American Greenfuels Standard Operating Procedure 30-10-0002 Methanol Column Operation & Control

American GreenFuels Standard Operating Procedure
30-10-0002 Methanol Column Operation & Control

rev-19a00 - Prepared by: Operations Coordinator
Approved by: Production Manager
Revisions Made to Documents
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
REVISION DATE: MAY 8, 2019
30-10-0002_19a00 UNCONTROLLED IF PRINTED page 0 of 17

1.0 Purpose and Scope

The purpose of this work instruction is to provide a description of the startup, shutdown & operation control of the
Methanol Distillation Column. Define its function, operating conditions, limits and consequences of deviations from
operating limits. Describing the controls, instrumentation, safety systems and setting the operating alignments(s).
The purpose of the work instruction is to set forth the proper steps for starting, monitoring normal operations,
stopping and re-starting the system. This procedure is to increase awareness of the parameters needed to be met
before Plant Operation begins. The necessary balance between composition, vacuum, temperature, interface and
reflux is highly recommended in order to proceed starting up the rest of the plant. With these parameters met
initially, distillation of methanol will be more effective early on. 5 key factors are present while distillation is taking
place: Composition of vapor, vacuum, temperatures, interface and reflux.
Work Instruction is applicable to: studying, training, and Operating the methanol distillation column
1.1 Definitions
Distillation Column: Distillation is the process of separating two or more miscible liquids by taking
advantage of the boiling point differences between the liquids. For methanol and water, heat is added to
the mixture of methanol and water and eventually the more volatile component (methanol) begins to
vaporize. As the methanol vaporizes it takes with its molecules of water.
The methanol-water vapor mixture is then condensed and evaporated again, giving a higher mole fraction
of methanol in the vapor phase and a higher mole fraction of water in the liquid phase. This process of
condensation and evaporation continues in stages up the column until the methanol rich vapor component
is condensed and collected as tops product (99.8% or higher pure) and the water rich liquid is collected
as bottoms product.
Reboilers are heat exchangers typically used to provide heat to the bottom of industrial distillation
columns. They boil the liquid from the bottom of a distillation column to generate vapors which are returned
to the column to drive the distillation separation.
Delta-V Operating System: Easy and flexible modern automation systems that eliminate operational
complexity and minimize project risk.
Chiller: A chiller is a machine that removes heat from a liquid via a vapor-compression or absorption refrigeration cycle.
This liquid can then be circulated through a heat exchanger to cool equipment, or another process stream (such as air or
process water). As a necessary by product, refrigeration creates waste heat that must be exhausted to ambience, or for
greater efficiency, recovered for heating purposes.
Cooling tower: A cooling tower is a heat rejection device that rejects waste heat to the atmosphere through the
cooling of a water stream to a lower temperature. Cooling towers may either use the evaporation of water to remove
process heat and cool the working fluid to near the wet-bulb air temperature or, in the case of closed circuit dry cooling
towers, rely solely on air to cool the working fluid to near the dry-bulb air temperature
1.2 Chemicals Used & Hazards Presented by the Chemicals Used

Methanol: See “SDS_Methanol_Mitsubishi”
Propylene Glycol =
SDS_safety kleen_Clearwater
SDS_formula 1590_Clearwater
SDS_formula 1150A_Clearwater
1.3 Precautions Necessary to Prevent Exposure

Wear standard level D PPE

1.4 Control Measures to be Taken if Physical Contact or Airborne Exposure Occurs

Notify supervisor and/or management immediately
Refer to SDS in section 1.2 for treatment
1.5 Quality Control for Raw Materials

• Programing & instruments have been implemented to ensure product is valved to correct
location for quality purposes.
• Monitor chemical balance on cooling tower, see: “SOP_30-10-0008_18a00_ Cooling Tower”
• Monitor purity of propylene glycol if running on chiller “ “
1.6 Any Special or Unique Hazards

• System is under vacuum ranging from 14.69 psia – 1.0 psia
• If valve order is not followed you can put propylene glycol in cooling tower and vis versa
1.7 Instrumentation and Safety Systems
Heating Side of System

Operating Operating Range Consequences of Deviation from Steps to Prevent or Correct
Parameters Set -Points Operating Range Deviation
Temperature Expected temperature is Will not recover good methanol, will *Run M1 & M2 Samples often
based off you desired send methanol into TK-226 (water * Monitor Delta-V for variation
vacuum setpoint wash tank) or problems.
(>99.8% MeOH / <3% MeOH at “M2”) *Run System in “Auto / Cas”
as much as possible
Pressure 14.69 PSIA - 1.0 PSIA Non-Ideal dryer efficiency Set killing air valve to “Auto”
and allow time to adjust
Flow Varies based on plant If flow is to fast column may not be Maintain steady flow with in
operating conditions and able to handle, depending on production dryers
flow rate concentration
Concentration High variation, Sending oil / bio /glycerin to column Maintain steady flow within
composition will be production dryers,
determined by plant understanding conditions that
process conditions. cause “carryover”
Cooling Side of System
Operating Operating Range Consequences of Deviation from Steps to Prevent or Correct
Parameters Set -Points Operating Range Deviation
Temperature
Vacuum system will heat up causing Monitor closely and adhere to
40 – 85ºF
vacuum lose audible alarms
Pressure
C.T. pump: 80 psi Monitor pump pressure stay
Pump failure
Chiller pumps: 80 psi within range
Flow
N/A N/A N/A

2.0 Work Instructions
ACTION STEPS
o Safety
o WEAR PROPER SAFETY EQUIPMENT!
o Level D PPE
o Reference to SDS in Section 1.2 for types of safety equipment used for clean up
Setup
o Equipment Preparation
o Inspect pump for wear and tear
o Inspect piping for leaks
o Check area is clean; free of oil, debris, water & other foreign items not belonging
o Proceed to “Initial Startup “Initial Startup Procedure”
NOTE The following Pre-Check & Start Up procedure is based on all equipment working as designed
a) Identify what cooling system you are on and which system you want to be on
o Chillier system
o Cooling Tower System
b) Power to the Cooling Tower Fan is on and in auto,

o panel is located outside (north side of plant)
o Cooling tower level
c) Confirm P4201 A or B are running (should be running at all times)
d) Ensure all tank valves are set to pre-determined destinations.
e) Ensure all face plates on the Methanol screen are in shutdown prior to starting up
o This is to ensure a pump doesn’t activate / start without authorization.
Initial f) Verify tanks to confirm all tanks have the desired liquid level:
Startup o most commonly are:
▪ TK-1010 “liquid ring vacuum seal tank” ____ (SP: 45-55%)
▪ TK-1006 “Reflux / Condensing tank” _______ (SP: 40-50%)
▪ E-1002 “Column kettle reboiler” ___________ (SP: 60-65%)
g) Flushing of the system with city water is also recommended when restarting from an extended shutdown
or if composition is suspected to contain high amount of methanol content. When flushed both contents
are pumped into TK-903 for reprocessing.
o TK-1010 is flushed through the inlet tank flush port.
o Kettle boiler is flushed through suction of p-1004 / outlet of kettle boiler.
h) Once everything has been checked over & flushed if needed, you are ready to proceeded to “Normal
Operation”

ACTION STEPS
Refer to Graphic 2 in section 3.3 of this SOP
a. TK-1001 Methanol distillation column

b. E-1002 Kettle Reboiler
c. P-1004 Kettle reboiler pump
d. E-1005 Condenser
e. TK-1006 Methanol reflux / recovery tank
f. P-1007 Methanol reflux pump
g. P-1008 Methanol recovery pump
Key h. P-1009 Vacuum Pump
Equipment
i. TK-1010 Liquid seal pot (for vacuum pump)
j. P-1011 Liquid seal pot pump
k. E-1012 Methanol column condenser
l. X-XXXX Filter Housing
• Filter on the discharge side of P-1004

o Located behind Trans 1
o Use a 200 – 400-micron filter in filter pot
o Steps to change filter
1. Shut P-1004 (On Delta-V put LC1004-L3 into shutdown, or valve to TK-903)
2. Shut down diaphragm pump
3. Shut vales directly before and after filter housing
4. Open bleeder valve to relief pressure
Support 5. Slowly loosen top nuts, then open lid (there may be a little bit of pressure)
Equipment 6. Remove old filter and replace with new
7. Examen gasket then replace lid and hand tighten top nuts
8. Re-Open valves directly before and after filter housing
9. Re-Start P-1004 (on Delta-V put LC1004-L3 into AUTO_Run)
10. Start dosing pump
• Strainer on P-1004 suction side
• Cooling heat exchanger
o Supplied from cooling tower or 40-ton chiller
o See Switching Cooling Heat Exchangers

ACTION STEPS
1. Follow cart below to switch from one system to other system
2. Radio to control room to verify temperature is within range
If running, Chiller System If running, Cooling Tower System

Valve # STATUS Valve # STATUS
Switching
Cooling
Systems
3. Monitor temperature maintains in range
4. If running on chiller system monitor chiller is running with no alarms
5. If running on cooling tower system monitor water and chemicals in basin

ACTION STEPS
1. Verify that manual valves before and after pumps are all open:
a. P-1004, P-1007, P-1008, P-1009, P-1011
P-1004
HV- HV-
HV- HV-
HV-
HV-
HV-
No Tags HV-
HV-
HV-
P-1007
HV-F01-? OPEN HV-
HV-F01-46 OPEN HV-
P-1008
HV-F01-? (TK-1006) OPEN HV-F01-? (BYPASS) CLOSE
HV-F01-47 OPEN HV-F01-? (TK-903) OPEN
HV-F01-48 CLOSE HV-F01-? (TK-902) OPEN
HV-F01-? (TK-903) OPEN HV-F01-? (TK-902) OPEN
Normal HV-F01-? (TK-904) OPEN HV-FO2-32 (TK-902) OPEN
Startup HV-F01-? (TK-904) OPEN - -
P-1009
HV- HV-
HV- HV-
HV-
HV-
HV-
No Tags HV-
HV-
HV-
P-1011
HV- HV-
HV- HV-
HV-
HV-
HV-
No Tags HV-
HV-
HV-

ACTION STEPS
2. Ensure the level in TK-1010 is Between 40-50%
a. if not add water by opening the water valve until desired level is reached (50%)
3. Verify valves for E-1009 A or B are open

If using E-1009 A If using E-1009 B
HV-F01-59 OPEN HV-F01-59 CLOSE
HV-F01-56 CLOSE HV-F01-56 CLOSE
HV-F01-49 CLOSE HV-F01-49 OPEN
HV-F01-53 CLOSE HV-F01-53 CLOSE
HV-F01-? CLOSE HV-F01-? CLOSE
HV-F01-? OPEN HV-F01-? OPEN
SEE: SOP_30-10-0019_18a00_Switching Vacuum Cooling
4. Verify cooling system being used

a. See: SOP_30-10-0019_18a00_Switching Vacuum Cooling
Normal 5. Verify E-1005 valves are open

Startup Valve # STATUS Valve # STATUS
(continued) HV- HV-
HV- HV-
HV-
HV-
HV-
No Tags HV-
HV-
HV-
6. Verify E-1004 valves are open

If running E-1004 A If running E-1004 B
HV- HV-
HV- HV-
HV-
HV-
HV-
No Tags HV-
HV-
HV-
E-1012
HV-F02-18 OPEN HV-F02-? OPEN
HV-F02-? OPEN HV-F02-? CLOSE

ACTION STEPS
E-1013
HV-F02-20 OPEN HV-F02-12 OPEN
HV-F02-? OPEN HV-F02-13 CLOSE
HV-F02-16 OPEN HV-F02-? OPEN
HV-F02-? OPEN ~~~~ ~~~~
9. Set faceplates listed below on Delta-V Methanol screen to “AUTO RUN”

a. LC1001-L3 (Kettle Boiler)
b. FC1007-L6 (Reflux)
c. LC1006-L7 (Recovered MeOH)
d. LC1010-L9 (Vacuum pump)
10. Set faceplates listed below on Delta-V Methanol screen to “MD: CAS”
a. TC1001-L32 (Column bottom temperature)
b. TC1001-L5 (Delta Deg F)
c. FC1007-L6 (Recovered MeOH)
i. Using CAS mode is recommended. This will allow the system to self-adjust towards
target-based parameters. (TT1001-L4)
11. Set faceplate PC1009-L11 to AUTO RUN

Normal a. Set faceplate as follow: (*SP may change depending on needs)
Startup i. MD: AUTO
(continued) ii. SP: 7.25 psia
12. Set faceplate PC1005 as follow: (*SP may change depending on needs)
a. MD: AUTO
b. SP: 8.5 psia
13. P-1009 will start automatically (*May need to click on pump and click start)
a. Operator in field will check & listen for leaks.
b. Monitor vacuum pressure closely for several minutes to ensure levels out and is steady.
c. Once vacuum is steady, Notify operator in field.
14. Start remaining of plant following “PLANT STARTUP” SOP

a. SOP_30-10-0001_19a00_Plant Startup & Shutdown

ACTION STEPS
Normal
Operation
1. Verify that manual valves before and after pumps are all open:
a. P-1009, P-1007, P-1008, P-1004, P-1011
2. Verify the level in TK-1010 is Between 40-50%
a. if necessary, add city water until desired level is reached (50%)
3. Verify valves for E-1009 A/B are open
4. Set faceplates listed below on Delta-V Methanol screen to “Manual”
5. Set faceplates listed below on Delta-V Methanol screen to “MD: MAN”
a. TC1001-L32 --- Adjust CO: as needed to reach desired temperature
Temporary b. TC1001-L5 --- N/A
Operation c. FC1007-L6 --- Adjust CO: as needed to reach desired reflux gpm to keep top temperature
6. Set faceplate PC1009-L11 to “Manual”
a. Set faceplate as follow: (*CO will need to be adjusted slowly to allow system to respond)
i. MD: MAN
ii. CO: “adjust slowly till desired psia is achieved”
7. Set faceplate PC1005 as follow: (*CO will need to be adjusted slowly to allow system to respond)
a. MD: MAN
b. CO: “adjust slowly until desired psia is achieved”
8. Click on P-1009, once popup faceplate; click start
a. Have operator in field check and listen for vacuum leaks.
b. Monitor vacuum pressure closely for several minutes to ensure levels out and is steady.
c. Once vacuum is steady, Notify operator in field.
9. Start remaining of plant following “PLANT STARTUP” SOP

ACTION STEPS
1. Shutdown the plant

a. “SOP_30-10-0001_18a00_Plant Startup & Shutdown”
2. Once plant is shut down and there is no feed into the column…
3. Set faceplates listed below on Delta-V Methanol screen to “SHUTDOWN”

4. Set faceplates listed below on Delta-V Methanol screen to “MD: MAN”

a. TC1001-L32 --- CO: 0
b. TC1001-L5 --- N/A
c. FC1007-L6 --- N/A
5. Set faceplate PC1009-L11 to “SHUTDOWN” (Vacuum system “P-1009-L11” will then shut down)
a. Set faceplate as follow:
i. MD: MAN
Normal ii. CO: 100
Shutdown
6. Set faceplate PC1005 as follow:
a. MD: MAN
b. CO: 100
7. Follow chart below to shutdown chiller & Cooling tower system
If running, Chiller System If running, Cooling Tower System
*** System will Take about 5-15 minutes to come back to atmospheric pressure before any work can be
performed.
a) Emergency shutdown procedure

o Follow “Normal Shutdown”
Emergency o If emergency and full plant shut down required
Shutdown i. Push E-STOP on Delta-V and / or MCC-1 cabinet (next to time clock)

ACTION STEPS
a) Column (TK-1001) is flooded
o Flush the stilling well by closing top and bottom valves on kettle boiler and open drain valve.
o Ensure DPIT-1002 is below 0.60 and adjust FC1007-CTRLCAS is between 1 & 2 Delta Deg F (the higher FC
1007-CTRLCAS is, the easier to prevent column flooding).
o Slow down P-401 to reduce amount of product being sent to column and let level catch up. Use this option only
if TK-903 level is lower than 7,500 gallons.
o If oil found in column, Test on QTA to identify the source form and follow trouble shooting guide for that
equipment.
b) Kettle Reboiler (E-1002) Has false reading

o Flushing Kettle Boiler Transmitter
i. Shut Top and bottom valves located east side of kettle on the side
ii. Open bottom sample port and drain into a bucket
iii. Close sample port valve and re-open top and bottom valves to allow product in.
c) P-1004 (FT1003) Low or No flow on & Location
o P-1004 pumps product from Kettle Boiler through F-1004 (filter housing) to TK-226
o Low Flow
i. Check F-1004 (filter housing) pressure: If over 20 psi, follow steps for changing filter
1. See “Support Equipment” Section in this SOP
o No Flow
i. Check Filter housing pressure: If over 20 psi, follow steps for changing filter
1. See “Support Equipment” Section in this SOP
ii. Check Filter housing pressure: If no pressure, prime P-1004 by opening
1. water valve is located on the suction side of P-1004 labeled “WATER”
d) Flushing TK-1010 & Destination
o Open water supply valve to TK-1010 (located near tank farm wall east side)
o P-1011 will automatically start
i. Ensure LC1010-L9 is in AUTO_RUN, MD: AUTO, SP: 50
o P-1011 will start and pump product into TK-903
Trouble- o Continue to flush 5 to 10 minutes to allow for a full flush
shooting o MONITOR IN DELTA-V
i. Ensure level is being pumped down fast enough
ii. Watch TT1010 to ensure flushing is adequate
e) Not meeting temperature on TT-1010
o If running on chiller
i. Check to make sure chiller in not in alarm
ii. Check TK-1010 has liquid level
iii. Flush TK-1010 with city water for 5 minutes
iv. Check pressure differential on E-1009 A/B inlet and outlet
v. If all above is tried switch to opposite heat exchanger
o If running on cooling tower
i. Check TK-1010 has liquid level
ii. Flush TK-1010 with city water for 10 minutes
iii. Check pressure differential on E-1009 A/B inlet and outlet
iv. Check cooling tower water level in not low
v. Check discharge pressure on P-4201 A/B
vi. If all above is tried switch to opposite heat exchanger
f) Propylene glycol in cooling tower / water in glycol tank

o Verify every valve on valve list for system you want online in “Normal Startup”
g) Loss of vacuum pressure

o “SOP_30-10-0002_18a01_Methanol Column Operation & Control.pdf”
i. Verify temperature on E-1009 A/B (TT1010)
ii. Verify temperature on E-1012/3
iii. Verify level on TK-1010

ACTION STEPS
a) Follow “Normal Shutdown” above
b) LOTO
o Lock out breakers on:
i. P-1009 [MCC-#], P-1011 [MCC-#], P-1008 [MCC-#], P-1007 [MCC-#] & P-1004 [MCC-#]
Cleanup /
o Tag out all closed valves
Maintenance
o Compleate LOTO, ECP & Line break paperwork
a) Follow “Normal Shutdown” above
b) LOTO
Cleanup / o Lock out breakers on any affected pumps / tanks (Breakers located in MCC room on mezzanine)
Report / o Tag out all closed valves
o Fill out LOTO, ECP & Line break paperwork
Record
Maintenanc
c) Hydro Blast heat exchanger
e
• E-1012 (Location F01)

• E-1009 A (Location F01)
• E-1009 B (Location F01)
Tank • E-1014 (Location F01)
Information
• Chiller (Location D01) “ N/A at this time“

• Cooling Tower (Location I01) “SOP_30-10-0008_18a00_ Cooling Tower”
Support
Equipment

3.0 References
3.1 Normative References - The following reference contains provisions which through reference
in this text, constitutes provisions of this document. References, which are subject to revision,
should always be used in the most recent form.
QSP x.x appropriate number & title (e.g. cross-ref procedure)
WI 10-10-0001 QCS - Access to Online Compliance System

WI 10-10-0401 QCS - Preparation & Release of Controlled Document
SOP Cross-reference Index

• SOP_30-10-0002_18a01_Methanol Column Operation & Control
• SOP_30-10-0003_17a02_Glycerin Operation & Control
• SOP_30-10-0006_17a00_Wash Water Purification
• SOP_30-10-0001_18a00_Plant Startup & Shutdown
3.2 Documentation/Records - The implementation of this document requires the use of the below
listed forms or reasonable facsimiles thereof and may result in records as so indicated in addition
to retained completed forms. References, which are subject to revision, should always be used
in the most recent form.
Form
• 30-10-1000_16a02 American GreenFuels formula
• 20-30-7000_17a03 Lab Analysis Request-Report Form
Log Book
• 20-20-0500_Lab Instrument List
• 30-20-0400_Production Instrument List
P&ID
• Drawing No. xxx-xxx-xx (Update when new P&ID are available)
QSP
• QSP04.1_16a02 Document and data control 05082016

3.3 Appendices, Tables or Attachments
(Not an exact replica, for reference only)
Graphic 1

QC Divert Liquid
Graphic 2 Valve Seal Ring
coolers
Distillation Methanol Methanol recovery
Column Steam reflux pump pump Vacuum Liquid seal
control Pump pot pump
Kettle reboiler Kettle Methanol reflux /
pump recovery tank Liquid seal pot
30-10-0002_19a00
Reboiler Condenser
UNCONTROLLED IF PRINTED
page 15 of 17
4.0 Training Records
Trainer Name: Trainer Signature:
Date Trainee Name Trainee Signature
Antoine, Jean
Armfield, Jeffery
Ayala, Joaquin
Bauer, Jan
Brick, Richard
Bridges, Keith
Bugg, Nolan
Caraballo, Kevin
Cavanaugh, Bill
Cawley, Robert
Chai, Ming
Comfort, Kevin
Coward, Divonne
Cunningham, Corey
Cunningham, Gerald
Dorman, Walter
Ellis, Daniel
Gagnon, Cory
Garcia, Albert
Gasparik, Mikulas
Gianini, Ricky
Giordano, Davis
Guliuzza, Joseph
Hart, Nick
Hayden, Sean
Hurlbul, James

Date Trainee Name Trainee Signature
Jones, Richard
Kimmel, Brian
Korner, Glenn
Leary, Justin
Lewis, Jonathan
Lorig, Christian
MacMichael, Chris
Marrette, Matthew
Mbaye, Khadim
Medina, Omar
Morris, Michael
Munck, Keith
Noble, Donovan
Rawlls, Derek
Raymond, Harold
Rosario, Lenin
Samuels, Hugh
Sileo, Ryan
Spivey, David
Strickland, Ken
Tourville, Glen
Vega, Michael
Wermann, William
Williams, Gilbert
Wong, Jeremy

American Greenfuels Standard Operating Procedure 30-10-0002 Methanol Column Operation & Control

Hochgeladen von

Dokumentinformationen

Originaltitel

Copyright

Verfügbare Formate

Dieses Dokument teilen

Dokument teilen oder einbetten

Freigabeoptionen

Stufen Sie dieses Dokument als nützlich ein?

Sind diese Inhalte unangemessen?

Copyright:

Verfügbare Formate

American Greenfuels Standard Operating Procedure 30-10-0002 Methanol Column Operation & Control

Hochgeladen von

Copyright:

Verfügbare Formate

American GreenFuels Standard Operating Procedure

30-10-0002 Methanol Column Operation & Control

Revisions Made to Documents

REVISION DATE: MAY 8, 2019

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 0 of 17

1.0 Purpose and Scope

1.2 Chemicals Used & Hazards Presented by the Chemicals Used

1.3 Precautions Necessary to Prevent Exposure

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 1 of 17

1.4 Control Measures to be Taken if Physical Contact or Airborne Exposure Occurs

1.5 Quality Control for Raw Materials

1.6 Any Special or Unique Hazards

1.7 Instrumentation and Safety Systems

Heating Side of System

N/A N/A N/A

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 2 of 17

2.0 Work Instructions

b) Power to the Cooling Tower Fan is on and in auto,

c) Confirm P4201 A or B are running (should be running at all times)

d) Ensure all tank valves are set to pre-determined destinations.

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 3 of 17

Refer to Graphic 2 in section 3.3 of this SOP

a. TK-1001 Methanol distillation column

• Filter on the discharge side of P-1004

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 4 of 17

2. Radio to control room to verify temperature is within range

If running, Chiller System If running, Cooling Tower System

3. Monitor temperature maintains in range

4. If running on chiller system monitor chiller is running with no alarms

5. If running on cooling tower system monitor water and chemicals in basin

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 5 of 17

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 6 of 17

3. Verify valves for E-1009 A or B are open

4. Verify cooling system being used

Normal 5. Verify E-1005 valves are open

6. Verify E-1004 valves are open

7. Verify E-1012 valves are open

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 7 of 17

9. Set faceplates listed below on Delta-V Methanol screen to “AUTO RUN”

11. Set faceplate PC1009-L11 to AUTO RUN

14. Start remaining of plant following “PLANT STARTUP” SOP

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 8 of 17

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 9 of 17

1. Shutdown the plant

3. Set faceplates listed below on Delta-V Methanol screen to “SHUTDOWN”

4. Set faceplates listed below on Delta-V Methanol screen to “MD: MAN”

a) Emergency shutdown procedure

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 10 of 17

b) Kettle Reboiler (E-1002) Has false reading

f) Propylene glycol in cooling tower / water in glycol tank

g) Loss of vacuum pressure

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 11 of 17

a) Follow “Normal Shutdown” above

a) Follow “Normal Shutdown” above

• E-1012 (Location F01)

• Chiller (Location D01) “ N/A at this time“

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 12 of 17

QSP x.x appropriate number & title (e.g. cross-ref procedure)

WI 10-10-0001 QCS - Access to Online Compliance System

SOP Cross-reference Index

30-10-0002_19a00 UNCONTROLLED IF PRINTED page 13 of 17

3.3 Appendices, Tables or Attachments

(Not an exact replica, for reference only)