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Applications
Mechanical Seals

59 E
Mechanical seals in
mixing and separating processes
in the chemical industry.
Processes, application examples,
seal designs
and supply systems.
Seal selection

Seal selection for top entry arrangements. Agitators for steel, stainless steel and glass-lined vessels
Connection sizes according to DIN
Medium toxic or dangerous for the environment Medium non-toxic, not dangerous for the environment

Single seal or double seal,


Single seal,
unpressurised quench, process
Double seal, pressurized with constant process leakage to the
leakage into the buffer liquid
barrier pressure, no process leakage to the atmosphere atmosphere is permitted or
is permitted or directed to the
directed to the drain
drain
Dry running, Lubricated, Contactless, Dry running, Lubricated,
pressure up to 6 bar, pressure up to 6 bar (16 bar), pressure up to 6 bar, pressure up to 6 bar, pressure up to 6 bar,
barrier medium gas (N2) barrier medium liquid barrier medium gas (N2) no barrier medium quench medium liquid
SeccoMix® 481...D.. M481K...D.. AGSZ 481K..D. SeccoMix® 481 M481K.. or M481K...D
SeccoMix® 461..D... M461K...D.. AGSZ 461K...D. SeccoMix® 461 M461K.. or M461K...D..
Seal supply system
Closed circuit
Gas supply Gas supply No supply system
TS system, Quench system
GSS4016/A ... GSS4016/A ... necessary
open circuit SPA, SPN

Seal selection for top, side or bottom entry arrangements. Agitators, dryers, mixers, filters and special equipment.
Connection sizes according to EagleBurgmann standards or as required
Sterile equipment No sterile equipment

Double seal, pressurized with constant barrier Double seal or multiple seal, pressurized with constant
pressure or with pressure adjustment barrier pressure or with pressure adjustment
Pressure up to 6 bar, Pressure up to 16 bar, Pressure up to 6 bar, Pressure up to 16 bar, Pressure up to 25 bar, Pressure up to 250 bar,
barrier medium gas (N2) barrier medium liquid barrier medium gas (N2) barrier medium liquid barrier medium liquid barrier medium liquid
HSH-D, HSHL-D,
AGSR3-D MR333-D AGSR5-D MR5-D
HS-D, HSL-D HSH(V)-D, HSH(V)L-D,
AGSR3L-D MR333L-D AGSR5L-D MR5L-D
series bottom entry HSHLU-D
series series series series
series
Seal supply system
Closed circuit Open circuit Open circuit
Gas supply Closed circuit Gas supply
TS system SPA SPA
GSS4016/A TS system, sterile GSS4016/A ...
DRU pressure booster SPN SPN

Front page:
Polymerisation reactor (Ekato) for producing ion exchanger
granules at Lanxess Bitterfeld.
2 Seals: AGS481KL-D, supply system GSS4016
Content

Seal selection 2

Seals for mixing and separating processes 4

Mixing processes 6

Separating processes 7

Mechanical seals in mixing processes 8

Mechanical seals in mechanical and thermal separation processes 12

EagleBurgmann agitator seals – the complete range 16

EagleBurgmann seal supply systems 20

HSMR in a vacuum dryer

M461L-D for glass-


lined tanks

Burgmann © is a Trade Mark of EagleBurgmann. 3


Seals for mixing and separating processes

The manufacturing of chemical and EagleBurgmann can provide technical An Atex declaration of conformity
pharmaceutical products puts consi- solutions for aggressive, corro- can be issued for every EagleBurgmann
derable strain on the sealing technology. sive, adhesive, viscous, toxic, mechanical seal provided that the
In addition to the process specific explosive, dry, environmentally technical design and the arrangement
properties, the sealing systems must hazardous or valuable media. Both meet the required operating conditions
meet ever increasing requirements in modular systems and process-optimised and the following precise operating
terms of service life and reliability in a engineered solutions are used. By conditions of use are known:
constantly growing global market. combining these with mature and
reliable seal supply systems, n Area of use (zone, device group)
Optimum quality, a worldwide service EagleBurgmann is able to offer the n Required temperature class
network and decades of experience complete range of services through to n Medium (medium class)

The range of application of of application engineering have made TotalSealCare™ – a modular service n Maximum pressure at the mechanical

EagleBurgmann agitator seals is wide: EagleBurgmann the leading manufac- from a single supplier. seal
Shaft diameter: 20 ... 500 mm turer of sealing systems in the chemical n Maximum temperature of the process

(0.787 ... 19.685“) and pharmaceutical industry, biotech- Beyond this in the pharmaceutical medium at the mechanical seal
Temperature: –80 ... +350 °C nology, food industry, agrochemical industry, EagleBurgmann seals fulfil n Rotational speed

(–112 ... 662 °F) industry, dispersion and micro-wet special requirements and directives, e.g. n Seal type, combination of face

Pressure: Vacuum ... 250 bar milling technology, flue gas desulphuri- materials and size
(3,625 PSI) sation and many other processes. We n SIP Sterilisation in Place n Buffer/barrier medium

Sliding velocity: ... 20 m/s (65 ft/s) have developed sealing solutions jointly n CIP Cleaning in Place
with our customers and engineers, with n cGMP current Good Manufacturing This brochure sets out a range of
due regard to the characteristics of the Practice solutions for different processes,
processes and equipment used. Today, n EHEDG Design of Mechanical Seals machines and equipment. The selection
reliable production would not be feasi- for Hygienic and Aseptic Applications matrix on page 2 will help you to
ble without these sealing solutions. n FDA Food and Drug Administration identify the right seal for many different
n QHD Qualified Hygienic Design applications.

EagleBurgmann dual mechanical seals


meet the requirements of the German
Clean Air Directive (TA-Luft).

4
Batch operations in process Mechanical and thermal
engineering separation processes
For the sake of simplicity, many Centrifugation, filtering, drying and
processes in the chemical, pharmaceu- evaporating are examples of
tical or biotech industries can be broken unit operations for separating
down into two main areas from the processes. The aim may be to obtain a
viewpoint of the sealing technology: high purity end product or to separate
out by-products.
Mixing processes
Agitating, mixing and kneading are
basic unit operations for combining of
materials. The aim is to balance out
differences in concentration and to
achieve greater homogeneity.

Top entry agitator with AGS481.


Applied in sun protection products
at BASF Ludwigshafen.

5
Mixing processes

Mixing processes are particularly impor- An agitator is generally used for mixing Suspending
tant in the chemical industry. For a start, and agitating operations involving mix- is the even distribution of solids in
intermediate or end products are often tures of substances consisting primarily liquids. In the starting phase, the solids
mixtures, dispersions or emulsions, for of the liquid phase. The requirement for at the bottom are whirled up. In the end
example. And, for a chemical reaction, a successful sealing solution is a clear phase, the solids are evenly distributed
the reactants must be distributed as ho- definition of the operating conditions. in the tank.
mogeneously as possible to guarantee
an optimum heat and mass transfer. We The tasks of the mixing technology can Dispersing
distinguish between homogeneous and be described as follows: Comminuting a substance or breaking a
heterogeneous mixtures. Homogeneous gas down and distributing it in a liquid.
mixtures consist of just one phase, e.g. Homogenisation The aim of dispersing is to increase the
salt solutions, alloys or air. creates a uniform phase of several surface area between the disperse pha-
Heterogeneous mixtures comprise liquids that are soluble in one another se and the continuous phase in order
several phases, such as emulsions or for the purposes of balancing out to improve the mass transfer between
suspensions. As a rule, we use agitating differences in concentration and them which increases in proportion with
for liquid phases, kneading for high- temperature. the size of the surface. Dispersing is
viscosity, paste-like media and mixing also used to stabilise emulsions.
for solid substances. Intensification
increases the heat exchange between A special technology has been
the liquid phase and the heat transfer developed for dispersing and micro wet
surface milling. The application requirements
extend from low to high viscosity pro-
ducts that have to be dispersed down to
nanometer range. For these applica-
tions, agitated media mills are used to
disperse powdered substances in liquid
phases as finely as possible.

This requires particularly robust seal


designs to guarantee successful operati-
on. EagleBurgmann can supply suitable
seal systems for all such mixing and
agitating applications.

Polymers production at BASF Ludwigshafen.


Stainless steel tank with top entry agitator.

Medium: Preproduct for polymers production


Temperature t1: 120 °C
Pressure p1: 4 bar
Rotational speed: 147 min-1
Seal: M451KL-D21/80-E2
with resublimation barrier with permanent
flow of deionised water
Supply system: TS1016/A007
Barrier medium : Glycol / water
6 Barrier pressure p3: 6 bar
Mechanical and thermal separation processes

The separation of mixtures of nologies have significantly increased air drying, the drying is carried out with
substances is one of the most important over the past few years. Separators and hot air at atmospheric pressure.
unit operation in processes. It normally decanters are used in the chemical, For vacuum drying a vacuum is used.
represents more than half of the pharmaceutical and biotech industries, This causes the boiling point and
investment in a chemical production oil and fat recovery and starch industry thus the drying temperature to drop
plant. The majority of the raw materials and in industrial biotechnology. considerably, which makes the process
and the products obtained by chemical gentler on the product.
reactions are mixtures of substances Filtering
that have to be separated into the Filtering is the mechanical separation Evaporation
different components for further of a suspension into the liquid and solid Evaporation uses the addition of heat to
processing or end use. We distinguish phases using a filter medium. Filters evaporate and remove the solvent from
between mechanical and thermal perform a large number of solid/liquid a solution. This method is used to con-
separation processes according to separating applications. For example, centrate a solution, for example, to re-
which physical properties are used modules of different designs are used in cover the pure solvent or to precipitate
for separation. Mechanical separation closed systems for optimised solutions the dissolved solid by crystallisation.
methods include e. g. centrifugation and that are matched to the specific
filtering where different densities of the application.
various components are used. Thermal
separation methods such as drying and Drying
evaporating utilise the different boiling By drying, we mean the removal or
points for separation. reduction of the liquid content in a
solid by thermal treatment. The liquid
is converted into the vapour phase and
The following separation processes removed. Drying involves a very high
are of particular importance in sealing power consumption and must be carried
technology. out gently to prevent product deteriora-
tion, so it requires particular attention.
Centrifugation Thermal drying always stresses the
Separators and decanters separate solid. It is therefore important to ensure
solids from liquids or liquid mixtures that the process is safe as well as
and remove the solids at the same time. maintains the product quality.
Centrifuges as stand-alone machines or
integrated into complete process lines We distinguish between convection,
are used to implement new process contact and radiant drying according to
technologies and make the production the heat transfer method.
efficient and cost-effective. The options It is also possible to distinguish by the
Gas-lubricated
for using mechanical separation tech- operating conditions. For example, with AGSRL-D

7
Mechanical seals in mixing processes

In closed agitator or vessels, the rota- application, but are still extremely
ting agitator shaft must be sealed off reliable. Engineered solutions are still
from the cover or bottom of the vessel. needed for special equipment. The seal
This type of arrangement is known as a design depends on the type of installa-
top or bottom entry installation. There tion and the process-specific load. The
are also horizontally arranged shaft mechanical, process-specific, physical,
entries and side arrangements that are chemical and safety requirements must
not horizontal. all be taken into account in the design
of the mechanical seal.
This creates very different requirements
for the mechanical seals. To meet users’ Seals may also have additional design
expectations of longer service life for features depending on the process
low investment costs, EagleBurgmann requirements. These may include a
has developed families of seals that
fully cover a wide range of applications Cooling flange
and are based on many years of for additional cooling of the seal for
experience and development. process temperatures in excess of
200 °C.
These seal designs are standardised
and thus provided the most Leakage drain
cost-effective solution for the required Leakages of media that could harm the
product or environment can be drained
off into an external system.

Polymerisation barrier
prevents polymerisation of the product
in the dynamic seal area by means of a
Production of dispersions at BASF
liquid reservoir on the process side or
Ludwigshafen. Stainless steel vessel with top
entry agitator. by flushing.
Medium: dispersions
Temperature t1: 50 °C Resublimation barrier
Pressure p1: 0 ... 3 bar prevents deposits in the dynamic seal
Rotational speed: 0 ... 30 min-1
Seal: M451KL-D20/200-E1
area released by product resublimation
Supply system: SPA 2020/A40-V1 by means of a liquid reservoir on the
Barrier medium : Glycol
process side or by flushing.
Barrier pressure p3: 5 bar

8
Top entry installation

A top entry installation is generally used Shaft deflections in the seal area of Dry running, with contact of the
to seal the gas containing headspace. 0.1 mm to 0.3 mm are tolerated as seal faces:
standard, depending on the size of the n EagleBurgmann SeccoMix
®

It should be noted that the dynamic drive system and agitator. Up to 2 mm Single seal with or without bearing
and stationary sealing elements on the is possible in special cases. n EagleBurgmann SeccoMix
®

product side can come into contact with Double seal with or without bearing
splasher and foam from the tank. There EagleBurgmann seal systems have
is also a risk of polymerisation in gaps proven successfully in many different Gas-lubricated without contact of
or in the dynamic sealing area. applications. the seal faces:
n EagleBurgmann AGSZ

The maximum speed, temperature Liquid-lubricated: Double seal with or without bearing
and system pressure to be sealed in n EagleBurgmann M481 n EagleBurgmann AGSR

the reactor are important factors that Single or double seal with or without Double seal with rotating seat on the
affect the design. The mainly overhung bearing for steel vessels product side, with or without bearing
agitator shafts are subject to bending n EagleBurgmann M461

stresses that cause the shaft to deflect Single or double seal with or without
in the seal plane. The mechanical bearing for glass-lined vessels
forces that act on the shaft seal and
bearing also have to be analysed May be equipped with cooling flange,
carefully, as well as unwanted vibrations leakage drain or polymerisation
caused by internals that affect the flow barrier to meet the process
or special cases, e.g. liquid bearing requirements.
missing from the agitator.

Glass-lined polymerisation reactor (Ekato) for


producing ion exchanger granules at Lanxess
Bitterfeld, Energizing Chemistry.

Medium: Styrene copolymer, aromatics


Temperature: 20 ... 150 °C
Pressure: p1: 0 ... 3 bar
Rotational speed: 15 ... 50 min-1
Seal: M481KL-D21/140-E1
Polymerisation barrier, ATEX zone 1
Supply system: TS2000/M226-D1
Barrier medium : White oil
Barrier pressure: Plan 53 9
Glass-lined stirred-tank reactor (EHW
Thale) with top drive for producing various
intermediate products for the pharmaceutical
industry, for example. Used at Chemie AG
Bitterfeld-Wolfen, Multi Purpose Center.

Temperature: -10 ... 200 °C


Pressure: p1: -1 ... 6 bar
Rotational speed: 30 ... 100 min-1
Seal: M461 KL-D20/100-00
Supply system: TS 1016/A007-00, Plan 53
Barrier medium : White oil

DIN standard agitator drives

DIN 28161 “Requirements on agitator Within the DIN range EagleBurgmann


drives” covers the most important supplies proven seal solutions tailored
requirements on the seal. It defines to different requirements, for steel or
speed limits, direction of rotation, glass-lined vessels, e.g. the M4 ...,
bearing, running accuracy and the SeccoMix® and AGSZ series.
stuffing box dimensions for mechanical
seals. The running accuracy of the
agitator is defined in relation to the
shaft diameter, but does not consider
dynamic loads on the agitator shaft
during mixing.

DIN 28161 applies to shaft diameters


from 40 mm to 220 mm and a sliding
velocity of up to 2 m/s, a pressure of
-1 to 6 bar and a temperature from
-25 °C to 200 °C.

Animal feed enzyme production at BASF


Ludwigshafen. Stainless steel vessels with top
entry agitator with sealed SeccoMix®

Medium: Aqueous solution


Temperature t1: 5 ... 15 °C
Pressure p1: unpressurised
Rotational speed: ... 45 min-1

10
Top entry stirred-tank reactor (Chema) in the
HAS system at DOMO Caproleuna.

Medium: Hydroxylammonium sulphate (HAS)


Temperature: max. 200 °C
Pressure p1: 5 bar
Rotational speed: 150 min-1
Seal: M481KL-D20/180-A2
Supply system: TS1016
Barrier medium: Deionate
(demineralised water)
Barrier pressure: 7 bar

Bottom entry installation

In contrast to top entry, it is the process To cope with these tough operating stresses, the shaft deflection and the
medium itself which is sealed in a conditions, mainly double seals with bearing must all be carefully analysed
bottom entry installation. The rotating pressurised barrier medium are used. and evaluated.
agitator shaft must be sealed off from Other design features, such as flushing,
the bottom of the tank and is totally may also be used. The materials must EagleBurgmann sealing systems from
immersed in the medium. also be selected carefully. One decisive the liquid-lubricated MR..., MR333 and
criterion in the choice of the barrier HSHLU series and process-optimised
It is characteristic for this installation medium is its compatibility with the gas-lubricated seals from the AGSR
that deposits may form in the area of process medium. series have proven successfully for
the dynamic and stationary sealing bottom entry installations.
elements, depending on the process As with the top entry installation, the
medium. These can then hang up the maximum speed and temperature, the
seal. Additionally, the seal directly faces sealed system pressure in the vessel,
the temperature of the process medium. the chemical requirements, the bending

Vitamin production at BASF Ludwigshafen.


Homogenisers in a vacuum dryer.

Medium: Vitamin pre-product


Temperature: 200 °C
Pressure: 1 ... 5 bar
Rotational speed: 1,500 / 3,000 min-1
Seal HSMR1S24-D55/65-E1-A25

11
Mechanical seals in mechanical and
thermal separation processes

The equipment used in separation sealing elements on the product side. bellows are designed for a specific type
processes are often engineered designs, They must not prevent the seal from of dryer and the additional forces are
so the seals must be selected and moving as required. Process-optimised taken into account.
designed particularly carefully. Top, seal design with rotating seals on the
bottom and side entry installations are product side (MR series) have proved EagleBurgmann seals can reliably fulfil
all used. The forces acting on the seal particularly successfully. the following process requirements:
during operation must be considered in
detail in advance and must be taken into High temperatures can lead to n No contamination of the product
account in the seal design in order to considerable thermal expansion n Possibility of sterile operation
guarantee an optimum sealing solution. between the dryer drum and drive shaft. n The mechanical seal’s functions are

There can also be excessive relative monitored by the supply system


The emphasis in the seal design is movement, depending on whether the n High MTBF

placed on both the relatively high seal is installed on the “drive side” or
thermal loads (can be in excess of the “non-drive side”. These movements
300 °C) and the product deposits in must be absorbed with metal bellows or
the area of the dynamic and stationary special deflector systems. Such metal

HSMR1AL with
metal bellows
for compensating
for large relative
movements in a
paddle dryer. Radial
decoupling of the
vessel / flange and
shaft.

Spherical dryer (Rosenmund Guedu) for


manufacturing pharmaceutical powders with
HSMR5L-D.

Werb.Nr. 2829

12
Examples of equipment used in mecha- vacuum. The operating cycle for such a Conical dryer
nical and thermal separation processes: nutsche consists of the following steps: This type of dryer is used primarily for
bulk goods that must not stick or cake
Nutsche filter n Filling the nutsche and filtration; the too much during drying. The material
(pressure nutsche filter) agitator distributes the suspension is circulated gently by a mixing screw
Nutsche filters are used for the uniformly over the filter surface. which rotates both about its own axis
discontinuous filtration of suspensions n Washing the filter cake and along the tank wall. The conical
with a relatively high solids content. n Removal of the filter cake, e.g. by dryer can be operated under vacuum or
They consist of a flat, cylindrical the agitator or by tilting the entire under overpressure. Heat is supplied via
container with a horizontal filter surface. container the wall heater and additionally via the
The modern types are equipped with heated screw. There are variants with
agitators, which are generally height- Filter dryer (nutsche dryer) top drive or bottom drive design which
adjustable. The filtration process is The filter dryer is a variant of the has significant effects on the operatio-
operated under overpressure or under nutsche filter that brings together the nal safety and the ability to empty the
filtration and the cake drying, generally apparatus. One particular challenge for
under vacuum, in a single apparatus the sealing technology in bottom entry
with no product transfer. The agitator, installation the sealing of two coaxial
tank walls and sometimes the tank base agitators moving at different speeds.
can be heated for drying. Filter dryers
are used to process sensitive materials
by gentle drying conditions to a low
residual humidity.

Pressure nutsche filter


(KHS) made of Hastelloy®
and steel, for drying various
intermediate products at
Chemie AG Bitterfeld-Wolfen,
Multi-Purpose Center.

Temperature: -10 ... 200 °C


Pressure: p1 = -1 ... 6 bar
Rotational speed: 5 ... 6 min-1
Filter dryer Seal: HSMR35AL-D/170-E9,
(Rosenmund Guedu, Supply system: Thermosiphon
Switzerland) system, Plan 53
Barrier medium : White oil
13
Paddle-dryer (Lipp Mischtechnik), frequency-
controlled, for producing and drying salicylic
acid at Rhodia Syntec.

Medium: Salicylic acid, various aromatics


Temperature: 40 ... 220 °C
Pressure: -1 ... 11 bar
Rotational speed: 8 ... 80 min-1
Seals: HSMR1AL-D/180-E1
Side drive, with 1 seal on drive and non-drive
side
Supply system: Thermosiphon system
Barrier pressure: Plan 53 with circulating
pump

Double cone dryer this case the apparatus can sometimes apparatuses can often be opened at the
(rotary dryer) be used to process paste-like media. end since the shaft is only mounted at
In a double cone dryer, the vessel is one end. Large paddle-dryers can reach
set in a tumbling motion by rotation. Paddle-dryer up to 20 m3, in which case the shaft
Thereby the product in the dryer is Paddle-dryers are suitable for the will be mounted at both ends.
mixed and comes into contact with discontinuous and continuous drying
the heated wall. This ensures a good of pastes or free flowing media. A
thermal transfer. Usually the double slowly-turning, generally heated shaft
cone dryer is operated under a vacuum that is fitted with mixing paddles keeps
and is suitable for drying free flowing the solids in movement. This intensive
media. The internal space generally has mixing means that even media that
no internals, so the apparatus is easy to tend to stick together during drying can
empty and clean. Choppers are some- be processed. Choppers can also be
times used to break up the product. In used to break up the media. Smaller

Paddle-dryers (Lödige) for drying active


ingredients for the pharmaceutical industry.
Operator: Berg chemical works.

Medium: Active ingredients for the


pharmaceutical industry
Temperature: 100 °C
Pressure: Vacuum ... 0 bar
Rotational speed: 32 min-1
Seal: HSMR5S1-D2/120-E1
Side drive, with 1 seal on drive and
non-drive side
Supply system: TS 1016 with 5000, plan 53
14 Barrier medium: White oil
Thin-film evaporator (Chema) in the
caprolactam plant at DOMO Capro Leuna.

Medium: Caprolactam
Temperature: 200 °C
Pressure: Vacuum
Rotational speed: 150 min-1
Seal: M45-D90/82
Central supply system SPA 4002/A03-D1
Barrier medium: demineralised water
Barrier pressure: 5 bar

Thin-film evaporators Chopper


are used to increase the concentration Additional units in the form of cutters or
of high-viscosity products, to recover rotor/stator systems can be integrated
solvents and for temperature-sensitive to accelerate mixing processes and
materials under vacuum. Rotor blades to break up clumps. These “choppers”
distribute the liquid uniformly, which are generally arranged at the side, at
forms a thin film on the heated wall. the base of the tank. High speeds up
to 3,000 min-1 are reached. The MR5
as a double seal with pumping screw
and with HS grooves, if necessary, has
proven particularly successfully for this
application.

MR5LF-D with integrated


bearing and directly attached
chopper (mixing accelerator)

Glass-lined polymerisation reactor (Ekato) for


producing ion exchanger granules at Lanxess
Bitterfeld, Energizing Chemistry.

Medium: Styrene copolymer, aromatics


Temperature: 20 ... 150 °C
Pressure: p1: 0 ... 3 bar
Rotational speed: 15 ... 50 min-1
Seal: AGS481KL-D21/140-E4-U polymerisation
barrier, Atex zone 0
(in the tank), zone 1 outside
Supply system: GSS4016/A003
or GSS4016/A214
Barrier medium: Air
Barrier pressure: 9 bar

15
EagleBurgmann

M481

EagleBurgmann SeccoMix® Operating limits


and SeccoMix® 481
SeccoMix® (cartridge units)
n Dry-running mechanical seals d1 = 25 ... 220 mm (0.984 ... 8.661“)
n FDA approved p1 = vacuum ... 6 bar (87 PSI)
t1 = –20 ... +150 (200) °C
Specific face material combinations (–4 ... 302 (392) °F)
allow dry-running with contact of the vg = 2 m/s (6 ft/s)
seal faces. The grade of carbon used Perm. axial movement: ± 1.5 mm
in the seal face is FDA-conform. For Radial movement: ± 2 mm
use in pharmaceutical applications, the
seal can be equipped on request with SeccoMix® (component seals)
a collecting cup (CIP). The SeccoMix® d1 = 25 ... 160 mm (0.948 ... 6.229“)
as a single seal does not need a supply p1 = vacuum ... 6 bar (87 PSI)
system. t1 = –20 ... +150 (200) °C
(–4 ... 302 (392) °F)
SeccoMix®
single seals
With a single seal, the process gas is vg = 2 m/s (6 ft/s)
dissipated to the atmosphere or can be Perm. axial movement: ± 1.5 mm
diverted into drainage system. If any Radial movement: ± 2 mm
leakage into the atmosphere is not per-
Werb-Nr. 2783
mitted, a SeccoMix® double seal should
be used. This should be pressurised
with a barrier gas (preferably N2) and a
barrier pressure of 0.5 to 1.0 bar above
the pressure to be sealed. The hydraulic
conditions ensure that the seal is closed
by both the product pressure and a
superimposed barrier pressure.

Agitator seals from the SeccoMix® se-


ries are available as components or as
factory-tested cartridge units (SeccoMix
481). Connections for steel (SeccoMix
481) and glass-lined (SeccoMix 461)
reactors are available to DIN standards SeccoMix®
or as required. component seal

SeccoMix®
double seals

16
Werb-Nr. 2784
agitator seals – the complete range

EagleBurgmann M461
and M481

n Liquid-lubricated mechanical seals The hydraulic conditions ensure that


n according to DIN 28136 and the seal is closed by both the product
DIN 28138 pressure and a superimposed barrier
n for steel and glass-lined vessels pressure.
n FDA approved

Operating limits according to


The seals can be used for a wide DIN 28138 T2
range of applications, and may be used d1 = 40 ... 220 mm (1.575 ... 8.661“)
as single or multiple seals with an vg = 2 m/s (6 ft/s)
unpressurised liquid reservoir (quench) p1 = vacuum ... 6 bar (87 PSI)
or pressurised with a supply system t1 = –25 ... +200 °C (–13 ... 392 °F)
(TS1016 or TS2000). With the double
seal, the operating limits are far higher EagleBurgmann operating limits
M461
for glass-lined
than the pressures and speeds defined (depends on the choice of materials
vessels in the DIN standards. Agitator seals and the supply system)
from the M461 and M481 series are d1 = 40 ... 220 mm (1.575 ... 8.661“)
supplied in the form of factory-tested vg = 5 m/s (16 ft/s)
cartridge units. p1 = vacuum ... 16 bar (232 PSI)
t1 = –80 ... +200 (+350) °C
Suitable options include cooling or (–112 ... 392 (662) °F)
heating flange, polymerisation barrier,
leakage drain and cleanability for use
in pharmaceutical applications. The
materials used are extremely flexible, so
practically all requirements can be met
with the standard design variants.

M481
for steel and
stainless steel
vessels

17
AGSZ

AGS481KL-D30.2/125-00-U
AGSZ 461 HS-D

AGSZ 481 HSH-D

Werb.Nr. 2820

EagleBurgmann AGSZ 461 AGSR ... for sterile applications EagleBurgmann HS-D and HSL-D EagleBurgmann HSHLV-D and
and AGSZ 481 in theWerb.Nr.
pharmaceutical
2821 industry HSHL-D
The “R” in AGSR standard for a rotating n Agitator seal up to 40 bar
n Gas-lubricated, contact-free seat on the product side. The AGSR is n with integrated bearing n Agitator seal up to 250 bar
mechanical seals particularly suitable for applications in n with integrated bearing
n according to DIN 28136 and the pharmaceutical, biotech and food Mechanical seals of the HS series can be
DIN 28138 industry. If certain requirements are ful- equipped with additional design feature, Agitator seals of the HSH-D series are
n for steel and glass-lined vessels filled and with a few additional design such as cooling and heating flange, specially designed for high-pressure
features, the seal can also be used in polymerisation barrier, leakage drain and applications. They are engineered
The AGSZ is not sensitive to radial direct contact with the product. cleanability for use in pharmaceutical solutions with connection sizes matched
deflection. A centrally rotating seat, operations. The materials used are to the specific application. The seals are
stationary spring-loaded seal face and Supply system for AGSZ... extremely flexible, so practically all operated with a supply system.
an integrated bearing, which acts at and AGSR... requirements can be met. The connection
the same time as a fixed bearing for A supply system from the GSS series sizes are matched to individual Combined with hydrodynamic grooves,
the seal and as a floating bearing for is needed for operation. A gas network requirements. these seals offer minimal load on the
the shaft, provide effective protec- connected upstream is sufficient to sliding faces, optimum formation of a
tion against negative influences on supply gas and pressure. The necessary The dual seals are operated with a supply lubricating film, high reliability and a
operation. barrier pressure must be 3 bar higher system. To run perfectly, the sliding faces long service life.
than the process pressure to be sealed. are equipped with EagleBurgmann
An optimum sealing gap stiffness The aerostatic design ensures that the patented hydrodynamic grooves, which Operating limits
ensures that the seal operates reliably gas consumption is approximately the provide an optimum lubrication with d1 = 20 ... 350 mm (0.787 ... 13.78“)
without contact, even under tough same across the whole operating range. minimal load on the sliding faces. These p1 = vacuum ... 250 bar (3,625 PSI)
operating conditions. Agitator seals from features ensure that the HS series is t1 = –30 ... +200 (+350) °C
the AGSZ series are supplied in the Operating limits highly reliable and has a long service life. (–22 ... 392 (662) °F)
form of factory-tested cartridge units. d3 = 40 ... 220 mm (1.575 ... 8.661“)
p1 = vacuum ... 10 bar (145 PSI) Operating limits
t1 = –30 (–80) ... +200 (+250) °C d1 = 20 ... 500 mm (0.787 ... 19.68“)
(–22 (–112) ... 392 (482) °F) p1 = vacuum ... 40 bar (580 PSI)
vg = 10 m/s (32 ft/s) t1 = –30 ... +200 (+350) °C
(–22 ... 392 (662) °F)
vg = 5 m/s (16 ft/s)
18
MR-D (standard)

HSHLU-D MR-333 (for sterile


applications)

EagleBurgmann HSHLU-D EagleBurgmann MR

n Agitator seal up to 60 bar n Mechanical seal for chemical and Connection sizes are matched to indivi-
n for bottom entry installation pharmaceutical applications dual requirements.
n for adhesive, paste-like and dry media The double acting seals are operated
Agitator seals of the HSHLU-D series with a supply system.
are typically used for bottom entry Agitator seals of the MR series are
applications such as plastics production. ideal for use with adhesive, paste-like Operating limits
The seals are fully immersed in the and dry media in agitators and all types d1 = 20 ... 200 (500) mm
process medium and are subject to of mixers, dryers, kneaders and reactors (0.787 ... 7.874 (19.68)“)
extreme stresses. On the product side, in the plastics, dyestuffs, food and p1 = vacuum ... 23 bar (333 PSI)
floating throttle rings with flush prevent pharmaceutical industry. p3 = 25 bar (362 PSI)
the intrusion of medium (e.g. polymer ∆p (p3 - p1) max. 10 bar (145 PSI),
powder) into the seal area. The double Building on many years’ practical min. 2 bar (29 PSI)
acting seals are operated with a supply experience and through the use of the t1 = –30 ... +300 °C (–22 ... 572 °F)
system. latest face materials, MR seals can be vg = 20 m/s (65 ft/s)
found operating successfully in almost
Operating limits all applications. The rotating seat on the
d1 = 20 ... 400 mm (0.787 ... 15.748“) product side is an outstanding design
p1 = vacuum ... 60 bar (870 PSI) feature.
t1 = –30 ... +200 °C (–22 ... 392 °F)
The MR333 version of the seal fulfils
all the criteria for sterile processes:
surfaces on the product side are
polished, smooth and free of gaps, CIP/
SIP compliant and conform to FDA
guidelines. They can be equipped with
aseptic connections, e.g. to DIN 11851.

MR-D

19
EagleBurgmann supply systems

Quench system Closed circuit: Thermosiphon system /


pressure booster or cooling circuit with
Quench is the term commonly used in refill unit
sealing technology for an arrangement
that applies an un-pressurised external Here, all the components are under the
medium (liquid) to a mechanical seal‘s same pressure. They are pressurised via
sliding faces. The quench performs at an external pressure source or nitrogen
least one of the following tasks: (TS system) via a refill system (SPN) or
by the process pressure (DRU system).
n Absorption or removal of leakage by
the quench medium Before double seals start-up it is vital,
Glass-lined agitated tank for producing n Monitoring of the mechanical seal‘s to ensure a sufficient rate of circulation
various intermediate products. Sealed with
AGS, supplied with nitrogen via GSS4016 leakage rate by periodic measure- of the barrier liquid. The barrier liquid
(background) and SP25 pressure booster ment of the level of the quench pressure should be 10 % or at least
pump (foreground).
medium in the circulation vessel or 1.5...2 bar above the maximum pressure
thermosiphon vessel to be sealed. To ensure that the sliding
Depending on the type of equipment in n Preventing of the contact between faces are lubricated well, the outlet
which they are used, and on the medium, leakage and atmosphere for media temperature of the barrier medium must
mode of operation and environmental which react undesirably with oxygen be regulated via the flow rate so that the
protection requirements, etc, agitator n Protection against dry running boiling point of the barrier medium in the
seals may need additional design features n Cooling sealing gap is not exceeded at atmosphe-
to ensure efficient operation. n Lubrication ric pressure. The maximum acceptable
inlet/outlet temperature differential is 15
As the requirements on mechanical seal Supply systems K. The barrier liquid outlet is situated at
increase, their design, mode of operati- the highest point of the seal chamber for
on and ultimately their supply systems Supply systems for liquid-lubricated automatic venting of any vapour.
are changing. The following pages show mechanical seals can essentially be
the most commonly used and proven divided into two types: The basic operating conditions define
supply systems used in state of the art the following functions of the supply
sealing technology for agitator seals. Open circuit: Buffer fluid system system:

Barrier or quench systems A circuit which provides both circulation n Build-up pressure in the barrier
for liquid-lubricated single and and pressurisation via a supply system interspace
multiple mechanical seals (e.g. EagleBurgmann SPA). The barrier n Compensation of leakage

medium is depressurised after it has n Circulation of the barrier medium

Mechanical seals can only be guaran- circulated and is collected in an un- n Cooling of the barrier medium

teed to work efficiently if the space pressurised tank. n Cooling of the seal

between the product and atmosphere n Lubricating of the sliding faces

side of the mechanical seal is com-


pletely filled with clean medium. The
liquid reservoir may be un-pressurised
or pressurised.
20
SPS
SPS
PI
N2
N2 SPK
PI

SPN
SPN SPN

SPU RP

SPU TI
SPU
TI
TI Seal
Seal
Seal

EagleBurgmann TS 1016 EagleBurgmann TS 2000 EagleBurgmann DRU


Thermosiphon system Thermosiphon system Pressure booster system

Pressure vessel with flat bottom and Pressure vessel with torispherical With the DRU system it is possible to
incorporated cooling coil and sight-glass heads and incorporated cooling coil and supply barrier fluid to double seals for
for level control. sight-glass for level control. a wide range of applications. It works
similar than the TS system but, in this
Perm. operating temperature Perm. operating temperature case, the barrier pressure is generated
–60 ... +120 (200) °C –60 ... +200 °C (–76 ... 392 °F) by the reference pressure (e.g. tank
(–76 ... 248 (392) °F) Perm. operating pressure 30 bar pressure) without additional superimpo-
Perm. operating pressure 18 bar (435 PSI) (TS 2000), sed nitrogen.
(261 PSI) 63 bar (913 PSI) (TS 2063)
Perm. operating temperature
–60 ... +200 °C (–76 ... 392 °F)
Perm. operating pressure 63 bar
(913 PSI) (DRU2063)
Transmission ratio 1:1.1 or 1:1.5

Thermosiphon systems

The EagleBurgmann TS system TS 1016 Design, construction and production


or TS 2000 is used to supply barrier according to the EU Pressure Equipment
fluid to double and tandem seal arran- Directive 97/23/EC. All pressure-loaded
gement for a wide range of applications. welds are butt-welded or counter
TS vessels are equipped as standard butt-welded by MIG and TIG process.
with all the necessary connections and Sockets with recessed gasket (no
brackets. Additional components (e.g. contamination of the circuit by thread
circulating and refill pumps, measuring sealant). Cooling water connections at
equipment, level switches and valve top (Out) and bottom (In) for venting
groups) may be installed as required. and draining.
The vessel is used for storage, pressure
maintenance and cooling of the quench
or barrier liquid in the sealing circuit.
21
Seal

TI

PI PI

PCV

M
LS

LG
TI

supply system SPA


2000 for supplying
an M481

Barrier pressure systems of Supply systems of the SPN series


the SPA series with SPU

The basic version performs and These are automatic refill units with SPA: pressurisation of the barrier
fulfils all four tasks of a supply system pressure switch (SPN 1000 series) or medium and compensation of leakage.
essential for operating double seals: pressure control valve (3000 series) The energy needed for
Circulation and cooling of the barrier for manual barrier pressure regulation. pressurisation (piston pump) is supplied
medium, pressurisation of the barrier The pressure control valve (SPN 3000 via a pneumatic and an electric drive,
medium and compensation of leakage. series) allows a constant barrier pres- either in combination or individually.
EagleBurgmann SPA units have a high sure irrespective of hysteresis-induced Separate components are installed
quality standard, are easy to operate pressure fluctuations (hysteresis of the in the seal barrier circuit to cool and
and maintain, and are adaptable and pressure switch). Temporary maintaining circulate the barrier medium.
rugged. Their function is based on the of the barrier pressure when the pump
principle of the open circuit. is switched off by the accumulator.
Several outputs can be provided for
setting different barrier pressures. The
basic version of the automatic refill unit
SPN only performs two of the four tasks
of a barrier system, compared to an

PIA PIA

TIA TIA

Seal M Seal M

PI FIS FIS

PS

M
LS_L SPN 3000 with
electric drive

LG

22
SPA 4002 for supplying
12 agitator seals on
thin-film evaporators at DOMO
Caproleuna.

SPA 4015

GSS 4016 EagleBurgmann supply systems


GSS 4016 for gas-lubricated,
pressurised agitator seals.

Gas-lubricated mechanical seals may Important GSS functions:


Key only be operated if the barrier pressure
is high enough. At any operating n Filtering of the barrier and flush gas
FIS Flow switch with indicator (sight-glass)
LG Level indicator condition the barrier pressure p3 must n Pressure monitoring and pressure
LS Level switch be at least 3 bar higher than the regulation
LS-L MIN level switch
M Motor product pressure p1 to be sealed. Gas n Flow rate monitoring

N2 Nitrogen supply systems of the GSS series are n Control and drainage of the leakage
PCV Pressure control valve
PI Pressure gauge
specially designed for dry running and
PIA Contact pressure gauge gas-lubricated mechanical seals. A single connection to the gas supply
PS Pressure switch (or cylinder with pressure reducer)
RP Reference pressure
TI Thermometer with an upstream EagleBurgmann GSS
TIA Contact thermometer 4016 gas supply and control system is
EagleBurgmann components: sufficient to operate the gas-lubricated
SPK Contact device agitator seals. We recommend the
SPN Manual refill pump / refill unit
SPS Level switch
application of the GSS 4016 gas supply
SPU Circulating pump system with two flow meters (FIAH,
FIAL) and a pressure monitoring unit
(PIAL).

Pressure nutsche filter (Gedue) in the HAS


plant at DOMO Caproleuna.

Medium: HAS, catalyst


Temperature: 200 °C
Pressure: Vacuum
Rotational speed: ... 20 min-1
Seal: HSSMR35AL-D/170-E8
Supply system: TS2000 + SPU2040
Barrier medium: Deionate
(demineralised water)
Barrier pressure: 5 bar 23
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© EagleBurgmann Marketing Communications Germany

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Lejtö utca 6 EagleBurgmann Taiwan Co. Ltd.
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122, Limassol Ave. PO Box 24371
1703 Nicosia, Cyprus
Telefax +36 /1/ 3 19 81 25 Telefax +218 21 4776 152 Bdul. Iuliu Maniu, Nr. 7
Cladirea E, Parter, Hala 3, Sector
Taiwan, R.O.C. Burgmann Industries
Phone +886 -2- 2581 0040
Phone+357 22 42 79 80 India
Burgmann India PVT. LTD.
Lithuania
Dmitri Melnikow RO-061072 Bucuresti Telefax +886 -2- 2523 2793 GmbH & Co. KG
Telefax +357 22 42 30 21 Balandziu 5 - 2 Tel. +40 / 314 25 09 09
A.K. Industrial Estate
Czech Republic Madina Manzil Compound LT-91188 Klaipeda Telefax +40 / 314 25 09 10 Thailand
EagleBurgmann (Thailand) Co. Ltd.
Äußere Sauerlacher Str. 6–10
Phone / Fax +370 46 31 29 49
EagleBurgmann Czech s.r.o.
Na Drahach 1364
S.V. Road, Goregaon (West)
Bombay 400 062 Mobile +370 69 82 14 27
Russia
EagleBurgmann OOO
Banga Tower C, Floor 18th D-82515 Wolfratshausen
40/14 Moo 12 Banga-Trad Rd.
CZ-15600 Praha 5 Zbraslav
Phone +420 / 2 / 57 92 05 05
Phone +91/ 22 / 28 74 15 34 Malaysia ul. Zheleznodorozhnaya, 1, str. 45
606524 Zavolzhye
Km. 6.5 Bangkaew, Bangplee Germany
Telefax +91/ 22 / 28 74 88 10
Telefax +420 / 2 / 57 92 05 08
EagleBurgmann (Malaysia)
Sdn. Bhd. Gorodetsky district,
Samutprakarn 10540
Phone +66 / 2 / 7 51 96 21 Phone +49(0)8171/ 23-0
59E / E2 / 3.000 / 08.08 / 9.7.1

Eagle Seals & Systems India Ltd.


KE-Burgmann Czech s.r.o. 212/2, Hadapsar No. 7, Lorong SS13, 6 B
Off Jalan SS13/6
Nizhny Novgorod region
Phone +7 / 831/ 6 93 05 58
Telefax +66 / 2 / 7 51 96 28 Telefax +49(0)8171/ 23-1214
V Láznich 395
CZ-254 01 Jilove u Prahy
Off. Soli Poonawalla Road
Pune 411 028 India Subang Jaya Industrial Estate Telefax +7 / 831/ 6 93 05 59 www.eagleburgmann.com
Phone +420 / 2 / 41 02 18 11 Phone +91 / 20 / 2699 3900 47500 Petaling Jaya Moscow Representation
Telefax +420 / 2 / 41 02 18 30 Telefax +91 / 20 / 2699 3921 Phone +60 / 3 / 56 34 86 24 Ul. Novotcheremuschkinskaja 61
Telefax +60 / 3 / 56 34 97 42 RF-117418 Moskau All technical specifications are based on extensive tests and our many years of
Phone +7 / 095 / 7 97 20 14 experience. The diversity of possible applications means, however, that they can
Telefax +7 / 095 / 7 97 20 78 serve only as guide values. We must be notified of the exact conditions of application
before we can provide any guarantee for a specific case. Subject to change.

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