-
titration
18/10 Experiment 6: Analysis of Bleach and Copper (II) unknown
QUIZ 3
8 21/10 – TOPIC 4: Titrimetric Analysis – Acid-base titrations & Back-
titration
25/10 Experiment 8: Determination of Fe in Fe solution by
Gravimetric Analysis
TEST 1

27/10 – MID SEMESTER BREAK

3/11
9 4/11 – TOPIC 4: Complexometric Titration
Experiment 9 : Separation of Amino Acid Mixture by Paper
8/11 Chromatography
Experiment 10: Separation of a Mixture of Alum Ferric and
Copper Sulfate using Column Chromatography
10 11/11 – TOPIC 4: Precipitation titrations & Redox titrations
15/11
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CHM 421 Lesson Plan (Sep19 – Jan20)

Wk Date Contents

11 18/11 – 22/11 TOPIC 5: Gravimetric Analysis

QUIZ 4

12 25/11 – 29/11 TOPIC 5: Gravimetric Analysis

QUIZ 5
13 2/12 – 6/12 TOPIC 5: Gravimetric Analysis
TEST 2
14 9/12 – 13/12 Topic 6 : Chromatography
TEST 3
SUFO ONLINE
EXIT SURVEY

16/12 – 22/12 REVISION WEEK

30/12 – 20/1 EXAMINATION

21/1 – 23/2 SEMESTER HOLIDAY

+CHM 421 ASSESSMENT 6

n Tests (3) : 30%

n Quizzes (5) : 10%
n Laboratory report : 20%
n  Writtenreport : 15%
n  Procedural skills : 5%

n Final Examination (5Q) : 40%

Attendance – AT LEAST 80% of lectures

(If less, students will be BARRED from sitting the
final exam)
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Reference Book

1.  Analytical Chemistry 7th. Ed

n  Gary D. Christian, Wiley, New York.

2. Fundamentals of Analytical Chemistry

n  Skoog/West/Holler, Sauders Publishing

3. Quantitative Chemical Analysis

n  Daniel C. Harris, W.H. Freeman and Company, New York.

4. Quantitative Chemical Analysis

n  Stanley E. Manahan, Brooke/Cole, Monterey.

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What Students have to do now
•  Students must register with the course CHM421 -
see the course coordinator (if not registered cannot sit
for exam)
•  Entrance survey - do it at ‘ilearn website– in the first
two weeks of semester (Learning survey- scale 1-3)
•  Download CHM421 notes at iLearn V3.(PW: zurai142)
•  Download at least 5 latest PYQ at EQPS,PTAR website.

At the end of semester

•  Exit survey (Learning outcome)
•  SUFO (survey of lecturer’s performance)

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Purchase

Lab Manual
 
Zuraidah Abdullah Munir, Zaini Hamzah and
Sabarina Md Yunus, Analytical Chemistry
Laboratory Manual, UiTM Press 2017
 
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Introduction

What is Analytical Chemistry?

ü  Analytical chemistry is a measurement science

consisting of a set of powerful ideas and methods
that are useful in all fields of science and
medicine.
Gary Christian, Analytical Chemistry, 7th. Ed. (Wiley)

ü  Analytical chemistry is the study of the

separation, identification, and quantification of the
chemical components of natural and artificial
materials.
n  http://en.wikipedia.org/wiki/Analytical_Chemistry

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+Some examples of chemical analysis 11

application

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+ Chemist
12

ry
Biology Physics

Engineeri
Geology ng

Analytical
Chemistry
Environ
mental Medicin
Science e
s

Agricultu Material
re Science
Social
Sciences

Some Fields of Application of Analytical

Chemistry
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Chemical Analysis

n  Chemical analysis is the determination of the chemical

composition (qualitative) and quantity of each composition
present in a sample (quantitative)

n  e.g. The chemical analysis of a water sample involves the

determination of its mineral content, pollutant content and
dissolved oxygen and the % of each.

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Some examples of chemical

analysis data

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+ QUALITATIVE or QUANTITATIVE analysis 15

QUALITATIVE QUANTITATIVE
Analysis conducted Analysis to
to identify what are determine how
the constituents much of each
present in the constituents present
sample in the sample
(identification of
sample component)

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Measurement : Qualitative or
Quantitative

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STEPS IN CHEMICAL ANALYSIS

Formulating the
question (to be
Compare results with Apply required
answered through
standards statistical techniques
chemical
measurement)

Selecting techniques
Performing the
(find appropriate Verify results
measurement
analytical procedures)

Sample preparation
Sampling (select
(convert representative
representative material Present information
material into a suitable
to be analyzed)
form for analysis)

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