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Mechanical Property Characterization of Fiber-Reinforced Polymer Wood-


Polypropylene Composite Panels Manufactured Using a Double Belt Pressing
Technology

Article  in  Journal of Materials in Civil Engineering · September 2012


DOI: 10.1061/(ASCE)MT.1943-5533.0000489

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Mechanical Property Characterization of Fiber-Reinforced
Polymer Wood-Polypropylene Composite Panels
Manufactured Using a Double Belt Pressing Technology
Sandeep Tamrakar1; Stephen M. Shaler, Ph.D.2; Roberto A. Lopez-Anido, Ph.D., P.E., M.ASCE3;
Douglas J. Gardner, Ph.D.4; Christopher H. West5; Yousoo Han, Ph.D.6; and Russell Edgar7

Abstract: A novel manufacturing process for wood-polypropylene composite (WPC) panels reinforced with fiber-reinforced polymer (FRP)
sheets was implemented using a double belt pressing technology. FRP sheets were placed on both sides of the WPC agglomerates during
fabrication, which resulted in increased productivity and reduced thermal stresses compared with secondary bonding processes. Significant
improvements in the mechanical properties of the FRP reinforced sheet panels were found during flexural and tensile tests on the coupon
level. Even with addition of only one layer of FRP reinforcement on both sides of a WPC panel, the flexural modulus and strength increased
by a factor of 2.6 and 3.8, respectively. Furthermore, the flexural and tensile properties of the WPC material considered in this study were
found to be superior compared with the properties of an extruded WPC material. The changes in the flexural modulus of the FRP reinforced
WPC panels with respect to the number of FRP layers were predicted using a model based on moment-curvature analysis. DOI: 10.1061/
(ASCE)MT.1943-5533.0000489. © 2012 American Society of Civil Engineers.
CE Database subject headings: Composite materials; Wood; Fiber reinforced polymer; Curvature; Panels; Mechanical properties.
Author keywords: Wood-polypropylene composite; Fiber-reinforced polymer; Double belt press; Moment-curvature analysis.

Introduction exhibit enhanced outdoor durability (versus certain species of solid


wood) and lower maintenance costs because the wood particles are
Wood polymer composite (WPC) materials are considered environ- encapsulated by the polymer resin (Klyosov 2007). These advan-
mentally friendly materials because of their use of recycled thermo- tages have prompted a great interest in using WPC materials
plastics and processing residue fillers such as sawdust, peanut for exterior structural applications.
shells, or rice hulls. The use of fillers can increase the stiffness Despite the relative improvements in material properties, it is
and decrease the total cost of the product (Clemons 2008). Several unlikely that WPC materials will replace load-bearing members,
studies have shown an increase in stiffness of WPC materials com- such as beams or columns, employed in building and transportation
pared to neat polymer materials (Alvarez-Valencia et al. 2010; structures. This restricted use is mainly because of the relatively
Tamrakar and Lopez-Anido 2011). Moreover, WPC materials low strength and time-dependent deformation of WPC materials
1
compared with traditional structural materials. The cause of low
Graduate Research Assistant, AEWC Advanced Structures and Com- strength can be attributed to the poor interfacial bond between
posites Center, Univ. of Maine, Orono, ME 04469. E-mail: tamrakar@udel
wood and polymer (Klyosov 2007). Several studies have been con-
.edu
2
Professor of Wood Science, AEWC Advanced Structures and Compo- ducted in an attempt to improve the compatibility between the
sites Center, Univ. of Maine, Orono, ME 04469. E-mail: shaler@maine.edu wood and polymer interface using various additives/coupling
3 agents. However, the research conducted by Raj et al. (1990)
Professor of Civil Engineering, AEWC Advanced Structures and Com-
posites Center, Univ. of Maine, Orono, ME 04469 (corresponding author). and Lu et al. (2005) show that using coupling agents alone might
E-mail: rla@maine.edu not be enough to achieve significant improvement in the mechani-
4
Professor of Wood Science, AEWC Advanced Structures and cal properties of WPC materials. The increase in deformation of
Composites Center, Univ. of Maine, Orono, ME 04469. E-mail: douglas
WPC materials over time under sustained load can be attributed
.gardner@umit.maine.edu
5
Wood Plastic Composites Research Associate, AEWC Advanced to its viscoelastic properties. Studies on time-dependent behavior
Structures and Composites Center, Univ. of Maine, Orono, ME 04469. of WPC material can be found in the research conducted by
E-mail: chris.west@umit.maine.edu Tamrakar et al. (2011) and Alvarez-Valencia et al. (2010).
6
Wood Plastic Composites Specialist, AEWC Advanced Structures and One approach to enhance the mechanical properties of WPC
Composites Center, Univ. of Maine, Orono, ME 04469. E-mail: yousoo members is to reinforce the surface with some other material with
.han@umit.maine.edu higher mechanical properties such as fiber-reinforced polymer
7
Wood Composites Manager, AEWC Advanced Structures and (FRP). Extrusion and injection molding technologies are the two
Composites Center, Univ. of Maine, Orono, ME 04469. E-mail: russell most commonly used manufacturing processes for fabricating
.edgar@umit.maine.edu
WPC materials (Stark 2006). However, there are several issues re-
Note. This manuscript was submitted on August 20, 2011; approved on
January 25, 2012; published online on January 28, 2012. Discussion period garding the placement of FRP materials during manufacturing.
open until February 1, 2013; separate discussions must be submitted for Dura (2005) conducted quasi-static flexural tests on extruded
individual papers. This paper is part of the Journal of Materials in Civil WPC hollow cross-section box beams reinforced on the top and
Engineering, Vol. 24, No. 9, September 1, 2012. © ASCE, ISSN 0899- bottom flanges with one-layer of E-glass FRP. The peak load
1561/2012/9-1193-1200/$25.00. for the reinforced members increased 2.4 times compared with

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J. Mater. Civ. Eng. 2012.24:1193-1200.


the unreinforced member, whereas the modulus of elasticity (MOE) sandwiched between FRP sheets to form the panels using a double
increased by a factor of 1.73. In as much as the FRP reinforcement belt pressing technology. Tensile and flexural tests were carried out
was placed by hand during layup, this method becomes labor in- at the coupon level to determine mechanical properties and
tensive and expensive, especially for mass production. Although subsequently explore the possibilities of using these panels for
WPC materials can be fabricated continuously with intricate pro- structural applications. Moreover, mechanical properties of WPC
files using extrusion processes, the difficulty in incorporating a dif- materials obtained from various fabrication methods were
ferent material by coextrusion hinders productivity. Inclusion of compared.
FRP reinforcement using injection molding would be very difficult
to accomplish, especially for large-scale production. Even were this
process feasible, productivity would be much lower than using Materials
existing fabrication methods.
As a consequence of these complexities in the application of The WPC material was composed of polypropylene (50% by
weight) and 40 mesh pine wood flour (50% by weight).
FRP reinforcement from a manufacturing point of view, a need
Raw WPC material was in the form of granulated, reground
for the development of a structural component with an economi-
pellets, the precompounds of wood and polymer, which were
cal and relatively quick manufacturing process exists. Jiang et al.
compounded using a Palltruder. No additives such as a cou-
(2007) worked on reinforcing WPC deck board with com-
pling or coloring agents were used. FRP composite sheets
mingled glass and polypropylene fiber. First, the WPC deck
made of 35% E-glass continuous fibers and 65% polypropylene
boards were fabricated through an extrusion process, and then
matrix were used as the reinforcement. One layer of FRP
the reinforcement was placed on the surface of the WPC deck
composite had a thickness of 0.72 mm with an orientation
boards using a hot press. For the specimens reinforced on both
of 0°∕90°∕0°.
sides, the modulus of elasticity (MOE) and modulus of rupture
(MOR) increased by 1.3 and 1.6 times, respectively. In another
study by Deng and Tang (2010), reinforcement was incorporated Double Belt Press Technology
into WPC materials by sandwiching sisal and glass fiber fabrics
within the WPC panel during compression molding of WPC The procedure for fabricating the WPC sheet panels using a double
pellets. In as much as the fabrics were not placed at the areas belt press technology consisted of spreading the raw reground
of extreme fiber stress, the panels did not take full advantage WPC material (between the FRP sheets in the case of the reinforced
of the superior mechanical properties of the reinforcement. treatments) atop the press belt followed by heating, pressing, and
Nonetheless, for the specimens with two layers of glass fabric cooling (Fig. 1). The WPC-FRP sandwich was heated to a temper-
reinforcement, the writers observed significant improvements ature of 230°C through the heating platens, which are attached to
in tensile strength (up to 3 times) and tensile modulus (up to the upper and lower belts. The lower belt is mounted rigidly,
2 times). In a study conducted by Naghipour et al. (2011), carbon whereas the entire upper belt can be moved vertically to adjust
and glass FRP composites were placed manually on the tensile panel thickness. Three pairs of calibration nip rolls were mounted
face of the WPC I-beams. WPC beams were reinforced with up between the heating and cooling zones. Pressure on the panel
to three layers of FRP sheets by placing one layer at a time using between the first pair of nip rolls was 200 kPa, which was increased
a bubble roller. Results from four-point bending tests on the to 300 kPa for the second and third pairs. Then the panels were
WPC beams reinforced with three layers of carbon and glass cooled through the cooling platens and were cut to the desired
FRP showed an increase in MOR by a factor of 1.8 (in both length of 2.4 m. The line speed was 0.5 m∕ min. For the reinforced
cases) compared with the unreinforced WPC beams. The WPC panels, FRP sheets were placed simultaneously on the top
MOE increased by a factor of 1.5 and 1.3 for the carbon and and bottom of the WPC pellets. The polypropylene present in
glass FRP reinforced beams, respectively. WPC and FRP melted under the heat of the platens and bonded
In this study, a novel method of fabricating reinforced WPC together when cooled down. As such, no adhesive was required
panels was implemented in which WPC agglomerates were to bond the FRP and WPC materials.

Fig. 1. Schematic representation of the double belt press technology adapted from Thermofix® Technology Center (T. T. C)

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J. Mater. Civ. Eng. 2012.24:1193-1200.


Double belt press technology is an appropriate method for fab- increasing number of FRP reinforcement to maintain a consistent
ricating WPC panels in large scales, especially when surface length to depth ratio (Table 1). Specimens were loaded at a strain
reinforcement is desired. The method is relatively fast as fabrication rate of 0.1% per minute in three-point bending in accordance to
of WPC panels and placement of reinforcement are achieved in a ASTM D790. Load was monitored and recorded using LabVIEW,
single step. Furthermore, because the materials are subjected to and the midspan deflection was measured using crosshead motion.
high temperature only once during fabrication, less thermal stress
is induced in the material compared with other methods, where the
placement of reinforcement is done using a hot press on previously Results
fabricated panels.
Panels measuring 1.2 × 2.4 m were fabricated with up to four Tensile Tests
layers of FRP. The average thickness values are presented in
Table 1. In the case of the WPC panels reinforced with four layers For the unreinforced WPC specimens, the mode of failure was brit-
of FRP, visible voids randomly spread throughout the cross section tle with no warning of impending failure and within the gauge
were present. It should be noted that regardless of the number of length. In contrast, the mode of failure for all reinforced specimens
FRP layers used, the same press temperature and pressures were was ductile and only one-third of the reinforced specimens failed
employed. Inadequate heating might be one of the reasons the within the gauge length.
WPC pellets did not melt fully for the four-layer FRP panels. Also, The typical stress-strain response for specimens cut in longitu-
studies conducted on deconsolidation phenomenon of wood par- dinal and transverse directions is shown in Fig. 2. For unreinforced
ticles have indicated that voids might be produced if the pressure WPC specimens in both directions, the response was initially linear,
is inadequate during the cooling period. This phenomenon is attrib- followed by a nonlinear region, and then yielding until failure. For
uted to the restoration of the elastic deformation incurred during the the reinforced specimens in both directions, the response was
initial stages of the fabrication process (Ye and Mai 2002). This roughly bilinear with two linear portions connected by a region
lack of homogeneity in the material yielded very high variability of nonlinearity. The location of the nonlinear region corresponds
in the results of the quasi-static tests, and hence these results were to the level of strain at which the WPC specimens started to yield.
not included in the data analysis. Clearly, optimized press cycles Tangent MOE values were calculated from the slope of the
would need to be developed for changing compositions of material, curve between strain values of 0.05 and 0.2%. Table 2 shows
such as the number of layers of FRP. the changes in tensile properties for unreinforced and reinforced
WPC specimens. In the longitudinal direction, compared with
the unreinforced specimens, the MOE and ultimate tensile strength
Experimental Work (UTS) for reinforced specimens increased by 1.6 and 3.8 times,
respectively. In the transverse direction, the MOE and UTS in-
Tensile and flexural tests were conducted on coupons cut from vari- creased by 1.3 and 2.8 times, respectively. However, the changes
ous parts of the panels in both machine (longitudinal) and cross in strain to failure for both directions were insignificant.
machine (transverse) directions using a flow water jet. Prior to test-
ing, specimens were conditioned at 23°C and at 50% relative hu- Flexural Tests
midity for 1 week. All tests were carried out using an Instron servo
hydraulic testing machine rigged with a 100-kN load cell. Unreinforced WPC specimens failed in tension, leaving an irregu-
lar fracture surface in the middle region of the specimen, whereas in
the FRP-reinforced WPC specimens, wrinkling of FRP in compres-
Tensile Tests sion was seen prior to failing in tension (Fig. 3). Typical stress-
Tensile test specimens were cut from the unreinforced WPC and strain curves for WPC and FRP-reinforced WPC specimens in
one-layer FRP reinforced WPC panels (2-layer, 3-layer, and 4-layer the longitudinal and transverse directions are shown in Fig. 4.
specimens only tested in flexure). Specimens were cut and shaped The stress-strain response for unreinforced WPC specimens was
to comply with the type III specimens specified in ASTM D638. initially linear followed by nonlinear behavior until failure. In
Specimens were loaded at a rate of 0.1% strain per minute
(5 mm∕ min) until failure. An extensometer was used for measur-
ing strain over the 50-mm gauge length in the middle portion of the
specimen.

Flexural Tests
Flexural tests were conducted on unreinforced and reinforced WPC
panels in three-point bending. Specimens had a width of 32 mm.
Span between the supports was increased for specimens with

Table 1. Dimensions of Flexural Test Specimens


No. of Total Distance
FRP thickness between Length-to-depth
layers (mm) supports (mm) ratio
0 7.9 124 15.7
1 9.1 143 15.7 Fig. 2. Typical stress-strain response of unreinforced and reinforced
2 10.6 162 15.3 WPC specimens under tensile loading in the longitudinal and trans-
3 12.1 187 15.6 verse directions

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Table 2. Tensile Properties as a Function of Reinforcement
Longitudinal direction Transverse direction
Specimen MOE (GPa) UTS (MPa) Strain at failure (%) MOE (GPa) MOR (MPa) Strain at failure (%)
Unreinforced WPC specimen 3.5 (5) 20.3 (6) 2.1 (10) 2.8 (2) 16.2 (3) 2.3 (13)
FRP reinforced WPC specimen 5.6 (7) 77.4 (2) 2.5 (5) 3.7 (5) 45.6 (5) 2.7 (5)
Note: Numbers in parentheses represent coefficient of variation (%).

contrast, the stress-strain response for reinforced specimens was justified from a cost versus additional performance basis. Fig. 6
fairly linear up to the initial failure of FRP, after which the response shows the normalized values of stored energy, yield strength,
became highly nonlinear until failure. and chord modulus as a function of the number of FRP layers.
Flexural offset yield strength and flexural strength were deter- Again, normalized values of yield strength and chord modulus
mined according to ASTM D790 (2007). Flexural offset yield seem to be asymptotically approaching a practical limit with an
strength was calculated with an offset of 0.5% and 0.1% for unrein- increasing number of FRP layers. This phenomenon could be
forced and FRP-reinforced specimens, respectively (Fig. 5). Chord attributed to the use of the same pressure and temperature for
modulus was calculated by performing a linear regression between all the panels during fabrication, which may have resulted in a
10 and 40% of maximum stress. Energy stored was calculated from weaker bond between the FRP layers and greater void content
the area under the load-deflection curve. The portion of the load- in the WPC core. Consequently, the shear transfer between the con-
deflection curve up to which the total deflection was less than secutive FRP layers and throughout the WPC core might have been
the depth of the specimen was considered for the calculation of hindered. This was evident from the flexural tests of the four-layer
energy stored because beyond this point, the assumptions of FRP reinforced specimens, where the specimens failed with a hori-
Euler-Bernoulli beam theory are not valid. zontal crack in the middle of the specimen parallel to the length
The incorporation of FRP layers significantly increased the propagating through the center of the specimen, suggesting
mechanical properties of the panels (Table 3). There is a significant decreased shear strength in the WPC core (Fig. 7).
difference between the mechanical properties of one-layer FRP re-
inforced and the unreinforced WPC specimens. In the longitudinal
direction, compared with the unreinforced specimens, chord modu-
lus of one-layer FRP-reinforced WPC specimens increased by a
factor of 2.6, whereas offset yield strength and maximum flexural
strength increased by a factor of 3.3 and 3.8, respectively. Perhaps
the most remarkable improvement was in the amount of energy
stored, which increased from 2.4 J for unreinforced to 10.4 J for
one-layer FRP-reinforced specimens in the longitudinal direction.

Discussion

Addition of FRP Layers


Experimental results showed that increasing the number of FRP
layers only marginally increased flexural performance. As such,
it is likely that increasing the number of FRP layers will not be

Fig. 4. Typical stress-strain response of unreinforced and reinforced


WPC specimens under flexural loading: (a) longitudinal; and (b) trans-
Fig. 3. Typical failure of FRP composite sheet during flexural testing verse directions

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J. Mater. Civ. Eng. 2012.24:1193-1200.


Fig. 5. Calculation of various parameters

The amount of energy stored increased almost linearly with the


increase in number of FRP layers used. Moreover, the increase in
normalized values of amount of energy stored is higher than that for Fig. 6. Normalized values of energy stored, yield strength, and chord
yield strength and chord modulus (Fig. 6). This suggests that the modulus in longitudinal and transverse directions
most appropriate structural application for these FRP-reinforced
WPC panels could be in blast-resistant buildings for the protection
of soldiers or in structures exposed to extreme events such as earth- attributable to high shear forces induced in the cross section has
quakes. This increase in ability to absorb energy is promising, been well documented (Yam et al. 1990; Grande and Torres
although it should be noted that the response of the full-scale panels 2005). Although wood flour was used as opposed to wood fibers
under a blast load might be different than the response observed at during the extrusion process, it is possible that the wood flour might
material level under quasi-static loading. have been damaged by high shear stresses. Various studies have
shown decrement in mechanical properties with reduction in filler
size (Klyosov 2007), which might be true in this case as well. In
Comparison of Mechanical Properties of WPC Material
contrast, during fabrication using double belted presses, the raw
as a Function of Fabrication Methods
materials are subjected to compressive stresses through the nip
The mechanical properties of the WPC material from the current rolls. As such, because of the differences in the loading conditions,
study were compared with the extruded WPC specimen. The ex- the shearing between the particles during double belt press would
truded WPC specimens were from the Z-section sheet pile fabri- be lower compared with extrusion processes. This could be one
cated at the AEWC Center, University of Maine. Specific details possible explanation for the higher mechanical properties of the
regarding the extruded specimen can be found in the paper by WPC materials produced using double belt press technology. An-
Alvarez-Valencia et al. (2010). Both tensile and flexural strength other possibility might be the multiple processing on the double
of the WPC material from the current study were found to be sig- belt pressing method using WPC pellets. Those two steps of
nificantly higher than those of the extruded specimens (Table 4 and processing, compounding in the Palltruder and thermal diffusion
Table 5). Because no additives were used in the formulation con- in the double belt press, might have resulted in a better dispersion
sidered in this study, it is worth mentioning that the addition of of fillers into the polypropylene matrix compared with the extrusion
coupling agents would likely result in a WPC material with even process.
higher mechanical properties. Similar trends in increase in strength
properties have been observed in WPC materials fabricated by
injection molding (Panthapulakkal and Sain 2006; Behravesh et al. Moment-Curvature Analysis
2010). A nonlinear model based on moment-curvature analysis was used
In the WPC extrusion process, higher pressure results in to predict the stress-strain response of WPC beams reinforced
higher shear forces. Fiber breakage during the extrusion process with FRP on the surfaces. The model takes as input the uniaxial

Table 3. Flexural Properties as a Function of Number of FRP Layers


Energy stored
Chord Offset yield Maximum Flexural Flexural up to deflection
Principal modulus strength flexural stress at strain at equal to the depth
direction Specimen (GPa) (MPa) strength (MPa) break (MPa) break (%) of beam (J)
Longitudinal WPC 3.6 (6) 36.8 (6) 40.1 (7) 29.0 (17) 2.5 (4) 2.4 (8)
1-Layer FRP 9.3 (3) 122.4 (4) 151.7 (5) 80.0 (63) 4.0 (9) 10.4 (3)
2-Layer FRP 11.6 (4) 157.8 (5) 169.8 (3) 59.9 (42) 5.1 (11) 17.6 (5)
3-Layer FRP 13.3 (4) 167.3 (3) 170.8 (2) 45.3 (43) 6.3 (14) 24.3 (3)
Transverse WPC 2.8 (3) 33.2 (4) 34.1 (4) 19.2 (43) 2.9 (9) 2.0 (4)
1-Layer FRP 5.4 (2) 76.3 (3) 104.3 (5) 102.8 (6) 3.2 (17) 6.8 (5)
2-Layer FRP 7.2 (4) 99.9 (5) 124.3 (7) 89.4 (45) 3.7 (18) 11.9 (2)
3-Layer FRP 7.9 (1) 112.6 (2) 134.1 (4) 106.5 (16) 3.6 (23) 16.3 (5)
Note: Numbers in parentheses represent coefficient of variation (%).

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Fig. 8. Theoretical versus experimental stress-strain response
Fig. 7. Failure of WPC specimen reinforced with four layers of FRP
sheets
σ ¼ A · tanhðB · εÞ (1)

stress-strain response of the materials (WPC and FRP), dimension where σ = stress; ϵ = strain; and A and B = the model parameters.
of the beam, number of FRP layers, and their location from the The parameters for the tensile model were obtained by curve
neutral axis. With this model, the mechanical properties of hybrid fitting the stress-strain response obtained from the tensile tests
composite beams exhibiting nonlinear behavior was predicted and of WPC in the longitudinal direction, as presented in the results
correlated with the experimental findings. section. From the result of the curve fit, the values of A and B were
The moment-curvature analysis was carried out based on the found to be 20.3 and 1.88 MPa, respectively. Because the stress-
following assumptions: strain response in compressive mode was not available, a linear
1. Plane sections of the beam remain plane during loading. model was used with the compressive modulus same as the tensile
Strains vary linearly along the cross section of the WPC core modulus. The compressive strength was assumed to be four times
and FRP sheets; the tensile strength. This was chosen arbitrarily to make sure that
2. Shear deformation is not accounted for; while performing moment-curvature analysis, the WPC material
3. There is perfect bonding between FRP sheets and the WPC would always fail in tension when loaded in flexural mode.
surface, i.e., no slipping between the two materials; and The uniaxial stress-strain response of the FRP material was ob-
4. The stress-strain response of both (WPC and FRP) materials tained from the tensile tests. The tests were conducted in accor-
is known. dance to ASTM D638 (2003) on the specimens cut from a sheet
Uniaxial constitutive model describing the stress-strain response of FRP material in the longitudinal direction. The specimen dimen-
of WPC material under tensile loading was used. A tangent hyper- sions conformed to the type II specimens specified in the test stan-
bolic model (Eq. 1) was chosen to describe the tensile response dard. A total of eight specimens was tested using an Instron servo
because of its use in the previous studies for describing stress-strain hydraulic testing machine with an 8.9-kN load cell. Specimens
response of WPC materials (Dura 2005; Davidow and Fridley were loaded at a strain rate of 0.1% per minute. Strain over the area
2003): of interest was monitored using an Aramis digital image correlation

Table 4. Tensile Properties of WPC Materials as a Function of Fabrication Method


Source Method of fabrication Ratio filler/polymer Polymer Filler MOE (GPa) UTS (MPa)
This paper Double belt press 50∕50 Polypropylene Pine 3.5 20.3
Alvarez-Valencia et al. Extrusion 46∕41 3.0 13.0
(2010)
Tamrakar and 3.1 13.5
Lopez-Anido (2011)

Table 5. Flexural Properties of WPC Materials as a Function of Fabrication Method


Method of Ratio filler/ Span-to-depth MOE MOR
Source fabrication polymer Scale and specimen Loading type ratio (GPa) (MPa)
This paper Double belt press 50∕50 Coupon cut from 3-point bending 16 3.6 40.1
sheet pile
Alvarez-Valencia et al. (2010) Extrusion 46∕41 Full-scale sheet 4-point bending 11–23 3.15 14.3
pile section
Tamrakar and Lopez-Anido (2011) Coupon cut 16 3.7 22.5
from panel

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J. Mater. Civ. Eng. 2012.24:1193-1200.


Table 6. Comparison of Experimental and Predicted MOE each layer with cross-sectional area of dA was calculated for a
Experimental Theoretical given strain distribution throughout the depth. Eq. 2 was then
Specimen MOE GPa MOE GPa solved for the location of the neutral axis by equating the tensile
and compressive forces. Eq. 3 was used to calculate the external
WPC 3.6 3.5
Reinforced WPC (1 layer) 9.3 8.8
applied moment ðM EXT Þ for a given curvature and neutral axis lo-
Reinforced WPC (2 layers) 11.6 11.5 cation. After obtaining the required parameters by balancing the
Reinforced WPC (3 layers) 13.3 13.1 equations, the strain was increased by a small amount and the pro-
cess was repeated. This iteration was continued until the failure
strain in tensile or compressive fiber was reached. After establish-
ing the moment-curvature relationship, the load-deflection re-
system. The maximum stress induced on the material was identified sponse was calculated by numerically integrating the curvature
as the tensile strength, which was 377.2 MPa with 10% coefficient twice over the length of the beam. Then, the stress-strain response
of variation (COV). The material failed at a strain of 2.6% (9% was calculated using the specimen geometry.
COV). The value of tensile modulus was 16.5 GPa (with 8% Z Z
COV), which was calculated using linear regression between 10
σdA þ σdA ¼ 0 (2)
and 40% of the tensile strength. It was assumed that the stress-strain AWPC AFRP
response of FRP material under tensile loading was linear up to
failure. Additionally, it was assumed that the stress-strain response
under compressive loading was identical to that in tension. While Z Z
performing the moment-curvature analysis, the WPC section was σ · zdA þ σ · zdA þ M EXT ¼ 0 (3)
divided into several small layers. However, each FRP layer was AWPC AFRP
treated as a single layer. Using the tangent hyperbolic model
and the linear model for the WPC in tension and compression zone, The predicted stress-strain responses of the unreinforced and
respectively and the linear model for the FRP, stress ðσÞ induced in FRP-reinforced WPC materials are shown in Fig. 8. Comparison
between the predicted and experimental flexural modulus is shown
in Table 6. The theoretically calculated modulus is accurate com-
pared with the experimental results. However, the model could not
accurately predict the flexural strength. One reason could be the
assumption made on the constitutive behavior of the FRP under
compressive loading. In the model, it was assumed that the tensile
and compressive failure strain of the FRP material was 2.6%.
However, during the experiments the initial failure of the specimens
was by buckling of compression fibers prior to tensile failure of the
FRP material. This suggests that the buckling occurred before a
strain of 2.6% was reached in the extreme fibers.
The stress distribution along the WPC cross section shown in
Fig. 9 was captured from the model just before failure. Because
the WPC material has higher compressive strength compared with
its tensile strength, a shift in the location of the neutral axis was
observed. Fig. 10 shows the stress distribution along the depth
of three layers of FRP-reinforced WPC specimens. A sudden
Fig. 9. Predicted stress distribution along the depth of unreinforced change in the stress values can be seen near the boundary of the
WPC material WPC and FRP material.

Fig. 10. Predicted stress distribution along the depth of three layers of FRP-reinforced WPC material

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J. Mater. Civ. Eng. 2012.24:1193-1200.


Conclusions ASTM. (2007). “Standard test methods for flexural properties of unrein-
forced and reinforced plastics and electrical insulating materials.” ASTM
WPC panels reinforced with FRP sheets were fabricated using an D790, New York.
innovative fabrication method. Significant increases in mechanical Behravesh, A. H., Aghdam, A. Z., and Soury, E. (2010). “Experimental
properties were observed for panels reinforced with one layer of investigation of injection molding of wood/plastics composites.”
J. Reinf. Plast. Compos., 29(3), 456–465.
FRP sheet on each side. The flexural modulus and strength of
Clemons, C. (2008). “Raw materials for wood-polymer composites.”
the one-layer FRP-reinforced WPC specimens were 2.6 and Wood-polymer composites, K. O. Niska and M. Sain, ed., Woodhead
3.8 times that of the unreinforced WPC specimens. Although Publishing Limited, Cambridge, UK.
the increase in the amount of energy stored with increasing number Davidow, S. A., and Fridley, K. J. (2003). “Development of design values
of FRP layers was found to increase almost linearly, the increase in for wood-plastic composite materials.” J. Mater. Civ. Eng., 15(5),
mechanical properties was observed to be approaching a practical 415–418.
limit with a higher number of FRP layers. Deng, S., and Tang, Y. (2010). “Increasing load-bearing capacity of wood-
The mechanical properties of WPC material fabricated by dou- plastic composites by sandwiching natural and glass fabrics.” J. Reinf.
ble belt press technology were compared to those produced Plast. Compos., 29(20), 3133–3148.
by an extrusion process. In addition to the advantages of this tech- Dura, M. J. (2005). “Behavior of hybrid wood plastic composite-fiber
reinforced polymer structural members for use in sustained loading
nology, such as ease of laying reinforcing materials and the
applications.” Master’s thesis, Univ. of Maine, Orono, ME.
increased speed of fabrication, it was found that the tensile and Grande, C., and Torres, F. G. (2005). “Investigation of fiber organization
flexural properties of the WPC material fabricated using this tech- and damage during single screw extrusion of natural fiber reinforced
nology improved compared with the extruded WPC material. Also, thermoplastics.” Adv. Polymer Tech., 24(2), 145–156.
the ductility of the material was found to increase with the addition Jiang, L., Wolcott, M. P., Zhang, J., and Englund, K. (2007). “Flexural
of FRP layers. properties of surface reinforced wood/plastic deck board.” Poly. Eng.
Finally, the stress-strain responses of the FRP-reinforced WPC Sci., 47(3), 281–288.
beams were predicted using moment-curvature analysis. The model Klyosov, A. (2007). Wood-plastic composites, John Wiley & Sons,
accurately predicted the flexural modulus of the reinforced WPC Hoboken, NJ.
Lu, J. Z., Wu, Q., and Negulescu, I. I. (2005). “Wood-fiber/high-density-
materials as a function of the number of FRP layers. Such a model
polyethylene composites: couopling agent performance.” J. Appl.
can be used for predicting the mechanical properties of a hybrid Polym. Sci., 96(1), 93–102.
composite material with varying material constituents prior to Naghipour, M., Nematzadeh, M., and Yahyazadeh, Q. (2011). “Analytical
the actual fabrication. and experimental study on flexural performance of WPC—FRP
The manufacturing method presented in this paper is suited for beams.” Construct. Build. Mater., 25(2), 829–837.
high-volume production of structural parts because fabrication of Panthapulakkal, S., and Sain, M. (2006). “Injection molded wheat straw
WPC panels and placement of the reinforcement is achieved in a and corn stem filled polypropylene composites.” J. Poly. Environ.,
single step without requiring secondary bonding. This novel WPC 14(3), 265–272.
material has potential to expand the use of wood-based composites Raj, R. G., Kokta, B. V., Grouleau, G., and Daneault, C. (1990). “Influence
of coupling agents on mechanical properties of composites containing
in construction to load-bearing applications.
cellulosic fillers.” Poly. Plast. Technol. Eng., 29(4), 339–353.
Stark, N. M. (2006). “Effect of weathering cycle and manufacturing method
on performance of wood flour and high-density polyethylene compo-
Acknowledgments sites.” J. Appl. Polym. Sci., 100(4), 3131–3140.
Tamrakar, S., and Lopez-Anido, R. A. (2011). “Water absorption of wood
This research project was carried out under Contract no. DTFH61- polypropylene composite sheet piles and its influence on mechanical
06-D-00022. The authors are grateful to the United States Federal properties.” Construct. Build. Mater., 25(10), 3977–3988.
Highway Administration (FHWA) for the financial support. Tamrakar, S., Lopez-Anido, R. A., Kiziltas, A., and Gardner, D. J. (2011).
“Time and temperature dependent response of a wood-polypropylene
composite.” Composites Part A., 42(7), 834–842.
Thermofix Technology Center. (2011). Development of new products
References designed for R&D, test and prototype runs small scale and pilot
production, Thermofix Technology Center, Mühlhausen, Germany.
Alvarez-Valencia, D., Dagher, H. J., Davids, W. G., Lopez-Anido, R., Yam, K. L., Gogoi, B. K., Lai, C. C., and Selke, S. E. (1990). “Composites
and Gardner, D. J. (2010). “Structural performance of wood from compounding wood fibers with recycled high density polyethyl-
plastic composite (WPC) sheet piling.” J. Mater. Civ. Eng., 22(12), ene.” Poly. Eng. Sci., 30(11), 693–699.
1235–1243. Ye, L., Lu, M., and Mai, Y. (2002). “Thermal de-consolidation of thermo-
ASTM. (2003). “Standard test method for tensile properties of plastics.” plastic matrix composites—I. Growth of voids.” Compos. Sci. Technol.,
ASTM D638, New York. 62(16), 2121–2130.

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