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Article history: In this paper, the microstructure and mechanical properties of 7075-T6 aluminum alloy joints joined by
Received 4 June 2012 refill friction stir spot welding (RFSSW) were investigated. The keyhole was refilled successfully, and the
Accepted 4 August 2012 microstructure of the weld exhibited variations in the grain sizes in the width and the thickness direc-
Available online 29 August 2012
tions. There existed defects (hook, voids, bonding ligament, etc.) associated to the material flow in the
weld. Mechanical properties of the joint have been investigated in terms of hardness and tensile/shear
Keywords: and cross-tension test, and the fracture mechanisms were observed by SEM (scanning electron micro-
A. Non-ferrous metals and alloys
scope). The hardness profile of the weld exhibited a W-shaped appearance in the macroscopic level,
D. Welding
E. Mechanical
which reached the minimum at the boundary of the sleeve and the clamping ring. The variation laws
between tensile/shear and cross-tension strength and processing parameters were rather complicated.
The void in the weld played an important role in determining the strength of the joint. On the whole,
the preferable strength can be obtained at lower rotational speed. Shear fracture mode was observed
under tensile–shear loadings, and nugget debonding, plug type fracture (on the upper sheet) and plug
type fracture (on the lower sheet) modes were observed under cross-tension loadings. It was also
observed that the main feature affecting the mechanical properties of the joint is the alclad between
the upper and lower sheets and the connecting qualities between the stir zone and thermo-mechanically
affected zone.
Ó 2012 Elsevier Ltd. All rights reserved.
0261-3069/$ - see front matter Ó 2012 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.matdes.2012.08.026
Z. Shen et al. / Materials and Design 44 (2013) 476–486 477
[4,5,10,11], relatively little are currently known about the detail of the cylindrical cavity is squeezed back by the sleeve, hence the
RFSSW. cylindrical cavity created by the sleeve is refilled successfully. (d)
The schematic illustration of the friction stir spot welding pro- The welding head of the workpieces is removed and a flat surface
cess is shown in Fig. 1. It can be seen that the RFSSW is performed connection is obtained [10].
using a tool assembly comprised of three parts: clamping ring, In the present study, the tests were conducted using lap-shear
sleeve and pin. Furthermore, the three components of the tool specimens of refill friction stir spot welded 7075-T6 aluminum
are operated by three separate actuators so that they are mounted alloy. The mechanical properties were evaluated and the micro-
coaxially and can be rotated and moved up and down indepen- structure, characteristics of defects and failure mechanisms were
dently of each another. Prior to welding, the clamping is moving discussed based on experimental observation.
the entire welding head against the work pieces to keep the sheets
to be welded tightly secured during the welding process and to 2. Experimental details
avoid plasticised material to be lost in the form of flash [10]. As
indicated in Fig. 1 the RFSSW process can be explained by four dis- The material used in the present study is 7075-T6 aluminum
tinct stages: (a) the clamping ring is fixed on the top surface of the alloy plate of 2.0 mm thickness, whose chemical composition and
upper sheet and both the sleeve, and the pin starts to rotate and mechanical properties are listed in Tables 1 and 2, respec-
rub on the sheet for a while to soften the material so that the pen- tively.7075-T6 is precipitation-hardened Al–Zn–Mg–(Cu) alloy that
etration could be more smoothly. (b) The sleeve and pin move has been used extensively in the aircraft structural components,
downwards and upward, respectively, therefore the plasticised mobile equipment, and other highly stressed applications for their
material displaced by the sleeve is squeezed into the cylindrical light weight and high strength [12–14].
cavity created by the upward movement of the pin. (c) After reach- Fig. 2 illustrates the configuration of lap-shear and cross-ten-
ing a predetermined plunge depth, both the sleeve and pin’s direc- sion specimens employed. The specimens were made by using
tion of movement begin to reverse, and the plasticized material in two 40 mm 150 mm sheets with a 40 mm 40 mm and
Table 1
Chemical composition of 7075-T6 aluminum alloys (wt.%).
Si Fe Cu Mn Mg Cr Zn Ti Other impurities Al
Single total
0.40 0.5 1.2 2.0 0.30 2.1 2.9 0.18 0.28 5.1 6.1 0.30 0.05 0.15 Rest
Table 2
Mechanical properties of 7075-T6 aluminum alloys.
As received Tensile stress rb (MPa) Yield stress r0.2 (MPa) Shear strength T (MPa) Elongation d (%)
T6 453.4 415.5 317 13.9
Fig. 2. Configuration of test specimens (in mm): (a) tensile/shear test specimen and (b) cross-tension test specimen.
478 Z. Shen et al. / Materials and Design 44 (2013) 476–486
Fig. 3. Microstructures on longitudinal section of RFSSW joint made at welding condition of the rotational speed of 1200 rpm and dwell time of 4 s: (a) cross section of weld
zone, (b) magnified views of the regions A1-D marked in a, respectively and (c) variations of the grain sizes in the thickness direction.
50 mm 50 mm overlap areas, respectively. Tensile/shear tests After welding, a longitudinal section through the center of the
and cross-tension tests were performed according to Japanese joint was polished and etched to reveal the weld structure using
Industrial Standard (JIS) Z 3136–1999 [15] and Z 3137–1999 an OLYMPUS DP700 optical microscope. The tensile/shear and
[16], respectively. All the specimens were welded in the middle cross-tension tests were performed using a CHANGCHUN CSS-
of the overlap area. RFSSW lap experiments were carried out on 44100 electronic universal testing machine. After the tests, fracture
the FSSW-SK-002 welding machine. The three-piece non-consum- morphologies of the failure specimens were examined in detail
able tool comprises a clamping ring, a sleeve and a pin, whose using a HITACHI Hatchis-4800 ESEM scanning electron micro-
diameters are 15, 9 and 5 mm, respectively. The rotational speeds scope. Vickers hardness profiles of the joint was measured using
and duration time were varied, which were 1500, 1750 and 432SVD Vickers micro-hardness tester in the middle location of
2000 rpm, and 3, 4 and 5 s, respectively. the upper sheet and lower sheet. A 5 kg force was used with
0.5 mm distance between indents and a dwell time of 10 s.
Fig. 4. Characteristics of the hooks and voids made at different processing parameters.
Z. Shen et al. / Materials and Design 44 (2013) 476–486 479
Fig. 5. Characteristics of the defects of the joint: (a) bonding ligament, (b) incomplete refill, (c) no mixing and (d) lack of mixing.
Fig. 6. Hardness profiles of the welds in the mid-thickness of the upper sheet.
Fig. 7. The mechanical properties of the joints: (a) diagram of the tensile/shear strength among the welds and (b) diagram of cross-tension strength among the welds.
480 Z. Shen et al. / Materials and Design 44 (2013) 476–486
Fig. 8. Shear fracture of nugget of the RFSSW joints under tensile/shear loadings: (a) close-up top view of the upper sheet, (b) close-up bottom view of the upper sheet and (c)
close-up top view of the lower sheet.
Fig. 10. Scanning electron micrographs of (a) a fracture surface on the lower sheet shown in Fig. 8b and (b) magnified views of the regions A–F marked in (a).
(see Fig. 3c), the grain sizes in the regions of G and I are smaller than of the base material. Furthermore, the formation of hook can be
those in the region of H. This can be attributed to the higher temper- attributed to the tool penetration into the bottom sheet and the lack
ature and severe plastic deformation under the pin and sleeve tips of mixing of the two sheets due to the poor flowability of materials
in the maintaining stage. and insufficient pressure in such a tight space. It also can be seen that
It should be noted that there were several kinds of defects the processing parameters scarcely affect the hook geometry. Mean-
formed in regions E and F (denoted in Fig. 3a) due to poor flowabil- while, various sizes of voids formed, which are also associated to the
ity of materials there, which will be discussed in detail later. material flow and related to the processing parameters. As shown in
Fig. 4, the voids get smaller and less with the increasing of duration
3.1.2. Characteristics of the defects time at a given rotational speed. However, the voids get bigger with
As shown in Figs. 4 and 5. Due to the inherent disadvantage of the increasing of rotational speed at a given duration time. Hence
this method, several kinds of weld defects were formed during the duration time plays a crucial role in increasing the fluidity of the
joining process, such as hook, voids, bonding ligament and incom- material. It can be attributed to a less violent caused by slip condi-
plete refill. All of them were defects associated to the material flow. tions between the rotating sleeve and the surrounding material with
As shown in Fig. 4 hooks are observed under all processing the increasing of rotational speed [10]. The presence of the void
parameters applied in the present study. Unlike the hook found by diminishes the integrity of the weld, which have an important effect
Rosendo et al. [10], in other words, the hook presents an L-shaped on the crack initiation when the weld is subjected to external
appearance and exhibits a poor continuity. Badarinarayan et al. loading.
[20] attributed the formation of hook to the upward bending of the Fig. 5a represents the bonding ligament in the joint welded at
sheet interface caused by the tool penetration into the bottom sheet. the rotational speed of 1500 rpm and duration time of 3 s. The
However, which is not true in the present study, because there was bonding ligament lies above the boundary between the two sheets
no upward bending of the sheet interface due to the poor plasticity because of the upward material flow of the lower sheet, which
482 Z. Shen et al. / Materials and Design 44 (2013) 476–486
Fig. 12. Macroscopic fracture appearances of RFSSW joints under cross-tension loadings.
Z. Shen et al. / Materials and Design 44 (2013) 476–486 483
Fig. 13. Scanning electron micrographs of (a) a nugget debonding fracture surface on the lower sheet shown in Fig. 9 and (b) magnified views of the regions A–H marked in
(a).
duration is 3 s, the difference of Vickers hardness is rather small 1500 rpm, higher tensile/shear strength can be obtained under
with the increasing of rotational speed. However, when the dura- three different duration times applied in the present study, and
tion time is 5 s, the difference of Vickers hardness is slightly bigger, the strength increases and then decreases with the increasing of
which can be attributed to the increasing of heating or cooling duration time. However, as rotational speed reaches 1750 or
rates during welding by increasing duration time, because the 2000 rpm, the strength decrease and then increase with the
increasing heating rate could reduce the time for the precipitates increasing of duration time. The tensile/shear strength reaches a
to grow [21]. maximum of 7031.0 N at the welding condition of the rotational
The deduction of hardness in the HAZ can be attributed to the speed of 1500 rpm and duration time of 4 s.
coarsening of precipitates and grains due to the only effect of ther- As shown in Fig. 7b, the variation laws between cross-tension
mal cycle during welding, which resulted in the lower hardness strength and processing parameters are rather complicated. Under
than that of the BM according to the Hall–Petch relationship, in all given processing parameters, the peak load can be obtained by
which the precipitation state plays a decisive role on the hardness appropriate combination of rotational speed and duration time. As
for the reason that the submicroscopic Mg2Zn and Al2CuMg precip- a whole, when the rotational speed is lower, the peak value can be
itates render a high hardness in the alloy [22], and Cavaliere et al. obtained by lowering the duration time, which can be attributed to
[23] attributed the reduction of hardness in HAZ to the competing the coarser structure associated to increasing heating input. How-
mechanisms of work hardening and over-aging. Compared to the ever, when the rotational speed is 2000 rpm, the strength is lower
HAZ, the grains in the TMAZ and SZ undergo severe intense plastic at the duration time of 3 s, however, the peak value could be ob-
deformation besides frictional heat, especially the SZ undergo dy- tained by prolonging the duration time, this also can be attributed
namic recrystallization, which induces the appearance of fine equi- to slip conditions between the rotating sleeve and the surrounding
axed grain structure, meanwhile, the larger amount of precipitates material at higher rotational speed [10], and the material can be
in the SZ were dissolved due to the higher temperature and then mixed adequately by prolonging the duration time. The maximum
reprecipitated during the following natural ageing [21]. Hence cross-tension strength of 2643.2 N can be obtained at the welding
the hardness in the SZ and TMAZ can be attributed to the compre- condition of rotational speed of 1500 s and duration time of 3 s. As
hensive effect of variations in the grain sizes and strengthening shown in Fig. 7a and b, in general, the preferable mechanical prop-
precipitates. erties can be obtained at lower rotational speed, this can be attrib-
uted the lower density of strengthening precipitates compared to
3.2.2. Tensile/shear and cross-tension tests higher heat input [24].
The variation laws between tensile/shear strength and process- As shown in Fig. 7, the mechanical properties of 7075-T6 joints
ing parameters are shown in Fig. 7a. When the rotational speed is are relatively lower. This are associated to the poor flowability of
484 Z. Shen et al. / Materials and Design 44 (2013) 476–486
Fig. 14. Scanning electron micrographs of (a) a plug type fracture surface shown in Fig. 9 and (b) magnified views of the regions A–D marked in (a).
the materials, as well as the alclad mentioned above. There is a di- and thermo-mechanically affected zone (see in Fig. 4) where con-
rect correlation between the mechanical properties and the sizes of siderable variation of hardness can be recognized (see in Fig. 6),
voids (see in Figs. 4 and 7), hence, the size of the void has a crucial then the crack propagated toward the weld center and along the
role in determining the mechanical properties. circumferential direction. The regions B, K, L and C, D, J correspond
with the hook’s tip and junction’s slope of the hook and bonding
3.2.3. Macroscopic and microscopic fracture morphology ligament, respectively. There exist fewer dimples in region B com-
One type of fracture mode was observed under tensile/shear pared to regions K and L, indicating the crack preferentially initiate
loadings–shear fracture. Fig. 8 reveals the typical macroscopic frac- in region B. The presence of numerous dimples of various sizes and
ture surfaces of the close-up top and bottom views of the upper quantities in regions D–I indicate the occurrence of shear fracture
sheet and close-up top view of the lower sheet. It can be clearly rec- in the remaining area of the nugget. Furthermore, striation-like
ognized that shear fracture took place along the boundary between patters can be clearly seen in the regions of A, B, K and L, which
the upper and lower sheets through the nugget of the weld, and the indicated that the crack propagated along the direction perpendic-
faying surface between the two sheets was completely sheared off. ular to the loading direction around the nugget. This phenomenon
There exhibits bulgy ridges in the periphery of the fracture surface can be attributed to rotation of the nugget, which is schematically
on the lower sheet, accordingly, sunk ridges formed on the upper shown in Fig. 11, the rotation of nugget gives rise to the generation
sheet because the crack propagated along the hook. The outside of the load component perpendicular to the loading direction and
fracture surface of the ridge is smooth, where bond did not form, in turn causes the crack to grow to the thickness direction [4,7].
but the inside fracture surface of the ridge is sunk because the crack Fig. 12 summarizes the fracture modes of the joint under cross-
propagated along the bonding ligament where stress concentration tension loadings. It can be seen that the fracture modes could be
could form when the weld is subjected to external loading. classified into three modes: nugget debonding, plug type fracture
In order to examine the fracture process in more detail, the (on the upper sheet) and plug type fracture (on the lower sheet).
crack propagation path is schematically shown in Fig. 9a, and It should be noted that nugget debonding is the dominant fracture
SEM micrographs of fracture surfaces on the failed tensile/shear mode under cross-tension loadings, plug type fracture rarely
specimen are represented in Fig. 10. Fig. 10a reveals SEM micro- occurs, with the exception of some specimens made at welding
graph of overall fracture surface on the lower sheet of the joint, conditions of rotational speed of 1500 rpm and duration time of
and Fig. 10b reveals the magnified views at the regions A–L in 4 s (on the upper sheet), rotational speed of 1750 rpm and duration
Fig. 10a, respectively. The crack initiated in the region A, where time of 5 s and rotational speed of 2000 rpm and duration time of
corresponds with the void in the boundary between the stir zone 4 s (on the lower sheet). Hence, the welded quality between the
Z. Shen et al. / Materials and Design 44 (2013) 476–486 485
upper and lower sheets is worse than that between the stir zone (2) The hardness profile of the weld exhibited a W-shaped
and the thermo-mechanically affected zone. As shown in Figs. 8 appearance in the macroscopic level. The change low of
and 12, the bonding ligament between the boundary of the two hardness can be attributed to the comprehensive effects of
sheets and the partial bonding around the boundary between the several factors, in which the precipitation state plays a deci-
stir zone and the base material play an important role in the crack sive role.
initiation and propagation. (3) Overall, the preferable mechanical properties can be
As shown in Fig. 12, the fracture surface of nugget debonding is obtained at lower rotational speed and shorter duration
similar to that of shear fracture (see in Fig. 8). SEM micrographs of time. Extending the duration time contributed to the
the overall fracture surface on the lower sheet of the joint are improvement of mechanical properties at higher rotational
shown in Fig. 13. Fig. 13b reveals the magnified views of the speed.
regions A–H marked in (a), respectively. The crick initiated at re- (4) Shear fracture mode is observed under tensile/shear load-
gion A at the boundary between the upper and lower sheets, and ings, and nugget dobonding, plug type fracture (on the upper
fracture surfaces with striation like patterns can be observed in sheet) and plug type fracture (on the lower sheet) modes are
the regions A and C, this indicates that the crack propagated along observed under cross-tension loadings. Moreover, the frac-
the circumferential direction around the SZ. Then the crack propa- ture modes under cross-tension loadings are associated to
gated toward to SZ, the fracture path is schematically shown in the processing parameters.
Fig. 9b, it can be seen that the fracture mode is similar to that of
shear fracture under tension/shear loadings mentioned above.
Meanwhile, the presence of equiaxed dimple in the regions B, C
and D, and the sizes of dimple increase gradually, which indicates Acknowledgements
that plasticity increases gradually and the metallurgy combination
becomes preferable. There exist numerous small shallow dimples The authors acknowledge the financial support for this work
associated with the second-phase particles in region E, indicating from the National Nature Science Foundation of China (No.
the poor plasticity of the material on the hook. In the region F, 50775159) and Nature Science Foundation of Tianjin (No.
the existence of alternant distribution of small and big dimples 10JCYBJC06700).
suggests the difference of plasticity. There exist small shallow dim-
ples associated with discontinuous second-phase particles in re-
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