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BRITISH STANDARD BS EN

12697-17:2004
Licensed Copy: SHU Athens, Sheffield Hallam University, 23/11/2007 09:09, Uncontrolled Copy, (c) BSI

Incorporating
amendment no. 1

Bituminous mixtures —
Test methods for hot
mix asphalt —
Part 17: Particle loss of porous asphalt
specimen

The European Standard EN 12697-17:2004, incorporating amendment


A1:2007, has the status of a British Standard

ICS 93.080.20

12&23<,1*:,7+287%6,3(50,66,21(;&(37$63(50,77('%<&23<5,*+7/$:
BS EN 12697-30:2004
Licensed Copy: SHU Athens, Sheffield Hallam University, 23/11/2007 09:09, Uncontrolled Copy, (c) BSI

National foreword

This British Standard is the UK implementation of EN 12697-17:2004,


incorporating amendment A1:2007.
The UK participation in its preparation was entrusted by Technical Committee
B/510, Road materials, to Subcommittee B/510/1, Coated macadam and hot
asphalt.
A list of organizations represented on this subcommittee can be obtained on
request to its secretary.
This publication does not purport to include all the necessary provisions of a
contract. Users are responsible for its correct application.
Compliance with a British Standard cannot confer immunity from
legal obligations.

Amendments issued since publication


This British Standard was
published under the authority
of the Standards Policy and Amd. No. Date Comments
Strategy Committee on
30 June 2004
17282 31 August 2007 Implementation of CEN amendment
A1:2007.
© BSI 2007

ISBN 978 0 580 59832 6


Licensed Copy: SHU Athens, Sheffield Hallam University, 23/11/2007 09:09, Uncontrolled Copy, (c) BSI

EUROPEAN STANDARD EN 12697-17:2004+A1


NORME EUROPÉENNE
EUROPÄISCHE NORM July 2007

ICS 93.080.20 Supersedes EN 12697-17:2004

English Version

Bituminous mixtures - Test methods for hot mix asphalt - Part


17: Particle loss of porous asphalt specimen

Mélanges bitumineux - Méthodes d'essai pour mélange Asphalt - Prüfverfahren für Heißasphalt - Teil 17:
hydrocarboné à chaud - Partie 17: Perte de matériau des Kornverlust von Probekörpern aus offenporigem Asphalt
éprouvettes d'enrobé drainant

This European Standard was approved by CEN on 1 April 2004 and includes Amendment 1 approved by CEN on 16 May 2007.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the
official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION


COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: rue de Stassart, 36 B-1050 Brussels

© 2007 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 12697-17:2004+A1:2007: E
worldwide for CEN national Members.
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EN 12697-17:2004+A1:2007 (E)

Contents page

Foreword..............................................................................................................................................................3
1 Scope ......................................................................................................................................................6
2 Normative references ............................................................................................................................6
3 Apparatus ...............................................................................................................................................6
4 Preparation of test specimen ...............................................................................................................6
5 Procedure ...............................................................................................................................................7
6 Calculation..............................................................................................................................................7
7 Test report ..............................................................................................................................................8
8 Precision .................................................................................................................................................8

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EN 12697-17:2004+A1:2007 (E)

Foreword
This document (EN 12697-17:2004+A1:2007) has been prepared by Technical Committee CEN/TC 227
“Road materials”, the secretariat of which is held by DIN.

This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by January 2008 and conflicting national standards shall be withdrawn at
the latest by January 2008.

This document includes Amendment 1, approved by CEN on 2007-05-16.

This document supersedes EN 12697-17:2004.

The start and finish of text introduced or altered by amendment is indicated in the text by tags ! ".

This European Standard is one of a series of standards as listed below:

EN 12697-1, Bituminous mixtures — Test methods for hot mix asphalt — Part 1: Soluble binder content

EN 12697-2, Bituminous mixtures — Test method for hot mix asphalt — Part 2: Determination of particle size
distribution

EN 12697-3, Bituminous mixtures — Test methods for hot mix asphalt — Part 3: Bitumen recovery: Rotary
evaporator

EN 12697-4, Bituminous mixtures — Test methods for hot mix asphalt — Part 4: Bitumen recovery:
Fractionating column

EN 12697-5, Bituminous mixtures — Test methods for hot mix asphalt — Part 5: Determination of the
maximum density

EN 12697-6, Bituminous mixtures — Test methods for hot mix asphalt — Part 6: Determination of bulk density
of bituminous specimens

EN 12697-7, Bituminous mixtures — Test methods for hot mix asphalt — Part 7: Determination of bulk density
of bituminous specimens by gamma rays

EN 12697-8, Bituminous mixtures — Test methods for hot mix asphalt — Part 8: Determination of void
characteristics of bituminous specimens

EN 12697-9, Bituminous mixtures — Test methods for hot mix asphalt — Part 9: Determination of the
reference density

EN 12697-10, Bituminous mixtures — Test methods for hot mix asphalt — Part 10: Compactability

EN 12697-11, Bituminous mixtures — Test methods for hot mix asphalt — Part 11: Determination of the
affinity between aggregate and bitumen

EN 12697-12, Bituminous mixtures — Test methods for hot mix asphalt — Part 12: Determination of the water
sensitivity of bituminous specimens

EN 12697-13, Bituminous mixtures — Test methods for hot mix asphalt — Part 13: Temperature
measurement

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EN 12697-17:2004+A1:2007 (E)

EN 12697-14, Bituminous mixtures — Test methods for hot mix asphalt — Part 14: Water content

EN 12697-15, Bituminous mixtures — Test methods for hot mix asphalt — Part 15: Determination of the
segregation sensitivity

EN 12697-16, Bituminous mixtures — Test methods for hot mix asphalt — Part 16: Abrasion by studded tyres

EN 12697-17, Bituminous mixtures — Test methods for hot mix asphalt — Part 17: Particle loss of porous
asphalt specimen

EN 12697-18, Bituminous mixtures — Test methods for hot mix asphalt — Part 18: Binder drainage

EN 12697-19, Bituminous mixtures — Test methods for hot mix asphalt — Part 19: Permeability of specimen

EN 12697-20, Bituminous mixtures — Test methods for hot mix asphalt — Part 20: Indentation using cube or
Marshall specimens

EN 12697-21, Bituminous mixtures — Test methods for hot mix asphalt — Part 21: Indentation using plate
specimens

EN 12697-22, Bituminous mixtures — Test methods for hot mix asphalt — Part 22: Wheel tracking

EN 12697-23, Bituminous mixtures — Test methods for hot mix asphalt — Part 23: Determination of the
indirect tensile strength of bituminous specimens

EN 12697-24, Bituminous mixtures — Test methods for hot mix asphalt — Part 24: Resistance to fatigue

EN 12697-25, Bituminous mixtures — Test methods for hot mix asphalt — Part 25: Cyclic compression test

EN 12697-26, Bituminous mixtures — Test methods for hot mix asphalt — Part 26: Stiffness

EN 12697-27, Bituminous mixtures — Test methods for hot mix asphalt — Part 27: Sampling

EN 12697-28, Bituminous mixtures — Test methods for hot mix asphalt — Part 28: Preparation of samples for
determining binder content, water content and grading

EN 12697-29, Bituminous mixtures — Test method for hot mix asphalt — Part 29: Determination of the
dimensions of a bituminous specimen

EN 12697-30, Bituminous mixtures — Test methods for hot mix asphalt — Part 30: Specimen preparation by
impact compactor

EN 12697-31, Bituminous mixtures — Test methods for hot mix asphalt — Part 31: Specimen preparation by
gyratory compactor

EN 12697-32, Bituminous mixtures — Test methods for hot mix asphalt — Part 32: Laboratory compaction of
bituminous mixtures by vibratory compactor

EN 12697-33, Bituminous mixtures — Test methods for hot mix asphalt — Part 33: Specimen prepared by
roller compactor

EN 12697-34, Bituminous mixtures — Test methods for hot mix asphalt — Part 34: Marshall test

EN 12697-35, Bituminous mixtures — Test methods for hot mix asphalt — Part 35: Laboratory mixing

EN 12697-36, Bituminous mixtures — Test methods for hot mix asphalt — Part 36: Determination of the
thickness of a bituminous pavement

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EN 12697-17:2004+A1:2007 (E)

EN 12697-37, Bituminous mixtures — Test methods for hot mix asphalt — Part 37: Hot sand test for the
adhesivity of binder on precoated chippings for HRA

EN 12697-38, Bituminous mixtures — Test methods for hot mix asphalt — Part 38: Common equipment and
calibration

EN 12697-39, Bituminous mixtures — Test methods for hot mix asphalt — Part 39: Binder content by ignition

EN 12697-40, Bituminous mixtures — Test methods for hot mix asphalt — Part 40: In situ drainability

EN 12697-41, Bituminous mixtures — Test methods for hot mix asphalt — Part 41: Resistance to deicing
fluids

EN 12697-42, Bituminous mixtures — Test methods for hot mix asphalt — Part 42: Amount of foreign matters
in reclaimed asphalt

EN 12697-43, Bituminous mixtures — Test methods for hot mix asphalt — Part 43: Resistance to fuel

According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and United Kingdom.

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EN 12697-17:2004+A1:2007 (E)

1 Scope
This European Standard describes a test method for determining the particle loss of porous asphalt mixtures.
Particle loss is assessed by the loss of mass of porous asphalt samples after turns in the Los Angeles
machine. This test enables the estimation of the abrasiveness of porous asphalt. The test applies to laboratory
compacted porous asphalt mixtures the upper sieve size of which does not exceed 25 mm. It does not reflect
the abrasive effect by studded tyres.

2 Normative references
This European Standard incorporates by dated or undated reference, provisions from other publications.
These normative references are cited at the appropriate places in the text, and the publications are listed
hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to
this European Standard only when incorporated in it by amendment or revision. For undated references the
latest edition of the publication referred to applies (including amendments).

EN 1097-2, Tests for mechanical and physical properties of aggregates — Part 2: Methods for the
determination of resistance to fragmentation

!EN 12697-6:2003+A1", Bituminous mixtures - Test methods for hot mix asphalt - Part 6: Determination
of bulk density of bituminous specimens.

EN 12697-8, Bituminous mixtures - Test methods for hot mix asphalt - Part 8: Determination of void
characteristics of bituminous specimens.

!EN 12697-30:2004+A1", Bituminous mixtures - Test methods for hot mix asphalt - Part 30: Specimen
preparation, impact compactor.

EN 12697-31, Bituminous mixtures - Test methods for hot mix asphalt - Part 31: Specimen preparation by
gyratory compactor.

!EN 12697-35:2004+A1, Bituminous mixtures - Test methods for hot mix asphalt - Part 35: Laboratory
mixing."

3 Apparatus
3.1 Los-Angeles-machine, as specified in EN 1097-2.

3.2 Thermometer, capable of covering the test temperature range with an accuracy of ± 0,5 °C.

3.3 Chamber, room or enclosure, large enough for the Los-Angeles-machine. During the test, the air
temperature in the chamber shall remain constant to the test temperature ± 2 °C. The air temperature shall be
measured near the Los-Angeles-machine.

3.4 Oven, equipped with a closed ventilation system or a chamber fitted with a thermostatic control to
maintain the test temperature constant in vicinity to the samples, stored prior to the test, to ± 1 °C.

3.5 Balances, of suitable capacity for the mass to be weighed with an accuracy of ± 0,1 g.

4 Preparation of test specimen


4.1 At least five specimens shall be prepared for each sample tested.

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EN 12697-17:2004+A1:2007 (E)

4.2 The cylindrical specimens shall have a diameter of (100 ± 3) mm and a height of
(63,5 ± 5,0) mm. !The asphalt shall be mixed in accordance with EN 12697-35:2004+A1 and specimens
compacted" as specified in !EN 12697-30:2004+A1", compacted by 2 × 50 blows, or EN 12697-31,
compacted by 40 gyrations.

NOTE The compaction method has an influence on the result.

4.3 After the specimens have been compacted and removed from the mould, their density and void content,
if required, shall be determined in accordance with !EN 12697-6:2003+A1" (Procedure D: bulk density by
dimensions) and EN 12697-8.

4.4 Prior to testing, the specimens shall be stored on a flat surface for at least 2 days at a temperature of
not more than 25 °C.

5 Procedure
5.1 The test temperature shall be defined and maintained in the chamber during the test with an uncertainty
of ± 2 °C. Before testing, specimens shall be kept at the test temperature for at least 4 h.

NOTE Test temperature has a very large influence on the test result. Temperatures between 15 °C and 25 °C are
usually used for design purposes. For porous asphalt in cold climate zones, temperatures representing the low
temperature local conditions can also be used. The test is not adequate for temperatures above 35 °C.

5.2 The mass of specimen shall be determined and W1 (see clause 6) shall be recorded. One specimen
shall then be placed inside the Los-Angeles-machine drum and, with the metal balls removed, the drum shall
be turned at 3,1 rad/s to 3,5 rad/s (30 rpm to 33 rpm) for 300 turns.

5.3 When the test is completed, the specimen shall be removed from the machine, slightly cleaned by
means of a cloth eliminating particles that are clearly loose, and weighed again. The reading W2 (see
clause 6) shall be recorded.

5.4 The test shall be repeated in the same way for each of the specimens prepared according to clause 4.

NOTE Observation as to whether the fractures occur within the stone particles, in the binder film or at the boundaries
between the stone particles and the binder can indicate the type of failure which can be used to redesign the mixture in
order to improve this property. These observations can be included in the test report.

6 Calculation
6.1 The particle loss PL shall be calculated for each specimen test using the following equation:

(W1 − W2 )
PL = 100 × (1)
W1

where
PL is the value of particle loss, in per cent (%);

W1 is the initial specimen mass, in grams (g);

W2 is the final specimen mass, in grams (g).

6.2 The result shall be given as average value of five single values. The result shall be rounded to the
nearest 1 %.

6.3 If required, the density and voids of the samples as well as the test temperature shall be included in the
test report.

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EN 12697-17:2004+A1:2007 (E)

!NOTE The density of the specimens can affect the result because the mass of a specimen will influence the
impact force imparted on contact during the test whereas it is loading from the mass of the vehicles, as imparted through
the tyres, that will affect the performance of the asphalt on site. Therefore, it is recommended that the density should be
given when asphalt with aggregates of particularly high or low density are tested."

7 Test report
The test report shall include the following information:

a) Identification of samples;

b) date of preparation and testing;

c) test temperature;

d) the average particle loss;

e) density and voids of samples, if required;

f) the type of failure, if required;

g) name of person performing the test;

h) number and date of this European Standard;

i) comments of any anomalies, if any, which might have affected the results.

8 Precision
8.1 The following uncertainties shall apply:

 For particle loss below 40 %: Uncertainties for repeatability r = 2 % and for reproducibility R = 4 %;

 for particle loss equal to or higher than 40 %: Uncertainties for repeatability r = 5 % and for reproducibility
R = 8 %.

8.2 The study of repeatability and reproducibility was carried out by 4 laboratories in accordance with
ISO 5725 under the following conditions:

 test temperature: 25 °C;

 two porous asphalts for each level of particle loss;

 mixture compacted according to !EN 12697-30:2004+A1" (2 × 50 blows);

 number of replicates: five.

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BS EN
12697-17:2004
BSI — British Standards Institution
Licensed Copy: SHU Athens, Sheffield Hallam University, 23/11/2007 09:09, Uncontrolled Copy, (c) BSI

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