FT X0.

raw
10000
PDF 01-072-1474 Co O Cobalt Oxide
PDF 01-074-1657 Co3 O4 tricobalt tetraoxide | Cobalt Oxide
PDF 01-077-2176 K2 O potassium dioxide | Potassium Oxide
9000 PDF 00-001-1308 Al2 O3 γ-Al2 O3 | Aluminum Oxide

8000

7000

6000
Counts

5000

4000

3000

2000

1000

0
10 20 30 40 50 60 70 80 90

2Theta (Coupled TwoTheta/Theta) WL=1.54060

Yes 0 PDF 01-072-1474 Pattern List #7 FT X0.raw #1 PDF 01-072-1474 Cobalt Oxide Co O Indexed 19.7103 %
Yes 1 PDF 01-074-1657 Pattern List #7 FT X0.raw #1 PDF 01-074-1657 tricobalt tetraoxide | Cobalt Oxide Co3 O4 Indexed 61.4540 %
potassium dioxide | Potassium
Yes 2 PDF 01-077-2176 Pattern List #7 FT X0.raw #1 PDF 01-077-2176 K2 O Indexed 9.8734 %
Oxide
Yes 3 PDF 00-001-1308 Pattern List #7 FT X0.raw #1 PDF 00-001-1308 γ-Al2 O3 | Aluminum Oxide Al2 O3 Blank 23.6886 %

3.160 13.68 % 1.0000 Yes 1.54060 Monoclinic C2/m (12) 5.18000 3.01500 3.01700 125.550
4.680 28.81 % 1.0000 Yes 1.54060 Cubic Fd-3m (227) 8.06500
3.910 5.54 % 1.0000 Yes 1.54060 Cubic Fm-3m (225) 6.09000
(1) 51.97 % 1.0000 Yes 1.54060 Cubic Fd-3m (227) 7.90000

2 38.34 6.491 No F26= 27.6(0.0185, 51)

8 524.58 6.098 No F30= 999.9(0.0002, 30)
2 225.87 1.385 No F20= 999.9(0.0002, 20)
11 493.04 3.610 No F3= 4.0(0.0840, 9)
 Co O
Cobalt Oxide 2.45213 36.617 858 -2 0 1
2.45213 36.617 858 1 1 0
2.13263 42.347 999 -1 1 1
2.10725 42.883 481 2 0 0
1.50850 61.413 187 0 2 0
1.50850 61.413 187 -2 0 2
1.49961 61.817 308 1 1 1
1.49828 61.878 308 -3 1 1
Monoclinic 74.93 1.28526 73.644 131 -2 2 1
C2/m (12) 38.34 1.28526 73.644 131 -1 1 2
6.49 1.27338 74.447 61 -4 0 1
1.27338 74.447 61 3 1 0
3.160
1.22606 77.846 127 -4 0 2
5.18000 1.22606 77.846 127 2 2 0
3.01500 125.55 1.06632 92.504 41 -2 2 2
3.01700 0
1.05362 93.957 19 4 0 0
1.71808
2 0.97759 103.990 17 1 3 0
1.00066
0.97759 103.990 17 -4 0 3
0.97312 104.666 28 -5 1 2
0.97312 104.666 28 2 2 1
0.95399 107.694 37 -1 3 1
0.95399 107.694 37 -3 1 3
0.95178 108.061 33 0 2 2
ANX: AX
Analysis: Co1 O1 0.95110 108.173 32 -4 2 2
Formula from original source: Co O 0.94496 109.208 31 3 1 1
ICSD Collection Code: 17013
0.94429 109.321 30 -5 1 1
Calculated Pattern Original Remarks: Probably tetragonal, pseudo-cubic,
cf. 28505 0.86947 124.735 26 -1 1 3
Cell in I12/m1-setting: a`=4.214, beta`=90.07 0.86857 124.963 55 -3 3 1
Minor Warning: No e.s.d reported/abstracted on the cell dimension. No R
factors reported/abstracted 0.86857 124.963 55 -5 1 3
Wyckoff Sequence: d a(C12/M1) 0.86430 126.061 13 2 0 2
Unit Cell Data Source: Single Crystal
0.86360 126.242 25 -6 0 2
0.86360 126.242 25 4 2 0
0.82027 139.794 23 -3 3 2
0.82027 139.794 23 -4 2 3
0.81822 140.588 5 0 0 3
0.81738 140.919 11 -6 0 3
0.81738 140.919 11 3 3 0
0.81177 143.213 11 -6 0 1
0.81177 143.213 11 5 1 0
Structure
Publication: J. Phys. Soc. Jpn.
Detail: volume 21, page 850 (1966)
Authors: Saito, S., Nakahigashi, K., Shimomura, Y.
Primary Reference
Publication: Calculated from ICSD using POWD-12++

CuKα1 Not specified

1.54060
27.6 (0.0185,51)
 Co3 O4
Cobalt Oxide 4.65633 19.045 150 1 1 1
2.85141 31.346 316 2 2 0

tricobalt tetraoxide 2.43169 36.936 999 3 1 1

2.32816 38.642 90 2 2 2
2.01625 44.921 204 4 0 0
1.85024 49.205 1 3 3 1
1.64626 55.797 84 4 2 2
1.55211 59.510 316 5 1 1
Cubic 240.8 1.42570 65.408 358 4 4 0
Fd-3m (227) 524.58 1.36323 68.812 13 5 3 1
6.1 1.34417 69.929 1 4 4 2
1.27519 74.323 25 6 2 0
4.680
1.22990 77.557 70 5 3 3
8.06500 1.21584 78.626 35 6 2 2
1.16408 82.863 20 4 4 4
1.12933 86.014 8 5 5 1
1.00000 8
1.07773 91.244 31 6 4 2
1.00000
1.04997 94.385 94 7 3 1
1.00812 99.653 36 8 0 0
0.98530 102.850 1 7 3 3
0.97803 103.925 1 6 4 4
0.95047 108.278 15 8 2 2
0.93127 111.615 58 7 5 1
ANX: AB2X4
Analysis: Co3 O4 0.92512 112.744 15 6 6 2
Formula from original source: Co3 O4 0.90169 117.361 21 8 4 0
Delete duplicate: Delete: See PDF 01-074-1656; WFM 12/04
0.88525 120.952 4 9 1 1
ICSD Collection Code: 27498
Minor Warning: No e.s.d reported/abstracted on the cell dimension. No R 0.87996 122.179 1 8 4 2
factors reported/abstracted 0.85973 127.268 5 6 6 4
Wyckoff Sequence: e d a(FD3-MS)
Unit Cell Data Source: Single Crystal 0.84544 131.321 51 9 3 1
0.82313 138.721 86 8 4 4
0.81056 143.730 2 9 3 3

Structure
Publication: J. Phys. Chem. Solids
Detail: volume 25, page 1 (1964)
Authors: Roth, W.L.
Primary Reference
Publication: Calculated from ICSD using POWD-12++

CuKα1 Not specified

1.54060
999.9 (0.0002,30)
 K2 O
Potassium Oxide 3.51606 25.310 883 1 1 1
3.04500 29.307 999 2 0 0

potassium dioxide 2.15314 41.925 607 2 2 0

1.83620 49.607 303 3 1 1
1.75803 51.973 179 2 2 2
1.52250 60.788 71 4 0 0
1.39714 66.918 95 3 3 1
1.36177 68.896 166 4 2 0
Cubic 94.2 1.24312 76.581 110 4 2 2
Fm-3m (225) 225.87 1.17202 82.180 60 5 1 1
1.38 1.07657 91.371 29 4 4 0
1.02940 96.887 55 5 3 1
3.910
1.01500 98.737 59 6 0 0
6.09000 0.96291 106.254 39 6 2 0
0.92872 112.079 21 5 3 3
0.91810 114.072 35 6 2 2
1.00000 2
0.87902 122.403 11 4 4 4
1.00000
0.85277 129.188 36 7 1 1
0.84453 131.595 30 6 4 0
0.81381 142.360 59 6 4 2

ANX: A2X
Analysis: K2 O1
Formula from original source: K2 O
ICSD Collection Code: 60489
Calculated Pattern Original Remarks: DIS O2( with disorderly orientation
in halide position. Stable from 590 to 645K, m.p
919 K, 645-719 K: trigonal (2nd ref., Tomaszewski)
Minor Warning: No R factors reported/abstracted. Magnitude of e.s.d. on
cell dimension is >1000 ppm
Wyckoff Sequence: b a(FM3-M)
Unit Cell Data Source: Single Crystal

Structure
Publication: Acta Crystallogr.
Detail: volume 5, page 851 (1952)
Authors: Carter, G.F., Margrave, J.L., Templeton, D.H.
Primary Reference
Publication: Golden Book of Phase Transitions, Wroclaw
Detail: volume 1, page 1 (2002)
Authors: Carter, G.F., Margrave, J.L., Templeton, D.H.
Publication: Calculated from ICSD using POWD-12++

CuKα1 Not specified

1.54060
999.9 (0.0002,20)
 Al2 O3
Aluminum Oxide 2.39000 37.604 1 3 1 1
1.98000 45.790 30 4 0 0
1.39000 67.307 100 4 4 0
γ-Al2 O3

Cubic 101.96
Fd-3m (227) 493.04

3.61
-1.000
7.90000

1.00000 11
1.00000

Color: Colorless
Delete duplicate: Deleted: similar to 00-002-1420,
General Comments: Transforms to hexagonal form at 750-1000 C

Primary Reference
Publication: Private Communication
Authors: New Jersey Zinc Co., Palmerton, PA, USA.

MoKα1 Not specified

1.54060
4 (0.084,9)