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AATCC Test Method 76-2000

Electrical Surface Resistivity of Fabrics


Developed in 1954 by AATCC Commit- 4.3 The radioactive bar emits alpha ra- the fabric.
tee RA32; revised 1963, 1968, 1970, diation which is externally harmless to
1972, 1973, 1982, 1995, 2000 (with ti- the human body. The radioactive isotope 7. Procedure
tle change); reaffirmed 1969, 1975, polonium 210 is toxic and precaution
1978, 1989; editorially revised 1974, should be exercised to prevent ingestion 7.1 Calibrate the electrical resistance
1984, 1985, 1997; editorially revised or inhalation of the solid material. Do not meter according to the manufacturer’s
and reaffirmed 1987. take the radioactive bar apart or touch the recommendations. This calibration should
radioactive strip under the grid. If the be repeated periodically (see 10.3).
strip is touched or handled, wash hands 7.2 Condition the test specimens in a
1. Purpose and Scope thoroughly at once. Return the device to suitable testing chamber or conditioning
1.1 The purpose of this test method is the manufacturer when it loses its effec- room at a predetermined relative humid-
to determine the electrical surface resis- tiveness as a static eliminator or for dis- ity that will reflect the conditions at
tivity of fabrics. The surface electrical re- posal if use is to be discontinued. Do not which information on the electrical resis-
sistivity may influence the accumulation discard as scrap. tivity of the fabric is needed.
of electrostatic charge of a fabric (refer to 7.2.1 For most fabrics which require an-
AATCC Method 84 for determination of 5. Apparatus and Materials tistatic treatments or whose static propen-
electrical resistance for yarns). sity is critical, measurements at 20% rela-
5.1 Electrical resistance meter (see tive humidity will be most meaningful.
2. Principle 11.1). 7.2.2 In less critical situations 40% rel-
5.2 Conditioning and test chamber (see ative humidity may be employed.
2.1 Specimens at equilibrium with 11.2). 7.2.3 For special requirements other
specified atmospheric conditions of rela- 5.3 Standard resistors (see 11.3). relative humidities may be used. For ex-
tive humidity and temperature are mea- 5.4 Radioactive bar (see 11.4). ample, preconditioning at 50% ± 2% RH
sured for electrical resistance between 5.5 Two rectangular flat metal surfaces at 21 ± 2°C is required for antistatic
parallel electrodes by means of an electri- of suitable size to serve as electrodes. sheeting, film and textiles for use in hos-
cal resistance meter. 5.5.1 As an alternative, two concentric pital operating rooms (see 11.2.1). Mea-
ring electrodes of spacing suitable to the surements may be made under other con-
3. Terminology material being measured and the purpose ditions or ranges of conditions that are
of the results (see 11.1.1). applicable to the end use (such as 65%
3.1 electrical resistivity, n.—material RH and 24°C). It is preferable to keep the
property of a substance whose numerical temperature or humidity consistent for all
value is equal to the ratio of the voltage 6. Test Specimens measurements.
gradient to the current density. 7.2.4 If it is necessary to measure elec-
NOTE: For the purposes of this method, 6.1 Adjust the size of fabric test speci-
mens to suit the electrodes of the particu- trical resistivity under a broad range of
surface resistivity is calculated by using conditions, additional tests may be run at
the measured electrical resistance be- lar equipment being used. When using
parallel plate electrodes, the width of the 65% RH and at 24°C or other settings ap-
tween superficially positioned parallel plicable to the end use. It is preferable to
plates or concentric rings and their spac- specimen must not exceed the width of
the electrodes. When using the concentric keep the temperature or humidity consis-
ing and is reported as ohms per square. tent for all measurements.
This test method in effect measures the rings, any size specimen at least as large
resistance of a material to the flow of cur- as the outer ring may be used. Avoid con- 7.3 Optionally remove static charges
rent between two electrodes. taminating the area on which the mea- on the surface of the fabric by passing a
surement is to be made. radioactive bar over both sides of the fab-
6.2 Specimens for use with instruments ric (see 11.4).
4. Safety Precautions
providing parallel plate electrodes. Pre- 7.4 Place a test specimen in firm con-
NOTE: These safety precautions are pare 2 sets of 3 test specimens each, 1 set tact with the electrodes. The contact with
for information purposes only. The pre- each so that the direction of testing is par- the electrodes should be such that, when
cautions are ancillary to the testing proce- allel to the yarns in the length direction of additional pressure is applied between the
dures and are not intended to be all inclu- the fabric and 1 set with the direction of fabric and the electrodes, the test results
sive. It is the user’s responsibility to use testing parallel to the width direction of are not affected.
safe and proper techniques in handling the fabric. 7.4.1 In the case of equipment using
materials in this test method. Manufac- 6.2.1 Test specimens for use with in- parallel plate electrodes, place the test
turers MUST be consulted for specific struments providing concentric ring elec- specimen in contact with the electrodes
details such as material safety data sheets trodes. Prepare 1 set (3 test specimens) with the direction of the test perpendicu-
and other manufacturer’s recommenda- since, with this type instrument, the resis- lar to the adjacent edges of the electrode.
tions. All OSHA standards and rules tance is measured in both fabric length Measure the electrical resistance of the
must also be consulted and followed. and fabric width directions simulta- fabric in both the length and width direc-
4.1 Good laboratory practices should neously. tions. Since the charge will follow the
be followed. Wear safety glasses in all 6.2.2 Depending on the fabric con- path of least resistance, record only the
laboratory areas. struction or end-use, it may be advisable lower reading by direction.
4.2 The safety recommendations pro- to differentiate between face and back 7.4.2 For concentric ring electrodes,
vided by the manufacturer of the radioac- measurements. Each test specimen the charge follows the path of least resis-
tive bar should be followed. should be taken from a different part of tance automatically.

AATCC Technical Manual /2004 TM 76-2000 101


7.5 Measure the electrical resistance of 9. Report described by Hayek & Chromey in American
the test specimen according to the operat- Dyestuff Reporter, Vol. 40, 1951, pp 164-8.
ing instruction and procedures for the 9.1 Report the following information: 11.1.4 Other resistance testers also may be
particular resistance meter being used. 9.1.1 The Log R for each sample and satisfactory for this test.
Allow the current to pass through the test for the lot. 11.2 A conditioning and testing chamber is
specimen for 1 min or until a constant 9.1.2 the number of specimens tested. required capable of providing relative humid-
reading is obtained. The criterion for con- 9.1.3 The relative humidity and tem- ity control of ± 2% (preferably effective over a
stant electrical resistivity is a change in perature used. range of 20-65% RH) and temperature control
9.1.4 The direction of testing if parallel of ± 1°C (± 2°F) with circulating air. Since
the value of Log R of less than 0.1 units equilibration of a test specimen from the dry
per minute. The time to reach a constant plate electrodes were used.
versus the wet condition relative to the humid-
reading may vary with the applied volt- ity of the test chamber may show hysteresis, it
age and with the resistance of the test is recommended that specimens approach
10. Precision and Bias
sample. High voltages for prolonged pe- equilibrium from the dry side relative to the
riods of time may damage the fabric. 10.1 Precision. Precision for this test humidity in the test chamber whenever possi-
7.6 For referee purposes, 80-100 volts method has not been established. There is ble.
at 25 mm electrode separation for 1 min no contemplated activity to establish pre- 11.2.1 National Fire Protection Association,
should be used for the parallel plate con- cision for this method. Users of the Standard NFPA Code #56 A-1973 Section
figuration, and a similar voltage gradient method should use standard statistical 4663.
for the concentric ring case (see 11.6). techniques in making any comparison of 11.3 Standard resistors suitable for calibra-
7.7 Avoid the use of any electrically test results for either within-laboratory or tion of the electrical resistance meter are avail-
conductive liquids on either the fabric able from Victoreen LLC, 6000 Cochran Rd.,
between-laboratory averages. Experience Cleveland OH 44139-3395; tel: 440/248-
test specimens or the apparatus. has shown that, with care, reproducibility 9300; fax: 440/248-9301.
should be ± ≤ 2% average Log R. 11.4 The following radioactive bar, Static-
8. Evaluation 10.2 Bias. Electrical resistivity can be master Ionizing Unit, Model 2 U 500, has
defined only in terms of a test method. been found to be suitable for the removal of
8.1 Compute the resistivity to the near- There is no independent method for de- electrostatic charges from fabrics and is avail-
est ohms per square as follows: termining the true value. As a means of able from NRD Inc., 2937 Alt. Blvd. North,
8.1.1 For the parallel electrode case: estimating this property, the method has Grand Island NY 14072; tel: 716/773-7634
no known bias. 11.5 Accumulation of static electricity gen-
R = O × W/D erally is greater the lower the relative humid-
ity (and vice versa). Fabrics which show a low
where: degree of static accumulation of 40% RH may
11. Notes
R = resistivity in ohms per square exhibit severe static accumulation of 20-25%
O = measured resistance in ohms 11.1 The resistance meter in conjunction RH, while fabrics which exhibit static prob-
W = width of specimen with the electrode system should be capable of lems at 40% RH may exhibit a low degree of
D = distance between electrodes measuring values in the range of 108-1015 for static accumulation of 65% RH. The relation-
any critical uses. Equipment that is capable of ship between the tendency for static accumu-
8.1.2 For the concentric ring case: measuring values in the range of 108 -1013 lation and relative humidity varies with the
ohms is suitable for work where the product specific antistatic agent, fiber, fabric construc-
R = 2.73(O)/log ro/ri performance is known to be acceptable if re- tion, surface character, etc. Therefore, 40%
sistance is < 1013 ohms. RH may not provide significant information as
where: 11.1.1 A concentric ring instrument com- to the probable antistatic performance proper-
R = resistivity in ohms per square plete with adequate shielding, capable of mea- ties of a fabric unless the tests are also run at
O = measured resistance in ohms suring values in the range of 108 -1015 ohms, is 20-25% RH, an atmospheric condition not un-
available from Keithley Instruments Inc., usual in modern heated and air-conditioned
ro = outer electrodes radius buildings. Complete information may also re-
28775 Aurora Rd., Cleveland OH 44139; tel:
ri = inner electrodes radius 440/248-0400. quire information of resistivity at the upper
11.1.2 Instruments capable of measuring level of 65% RH.
8.2 Calculate the average resistivity for values in the range of 108 -1013 ohms are avail- 11.6 For more detailed information regard-
each sample and for the lot. able from GenRad, 300G Baker Ave., Con- ing the measurement of resistances, see
8.3 Determine the logarithm (base 10) cord MA 01742; tel: 978/287-7000. ASTM Test D 257, Tests for D-C Resistance
of the resistivity (Log R) for each sample 11.1.3 A description of an instrument that or Conductance of Insulating Materials
and for the lot. will not allow measurements > 1013 ohms is (ASTM Committee D-20).

102 TM 76-2000 AATCC Technical Manual/2004

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