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TITLE NO.

73-31

Time and Temperature Effects on Tensile,

Bond, and Compressive

Strengths

By N. J. GARDNER and S. M. POON

Describes an experimental investigation into (compression, tension, bond, and shear) vary
the relationship between bond strength, tensile with time is essential in construction as many
strength, and cylinder strength of concretes made construction sequences impose significant loads
of Type I cement and Type Ill cement moist cured
at 72 F (22 CJ for I, 3, or 7 days and then cured on the concrete structure even though it may not
under extended low temperatures of 55 F ( 13 CJ have attained its full design strength.! An addi-
and 35 F (2 CJ. Compression strength, tensile tional complication in northern latitudes like
strength, and bond strength are all related, and Canada is that much of the construction is carried
an increase in one is reflected similarly in the out in cold weather, i.e., below 72 F (22 C). The
others.
The commonly assumed relationship that the
hydration of the cement powder in concrete is a
tensile and bond strengths of concrete are propor- chemical reaction which is retarded at low tem-
tional to the 0.5 power of the cylinder strength with peratures, hence the rate of strength gain of a
time was found to be inaccurate. The tensile fresh concrete member at low temperatures is
strength and bond strength were found to be pro- slower. The collapse of many reinforced concrete
portional to the 0.8 power of the cylinder strength buildings during construction in cold weather 2 has
with respect to age.
The longer the concrete is cured at 72 F (22 C) been attributed partly to the low strength capa-
the higher the initial rate of gain of strength (up to bility of the concrete members.
28 days). However, the longer the concrete is
cured at 72 F (22 CJ the lower the ultimate (3 Even though most reinforced concrete elements
month) strength of the concrete. are designed to fail by the steel yielding, failures
are still possible in bond or shear. Knowledge of
Keywords: age-strength relation; bonding; cold weather
construction; compressive strength; concretes; curing; high-
the variation of bond strength, tensile strength,
early-strength cements; low temperature: moist curing; port- and shear strength of the concrete is essential.
land cement type I; setting (hardening); tensile strength.
It has generally been assumed that the tensile
strength, bond strength, and shear strength of
concrete are proportional to the 0.5 power of the
• IT IS WELL ESTABLISHED THAT the rate of gain of cylinder strength. While this may be acceptable to
strength of plain concrete is a function of age, describe the 28-day performance of different con-
curing method, and temperature of curing. Knowl- crete mixes, it does not necessarily hold that this
edge of how the various concrete strengths relationship could adequately describe the rate of

ACI JOURNAL/ JULY 1976 405


All specimens were cast at 72 F (22 C). To ex-
amine the effect of time on the concrete, speci-
ACI member N. J, Gardner is a professor of civil en- mens were cured at 72 F (22 C) for different
gineering at the University of Ottawa, Canada. His cur-
rent rese~rch interests are into the strength behavior of periods before exposing them to low temperatures.
fresh concrete as it relates to construction and the hori- One-third of the specimens of each series were
zont~l pressure exerted by wet concrete on vertical form
surf~ces. Dr. Gordner is a member of ACI Committees 215, cured for 1 day, one-third were cured for 3 days,
Fatigue of Concrete, and 347, Formwork for Concrete. and the remainder were cured for 7 days at 72 F
S. M. Poon was formerly a research assistant with the (22 C) before being transferred to the cooler en-
Department of Civil Engineering at the University of Ottawa.
The work described in this paper is based upon Mr. Poon's vironment.
M. Eng. thesis.
Each series involved the casting of 160 standard
6 x 12-in. (150 x 300-mm) cylinders and 80 bond
specimens. Single-use waxed paper molds were
used as tests have shown that cylinders cast in
gain of tensile, bond, or shear strength with time. single-use molds are as consistent an indicator of
Unfortunately no references are available on the concrete quality as cylinders cast in steel molds. 4 •5
variation of. the bond or shear strength of concrete Five specimens were tested for compressive
with age and curing temperature and only one, strength, tensile strength, and bond strength at
Klieger, 3 on the gain of tensile (flexural) strength. 1, 3, 7, 14, and 28 days and at 3 months for each of
Klieger found that the compressive and flexural the 14 curing schedules. All concretes had a speci-
strengths obtained from different types of port- fied cylinder strength of 4000 psi (28 MN/m 2 ), a
land cement concretes initially increase with an specified slump of 2-3 in. (50-75 mm), and a
increase in initial curing temperature; but the water-cement ratio of approximately 0.5.
higher the early-age curing temperature, the
lower the final strengths of the concrete. The
variation of compressive strength and flexural CURING PROCEDURE
strength with temperature for concrete made with Wet burlap was used to cover the molds and
different cements were similar in behavior and specimens until the specimens were removed
varied in degree only. from the molds. A polyethylene sheet was placed
The investigation described here had as its ob- over the burlap to minimize evaporation. At 1,
jective to determine the variation in compressive 3, or 7 days the appropriate number of specimens
strength, tensile strength, and bond strength of were stripped and transferred to the cold rooms
various standard concretes with age when cured for extended curing at either 55 F (13 C) or 35 F
at steady below normal temperatures. Shear (2 C), or to the moist curing cabinets, depending
strength was not included in this study partly on the series of tests. During the extended curing
because pure shear failures are rare, and partly the specimens were also covered with wet burlap
because there is no standard simple test to de- kept moist until the day of test.
termine shear strength.
COMPRESSION TEST
EXPERIMENTAL INVESTIGATION The compressive strength was determined using
A total of six series of specimens were cast; the standard compressive strength test as de-
three series were made using Type I ordinary scribed in ASTM C 192 and C 39, using the stand-
portland cement concrete and three series using ard 6 x 12-in. (150 x 300-mm) cylinders, except for
Type III, high-early-strength, cement concrete. the temperature and humidity provisions.
The specimens for each series of tests were cast
from a single batch of ready-mixed concrete. TENSILE STRENGTH
Two series of tests, one made with Type I ce- Due to the large number of specimens required
ment concrete and one with Type III cement con- the split cylinder test as specified in ASTM C 496
crete, were carried out with the concrete con- was chosen as the indicator of tensile strength.
tinuously moist cured at 72 F (22 C). Two series
of specimens, one made using Type I cement con-
crete and one with Type III cement concrete, were BOND STRENGTH TEST
subjected to extended curing, under wet burlap, The standard bond strength test procedure de-
at a steady temperature of 55 F (13 C). The re- scribed in ASTM C 234 uses a #6 (19 mm) rein-
maining two series were subjected to extended forcing bar cast either into a 6 in. (150 mm) con-
curing under wet burlap at a steady temperature crete cube or a 6 x 6 x 12-in. (150 x 150 x 300-mm)
of 35 F (2 C). block of concrete. The test consists of placing the

406 ACI JOURNAL/ JULY 1976


TABLE I--SUMMARY OF STRENGTH RESULTS, TYPE I CEMENT CONCRETE
Curing temperature 35 F (2 C) 55 F (13 C) 72F (22C)

Days at 72 F (22 C) 1 3 7 1 3 7 All

! Strength,
I
I
Age psi Mean (o) • Mean (o) Mean (o) Mean (o) Mean (o) Mean (o) Mean (o)

1 day Compressive 1150 (37) 1140 (43) 919 (26)


Tensile 173 (5) 176 (6) 159 (12)
Bond 322 (15) 314 (13) 339 (29)
3 days Compressive 1720 (59) 1850 (52) 1828 (66) 1870 (91) 1632 (41)
Tensile
Bond
225
467 (11)
(20) I 252 (13)
496 (23)
236 (11)
480 (21)
246 (6)
505 (24)
272 (25)
559 (32)
7 days Compressive 2380 ( 101) 2510 (72) 2650 (92) 2570 (79) 2650 (73) 2720 (91) 2554 (48)
Tensile 278 (14) 304 (14) 336 (13) 305 (17) 315 (11) 330 (8) 386 (28)
Bond 612 (27) 645 (29) 735 (35) 632 (19) 680 (24) 710 (26) 788 (42)
14 days Compressive 3232 (83) 3404 (138) 3515 (123) 3407 (96) 3560 (98) 3573 (169) 3048 (176)
Tensile 355 (20) 380 (14) 403 (17) 358 (22) 374 (18) 410 (19) 423 (30)
Bond 792 (21) 816 (28) 840 (37) 790 (25) 855 (36) 875 (28) 833 (36)
28 days Compressive 3603 (145) 3645 (164) 3726 (113) 3761 (161) 3680 (136) 3738 (112) 3540 (184)
Tensile 392 (15) 402 (17) 420 (18) 435 (60) 410 (33) 430 (55) 459 (18)
Bond 840 137) 855 (46) 870 (41) 865 (45) 882 (30) 905 (25) 920 (66)
3 months Compressive 4016 ( 179) 3940 (119) 3890 ( 172) 4393 (141) 4140 (144) 4033 (112) 3878 (174) t
Tensile 442 (19) 447 120) 430 (12) 575 (92) 567 (60) 513 (48) 516 (39) t
Bond 935 (46) 915 (35) 905 131) 955 (27) 950 (31) 925 (27) 1033 (122) t
-------- I I
* o = standard deviation
·!·Different test operator
Note: 1 psi =6895 N/m'.

block in a testing machine so that the reinforcing curing at the low temperatures is commenced the
bar can be drawn out of the concrete. However, in higher the ultimate strength. Curing for 1 day at
view of the large number of specimens it was 72 F (22 C) and then at 35 F (2 C) gives a higher
not possible to purchase enough cube molds to strength at 90 days than curing for 3 days or 7
use the standard procedure. As the object of the days at 72 F (22 C) and then at 35 F (2 C). How-
investigation was to study the variation in ever, in the context of construction practice it is
strength with age and temperature a modified the rate of strength gain from placing to 28 days
test specimen was devised. Specimens were made which is important and for this criteria the longer
by casting a #6 reinforcing bar into a 6 x 6-in. the specimens are cured at 72 F (22 C) the higher
(150 x 150-mm) cylindrical block of concrete to the strength between 7 days and 28 days.
approximate as closely as possible the standard It was assumed that the relationship between
specimen. tensile or bond strength and the compressive
All specimens behaved in essentially a similar strength would be a simple power law relationship,
manner with failure occurring by longitudinal as a more involved relationship, however accurate,
splitting of the concrete. would be too cumbersome to use. By reduction of
the experimental data it was determined that both
DISCUSSION OF RESULTS the tensile strength and the bond strength are
The experimental results are summarized in proportional to the 0.8 power of the cylinder
Tables 1 and 2 for Type I and Type III cement strength at a given age. As shear capacity is gen-
concretes. For each group of five test results the erally limited by diagonal tensile failure, it can
mean and the standard deviation of the five in- be assumed that this relationship also holds for
dividual results are given. It can be concluded that the shear stress.
the in-batch variations were acceptably small with To verify that the 0.8 power relationship does not
coefficients of variation of the order of 6 percent. have a trend with age the quantities f',r""inll(hnnd 1/
For vis u ali z a ti on the respective concrete (f,.'} o.R normalized with respect to the 28-day
strengths are plotted against log time in Fig. 1 for quantity are given in Tables 3 and 4 for tensile
concrete made with Type I cement and subjected strength and bond strength. Noting that for con-
to extended curing at 35 F (2 C). This visualization struction problems the strength gain from 3 to 28
is typical of all six batches of concrete. It can be days is of interest, it can be seen that the 0.8 power
observed that all variants of concrete strength law exhibits no significant trend for Type I ce-
increase with age for each of the curing schedules. ment concrete for either tensile strength or bond
It is interesting to note, and consistent with the strength. There is a slight trend for Type III ce-
results of other investigations, that the earlier the ment concretes for both tensile strength and bond

ACI JOURNAL/JULY 1976 407


TABLE 2-SUMMARY OF STRENGTH RESULTS, TYPE Ill CEMENT CONCRETE

Curing temperature 35 F (2 C) 55F (13C) 72 F (22 C)

Days at 72 F (22 C) 1 3 7 1 3 7 All


----- ----
Strength
Age psi Mean (a)* Mean (a) Mean (a) Mean (a) Mean (a) Mean (a) Mean (a)

1 day Compressive 1650 (43) 2080 (94) 2468 (99)


Tensile 210 (14) 260 (8) 382 (24)
Bond 475 (14) 593 (27) 852 (36)
3 days Compressive 2540 (121) 2710 (112) 3050 (86) 3140 ( 127) 3392 (117)
Tensile 260 (13) 309 ( 12) 336 (14) 354 (17) 450 (12)
Bond 693 (37) 776 (34) 823 (39) 850 (40) 991 (42)
7 days Compressive 3490 (183) 3560 (167) 3620 (159) 4110 (166) 3780 (142) 4030 (187) 3837 (154)
Tensile 332 (14) 347 (15) 390 (18) 410 (11) 388 (18) 426 (18) 483 (9)
Bond 890 (29) 925 (68) 950 (29) 1030 (32) 925 (32) 1020 (46) 1050 (24)
14 days Compressive 3879 (158) 4010 (122) 4079 (170) 4760 (155) 4386 (185) 4563 (196) 4269 (95)
Tensile 362 (17) 380 (27) 408 (18) 465 (13) 427 (11) 433 (17) 513 (19)
Bond 970 (64) 1010 (31) 1045 (47) 1160 (32) 1030 (35) 1100 (52) 1090 (38)
28 days Compressive 4348 (222) 4300 (122) 4363 (136) 5082 (208) 4633 (139) 4916 (192) 4986 (151)
Tensile 410 (19) 397 (22) 418 (17) 495 (19) 450 (15) 456 (30) 550 (29)
Bond 1020 (39) 1050 (44) 1060 (58) 1195 (40) 1070 (31) 1130 (52) 1165 (24)
3 months Compressive 4820 (275) 4750 (194) 4260 (208) 5750 (219) 5597 (221) 5433 (234) 5364 (375) H
Tensile 450 (18) 422 (19) 428 (26) 540 (20) 503 (26) 488 (14) 582 (57)!
Bond 1100 (36) 1110 (25) 1080 (52) 1250 (40) 1210 (71) 1190 (47) 1276 (91)

*a = standard deviation
tThree specimens only
tDifferent test operator
Note: 1 psi = 6895 N/m2 •

strength but the 0.8 power is conservative if the


28-day strength is taken as the base quantity.
~
z SPEC. STRENGTH =
4000 psi (28MN/m2 J This conclusion is significant because the tensile,
::E 4000 AVE. SLUMP =: 2 TO 3 in (50 TO 75 mm J
':!1. Wfc RATIO 0.5 = bond and probably the shear strength available
:c
• NO AIR CONTENT at day x (x < 28 days) is less, as a fraction of the
......
~ 3000
28-day quantity, than would be calculated using
w
g:c2o.oJ COMPRESSIVE // CURED 7 DAYS AT 72"FC22b ft', f' bond, or vc' proportional to 'Y fc'. While very
/~.'}(_CURED
(f)

w 3 DAYS AT 72"FC22"CJ
few structures are sensitive to the compressive
>
Ui 2000 /
/
. . strength of concrete, the available tensile, bond,
...--
(f)
w ,--./ CURED 1 DAY AT 7tFC2tCJ and shear capacity of a reinforced concrete ele-
cr
a._ ./' ment should be verified against the required ca-
:::i:( 10.0 )
0 EXTENDED CURING AT 35°F ctc J pacities for construction loads or other early age
u 1000~---~--~--~--~----L--J
1 7 14 28 90 loads. In the context of construction there is ap-
AGE OF TEST - DAYS
proximately a 5 percent and 9 percent gain in the
1000,_------------------~ 7-day and 14-day strengths of Type I cement con-
cretes subjected to extended curing at 35 F (2 C)
z~ ( 6,0) and 55 F (13 C) by increasing the curing time at
::;: 8 00
Ul
72 F (22 C) from 1 day to 3 days and 1 day to 7
I
.
c..
days, respectively. Similarly the 7-day and 14-day
......
BOND
strengths of Type III cement concretes extended-
~ 600
~ (4.0) cured at 35 F (2 C) increase by some 3 percent
(f)

D
and 6 percent by increasing the curing time at
z 72 F (22 C) from 1 day to 3 days and 1 day to 7
0
m 40 0
cr days, respectively. However for Type III cement
0
concretes cured at 55 F (13 C) no conclusions can
~ ( 2.0)
g,! 20 0
be inferred on the benefits of extended curing at
w
......
72 F (22 C).

7 14 28 90
AGE OF TEST- DAYS CONCLUSIONS
Fig. !-Variation of concrete strength with temperature 1. Temperature influences tensile and bond
for Type I cement concrete cured at 35 F (2 C) strength development of concrete in much the

408 ACJ JOURNAL/ JULY 1976


TABLE 3-VERIFICATION 0~ NORMALIZED POWER TABLE 4--VERIFJCA TION OF NORMALIZED POWER
LAW RELATIONSHIP-TENSILE STRENGTH LAW RELATIONSHIP-BOND STRENGTH

Type I cement concrete Type I cement concrete

Curing 72 F Curing 72 F
temperature 35F (2C) 55 F (13 C) (22C) temperature 35 F (2C) 55 F (13 C) (22 C)

Average Average
Da[s cured Days <'Ured
at 7 F (22 C) 1 3 7 1 3 7 All at 72 F (22 C) 1 3 7 1 3 7 All
---------- - - -- ------ -- - - ---
Age at test, Age at test,
days days
1
3
1.10
1.04
-
1.08
-
-
1.05
0.97
-
1.03
-
-
1.02
1.10
1.06
1.04
1
3
0.96
1.00
-
1.00
-
-
0.94
0.99
-
0.98
-
-
1.08
1.13
0.99
1.02
7 0.99 1.02 1.05 0.95 1.00 0.99 1.09 1.01 7 1.02 1.02 1.11 0.99 1.00 1.01 1.11 1,04
14 0.99 1.00 1.01 0.89 0.94 0.99 1.04 0.98 14 1.03 1.01 1.01 0.99 1.00 1.00 1.02 1.01
28 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 28 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00
90 1.03 1.04 0.99 1.17 1.26 1.12 1.05 1.09 90 1.02 1.01 1.01 0.98 0.98 0.96 1.04 1.00

Type Ill cement concrete Type Ill cement concrete

Curing 72 F Curing 72 F
temperature 35 F (2 C) 55 F (13 C) (22C) temperature 35 F (2 C) 55 F (13 C) (22 C)
Average -- Average
Days cured Days cured
at 72 F (22 C) 1 3 7 1 3 7 All at 72 F (22 C) 1 3 7 1 3 7 All
-------- -- -- ------ -----------
Age at test, Age at test,
days days
1
3
1.11
0.98
-
1.13
-
-
1.07
1.02
-
1.07
-- 1.22
1.11
1.13
1.06
1 1.01 - - 1.01 - - 1.28 1.10
7 0.97 1.02 1.08 0.98 1.01 1.10 1.08 1.03
3 1.04 1.07 - 1.04 1.08 - 1.16 1.08
7 1.04 1.02 1.04 1.02 1.02 1.06 1.11 1.04
14 0.97 1.01 1.03 0.99 0.99 1.08 1.06 1.02 14 1.04 1.02 1.04 1.02 1.01 1.03 1.06 1.03
28 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 28 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00
90 1.01 0.98 0.98 0.99 0.96 0.99 1.00 0.99 90 0.99 0.98 0.97 0.95 0.97 0.97 1.03 0.98

same manner as it does compressive strength de- initial curing at 72 F (22 C) when subjected to
velopment. Compressive strength, tensile strength, extended curing at 55 F (13 C).
and bond strength are all related, and an increase
in one is reflected similarly in the others.
ACKNOWLEDGMENT
2. The compressive strength, tensile strength, The authors gratefully acknowledge the financial
and bond strength of concrete at early ages in- support of the National Research Council of Canada
creases with increased curing temperature. The under Grant No. A5645.
lower the initial curing temperature the greater
the eventual ultimate strength of the concrete, REFERENCES
provided curing is continuous.
1. Agarwal, R. K., and Gardner, Noel J., "Form and
3. Bond strength and tensile strength are pro- Shore Requirements for Multistory Flat Slab Type
portional to the 0.8 power of the cylinder strength Buildings," ACI JouRNAL, Proceedings V. 71, No. 11,
at the appropriate age. Neither extended curing Nov. 1974, pp. 559-569.
at temperatures of 35 F (2 C) and 55 F (13 C) or 2. McKaig, Thomas H., Building Failures; Case Studies
in Construction and Design, McGraw-Hill Book Co.,
type of cement appear to have any significant New York, 1962, 261 pp.
effect on the interrelationship of bond strength or 3. Klieger, Paul, "Effect of Mixing and Curing Tem-
tensile strength and cylinder strength. perature on Concrete Strength," ACI JouRNAL, Proceed-
4. With respect to construction schedules there ings V. 54, No. 12, June 1958, pp. 1063-1081.
is a 5 percent to 9 percent gain in the 7-day and 4. Burmeister, Robert A., "Tests of Paper Molds for
Concrete Cylinders," ACI JouRNAL, Proceedings V. 47,
14-day strengths due to casting and curing Type I No. 1, Sept. 1950, pp. 17-24.
cement concretes for 3 days and 7 days, respec- 5. Price, Walter H., "Factors Influencing Concrete
tively at 72 F (22 C), compared to casting and Strength," ACI JouRNAL, Proceedings V. 47, No. 6, Feb.
curing for 1 day at 72 F (22 C). 1951, pp. 417-432.
5. Type III cement concretes exhibited a small
strength gain due to prolonged initial curing at
72 F (22 C) when subjected to extended curing
Received July II, 1975, and reviewed under Institute publication
at 35 F (2 C) but no strength gain for prolonged policies.

ACI JOURNAL/ JULY 1976 409

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