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Reducing porosity in AlSi10Mg parts
processed by selective laser melting Selective Laser Melting, an alternative manufacturing technique for complex and customized parts. The chemical addition manufacturing (AM) of metallic materials from metallic powder using a heat source is referred as Selective Laser Melting. It is a sharp process, with less requirement of machines for post processing which depend on final application. SLM is environmental friendly technology as little waste is produced. Aluminum alloy powders are light with poor flowability and high reflectivity along with high thermal conductivity as compared to other SLM candidate materials. Al alloys are prone to oxidation which results in porosity. AlSi10Mg powder were used for experiment to produce test cubes. Particle size distribution for powder was determined by using laser diffraction. Parameters involved in process of SLM are scanning speed, hatch spacing, laser power and layer thickness. The aim of this study was to use design of scanning strategy to enhance the relative density of parts being processed (i.e to minimize porosity). At 50 to 100 um hatch spacing, sufficient overlap between adjacent melt pools was achieved. Small hatch spacing result in heat accumulation in melt pool since it allows slow cooling of layer giving a homogenous and continuous layer. It is suggested to use small hatch spacing. The effect of scanning speed was investigated based on the hatch spacing. At lower speed metallurgical pores are formed where as key hole pores are created with high scanning speed. Non molten powder is enclosed by keyhole pores and their formation is parameter dependent. Balling is observed on surface with increasing scan speed, it promotes the capture of powder that is not fully melted by laser beam scanning the following layer, hence keyhole pores are formed. This issue has been resolved by altering scan strategy. The best results were found at a speed of 500 mm/s, hatch spacing 50 um, and100 W laser power when using a layer thickness of 40 um and employing the pre-sinter scan strategy yielding a relative density of 99.77 ± 0.08%. However, use of Al alloy in SLM is limited because it results in parts with high degree of porosity. Al alloy are favorable in high end applications for their strength and stiffness to weight ratio. AlSi10Mg are used in die casting, automotives and aerospace industries.
Selective laser melting of AlSi10Mg alloy:
Process optimization and mechanical properties development Additive layer manufacturing (ALM) has been used for various materials. It is based on electron beam melting (EBM), direct laser fabrication (DLF), and selective laser melting (SLM). Factors affecting final quality of SLM samples are feedstock material characteristics (powder size, morphology and size distribution) and laser heat input. Statistical design approach has been adopted to optimize the process parameters and to minimize defects. To eliminate porosity with in material, a high laser power, at low scan speed with small hatch spacing should be used. Kempen et al. [2013] suggested optimum process parameter of 200W, 1400mm/s, with scan spacing 105um. Additionally, Brandl et al. [2012] used 250W, 500mm/s, 150 um scan spacing, with 50um layer thickness to achieve defect-free SLM of the AlSi10Mg alloy. The porosity content decreases with increasing the energy density. Olakanmi [2010] also indicated that there is a certain threshold energy density that gives maximum material density, which is 60–75J/mm3 for Al, Al–Si and Al–Mg alloys. A statistical method has been used to evaluate the influence of process parameters on the porosity of SLMed AlSi10Mg, which shows the trends of porosity in the SLM fabricated samples. There is a critical energy density point that gives the minimum pore fraction for this alloy, approximately 60J/m3. The build direction does not strongly influence the tensile or creep strength of SLMed AlSi10Mg. Both building directions show higher strength than die cast A 360, although the elongation is inferior to that of A360. Fracture surfaces show the presence of significant amounts of un-melted powder, which give rise to local cracking. Further work is required to see if it is possible to eliminate these regions.
Selective laser melting of AlSi10Mg:
Influence of post-processing on the micro structural and tensile properties development Impact of thermal post processing using Hot Isostatic Pressing (HIPping ) and/or T6- peak aging treatment, post-process machining, as well as the build orientation on the microstructural and mechanical properties development inAlSi10Mg alloy fabricated using Selective Laser Melting (SLM) has been studied. The builds are found to contain fine columnar grains, with a fine Si-enriched cellular dendritic network, resulting in tensile strengths exceeding the castings. This development was attributed to the high cooling rates experienced during SLM. To clarify the as-fabricated microstructure and strength, thermal modelling was engaged which predicted cooling rates of 105–106 °C/s during solidification. Voids formed as result of oxide films were observed using Micro-C T in the as-fabricated condition. HIPping results in collapsed of most voids, showing no trace even after a additional T6 treatment. Generally, the tensile properties of the majority of conditions were significantly better than in the cast + T6 equivalent alloy. Post-process machining plays role to improve the strength (compared to the as fabricated surface). On other side, HIPping+T6 allowed the builds to achieve the required tensile properties, with no surface machining. By assessing the influence of powder recycling, it was realized that the void content linked to oxide layer formation amplified following powder recycling, resulting in drop in tensile properties.
Effect of heat treatment on AlSi10Mg alloy
fabricated by selective laser melting: Microstructure evolution, mechanical properties and fracture mechanism The influence of solution and artificial aging heat treatments on the microstructures and mechanical properties of SLM-produced AlSi10Mg alloy parts was investigated. Owing to the high cooling rate of SLM, an ultrafine eutectic microstructure in the as-built samples is characterized by using spherical nano-sized network eutectic Si embedded in the Al matrix, which gives rise to significantly better tensile properties and Vickers micro-hardness. The solubility of Si atom in the Al matrix of as-built SLM samples is calculated to be 8.89 at%. With the increase in the solution temperature, the solubility decreases swiftly. The artificial aging result in decrease of the solubility of Si atoms in the Al matrix. Upon solution heat treatment, Si atoms are rejected from the super saturated Al matrix to form small Si particles. With rising the solution temperature, the size of the Si particles increases, whereas their number decreases. After artificial aging, the Si particles are further coarsened. The variation in size of Si particles has a significant influence on the mechanical properties of the AlSi10Mg samples. The tensile strength decreases from 434.25710.7 M Pa for the as-built samples to 168.1172.4 M Pa, while the fracture strain remarkably increases from 5.370.22% to 23.770.84% when the as-built sample is solution-treated at 550 °C for 2 h. This study indicates that the microstructure and mechanical properties of SLM-processed AlSi10Mg alloy can be customized by suitable solution and artificial aging heat treatments. The microstructure and mechanical properties of selectively laser melted AlSi10Mg: The effect of a conventional T6- like heat treatment The nano-, micro-, and macro-scale mechanical properties of SLM AlSi10Mg were studied. In adding up the effect of a conventional T6-like heat treatment was investigated and correlated to the generated microstructure. Nanoindentation showed uniform hardness within the SLM material. Significant spatial variation was observed after heat treatment as a result of phase transformation. It was found that the SLM material's micro- hardness exceeded its die-cast counterpart. Heat treatment softened the material, reducing micro-hardness from 12571 HV to 10071 HV. An ultimate tensile strength (333 MPa), surpassing that of the die cast counterpart was achieved, which was slightly reduced by heat treatment (12%) alongside a significant gain in strain-to-failure ( threefold). Significantly high compressive yield strength was recorded for the as-built material with the ability to withstand high compressive strains. The SLM characteristic microstructure yielded enhanced strength under loading, outperforming cast material. The use of a T6- like heat treatment procedure also modified the properties of the material to yield a potentially attractive compromise between the material's strength and ductility making it more suitable for a wider range of applications and opening up further opportunities for the additive manufacturing process and alloy combination.