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5/11/2012

Overview
Brewing With Fruit  Fruit Characteristics important to Brewing
Kevin Wright – Hangar 24 Brewery
 Available Fruit Products
◦ Manufacture of
◦ Processing Pros/Cons
 Adding Fruit to Beer
◦ When in process
◦ Yeast Impacts
◦ Flavor Impacts
 Microbiological Impact

Nutrient Content (Fresh Fruit) Nutrient Content (Fresh Fruit)


Sugar (%) Water (%) Protein (%)
Fig 16.3 Watermelon 91.5 Guava 2.6
Grape (Table) 15.5 Strawberry 91.0 Pomegranate 1.7
Pomegranate 13.7 Grapefruit 90.9 Apricots 1.4
Mango 13.7 Lemon 89.0 Currant (red) 1.4 Sugar Water Protein
Cherry (Sweet) 12.8 Peach 88.9 Blackberry 1.4
Banana
Kiwi
12.2
11.0
Lime
Blackberry
88.3
88.2
Kiwi
Raspberry
1.2
1.2
Apricot 9.2% 86.4% 1.4%
Tangerine 10.6 Papaya 88.1 Lemon 1.1
Apple 10.4 Plum 87.2 Banana 1.1 Blueberry 10.0% 84.2% 0.7%
Blueberry 10.0 Cranberry 87.1 Cherry (Sweet) 1.1
Plum
Pineapple
9.9
9.9
Orange
Apricots
86.8
86.4
Cherry (Sour)
Orange
1.0
0.9
Cherry(Sour) 8.5% 86.1% 1.0%
Pear 9.8 Cherry (Sour) 86.1 Peach 0.9
Orange 9.4 Pineapple 86.0 Mango 0.8 Cherry(Sweet) 12.8% 82.3% 1.1%
Apricots 9.2 Raspberry 85.8 Tangerine 0.8
Guava
Cherry (Sour)
8.9
8.5
Tangerine
Apple
85.2
85.0
Fig
Blueberry
0.8
0.7
Orange 9.4% 86.8% 0.9%
Peach 8.4 Blueberry 84.2 Grape (Table) 0.7
Papaya 7.8 Currant (red) 84.0 Lime 0.7 Raspberry 4.4% 85.8% 1.2%
Currant (red) 7.4 Pear 83.7 Plum 0.7
Grapefruit 7.0 Mango 83.5 Strawberry 0.7
Watermelon 6.2 Kiwi 83.2 Grapefruit 0.6
Strawberry 4.9 Cherry (Sweet) 82.3 Watermelon 0.6
Blackberry 4.9 Guava 80.8 Pineapple 0.5
Raspberry 4.4 Grape (Table) 80.5 Papaya 0.5
Cranberry 4.0 Fig 79.1 Cranberry 0.4
Lemon 2.5 Pomegranate 77.9 Pear 0.4
Lime 1.7 Banana 74.9 Apple 0.3

http://www.ars.usda.gov/SP2UserFiles/Place/12354500/Data/SR24/reports/sr24fg09.pdf

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Sugar Breakdown (Fresh Fruit) Sugar Breakdown (Fresh Fruit)


Total Sugars Sucrose Glucose Fructose Other
Grape (Table) 15.5% 1.0% 46.5% 52.5% 0.0%
Mango 13.7% 51.0% 14.7% 34.3% 0.0%
Cherry (Sweet) 12.8% 1.2% 51.4% 41.9% 5.5%
Total
Banana 12.2% 19.5% 40.7% 39.7% 0.1%
Kiwi 11.0% 0.5% 47.4% 51.7% 0.5%
Sugars Sucrose Glucose Fructose Other
Tangerine 10.6% 57.2% 20.1% 22.7% 0.0%
Apricot 9.2% 63.5% 25.6% 10.2% 0.6%
Apple 10.4% 19.9% 23.4% 56.8% 0.0%
Blueberry 10.0% 1.1% 49.0% 49.9% 0.0% Blueberry 10.0% 1.1% 49.0% 49.9% 0.0%
Plum 9.9% 15.8% 51.1% 30.9% 2.2%
Pineapple 9.9% 60.8% 17.6% 21.5% 0.0% Cherry (Sour) 8.5% 9.4% 49.2% 41.3% 0.0%
Pear 9.8% 8.0% 28.2% 63.6% 0.2%
Apricots 9.2% 63.5% 25.6% 10.2% 0.6%
Cherry (Sweet) 12.8% 1.2% 51.4% 41.9% 5.5%
Cherry (Sour) 8.5% 9.4% 49.2% 41.3% 0.0%
Orange 9.4% 50.4% 23.2% 26.5% 0.0%
Peach 8.4% 56.7% 23.2% 18.2% 1.7%
Papaya 7.8% 0.0% 52.3% 47.7% 0.0% Raspberry 4.4% 4.5% 42.1% 53.2% 0.0%
Currant (red) 7.4% 8.3% 43.7% 47.9% 0.0%
Watermelon 6.2% 19.5% 25.5% 54.2% 1.0%
Strawberry 4.9% 9.6% 40.7% 49.9% 0.0%
Blackberry 4.9% 1.4% 47.3% 49.2% 2.0%
Raspberry 4.4% 4.5% 42.1% 53.2% 0.0%
Cranberry 4.0% 3.2% 81.2% 15.6% 0.0%

Acidity (pH & TA) Acidity (pH & TTA)


Total Acidity
1(low) - 5(High) Type pH

 pH  Total Acidity (TA) Cranberry


Currant (red)
5
5
Citric/Malic
Citric
2.4

◦ Measure of [H+] ions ◦ Measures amount of Acids


Grapefruit 5 Citric 3.3
Kiwi 5 Citric

 Dissociated  Dissociated & Bound Lemon


Lime
5
5
Citric
Citric
2.3
1.9

◦ Gives indication of acidic ◦ Used Primarily in Wine & Apricots


Blueberry
4
4
Malic
Citric
3.5
3.3

“strength” Mead Making Cherry (Sour)


Guava
4
4
Malic 3.2

◦ Many impacts (buffers) ◦ Measured by Titration Orange


Raspberry
4
4
Citric
Citric
3.5
3.3

◦ Measured by Meter ◦ Malic, Citric & Tartaric Tangerine


Apple
4
3 Malic 3.6

◦ More impact on ◦ More impact on Taste & Blackberry


Cherry (Sweet)
3
3
Malic
Malic
4.2
4.5

Processes Mouthfeel Grape (Table)


Pineapple
3
3
Tartaric/Malic
Citric
4

◦ Wine Levels: 0.50% - 0.85% Pomegranate


Strawberry
3
3 Citric 3.4

◦ Mead: 0.35% - 1.0% Fig


Mango
2
2
Malic
5.9

◦ Beer: 0.3% - 1.5% Peach


Plum
2
2
Malic
Malic
3.7
2.9
Banana 1 Malic/Citric 4.8
Papaya 1
Pear 1 Malic 3.8
Watermelon 1 5.4

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Acidity (pH & TTA) Tannins


 Polyphenol Compounds found in Grain
Total Acidity Husks, Hops, Spices, Fruits, etc
1(low) - 5(High) Type pH
 Astringency sensation in Mouthfeel
Apricot 4 Malic 3.5
 Haze
Blueberry 4 Citric 3.3
Cherry(Sour) 4 Malic 3.2  Balance in character
Cherry(Sweet) 3 Malic 4.5
Orange 4 Citric 3.5  Wide variety & intensity in Fruit Products
Raspberry 4 Citric 3.3
 Decrease as Fruits Ripen

Tannins in Fruit Pectin


 High Tannins  Polysaccharide found in Plants
◦ Apricots
◦ Berries (Black, Blue, Rasp)  High concentration in Skins
◦ Currants
 Used primarily in Jam Production also in
◦ Peaches
◦ Persimmons Pharmeceuticals
◦ Pomegranates
 Can Cause Haze in Beer
 Medium Tannins
◦ Apples  Needs High Temp to “Set” (180F)
◦ Cherries
◦ Grapes  Cleared with Pectinases
 Low or No Tannins
◦ Bananas
◦ Citrus Fruits
◦ Pineapple Image 1

◦ Strawberries
◦ Watermelon
Image 2

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5/11/2012

Fruit Products Available Fresh Fruit


 Fresh  Locally Picked/Sourced
 Frozen  Ripeness important – ripe flavor & aroma
 Puree vs appearance
 Concentrate  Use resources to obtain
 Dehydrated ◦ Work with Local Farmers
◦ Farmers Markets
 Freeze-Dried
◦ Contact Packing Houses
 Powdered
◦ Fruit Boards
 Extract & Essence
◦ Ag. Department

Image 3

Fresh Fruit Pros & Cons Processing Fresh Fruit


 Pros  Cons  Juicing  Pureeing
◦ Local Partnership ◦ Availability
◦ Authenticity  Seasonality
 Regionality
◦ Flavors & Aromas
◦ Variety ◦ Difficult to Process
◦ Know the Source ◦ Consistency
◦ Can be Cheaper ◦ Difficult to Incorporate Image 4

 Local = Less Shipping ◦ Pesticides & Fertilizers


 Less than Perfect ◦ Microbial Fruit Press
Appearance Contamination Risk
◦ Shelf Life Image 5

◦ Solids
Doing it Yourself vs. Sourcing Out – Talk with Growers

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5/11/2012

Frozen Fruit Fruit Puree


 Commercially Bought or Do-It-Yourself  Should be 100% fruit
 Effect on Cellular Structure  Fruit pressed through various sized
◦ Flash Freezing vs. Regular Freezing screens
 Similar Pros & Cons to Fresh Fruit  Some Loss of Material
◦ No Seasonality ◦ ~20% (by weight) for Pitted Fruit
◦ Less Contamination Risk ◦ ~12% for Seeded Fruit
◦ Potential Flavor Loss  Flash Pasteurized
◦ Storage Space/Costs  Packaged Aseptically
◦ Check for Additives

Image 6 Images 7 & 8

Fruit Puree Pros & Cons Fruit Puree – Solids Testing


 Pros  Cons  15 mL puree (6 samples each) Massed
◦ Easier to work with ◦ Expensive  Centrifuge 10 min
◦ Aseptic ◦ Heavy  Supernatant Liquid Removed
◦ Consistent ◦ Heat Pasteurization  Precipitate Massed
◦ Availability  Flavor Degradation
 Percentages (average)
 Pectins
◦ Apricot: 34.2% Solids
◦ Source
◦ Blueberry: 55.2% Solids
◦ Storage
◦ Cherry: 51.4% Solids
◦ Solids
◦ Raspberry: 39.9% Solids
 Some Potential Breakdown by Yeast

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5/11/2012

Fruit Concentrate Fruit Concentrate Pros & Cons


 Fruit cleaned, separated, pureed &  Pros  Cons
pasteurized (if concentrate is frozen) ◦ Easy to Use ◦ Flavor Degradation
 Cold Extraction ◦ Consistent ◦ Heat processing =
◦ Less Storage Space pectin
 Evaporation Plant ◦ Costs?
◦ Aseptic
 Finished Sugar Concentration: 10 – 65 Brix ◦ Processing Aids
 Pasteurization ◦ Origin
◦ Solids (Puree)
 Concentrated Puree
 Concentrated Juice (more processing)

Dehydrated Fruit Dehydrated Fruit Pros & Cons


 Start with Fresh Whole or Sliced Fruit  Pros  Cons
 Dehydrator to Dry (Slight Heating) ◦ Flavor Concentration ◦ Processing Aids
◦ Less Space ◦ Preparing for Use
 Finished Product has 10-15% Moisture
◦ Lower Cost ◦ Flexibility
◦ Less Water Added ◦ Flavor Extraction
◦ Flavor Degradation
◦ Consistency
◦ Origin
◦ Solids

Image 9

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5/11/2012

Freeze Dried Fruit Freeze Dried Fruit


 Freeze Drying Process  Fruit Rapidly Cooled to Freeze Water
◦ Rapid Freezing Protects Cellular Structure

Freeze Dried Fruit Freeze Dried Fruit Pros & Cons


 Pressure Reduced with Slight Heat to  Pros  Cons
Promote Sublimation ◦ Availability ◦ Check for Processing Aids
◦ Finished Moisture ~1% ◦ Very Light ◦ Use in Production
◦ Very Stable ◦ Cost
◦ Less Needed ◦ Consistency?
◦ Flavor Integrity ◦ Origin
◦ Minimum Water
◦ Astronaut Technology

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5/11/2012

Fruit Powder Fruit Extract


 Starts as Dehydrated Fruit  Natural vs. Artificial
◦ Natural: “Natural” Source (WONF)
 Dried to 3% Moisture ◦ Artificial: Manufactured Flavor & Aroma
 Milled to Size (Pieces, Granules, Powder) Chemicals
 Solvent Extract
 Pros & Cons Similar to Dehydrated ◦ Alcohol
◦ Easier to Use ◦ CO2
◦ Faster Flavor Extraction ◦ Propylene Glycol
 Cold Press/Maceration & Settling
 Homogenized Oils
 Powdered Extract = Spray Dried

Image 10

Fruit Extract Pros & Cons Adding Fruit


 Pros  Cons  Mash
◦ Simple to Use ◦ Flavor Authenticity  Kettle
◦ Extremely Consistent ◦ Production Of
 Whirlpool
◦ Low Cost ◦ Balance Needed
◦ Easy Storage ◦ “Real” vs “Not Real”  Fermenter
◦ No Pectins ◦ Labeling  Long-Term Storage
 At Packaging

Image 11 Image 12

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Mashed Fruit? Mashed Fruit?


 Most Practical for Whole or Pureed  Significant Loss of Flavor
 Easy to Add  Bad Bang for Buck
 Easy to Clean up “Fruit Trub”  Color Pickup

 No Risk of Contamination  No Real Benefit for


Concentrate, Powder or
 Limited Pectin
Extract

 Verdict: Not Most Practical

Kettle Addition Whirlpool Addition


 Easy To Add  Easy to Add
 Limited Contamination Risk
 No Contamination Risk
 Removal of “Fruit Trub”
 Removal of “Fruit Trub”  Pectin Issues
 Pectin Issues  Pumping & Transferring Issues
 Calandria Issues  Heat Exchanger Issues
 Mechanical Separation
 Pumping/Transferring Issues ◦ Decanter
 Volatilization of Aromas ◦ Centrifuge?
◦ Filter
◦ Settling
 Verdict: Practical in Some Applications
 Verdict: Practical in Some Applications

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5/11/2012

Pre Heat Exchanger Bag Filter Pre Heat Exchanger Bag Filter

Whirlpool
Polyester Filter Bag Pump Heat Exchanger
Bag Filter
Multiple Mesh Sizes: 10 – 800 micron
Stainless Steel Filter Housing
Multiple Sizes 4” – 8” Diameter (McMaster #s 9307T7, 98315K66)
Images 13 & 14

Fermenter Ways to Add Fruit


 Volatilization (Primary Fermentation)  Open Fermenter or Large Top Access
 Greatest Risk for Microbial Contamination
 Challenges Adding
 Flavor Extraction (Time) 6” Port
 Secondary Fermentation
 Minimal Pectin
 Difficult Removal of “Fruit Trub”
 Maximum Flavor Pickup for Many Forms

 Verdict: Practical in Many Applications

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Ways to Add Fruit Ways to Add Fruit


 Secondary Vessel  Push in Puree/Concentrate/Liquid

CO2

Ways to Add Fruit Ways to Remove “Fruit Trub”


 Recirculation with Secondary “Dosing” Tank  Leave Behind
◦ Racking Arm
◦ Stand Pipe

 Removal
Fruit Added In ◦ Filtration
◦ Centrifuge

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Long Term Aging At Packaging


 In Tanks  Need for Control
 In Barrels  Direct into BBT
 Long Flavor Extraction ◦ Aroma Loss if Force Carbonating
 Some Challenges Adding Fruit  In line into Bottling/Kegging
 Settling of Pectins
 Challenge Adding
 Microbial Contamination – May be
Desired for Sour Beers
 Verdict: Practical for Liquid and Maybe
 Verdict: Practical for Some Applications Powdered Extract

How Much Fruit To Add? Equivalencies


 Wide Variations Depending on Source Apricots
Fresh
1.00
Puree Concentrate Dehydrated Freeze Dried
0.80 0.20 0.25 0.15
lbs/gal lbs/bbl Blackberries 1.00 0.90 0.15 0.30 0.10
Apples 0.5 - 1.0 15 - 30 Blueberries 1.00 0.90 0.15 0.25 0.15
Apricots 0.25 - 2.0 8 - 60 Cherries(Sour) 1.00 0.85 0.30 0.25 0.10
Blackberries 0.5 - 4.0 15 - 120 Cherries(Sweet) 1.00 0.85 0.30 0.25 0.13
Blueberries 0.5 - 3.0 15 - 90 Citrus 1.00 0.85 0.15 0.25 0.10
Cherries(Sour) 0.25 - 2.0 8 - 60
Currants 1.00 0.95 0.15 0.25 0.10
Cherries(Sweet) 0.33 - 4 10 - 120
Peaches 1.00 0.80 0.20 0.40 0.12
Citrus 0.25 - 1.0 8 - 30
Plums 1.00 0.80 0.20 0.40 0.12
Currants 0.33 - 1.5 10 - 45
Raspberries 1.00 0.90 0.13 0.30 0.10
Peaches 0.5 - 5.0 15 - 150
Strawberries 1.00 0.90 0.15 0.25 0.15
Pears 0.5 - 2.0 15 - 60
Plums 0.5 - 2.0 15 - 60
Raspberries 0.25 - 2.0 8 - 60

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Fermentation Pilot Specs Flavor Impact Studies


20 lbs per bbl (Equivalent Fruit Weight) Cherry(sweet) Puree
 92% 2-row, 8% Caramel 10 
added to Mash
◦ No Perceivable Flavor Impact
 12 Plato S.G.
◦ Appreciable Color Pickup
 152 F Mash  10 & 20 lbs per bbl (EFW) Cherry(sweet) Puree added to
Whirlpool
 15 IBU ◦ Perceivable Flavor Difference
◦ Very Subtle Flavor Contribution
 60 min boil ◦ Specific Fruit Flavor Unidentifiable
5, 10 & 20 lbs per bbl (EFW) Cherry(sweet) Puree added to
 1 mil cells/mL/P

Fermenter after Primary Fermentation
◦ 5 – No Real Flavor Perception (Slight Color)
 Fermented @ 70 F
◦ 10 – Flavor/Color Perception Slight. No Identification of Cherry
Flavor
◦ 20 – Flavor/Color Perception. Split Identification of Cherry Flavor

Flavor Impact Studies Yeast Health Impact Studies


 Dosing in Cherry Extract to Light Lager Fruit Pilot Fermentation Plots

◦ Recommended Rate 0.35% - 0.65% 16

 0.35% - Strong Aroma, “Cherry Candy” Flavor 14


 0.65% - Overly Strong Aroma & Flavor
◦ Acid addition (Phosphoric) at 0.025% 12

 pH drop approximately 0.2 10


 Improved Mouthfeel & “Brightness” of Flavor
Gravity (P) 8 Control
Cherry

 Overall: Better Aroma w/ Extract, Flavor is Subjective 6 Orange

0
0 20 40 60 80 100 120 140
Time in Hours from Pitch

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5/11/2012

Microbial Impact Sources of Fruit Products


Fruit Sources

 All Fresh Fruit has Microbes on Surface Company Fruit Types Website
American Spice Powder, Dehydrated www.americanspice.com
 Some Studies show 100s of Different Bare Fruit
Bella Viva Orchards
Dehydrated
Dehydrated
www.barefruitsnacks.com
www.bellaviva.com

 Small Scale Collection & Growth Project


Beta Foods Puree, Concentrate, Frozen, Dehydrated www.betapure.com
Bulk Foods Dehydrated www.bulkfoods.com
Dennick Fruit Source Puree, Concentrate www.dennickfruitsource.com

◦ Succeeded in Growing Bacteria & Yeast Faerie's Finest


Fruit Fast
Extract, Powder
Concentrate
www.faeriesfinest.com
www.brownwoodacres.com

◦ Limited Translation to Beer


Greenwood Associates Juice, Concentrate, Puree, Essence www.greenwoodassociates.com
Hill View Packing Co. Juice, Concentrate www.hillviewpacking.com
iTi Tropicals Puree, Concentrate www.ititropicals.com
◦ No Identification Yet Juice Products Unlimited
Just Tomatoes
Concentrate
Freeze Dried
none (312) 654-5000
www.justtomatoes.com

Peracetic Acid Wash


Kanegrade Concentrate, Puree, Essence, Freeze Dried www.kanegrade.com
 Kerr Concentrate
Mayan Sun
Concentrate, Puree, Essence
Powder
www.kerrconcentrates.com
www.mayansun.net

◦ 80 ppm wash North Bay Trading Co.


Northwest Berry Co-op
Freeze Dried
Puree, Concentrate
www.northbaytrading.com
www.nwberrycoop.com

◦ Interesting Results – Need More


Northwest Naturals Concentrate www.nwnaturals.com
Northwestern Extracts Extract www.nwextract.com
Oregon Fruit Puree Puree www.oregonfruit.com
Experimentation Perfect Puree
San Francisco Herb Co.
Puree, Concentrate
Dehydrated, Powder
www.perfectpuree.com
www.sfherb.com
Traverse Bay Farms Concentrate, Dehydrated, Powder www.traversebayfarms.com
Vita-Pakt Citrus Puree, Juice, Frozen, Dehydrated www.vita-pakt.com

Flavor Impact Studies


 Raspberry Puree addition at 60 lbs per bbl (EFW)
to Fermenter after Primary Fermentation (Brown Questions???
Porter Base Beer)
◦ Overpowering Flavor & Aroma
 Freeze Dried Apricot addition at 13 lbs per bbl
(EFW) to Whirlpool (Wit Base Beer)
◦ Perceivable Apricot Flavor & Aroma
◦ Taste for Yourself
 Raspberry Extract (WONF) addition at 0.5% total
Volume at Packaging (Strong Porter Base Beer) kwright@hangar24brewery.com
◦ Perceivable Raspberry Flavor & Aroma
◦ Taste for Yourself

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Bibliography Image Credits


 Daniels, Ray. Designing Great Beer. Brewers Publications, Boulder,  Image 1: http://www.nicolaiswallner.com/how-to-treat-skin-healthy-fruit.html
CO. 2000.  Image 2: http://sci-toys.com/ingredients/pectin.html
 Kunze, Wolfgang. Technology Brewing & Malting. Versuchs und  Image 3: http://uwfcenteronaging.wordpress.com/2011/11/22/get-involved-pensacola-area-
pick-fruit-to-fight-hunger/
Lehranstalt, Berlin, Germany. 2004.  Image 4: http://www.cookiescotland.com/blog/tag/wine/
 Lewis, Michael J & Young, Tom W. Brewing 2nd Edition. Aspen  Image 5: http://www.hobartcorp.com/products/food-prep/cutter-mixers/
Publishers, New York, NY. 2001.  Image 6: http://www.almightydad.com/fitness-nutrition/fresh-fruits-and-vegetables-buy-
 Mosher, Randy. Radical Brewing. Brewers Publications, Boulder, CO. frozen
2004.  Image 7: http://www.123rf.com/photo_7501072_baby-food-puree-of-fruit.html
 Image 8: http://www.pregnancyandbaby.com/baby/articles/945537/homemade-pureed-
 Rivard, Dominic. The Ultimate Fruit Winemaker’s Guide. Bacchus baby-food-recipes
Enterprises Ltd. 2009.  Image 9: http://www.backpackingchef.com/dehydrating-fruit.html
 Schramm, Ken. The Compleat Meadmaker. Brewers Publications,  Image 10: http://www.mayansun.net/products.html
Boulder, CO. 2003.  Image 11: http://www.pony.us/2010/06/08/crafts/craft-of-the-month-summer-mist-
spray.html/attachment/eye-dropper
 Sparrow, Jeff. Wild Brews. Brewers Publications, Boulder, CO. 2005.
 Image 12: http://www.hangar24brewery.com/media_files/OW_3D_Bottle.jpg
 USDA Nutritional Facts. 2012. USDA. April 2, 2012,  Image 13 & 14: www.mcmaster.com
<http://www.ars.usda.gov/SP2UserFiles/Place/12354500/Data/SR24/
reports/sr24fg09.pdf>.

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