Beruflich Dokumente
Kultur Dokumente
3KL )
Purpose : To provide a documented procedure for operation and cleaning of Glass
Lined Reactor
Objective : To provide a guide line for safe operation and cleaning of Glass Lined Reactor
Scope : This SOP is applicable for operation and cleaning of Glass Lined Reactor
4.0 Responsibility :
Primary: Production chemist.
Secondary: Production officer.
5.0 Procedure:
Safety Precaution.
The area of operation should be well ventilated.
There should be no open flame in adjacent areas.
A continuous watch should be kept on reactions, which are 1) Exothermic, 2)
involving highly reactive compounds etc.
If found necessary, concrete /steel barricades should be built around
the apparatus.
The Reactor is manufactured out of glass, coated on Mild Steel.. Hence chemicals of corrosive
nature with Glass should not be used in the apparatus.
Operation:
Opening the Reactor for charging / discharging:
The glass Lined reactor is in assembled condition with all accessories.
Open the manhole, first open the vent valve to release the internal pressure if any.
Remove the nut/bolts of the manhole and slide to the side.
Check that the reactor is cleaned as per SOP. Charge the material in the Reactor. Solid Material to be
charged from the manhole and liquid materials to be charged through charging line under negative
pressure.