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2. Explain Wallace- Tierman method of measuring ionization detector in process gas chromatog-
raphy.
3. (a) Give the principle and operations of photo ionization detector in process gas chromatog-
raphy.
(b) Explain with sketches electron capture detector in gas chromatography.
4. Explain the principle of operation and working of oxygen analyzer. Describe detectors and
sampling used.
7. With schematic diagram, describe the working and principle of time of flight mass spectrometer.
8. (a) Draw the schematic of Geiger counter and explain the principle of operation.
(b) Describe with a neat sketch the construction and application of a proportional counter.
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Code :R7411003 2
IV B.Tech I Semester(R07)Regular Examinations, November/December 2010
ANALYTICAL INSTRUMENTATION
(Electronics & Instrumentation Engineering)
Time: 3 hours Max Marks: 80
Answer any FIVE questions
All questions carry equal marks
?????
3. (a) Explain with neat sketches photometric detector operation in liquid chromatography sys-
tem.
(b) Explain in detail fluorometric detector use in liquid chromatography.
7. Write short notes operation and merits, demerits of the following instruments.
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Code :R7411003 3
IV B.Tech I Semester(R07)Regular Examinations, November/December 2010
ANALYTICAL INSTRUMENTATION
(Electronics & Instrumentation Engineering)
Time: 3 hours Max Marks: 80
Answer any FIVE questions
All questions carry equal marks
?????
1. (a) Explain how output potential of pH electrode is related to pH value and also for H + ion
concentration? Give related equations.
(b) How the potential of pH electrode changes with temperature?
(c) Write about reference electrodes for pH measurement.
2. (a) With block diagram explain any one type of sodium analyzer.
(b) Write short notes on clinical sodium analyzer.
4. Compare and list merits and demerits of non-dispersive infrared analyzer over gas chromatog-
raphy in carbon monoxide estimation.
5. Give principles and operation of IR spectrophotometer. Describe various sources and detectors
used IR spectrophotometer.
7. (a) Write the range of radio frequency(RF). Discuss the working principle of radio frequency
mass spectrometer.
(b) Point out differences between RF mass spectrometer and other types of mass spectrometer.
8. (a) Describe various radiation detectors used for measuring the radio activity?
(b) Explain the principle and working of any one radiation detector.
?????
Code :R7411003 4
IV B.Tech I Semester(R07)Regular Examinations, November/December 2010
ANALYTICAL INSTRUMENTATION
(Electronics & Instrumentation Engineering)
Time: 3 hours Max Marks: 80
Answer any FIVE questions
All questions carry equal marks
?????
1. (a) Explain the working principle of Beckman zeromatic pH meter, with diagrams.
(b) Discuss the temperature compensation for direct reading type pH meter.
2. (a) Explain with neat sketch the dissolved oxygen electrode system.
(b) Explain the construction and operation of hydrogen gas electrode.
5. (a) Explain the advantages and disadvantages associated with single and double beam spec-
trophotometers.
(b) Discuss the requirement of chopper in spectrophotometer.
7. With block diagram, explain the operation and constructional details of NMR spectrophotome-
ter.
8. Explain the characteristics of ionization type of detectors with necessary sketches and graphs.
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