JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201

LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

Data Koreksi Timbangan BAA 09.09 Tahun 2016

No Koreksi x x+s x+2s x+3s x-s x-2s x-3s
1 0.00017 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
2 0.00017 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
3 0.00027 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
4 -0.00003 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
5 -0.00043 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
6 0.00012 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
7 0.00012 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
8 0.00012 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
9 0.00022 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
10 0.00002 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
x 0.000075 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
s 0.000198 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
x+s 0.000273 0.0001 0.0003 0.0005 0.0007 -0.0001 -0.0003 -0.0005
x+2s 0.000471
x+3s 0.000669
x-1s -0.000123
x-2s -0.000321
x-3s -0.000519
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANALITIK AT-201

LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

Tahun 2016

Control Chart Balance Analytical (BAA 09.09) Tahun 2016

Massa Anak Timbang = 50.00003

0.0029 s
No Tanggal Koreksi Paraf
0.0027

1 1/7/2016 0.00017 0.0025

0.0023
2 2/1/2016 0.00017
0.0021

3 4/6/2016 0.00017 0.0019

0.0017
4 5/2/2016 0.00017
Koreksi

0.0015

0.0013
5 6/3/2016 0.00002
0.0011
6 7/4/2016 0.00023 0.0009

0.0007
7 8/1/2016 0.00017
0.0005

8 9/2/2016 0.00023 0.0003

0.0001
9 10/4/2016 0.00013
-0.0001 1 2 3 4 5 6 7 8 9 10 11 12 13

10 11/3/2016 0.00043 -0.0003

-0.0005
11 12/7/2016 0.00258
-0.0007

12 Rusak
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201
LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

Data bobot anak timbang

No Koreksi x x+s x+2s x+3s x-s
1 0.00017 0.0001 0.0004 0.0008 0.0011 -0.0003
2 0.00002 0.0001 0.0004 0.0008 0.0011 -0.0003
3 0.00007 0.0001 0.0004 0.0008 0.0011 -0.0003
4 0.00002 0.0001 0.0004 0.0008 0.0011 -0.0003
5 0.00092 0.0001 0.0004 0.0008 0.0011 -0.0003
6 0.00012 0.0001 0.0004 0.0008 0.0011 -0.0003
7 -0.00008 0.0001 0.0004 0.0008 0.0011 -0.0003
8 0.00012 0.0001 0.0004 0.0008 0.0011 -0.0003
9 -0.00008 0.0001 0.0004 0.0008 0.0011 -0.0003
10 -0.00043 0.0001 0.0004 0.0008 0.0011 -0.0003
x 0.000085 0.0001 0.0004 0.0008 0.0011 -0.0003
s 0.000339 0.0001 0.0004 0.0008 0.0011 -0.0003
x+s 0.000424
x+2s 0.000763
x+3s 0.001102
x-1s -0.000254
x-2s -0.000593
x-3s -0.000932
LITIK AT-201
IKAMPEK

x-2s x-3s
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
-0.0006 -0.0009
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201

LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

Tahun 2016

Control Chart Balance Analytical BAA 03.06

Massa Anak Timbang = 50.00003

x x+ s x + 2s x + 3s x- s x- 2 s x- 3 s %Biu re t

No Tanggal Koreksi Paraf

0.0012
1 1/18/2016 -0.00008
0.0010
2 2/1/2016 -0.00033
0.0008
3 3/1/2016 0.00002
0.0006
4 6/6/2016 0.00027
0.0004
5 5/2/2016 0.00062
0.0002
6 6/3/2016 0.00002
0.0000
1 2 3 4 5 6 7 8 9 10 11 12
7 7/4/2016 0.00013
-0.0002
8 8/1/2016 0.00003
-0.0004
9 9/2/2016 0.00023
-0.0006
10 10/4/2016 0.00053
-0.0008
11 11/3/2016 0.00003
-0.0010
12 12/7/2016 0.00023
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201
LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

description : 10 points - control chart initial data

SOP : Direct comparison
balance used : Mettler Toledo AT 201/0.01 mg
load : 200,000092 gram
unit : mg
check standard : stainless steel 1 ASTM class
measurement process : calibration of 50 g 1 ASTM class
Data bobot anak timbang
No Bobot AT x x+s x+2s x+3s x-s
1 -0.00033 0.0001 0.0002 0.0004 0.0006 -0.0001
2 0.00027 0.0001 0.0002 0.0004 0.0006 -0.0001
3 0.00012 0.0001 0.0002 0.0004 0.0006 -0.0001
4 0.00003 0.0001 0.0002 0.0004 0.0006 -0.0001
5 0.00017 0.0001 0.0002 0.0004 0.0006 -0.0001
6 0.00002 0.0001 0.0002 0.0004 0.0006 -0.0001
7 0.00005 0.0001 0.0002 0.0004 0.0006 -0.0001
8 0.00003 0.0001 0.0002 0.0004 0.0006 -0.0001
9 0.00023 0.0001 0.0002 0.0004 0.0006 -0.0001
10 0.00013 0.0001 0.0002 0.0004 0.0006 -0.0001
x 0.000072 0.0001 0.0002 0.0004 0.0006 -0.0001
s 0.000166 0.0001 0.0002 0.0004 0.0006 -0.0001
x+s 0.000238
x+2s 0.000404
x+3s 0.000570
x-1s -0.000094
x-2s -0.000260
x-3s -0.000426
LITIK AT-201
IKAMPEK

x-2s x-3s
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
-0.0003 -0.0004
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201

LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

Tahun 2016

Control Chart Balance Analytical BAA 05.07

Massa Standar : 50.00003

No Tanggal Koreksi Paraf

x x +s x + 2s x +3 s x- s x- 2 s x- 3s %B iu re t

0.0008
1 1/6/2016 -0.00033
0.0007
2 2/2/2016 0.00027 0.0006
0.0005
3 3/3/2016 0.00012
0.0004
4 4/4/2016 0.00003 0.0003

5 5/3/2016 0.00017 0.0002

0.0001
6 6/1/2016 0.00002
0.0000
1 2 3 4 5 6 7 8 9 10 11 12
7 7/1/2016 0.00005 -0.0001
-0.0002
8 8/2/2016 0.00003
-0.0003
9 9/5/2016 0.00023 -0.0004

10 10/5/2016 0.00013 -0.0005

-0.0006
11 11/2/2016 0.00033
-0.0007

12 12/5/2016 0.0003
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201
LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

description : 10 points - control chart initial data

SOP : Direct comparison
balance used : Mettler Toledo AT 201/0.01 mg
load : 200,000092 gram
unit : mg
check standard : stainless steel 1 ASTM class
measurement process : calibration of 50 g 1 ASTM class
Data bobot anak timbang
No Bobot AT x x+s x+2s x+3s x-s
1 -0.0003 0.0001 0.0003 0.0005 0.0008 -0.0002
2 -0.0001 0.0001 0.0003 0.0005 0.0008 -0.0002
3 0.0001 0.0001 0.0003 0.0005 0.0008 -0.0002
4 0.0001 0.0001 0.0003 0.0005 0.0008 -0.0002
5 0.0006 0.0001 0.0003 0.0005 0.0008 -0.0002
6 0.0000 0.0001 0.0003 0.0005 0.0008 -0.0002
7 0.0000 0.0001 0.0003 0.0005 0.0008 -0.0002
8 0.0000 0.0001 0.0003 0.0005 0.0008 -0.0002
9 -0.0001 0.0001 0.0003 0.0005 0.0008 -0.0002
10 0.0002 0.0001 0.0003 0.0005 0.0008 -0.0002
x 0.000065 0.0001 0.0003 0.0005 0.0008 -0.0002
s 0.000234 0.0001 0.0003 0.0005 0.0008 -0.0002
x+s 0.000299
x+2s 0.000533
x+3s 0.000767
x-1s -0.000169
x-2s -0.000403
x-3s -0.000637
LITIK AT-201
IKAMPEK

x-2s x-3s
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
-0.0004 -0.0006
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANALITIK AT-201

LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

Tahun 2016

Control Chart Balance Analytical BAA 04.08

Massa Anak Timbang : 50.00003

x x+ s x +2s x + 3s x- s x- 2 s x- 3 s %Biu re t

No Tanggal Koreksi (C ) Paraf

-0.0008
1 1/6/2016 -0.00013

2 2/2/2016 -0.00023 -0.0006

3 3/4/2016 -0.00008
-0.0004

4 4/4/2016 -0.00008
-0.0002
5 5/3/2016 0.00002

6 6/1/2016 -0.00028 0.0000

7 7/1/2016 -0.00027
0.0002

8 8/3/2016 -0.00038
0.0004
9 9/5/2016 -0.00002

10 10/5/2016 -0.00037 0.0006

11 11/5/2016 -0.00012
0.0008
1 2 3 4 5 6 7 8 9 10 11 12
12 12/6/2016 -0.00007
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201
LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

description : 10 points - control chart initial data

SOP : Direct comparison
balance used : Mettler Toledo AT 201/0.01 mg
load : 200,000092 gram
unit : mg
check standard : stainless steel 1 ASTM class
measurement process : calibration of 50 g 1 ASTM class
Data bobot anak timbang
No Bobot AT x x+s x+2s x+3s x-s
1 49.9999 49.9999 50.0000 50.0001 50.0002 49.9998
2 50.0000 49.9999 50.0000 50.0001 50.0002 49.9998
3 49.9998 49.9999 50.0000 50.0001 50.0002 49.9998
4 49.9999 49.9999 50.0000 50.0001 50.0002 49.9998
5 49.9999 49.9999 50.0000 50.0001 50.0002 49.9998
6 49.9999 49.9999 50.0000 50.0001 50.0002 49.9998
7 50.0000 49.9999 50.0000 50.0001 50.0002 49.9998
8 50.0000 49.9999 50.0000 50.0001 50.0002 49.9998
9 49.9997 49.9999 50.0000 50.0001 50.0002 49.9998
10 49.9998 49.9999 50.0000 50.0001 50.0002 49.9998
x 49.999890 49.9999 50.0000 50.0001 50.0002 49.9998
s 0.000099 49.9999 50.0000 50.0001 50.0002 49.9998
x+s 49.999989 49.9999 50.0000 50.0001 50.0002 49.9998
x+2s 50.000089 49.9999 50.0000 50.0001 50.0002 49.9998
x+3s 50.000188 49.9999 50.0000 50.0001 50.0002 49.9998
x-1s 49.999791 49.9999 50.0000 50.0001 50.0002 49.9998
x-2s 49.999691 49.9999 50.0000 50.0001 50.0002 49.9998
x-3s 49.999592 49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
49.9999 50.0000 50.0001 50.0002 49.9998
LITIK AT-201
IKAMPEK

x-2s x-3s
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
49.9997 49.9996
 Control Chart Balance Analytical
No Tanggal Bobot AT x x+ s x + 2s x + 3s x- s x- 2 s x- 3 s %B iu re t

1 1/9/2015 50.0000
2 2/3/2015 49.9999 50.0003

3
50.0003
4
5 50.0002

6 50.0002
7
50.0001
8
9 50.0001
10
50.0000
11
12 50.0000
13
49.9999
14
15 49.9999

16 49.9998
17
49.9998
18
19 49.9997
20
49.9997
21
22 49.9996
23
49.9996
24
25 49.9995

26 49.9995
27
49.9994
28 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30
29
30
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201
LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

description : 10 points - control chart initial data

SOP : Direct comparison
balance used : Mettler Toledo AT 201/0.01 mg
load : 200,000092 gram
unit : mg
check standard : stainless steel 1 ASTM class
measurement process : calibration of 50 g 1 ASTM class
Data bobot Koreksi
No Koreksi x x+s x+2s x+3s x-s
1 0.00027 0.0002 0.0003 0.0005 0.0006 0.0000
2 0.00027 0.0002 0.0003 0.0005 0.0006 0.0000
3 0.00007 0.0002 0.0003 0.0005 0.0006 0.0000
4 0.00032 0.0002 0.0003 0.0005 0.0006 0.0000
5 0.00037 0.0002 0.0003 0.0005 0.0006 0.0000
6 0.00002 0.0002 0.0003 0.0005 0.0006 0.0000
7 0.00018 0.0002 0.0003 0.0005 0.0006 0.0000
8 -0.00007 0.0002 0.0003 0.0005 0.0006 0.0000
9 0.00023 0.0002 0.0003 0.0005 0.0006 0.0000
10 0.00003 0.0002 0.0003 0.0005 0.0006 0.0000
x 0.000169 0.0002 0.0003 0.0005 0.0006 0.0000
s 0.000148 0.0002 0.0003 0.0005 0.0006 0.0000
x+s 0.000317
x+2s 0.000464
x+3s 0.000612
x-1s 0.000021
x-2s -0.000126
x-3s -0.000274
LITIK AT-201
IKAMPEK

x-2s x-3s
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
-0.0001 -0.0003
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201

LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

Tahun 2016

Control Chart BAA 15.10

Massa Anak Timbang : 50.00003

x x+ s x +2 s x + 3s x- s x- 2s x- 3 s %B iu re t

No Tanggal Koreksi Paraf

0.0009
1 07/01/16 0.00027
0.0008

2 01/02/16 0.00027 0.0007

3 01/03/16 0.00007 0.0006

0.0005
4 06/04/16 0.00032
0.0004
5 02/05/16 0.00037
0.0003

6 03/06/16 0.00002 0.0002

0.0001
7 01/07/16 0.00018
0.0000
1 2 3 4 5 6 7 8 9 10 11 12
8 01/08/16 -0.00007
-0.0001

9 02/09/16 0.00023 -0.0002

10 04/10/16 0.00003 -0.0003

-0.0004
11 03/11/16 0.00013
-0.0005
12 07/12/16 0.00013
 JAMINAN MUTU HASIL KALIBRASI TIMBANGAN ANANLITIK AT-201
LABORATORIUM KALIBRASI PT. PUPUK KUJANG CIKAMPEK

description : 10 points - control chart initial data

SOP : Direct comparison
balance used : Mettler Toledo AT 201/0.01 mg
load : 200,000092 gram
unit : mg
check standard : stainless steel 1 ASTM class
measurement process : calibration of 50 g 1 ASTM class
Data bobot Koreksi
No Koreksi x x+s x+2s x+3s x-s
1 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
4 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
6 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
7 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
8 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
9 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
10 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
x #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
s #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
x+s #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
x+2s #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
x+3s #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
x-1s #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
x-2s #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
x-3s #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
LITIK AT-201
IKAMPEK

x-2s x-3s
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
#DIV/0! #DIV/0!
 Control Chart BAA 15.10
No Tanggal Koreksi 3*Deviasi Paraf x x +s x + 2s x +3 s x- s x- 2 s x- 3 s %B iu re t

1
2 0.0009

3
0.0008
4
5
0.0007
6
7
0.0006
8
9 0.0005
10
11 0.0004
12
13 0.0003

14
0.0002
15
16
0.0001
17
18 0.0000
1 2 3 4 5 6 7 8 9 10 11 12
19
20 -0.0001
21
22 -0.0002

23
-0.0003
24
25
-0.0004
26
27
-0.0005
28
29
30