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Lec – 08
Filtration and Batch Filtration (Part -03)
Welcome to the 3rd lecture of week 2 and which is on filtration we are discussing filtration and
we have already discussed this in lecture 1 and lecture 2 and here we will discuss filtration cycle
and further we will solve a few examples based on filtration process, so let us start this filtration
cycle now if you see the filtration cycle.
How the filtration cycle is defined is the time required for filtration time required for washing
and time required for cleaning dumping and reassembling of the system so that complete time is
basically called as the filtration cycle, so filtration cycle that is t cycle is defined as t f + t wash + tetc.
so t cycle is defined as tf + t wash +t etc. tf is the time required for filtration t wash is the time
required for washing the cake that can be defined as volume of wash water / rate of washing and
t etc is time for draining filling opening dumping the cake and reassembling here we are
considering the case the constant pressure with incompressible slug and we are assuming filter
media resistance to be negligible.
So considering all these factors we have the equation dt / dV – K PV that is constant pressure and
incompressible slug KP we have defined like this as we have seen in the last lecture so once we
integrate it we can get the expression t – KP V 2/ 2 = tf because this t if is we see that will be the
time associated with the filtration, so this t value we can equate to tf that is time required for
flirtation.
Now here we can define x which is nothing but the ratio of volume of wash water used to the
final volume of literate collected it means x is the factor which is which gives the ratio of ratio
between volume of water required in washing divided total volume collected during filtration
process and why is the ratio of rate of washing to the final rate of filtration, so this x and y are
basically relating the parameter associated with washing and parameter associated with
filtration, so time required for washing is t wash = x V f / y 1/ KP Vf now x Vf, Vf is the final
volume of filtrate that is collected and into x so that should be the volume of wash water and
similarly y x 1/ KP Vf now if you see the filtration equation when we consider d V / dt that should
be the rate of filtration so it is value should be 1/KPV so that we have put over her and y is the
ratio so this complete factor will give the rate of filtration.
So x/ y KPVf 2 now t cycle is t cycle consists of tf twash and t etc putting the value of tf and putting
the expression if tf and t wash over here we can get this expression as t cycle now we have to
optimize the cycle time and the bases of this we have considered the totals volume collected in 1
day that is the bases, so that volume which you have to collected that should we have to
maximize to optimize the cycle time so number of cycles per day so 24 / t c ycle is the time
associated with one cycle so 24 as we have to perform for single days so 24/t cycle.
So daily collection of the filtrate V f is the volume of filtrate collected in a single cycle so 24c / t
e that it should be the total number of cycles into V f so that we have defined as Vd now putting
cycl
here the expression of t cycle this is the expression of Vd ay that is volume collected in a day, now
if we consider this particular expression Vday is a function of Vf
So tf + t wash = t etc. So when we consider constant pressure with incompressible slug considering
0 media resistances the optimum cycle for this optimum cycle time for this is the time required
for filtration as well as washing should be = to the time required for dumping cleaning
reassembling etc…
So this is the case of constant pressure and in compressible cake now what we have to do over
here is in part a compute the time required to wash the cake form at the end of 90 minutes of
flirting at the same pressure using 5m 3 of wash water so here we have to calculate the washing
time and second part if the time for during the cake and reassembling the press is 1 hour what is
the optimum cycle time And volume of filtrate collected per day wash water is used in the same
proposition to the final filtrate as in part A.
So here first of all we have to calculate the time required for washing and then we have to
optimize the filtrations cycle. So as for us operating data is concern this is the data we have
optioned by batch filtration where according to the tome filtrate volume vary so this is the data
for batch filtration.
So we can calculate Δt over here that is this time – this time and similarly this minus this that is
squared easy calculation and here we have Δv difference in the volume so this minus this 1.99
further this minus this 1.56 in the similar line we can calculate other values of Δv. Now once we
have the value of v and Δv we can calculate V avg how that Vavg expression is if you see that is V +
Δv/ 2.
So here 1 point so here 6.1 + 1.99/2 so that should be 7.095 and for other cases we can also
calculate Vavg and here we have Δt as well as Δv division of this two will give these value now
we can draw the graph between Δt/Δv and Vavg.
Now if we reverse this if we reverse dv/dt that should becomes the rate of filtration so time of
washing is to be predicted at the end of 90 minute of filtration at the same pressure, so here what
we have to do is whatever rate of filtration at the end of 90 minute the same rate we can consider
as the rate of washing because operation is carried out at same pressure. So here we have dv/dt F
because we have used the final rate so that should be equal to 1/40 V f + 40. Vf is the volume Vf is
the final volume of filtrate collected at the end of 90 minutes.
And we solving this equation we can find V f as 15.4621 m3 and final rate of filtration as we have
seen in the last slide is dv/dt = 1/40 V f + 40, now this Vf is the final volume of filtrate when we
put its value which is 15.4621 over here, we can get final rate of filtration which should be equal
to 0.00152 m3 / s and here you can understand that as per the problem the rate of washing will
depend on final rate of filtrations.
So rate of washing in this case should also be equal to 0.00152 m 3 /sec so we already know the
rate of washing we know the volume of wash water used and that should be 5m 3 therefore time
required to wash the cake should be volume of wash water / rate of filtration. So that comes as
3292.42 second that is 54.87 minutes, so here we have solved the first part of this, now the ratio
of volume of wash water to final filtrate volume.
That is V wash/ Vf if you remember this factor we have defined as x so that factor comes as
0.3234.
So Vf is the total volume collected in single cycle so that we should multiplied with total number
of cycle. So 24 x 300 x V f / tcycle and further while putting all values of all known values we can
get Vday = 86400Vf / this expression that is the expression of tcycle , now to maximize this Vday we
will differentiate with respect to Vf and equate it to 0, so Vf optimum is 10.455 m3 and tcycle
optimum cycle time is this much, so while putting the value of V f over here we can get 7753.46
second that is 2.154 hours, so that is total cycle time which is already optimized, so that is
optimum cycle time. So in this way we can calculate we can optimize the cycle time we can
calculate total time required for washing.
The experimental data of constant pressure filtration is already given, now if you see this table
here we have 3 values of pressure but for one pressure whole filtration process will be carried out
and then the pressure value is change and then whole filtration process will be carried out then
the pressure value is changed and then hold filtration process will be carried out so here we have
though here we have three different values of pressure but this is constant pressure phenomenon.
So K 'p we have find out like this there we have we can found the value of s and value of R m can
be found by the value of B so here we have to find the ∆t/∆V and the average so ∆t for all
different pressures we can find at this discussing the last example ∆V we can calculate because
volume corresponding time is known so ∆V we can calculate and for V average we can calculate.
As we have see in the last example and see only ∆t/∆v it can be calculated for different pressures
now what we have to do we have to draw the graph between ∆t/∆V at this average.
(Refer Slide time: 19:48)
So you see here we have for three different pressures three lines are here so here we have three
different pressures and therefore three different curve R m at clearly in this graph it is drawn
between ∆t/∆V and the average while drawing the line for each case we can find different slopes
as well as different B values.
So for ∆P that is 10 if we consider this 10 so this is the graph it has K'p, K'p it has the slope like
this and B we have like this so if you see all this graph we can conclude if we observe the slope it
has a higher slope then this and then this. Similarly the values are appear in this table. We can
also calculate from the intersect and those are available over here.
Once you know the value of B we can calculate R m value because we know other factors other
parameters so Rm can be calculated directly from the B value. So as we have three values three
Rm value we will operate and every time these three R m value will be the final value of Rm that is
filter may be an resistance.
So if we consider the value of this that should be equal to 1-s which is .8889 so from here we can
calculate value of s which comes as .111 so in this we can calculate factors which are associated
with the filter as well as compressible cake.
So what we have to calculate the washing time if washing rate is 1/3 rd of filtration rate and
secondly filtering surface is double, remaining other conditions constant, how long it take to
produce 25m3 of filtrate.
So washing rate if you see washing rate is basically consider as 1/3rd of the rate of filtration so
2m3/h is the rate of the equation so washing rate of filtration the rate of washing should be .667
1/3rd of that. Therefore washing time should be total volume of the wash water we are using
divide by .6667, so 6 hours should be washing time.
So revised coefficient value should be 4*160 160 is the previous coefficient values so final k'
should be 40m 6 per hour time to produce 25m 3 of filtrate that should be V2/K' is which you see
the phenomena equation volume we can put as 25m 3 solving this we can get .976 hour that is
58.6 minutes.
Now here we would like this to see should be the time required to generate for 40m 3 of filtrate
then filtered area when area of filter is doubled so in that case because k is proportional to area
square so when we doubled the area 4 times for 40m3 for generation of 40m3 of filtration will
required 2.5 hours instead of 10 hours.
So you have seen the examples we make you to understand how the equations will be used to
calculate the factors as well as you see the equation process so here we have the summary of the
lecture and you should keep in mind that the summary is for lecture 1 2 and 3 so in this series the
3 lectures filtration operations along with its types and operation is discussed.
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