Beruflich Dokumente
Kultur Dokumente
3
GEA Westfalia Separator
1. Introduction
The history of industrial citrus processing for fruit juice and the consumption of fruit juice,
is relatively recent. Citrus fruits used to be and thus sales opportunities, are increasing
principally marketed as fresh fruit, because it was throughout the entire world.
not possible to preserve them and sell them in
a preserved condition. The citrus industry took Figure 1 details the quantities of citrus fruits
an upturn in the mid-1940s. This was primarily which are harvested. Figure 2 demonstrates per
brought about by the introduction of modern capita consumption of fruit juice and nectar.
juice extraction processes. Since then, the market
Fig. 1 Quantities
of citrus fruits
harvested.
The largest
manufacturing
countries of the
respective products
are printed bold.
Liters
The increasing popularity of citrus beverages GEA Westfalia Separator has been heavily involved
with the consumer, together with the importance in developing a large number of new processes.
which food scientists attach to the citrus fruit, has Modern citrus fruit processing methods provide
led to an impressive development in this market. many possibilities for the application of clarifying
and separating technology.
Two technological developments were among
the most important reasons for this rapid The wide range of application possibilities is due
growth process. to the many different stages involved in citrus
fruit processing. The individual components
These developments were: which are recovered can, in turn, be used for
• Automatic juice extractors recovering a wide range of new products.
• Gentle concentrate production processes Each method poses very specific requirements
with respect to process engineering and
Nowadays, technical experts and engineers are machine equipment.
increasingly devoting their attention to recovering
new products from citrus fruit, to increasing This technical-scientific documentation details
the amount of valuable components obtained, the wide range of methods and technological
to improving the quality of these components stages of citrus fruit processing. In particular, it
and to automating and optimizing the will discuss the use of centrifuges for solving a
traditional processes. wide range of problems encountered in the fields
of separation and clarification.
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GEA Westfalia Separator
2. Citrus Fruit as the Raw Product
The processing method and procedure are Because citrus fruits grow throughout the year and
determined principally by the type of fruit and because the ripening period can last for a total of
the structure of the fruit. five months, the fruits obtained at one particular
harvest are different from fruits obtained at other
The fruit types can be roughly classified as follows: periods of the harvest, particularly with respect
to acid, sugar and pigment content. The different
Orange-fruit types: types of fruit, depending on type and ripening
• Sweet orange conditions, also differ in other respects (vitamin
• Bitter orange C, pectin, carotenoids, flavonoids, etc.).
• Mandarine
The characteristic properties of the raw product
Yellow-fruit types: exert a great influence on the final product. Today,
• Lemon the assessment of juice quality is simplified by
• Lime, limetta statistical indices obtained from genuine raw
• Grapefruit product samples.
The orange (citrus sinensis) ist the most important Figure 4 shows typical analytical values for
basic product in the citrus industry, followed by orange juice.
grapefruits, lemons and mandarines.
The first stage of industrial processing of citrus
Following is a list of the main types of oranges fruit is to extract juice from the endocarp.
grown in the individual citrus fruit countries: The residues which are created in this process
• Brazil: Hamlin and Pera are the basis for producing a wide range of
• USA: Navel in Florida, Valencia in California, additional marketable by-products. Many of these
Jaffa and Pineapple by-products come from those parts of the fruit
• Italy: Biondo Comune, Ovale which several years ago were discarded as they
• Spain / Marocco: Navel, Valencia, Jaffa were not considered to be of any value.
• Israel: Shamuty, Valencia
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GEA Westfalia Separator
Fig. 4 Standard
values for
orange juice
(AIJN – Code
of Practice)
1
8
7
6
5
4
3
2.1. Structure of the fruit Compared to the flavedo, the cells of the albedo
The following is a simplified explanation of the are larger, less compact and very high in pectin
structure of the citrus fruit: content. The albedo borders on the edible part
of the fruit.
Peel (pericarp)
This is made up of two layers, namely the flavedo Flesh (endocarp)
and the albedo. The flavedo is the outer layer of The flesh of the fruit is divided up into radial
the peel. It is pigmented and relatively thin. In segments. These segments consist of a large
ripe fruits, the flavedo contains the vesicles and number of juice sacs which are held together by
also the pigments which contain carotene. The high-molecular adhesive substances. The seeds
vesicles contain essential oils. The outer epidermis are located towards the center of each segment,
is covered by natural wax. This layer of natural near the fruit axis. Short vascular bundles connect
wax prevents water losses and protects the fruit the seeds to the main (threadlike) bundles which
against fungal infections. run along the main axis of the fruit.
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GEA Westfalia Separator
3. Processing
There are two main production fields in industrial
citrus processing, and the differences between the
two are related to the geographical area where
the fruits are processed. In the Americas (Brazil,
USA), large quantities of fruit are processed into
standard products in a relatively small number of
very large companies.
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GEA Westfalia Separator
Citrus fruits
Segments Alcohol
Candied peel
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GEA Westfalia Separator
4. Process Lines for the Production and
Recovery of Citrus Fruit Products
BROWN method
In this method, the fruits are cut in half. The juice
is then extracted from each half by means of a
rotating squeezing head. This system is simply a
mechanized and automatic version of the simple
Fig. 9 Diagram of juice extraction from whole fruits, manual lemon press found in every kitchen. The
using extractor JBT fruit holder replaces the hand, and the rotating
squeezing head replaces the pointed section of
the lemon press.
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GEA Westfalia Separator
1 2 3 5 6
F
W
T
N P
U
4
7 10
D
H
D
K
8 9 11 12
The orange juice is discharged from both during the process of centrifugal clarification. In
extraction systems with approximately 11° Brix this way, it is possible for the product to be adapted
and a pulp content of between 20 and 25 at the stage of juice recovery to suit the specific
percent (by volume). The pulp is then reduced requirements or expectations of the consumer.
to approximately 10 – 12 percent (by volume) in The fruit juice which is recovered is then subjected
downstream finishers (horizontally-mounted to heat treatment (pasteurization or flash
screen drums). Coarse trub particles such as cells, pasteurization) and is subsequently directly filled
rags and other fibrous materials are separated into containers (single strength juice). However, it
out in these finishers. Centrifuge systems is usual for this pre-clarified juice to be evaporated
can then be used to reduce the trub particles in order to obtain concentrates. Approximately
to almost any desired residual level. All 10 – 12 tonnes of fruit are necessary to produce 1
intermediate stages of residual solid level tonne of concentrated orange juice with 65° Brix.
can be achieved by varying the throughput
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GEA Westfalia Separator
60
50
Clarification performance in m3 / h
40
30
8 %
6 %
20
4 %
2 %
10
0
GSC 45 GSE 75 GSE 125 GSC 150 GSE 200 GSE 300
Fig. 11 Capacities of various clarifiers used for pulp reduction as a function of clarification efficiency.
The value shown here refers to machines without continuous pulp removal.
The centrifugal pre-clarification of the raw juice sediment, can be separated off. Only the extremely
permits the production of juices with a high cloud stable fine particles remain in the juice. The
degree of cloud stability since centrifuges classify risk of deposits forming is therefore reduced to
trub particles according to particle size. All coarse a minimum.
trub particles, which have a strong tendency to
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GEA Westfalia Separator
Italian method clarification stage. Pre-clarification is carried
If a solid content below 1 percent (by vol.) is out in a decanter, and subsequent clarification
desired, a 2-stage process using a decanter can be is performed by a clarifier in the second stage.
provided. The juice is heated in a tubular heater This method is used principally in Italy. It is not
to between 75 and 85° C before entering the first necessary to use an upstream finisher when the
Italian method is used.
F
T W
P
1 2 3 4 5
H
B
K
D
11 10 9 8 7 6
* The capacity figures listed above are based on a pulp content in the decanter feed of 25 percent (by vol.) and 3 percent (by vol.) in the decanter discharge.
** For clarifiers, the pulp contents are 3 percent (by vol.) in the feed and 0.5 percent (by vol.) in the discharge.
Fig. 14 Sample of types and capacities of decanters and clarifiers used for pulp reduction in the production ot citrus juice
(“Italian method”)
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GEA Westfalia Separator
Separators with continuous de-pulping
In an alternative process configuration, the pulp
is discharged from the clarifier bowl by means of
a special centripetal pump. This reduces the load
on the disk stack. The intervals between the solid
ejection cycles are considerably lengthened. The
clarification efficiency of the centrifuge is vastly
improved. Consequently, higher throughput
capacities and / or residual pulp contents in the
juice of 1 percent (by vol.) can be obtained.
1 Tank
2 Pump
3 Solids tank
4 Clarifier
5 Flowmeter
6 Reversing valve
7 Pulp sensor
8 Pressure sensor
9 Control valve
* The capacity figures listed are based on a residual pulp content in the separator feed of between 10 and 12 percent (by vol.).
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GEA Westfalia Separator
4.2 Automatic de-pulping and de-bittering Centrifugal separation technology allows gentle
product treatment for this purpose.
De-bittering and acid adjustment of
citrus products De-bittering (“adsorption”)
Depending on the raw material used and on the In the adsorption process, the juice is sent through
desired end product, the extracted juice may have a column containing an adsorbent polymer resin.
to be de-bittered or de-acidified. To achieve this, Polymer resin adsorbs the bitterness (e. g. limonin
citrus juice is processed with adsorption plants or naringin).
in order to improve the quality and value of
the product. De-acidification (ion exchange)
In the ion exchange process, the juice or fruit
Adsorber columns containing resin reduce the extract is sent through a column containing an
bitterness and acidity respectively. ion exchange resin. In this way fruit acids are
exchanged onto an absorbent medium.
Perfect operation of the adsorption plant requires
a juice with a pulp content below 1 percent. In both cases, when the capacity of the resin has
been exhausted, the resin has to be regenerated
so that it can be reused. Stainless steel columns
are used to contain the resins. For continuous
processing, equipment with twin alternating
columns is used. One adsorber unit is processing
while the other one is regenerating.
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GEA Westfalia Separator
1 Separator
2 Supply tank
6
3 Pump
4 7 4 Adsorption unit
5
2 (column 1)
5 Adsorption unit
(column 2)
6 Resin purification
7 Tank
Juice with 0.05% oil 8 Pump
Juice with
9 Mohno pump
max. 1% pulp
3 8
Excess pulp
e. g. with 10% pulp content
1 9
Fig. 20 Processing of citrus juices with a separator (left) and adsorption unit (right)
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GEA Westfalia Separator
4.3 Juice de-oiling – “Top oil separation” The machines used are separators (liquid-liquid
Juice de-oiling is a special application for the separation).
production of nfc juices (not from concentrate).
Depending on the extraction system used, more These machines are adapted to the very small
or less high quantities of peel oil enter the juice. contents of light phase (citrus oil). The separated oil
When producing concentrate, this oil is evaporated is generally not used because of the low quantity.
which presents no problem. In the production of
nfc juices, however, this oil cannot be thermally In addition to the ESE 140 and ESE 230 models,
separated. Due to the fact that the oil remains there is a demand for even larger machines as
in the juice, an unpleasant, astringent taste may a result of rapid market growth. GEA Westfalia
develop. This makes it necessary to separate the Separator responded by presenting the ESE 500
oil in order to obtain a high-quality juice. The oil for the high capacity range and by successfully
content is reduced to maximum 0.035 percent (by putting this separator into operation.
vol.). Some producers demand values smaller than
0.03 percent (by vol.). The separator type ESE 500 offers feasible
economic possibilities for producing large volumes
This limitation of the oil content can be of nfc.
achieved by appropriately modifying the
extraction systems. However, in most
cases a compromise has to be accepted
in terms of yield and hence the economy of
the process. For this reason, there is a growing
interest in centrifugal polishing of the oil from
the partially pulped juice.
* The figures are based on an oil content in the separator feed of
maximum 0.1 percent (by vol.) and of maximum 0.035 percent
The oil content is centrifugally separated gently (by vol.) in the discharge.
so that values between 0.02 and 0.03 percent (by
vol.) can be obtained (based on feed oil contents of Fig. 21 Guide values for processing orange juice with
0.1 percent (by vol.). Product losses are minimal. 1 – 8 percent (by vol.) pulp
J Juice
J O P O Oil discharge
J P Solids
D Steam
2 3 5 6
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GEA Westfalia Separator
1 2
F
W
T
J
3 4 5 6
P
J P
11 10 9 8 7
4.4 Pulp wash The pulp wash obtained in this process has a Brix
In the production of pulp wash, the cells which content of between 4 and 5° and still contains a
have been separated out by the finisher are treated high proportion of trub particles. These can be
in a multi-stage counter-current washing system. separated out with the aid of clarifiers. The pre-
With the aid of scroll mixers and finishers, it is clarified product is concentrated to 60° Brix in
possible to extract up to 90 percent of the valuable an evaporator.
juice components such as fructose, fruit acids,
minerals, carotenes, etc., from the cells. Pulp wash can be marketed as a product in its
own right. It is also usual and allowed in some
markets to mix orange juice with the pulp wash
before the concentration process. The maximum
amount of pulp wash which may be blended with
the first-class juice is governed by the statutes and
standards in each individual country.
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GEA Westfalia Separator
4.5 Clear lemon juice
The production of clear lemon juice used to be
very difficult, time-consuming and associated
with a high level of risk in terms of quality.
Using traditional methods, the clarification
process involved allowing the juice to stand.
Several weeks were frequently necessary for
this process. In view of the lengthy amount
of time necessary for the sedimentation
process, the juice had to be protected
a ga i n s t ox i d a t i o n a n d a l s o a ga i n s t
u n d e s i r a b l e m i c r o b i o l o g i c a l a c t i v i t y.
Today it has been possible to reduce process
Fig. 24 2-stage plant with GSC separators
times to between approximately 6 and 8 hours.
This has been achieved by making use of
traditional pre-clarifiers combined with modern
high-performance clarifying centrifuges (g force:
15,000) and also by making use of newly developed
enzyme preparations.
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GEA Westfalia Separator
Fig. 26 Process for the production of clear lemon juices
For clarifying the juice, the Kieselsol is mixed of ultradispersion), thus providing a poor
intensively with the product. The mixing clarification effect.
equipment is then switched off and the mixture is
permitted 30 minutes reaction time. The very fine The clear juices are usually then further processed
particles coagulate during this period. In the fine into concentrates.
clarification process, the fined juice must be fed
smoothly into the centrifuge, avoiding excessive Instead of the high performance centrifuges a
shear forces. Gravity feed or specially chosen membrane filtration plant can be used. More
smooth-action pumps are suitable for conveying information on this topic can be found in chapter
this product. 5.5. Capacities of high performance centrifuges
and membrane filters will be communicated
Poorly designed pumps lead to the mechanical on request.
destruction of coagulated trub particles (principle
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GEA Westfalia Separator
4.6 Natural cloudy peel products • Centrifugal pre-clarification by means
Cloudy peel products are obtained principally from of decanter: Reduction of solids to
citrus peel. However, the basic product may also be approximately 1⁄4 of level in feed
a mixture of peel and pulp. The product which is • Centrifugal clarification by means of clarifiers:
obtained from the peel by extraction with water is Reduction of solids in decanter discharge to
concentrated from an initial level of 4 to 5° Brix to a less than 1 percent (by vol.)
final level of approximately 50 ° Brix. It contains the
natural components of the original material. The The products obtained from this process are used
product is cloudy, but at the same time it exhibits as basic products in the soft drink industry. The
extreme cloud stability. The cloudiness is most important property of this product is its
attributed to the effect of pectins, polysaccharides excellent cloud stability. It is also very important
and waxes and the essential oils. for the beverage industry as an aroma, trub and
coloring agent.
Cloudy peel products can be obtained via a number
of methods. However, processes which make use
of pectolytic, cellulytic and proteolytic enzymes
and which permit enzymatic liquefaction of
the original material appear to be gaining the
upper hand.
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GEA Westfalia Separator
1
2
W
3
U U
4 5 6 7 8 9
16
10
18 17 15 14 13 12 11
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GEA Westfalia Separator
4.8 Essential oil Juice and oil are extracted in one process step
Citrus peel contains essential oils. These oils are where JBT extractors are used for processing citrus
formed in the cells of the so-called oil glands, and fruit. The peel of the fruit is cut and squeezed
they are some of the most important by-products during the processing procedure. This releases
obtained from the processing of citrus fruit. the oil which is contained in the peel. The oil is
obtained from the flavedo during this mechanical
Essential oils are in demand as taste and aroma treatment. The valuable essential oils are then
agents for the food industry and for the production washed out and separately collected during this
of odorous substances. Several methods are process step.
available for recovering essential oil.
1 Extractor
1 2 4 2 Vibrating screen
3 Pump
4 Tank
5 Pump
T 6 Hydrocyclone
W 7 Separator (first stage)
F
J 8 Buffer tank
U 9 Mohno pump
13
12 10 Separator (second stage)
3 5
11 Pure oil tank
12 Automatic filter
W
13 Treatment tank
14 Pump
14
F Fruits
J Juice
O
O Essential oil
W 6
O T Emulsion
U Solids, sand
W Water
U U
U W
11 10 9 8 7
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GEA Westfalia Separator
In other juice recovery methods, either the
peel of the citrus fruit is pricked before the
extracting process and the oil which appears is
washed away with water (BROWN), or the outer
section of peel (flavedo) is rasped before being
mixed with water and then further processed
(INDELICATO). The first stage configuration is based on an emulsion with an oil content of
0.8 – 1.2 percent (by vol.).
The oil-water emulsion obtained in modern fruit Fig. 30 Essential oil concentration (first stage) with separators
processing lines contains approximately 70 to 90
percent of the essential oil naturally present in
the peel. The peel wash water contains between
2 and 5 kg essential oil as an emulsion per
100 kg of raw material processed, depending
on the type of fruit and the processing
technology used.
Fig. 31 Polishing of essential oil (second stage) with separators
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GEA Westfalia Separator
Depending on the type of fruit, the proportion action displacement pump delivers the
of oil in the wash water is between 0.5 and 2.0 essential oil into an overhead tank. It is then
percent (by vol.). In the concentration stage (first conveyed to a de-waxing stage. The level of liquid
stage), this oil is generally concentrated up to 70 in the overhead tank and thus the delivery head
to 85 percent (by vol.). At the same time, relatively of the pump are kept constant by means of an
coarse solids fractions are separated off. Figure 30 overflow. This also provides a constant pressure
shows the first separation stage with separators for the partial stream diverted off to the separator.
and capacities. This partial stream is also called the impulse oil.
The total volume of oil contained in the peel wash The quantity flowing into the separator can be
water can be efficiently recovered as clear essential set by means of a throttle valve. The impulse
oil with a suitably rated 2-stage centrifuge system. oil is recycled into the sediment holding space
of the separator. When the sediment holding
The process of phase separation is described in space is optimally filled with water and solids,
detail in section 5.3. In the polishing stage (second the flow of the impulse oil is blocked. This causes
stage), the remaining water is removed and the the pressure in the impulse oil line to rise. The
very fine solids particles are separated off. pressure switch in the impulse oil line registers
the pressure differential and triggers the solids
The second processing stage with separators and ejection signal.
capacities is illustrated in figure 31.
The operation of this “self-thinker” control system
Under certain conditions, the polishing separators is not time related. A timing unit is not required.
of the second stage can be provided with a “self-
thinker” control system ensuring bowl ejections The advantages of this “self-thinker” control
are triggered at the optimum fill level of the system are as follows:
solids holding space. Figure 32 illustrates the • A high level of reliability
corresponding system. • Solids are ejected from the bowl only when
the optimum level is reached
Depending on the type of separator, the pure • Solids not ejected at inappropriate moments,
essential oil discharges either under gravity e. g. if product feed is interrupted
or is pressure-discharged via a centripetal • Optimum oil yield
pump. It is then collected in a tank. A smooth-
1 Separator
2 Collecting tank
4 3 Pump
4 Overhead tank
5
5 Needle valve
T O Essential oil
O
5 T Emulsion
O U Solids
W Water
U
W
1 2 3
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GEA Westfalia Separator
This “self-thinker” control system is suitable for Cost-effectiveness and waste water disposal
plant automation and is used in the USA. considerations resulted in a large number of
companies recycling water discharged by the
The following technical process parameters must separators back into the process after appropriate
also be observed in order to achieve optimum treatment.
yield values:
• Use of smooth-action pumps for conveying The advantages are as follows:
product (avoidance of shearing forces) • Reduction of water consumption
• Addition of water in correct quantities during • Quantity and pollution level of waste water
extraction or during pricking reduced (essential oil has a bacteriostatic
or rasping effect even in low concentrations)
• Avoidance of excessively high temperatures
(danger of evaporation)
Emulsion
recycling
Extraction
Up to 25%
in the peel
Pre-screening
of light emulsion 1% in the trub
(de-pulping) particles
Separator,
first stage 2 – 6%
(concentration) in the water
Separator,
Approximately
second stage
2% in the water
(polishing)
Storage
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GEA Westfalia Separator
4.9 Citrus oil de-waxing 4.10 Aroma water
Waxes in the citrus fruit peel form a natural Citrus juices are frequently concentrated in
protective shield. In particular, these waxes multi-stage evaporators. Considerable quantities
prevent the fruit from drying out. of steam condensate and vapor condensate are
produced in this process.
In the technical process of recovering valuable
essential oil (cf. section 4.8), a proportion of this Certain quantities of aroma components and
wax enters the oil phase. The quantity of wax will essential oils are lost in the vapor condensate.
depend on the extraction system which is used. These valuable fruit components occur almost
These waxes are undesirable products. After the exclusively in the first evaporation stage.
clear oil has been stored for a certain time, the
waxes become insoluble and lead to a deterioration For this reason, the condensate at this point is
in the quality of the oil and must be removed for also described as aroma water. Almost all citrus
this reason. There are various methods which are factories recover the aroma water and subject it
suitable for this process. to further treatment. The process of aroma water
recovery is useful and advisable for both quality
In most cases, the de-waxing procedure involves and flavor reasons, particularly in conjunction
storing the essential oil at low temperatures. with the citrus fruits grown in regions with a less
Depending on the temperature and type of fruit, favorable climate.
a period of up to two months may be required for
the total cold-sensitive wax content to precipitate The recovery process is as follows:
out of solutions.
The aroma-containing condensate obtained in the
first evaporation stage is collected separately and
cooled down to ambient temperature. However,
oil components of the juice are also separated
out in the evaporator, and these are precipitated
with the condensate. This necessitates a process
of separating aroma water and oil. Separators
(2-phase separation) have proved to be particularly
suitable for this task. The separated oil-free aroma
water is used either for blending the concentrate
(cf. figure 36) or marketed as aroma water which
is surplus to requirements. The separated oil
is used in many applications, e. g. in the
cosmetics industry.
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GEA Westfalia Separator
1 2 4
D H
B
J J
K A
A, O
O A
5 6 7 8 9 10 11 12 13
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GEA Westfalia Separator
4.11 Alcohol from citrus peel The press liquor is clarified with the aid of
In light of continually fluctuating crude oil decanters. This process stage prevents the
prices, diminishing natural resources and strong occurrence of trub particles and lime deposits in
political dependence on oil exporting countries, the downstream evaporator stage, ensuring that
attempts to provide safe energy supply are one of the evaporator operates in a cost-effective manner
today’s mega trends. without malfunctioning.
Many countries are turning to the possibility of The pre-concentrated press liquor is a
introducing savings in traditional energy sources, fermentable substrate. The fermentation yeast
particularly crude oil. All imaginable alternative can either multiply if oxygen is added, or, if
energy sources are used for generating energy. most air is excluded, it can produce alcohol from
carbohydrates.
The recovery of energy from biomass, and in
particular from sugar cane, is now very important In this biochemical process, the sugar content in
in Brazil. the press liquor is broken down into alcohol and
CO2. When the alcoholic fermentation process has
Solar energy can also be used indirectly by finished, the yeasts as well as other coagulated
recovering energy from the vegetable biomass solids are separated off in a nozzle bowl centrifuge.
“citrus peel.” Large quantities of citrus fruit peel
are obtained in the course of citrus juice recovery The pre-clarified alcohol solution is then distilled.
(up to 50 percent by weight of the fruit). The alcohol is separated and fractionated in modern
distillation columns. The bioalcohol obtained
It is possible to use biotechnological methods to from this process is a very energy efficient fuel for
convert citrus peel into various forms of energy, combustion engines, both in terms of efficiency
and principally mobile forms of energy. and power yield. One significant advantage of this
fuel when compared with gasoline is its high level
For instance, it is possible to obtain alcohol from of environmental friendliness.
citrus peel as described below.
Alcohol recovered from citrus peel is also used
The de-oiled citrus peel which is discharged from in the chemical and pharmaceutical industries,
the extractor is disintegrated, neutralized with e. g. for plastics, chemicals and also as a solvent.
lime (CaCO3) and conveyed to a special press.
The pressed peel is further processed into animal
fodder, as used to be the case in the past.
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GEA Westfalia Separator
1 4 5 6 9
V
X 2
Y
10
3 15 U
7 8
B
18 Z H
11
U
Z
19 16 14 13 12
17
H H
21 21
D D
20 20
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GEA Westfalia Separator
5. Systems for the Citrus Industry
9.1 Decanters The scroll rotates slightly faster than the bowl
When clarifier operation is no longer feasible shell and conveys separated solids continuously
due to high proportions of solids in the towards the narrow end of the bowl. Due to the
suspension to be processed, decanters are conical shape of the bowl here, the solids are lifted
used. The decanter design is based on decades out of the liquid and, on passing through the
of experience in centrifugal separation “drying zone” which is no longer filled with liquid,
techniques as well as intensive research and freed from any adhering liquid by centrifugal force.
development by GEA Westfalia Separator. The solids are then discharged into the collecting
Decanters have been developed for chamber of the housing through openings in the
high clarifying performance and the end of the bowl. The liquid flows out between the
maximum possible degree of solids flights of the scroll to the other end of the bowl.
de-watering. Essential conditions for this include, Slight impurities remaining in the liquid are
among others, high bowl speed and an enormously spun out by centrifugal force as the liquid flows
high scroll torque in conjunction with a control through the clarifying zone and is pumped by
system to synchronize differential speed and the scroll to the “solids discharge” point together
solids load. with the solids which have already been collected
in the feed zone. The clarified liquid leaves the
In this process the product enters the decanter separation chamber under pressure by means of
through the feed tube and the distributor centripetal pumps. Depending on the decanter
conveys it into the separating chamber where it type, it may be driven by a 3-phase AC motor
is accelerated to operating speed. The action of for controlled torque starting or alternatively by
centrifugal force quickly causes solid particles to 3-phase AC motors with a frequency converter.
sediment on the bowl wall. This allows start-up current and current peaks on
start-up to be reduced. The power is transferred
The bowl is of a cylindrical / conical shape. In the by belts.
cylindrical section, this shape allows effective
clarification of the liquid, while in the conical
section, the solids are effectively dried.
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GEA Westfalia Separator
5.1.1 GEA Westfalia Separator varipond ® –
reliable mastery of solids concentration
This control system uses existing capacities so
accurately that maximum results are achieved for
minimal duty. GEA Westfalia Separator varipond
means “variable pond depth with machine running.”
Even if feed concentration varies dramatically, the
system controls the liquid level in the decanter
bowl so accurately that the concentration of the
concentrated solids can be set to a constant value
and maintained.
2-gear drive
With this drive, the main drive motor drives the bowl
and the housing of the primary gear. An additional
secondary gear allows part of the power required
for the scroll drive to be provided by the secondary
motor. The current of this motor serves as a measure Fig. 40 2-gear drive
of torque-dependent differential speed control. The
drive is electronically monitored and can be
restarted. Downtimes due to overloading are
ruled out and smooth operation is guaranteed.
Decanters with this drive, which is patented in many
countries, are used when high torques are required
for maximum yields at low differential speeds.
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GEA Westfalia Separator
2.2 Clarifiers – The performance factor is calculated from:
high product quality and yield • Bowl speed
The expertise gathered from decades of experience • Disk angle
enabled GEA Westfalia Separator to adapt the • Number of disks
design of its separators to suit the requirements • Disk diameter
of the juice industry completely. Self-cleaning
separators are used for juice clarification and Separators are designed for the greatest
these naturally satisfy the requirement for a possible effective capacity, but there
continuous process. are limits. Bowl speed is limited by
the permitted material loading. Further,
The separators are equipped with a disk bowl and disk angle, disk diameter and number
sliding piston. The liquid is quickly and gently of disks have to be matched to the
clarified in a disk stack, the solids being spun different products.
outwards into the solids chamber. Once the
optimum emptying point has been reached, At a relatively high loading with solids in the feed,
the sliding piston is opened hydraulically. e. g. in juice clarification, effective capacity also
Once operating speed is reached, the solids are depends on the size of the solids chamber and
suddenly ejected and the sliding piston returns possible ejection frequency.
to the closed position. The clarified liquid is
taken away without foam and under pressure by Effects on clarification
centripetal pumps. If the liquid should not come There are many factors influencing the
into contact with the outside air, these separators efficiency of centrifugal clarification
can be supplied in a hydrohermetic (liquid seal) of liquids. Both product-specific and
variant. mechanical parameters have an effect. The
first group includes particle size, specific
Hydrohermetic variant density, viscosity and the proportion of solids in
With these separators, the seal to the atmosphere the liquid to be clarified. In mechanical terms, it
is achieved without using seals subject to wear by is primarily g-force, equivalent clarification area
means of an immersion disk arranged above the and the solids storage volume of the bowl which
product’s centripetal pump. This prevents the spun are the key factors.
product coming into contact with the outside air.
On a specified separator, there are options for
High-performance clarifiers improving the degree of clarification. Measures
Separators of this series can be supplied with the frequently used include:
hydrohermetic variant. Use of new, high-strength • Reducing capacity
materials means that centrifugal forces 15,000 • Adding fining agents to form particles
times those of the acceleration due to gravity can • Increasing temperature to reduce viscosity
be achieved. That way, solids particles up to an • Diluting with water to reduce density
order of magnitude of approximately 0.5 μm can and viscosity
be separated.
34
GEA Westfalia Separator
GEA Westfalia Separator hyvol® and A final feature shared by all GEA Westfalia
hydry® generations of machines cover the Separator hyvol® systems is their very fast ejection
full capacity range valves. The focus with these machines is on a very
GEA Westfalia Separator hyvol ® and hydry ® high hourly output.
machines are two families of separators. Both
cover the full range of capacities in the beverage The focus in developing GEA Westfalia
industry with optimum machine sizes for each Separator hydry® separators was on achieving
application. GEA Westfalia Separator hyvol® and the greatest possible dry substance content in
hydry ® separators have been optimized in terms the solids. With these machines, the greatest
of customer benefit and rapid integration in a content of dry substance is in the normal
user’s individual process. The principle of GEA range thanks to the GEA Westfalia Separator
Westfalia Separator hyvol® is to provide maximum hydrostop ejection principle. The optimum solids
effective capacity for the specified volume concentration is reflected in very short pay-back
of investment. times, especially if, as in the juice industry, large
quantities of liquid have to be processed.
GEA Westfalia Separator hyvol ® refers to a Product losses are extremely low. All GEA
separator with an ejection system for piston Westfalia Separator hydry ® and hyvol ®
valves. Use of the hydrohermetic feed minimizes separators are equipped with a belt drive. They
the negative impact of shear forces and guarantees are characterized by their ability to be put
optimum separating efficiency. to multifunctional use. The benefits of GEA
Westfalia Separator hydry® separators become
Separation performance and product quality are particularly clear when the objective is to clarify
consequently ideal. The hydrohermetic seal high-quality products. The minimized product
prevents the product from becoming contaminated losses can lead to a short pay-back time for
by ambient air. This seal simultaneously combines the lines.
optimum compatibility for CIP (Cleaning-In-
Place) with no need for maintenance.
35
GEA Westfalia Separator
In this case, both liquid phases are pressure
discharged. For this purpose, a double centripetal
pump is installed in the bowl top.
5.4 Hydrocyclone
Initial separation of coarse and abrasive solids
If the starting product for processing contains
a high quantity of abrasive and coarse
solids, these impurities need to be separated
off beforehand so that the continuous
Fig. 43 Separator of the ESE series separation process is guaranteed and
damage due to abrasion and other malfunctions
can be avoided on the separator.
36
GEA Westfalia Separator
5.5 Ceramic membrane filtration
Filtration of juices
A filtration step is required to produce clear juices.
Colloidal trub material as well as particles have
to be removed to prevent the juice or concentrate
from subsequently becoming turbid. As more
stringent requirements are placed on the type
of membrane in these applications, the ceramic
membrane has been tried and tested in the field.
37
GEA Westfalia Separator
6. Summary
The most important process is the extraction of Waxes are precipitated when essential oils are
the juice from citrus fruits. Such a process must stored. These must be removed from the citrus oil.
ensure reliable separation of juice, essential oil A “winterization” process is necessary for this
and peel. purpose. The precipitated wax is then separated
off via a separator.
The pulp content of the juice is reduced in
downstream finishers. Centrifugal separation Essential oils and aroma components are
technology is then used for setting the desired contained in the evaporator condensate which is
residual pulp content. Centrifugal pulp reduction referred to as aroma water. Separators are used for
of the juice enables the production of juices with separating the oil from the aroma water.
a high cloud stability.
Citrus pectin is a further by-product obtained
The pulp, which is obtained during the production during the processing of citrus fruits. It is also
of juice, and concentrate still contains valuable juice recovered from the peel. In order to obtain the
components. These valuable substances can be citrus pectin, the peel is blanched, dried and
extracted in a counter-current washing process. stored before being conveyed to the extraction
The recovered pulp wash is clarified by means of process. Centrifuges are used for removing the
centrifuges and then concentrated in evaporators. solids from the liquids in the extraction solutions.
A further area of application is the production of The pectin which is precipitated by alcohol is also
clear lemon juice. After finishers have reduced recovered by means of decanters. A detailed pro-
the solids content, centrifuges are used for cess technology description is found in the separate
pre-clarifying the lemon juice. Enzymes are brochure Extraction.
then added to the juice and the subsequent
precipitation ensures that the juice is capable of Citrus peel also contains substances which are rich
being clarified. High-performance clarifiers are in carbohydrates. After appropriate pretreatment,
used for the process of fine clarification. The the peel can be conveyed to a fermenter for alcohol
pure lemon juices which are obtained are mostly production. Clarifiers are again used for clarifying
processed into concentrates. the fermentation broth.
In addition, so-called cloudy peel products are also This paper illustrates the wide range of application
obtained as a by-product during the processing possibilities for separators, clarifiers and decanters
of citrus fruits. These products are made from in the processing of citrus fruit.
the peel. After the peel has been disintegrated
and extracted, decanters remove the solids from In view of the company’s many decades of
the liquid. Once the solids have been reduced experience in this complex field and in view of
in the liquid, centrifuges are used for polishing the company’s advanced centrifugal separation
the liquid. technology, GEA Westfalia Separator can be
regarded as your competent partner in the citrus
The beverage industry uses this liquid as a basic processing industry.
material. The peel of citrus fruits contains valuable
essential oil. During juice extraction, an emulsion
is produced as a result of squeezing or pricking
and simultaneous washing. Clear and valuable
essential oil can be obtained with minimum losses
by means of a 2-stage centrifuge system.
38
GEA Westfalia Separator
7. Bibliography
1 AIJN-Code of Practice for evaluating the quality 12 Hendrickson, R. / Braddock R. J.: Technical
of fruit and vegetable juices, edited by Bulletin 749, University of Florida, Gainsville, 1971.
AIJN (Association of the Industry of Juices and 13 Kersterson, J. W.: Florida Citrus Oils.
Nectars from Fruits and Vegetables of the 14 Kimball, D. A.: Citrus Processing:
European Economic Community), Avenue de Quality Control and Technology,
Roodebeck 30, B-1030 Brüssel, November 1996. AVI Book of Van Nostrond Reinhold.
2 Bartholome, Prof. Dr. E.: Ullmans Enzyklopädie 15 Nagy, S.: Citrus Science and Technology.
der technischen Chemie. 16 Novo-Ferment, Firmen-Information 4013
3 Biekert, Prof. Dr. E.: Band 19, S. 237 ff. (Switzerland) Ud.
4 Chen, C. / Nagy, S. / Shaw, Ph. E.: Fruit Juice 17 Pecoroni, S.: Citrus Oil Recovery – Using Modern
Processing Technology, AG Science, „State of the Art“ Centrifuge Technology as Part of
Inc. Auburndale, 1993. Economical Citrus Processing, Citrus Engineers
5 Citrosuco Paulista S.A., Firmen-Information, Conference 2006.
Matao, Brasilien, The AVI Publishing Comp. lnc., 18 Pecoroni, S.: New and Improved Technique for the
1977, S. 12. Deoiling of Not From Concentrate (nfc) Juice,
6 Cohn, R.: Über die vielfältigen Wege der Proceedings IFU Congress 2003 Moscow, IFU Paris.
Citrusverarbeitung, Confructa-Studie 11, 19 Rabobank International, The World Fruit Juice
Verlag „Flüssiges Obst“, Schönborn 1985, S. 178. Market, Market Study, October 2007.
7 FAO-Database 20 Röhm GmbH, Firmen-Information, Darmstadt.
8 Gierschner, K. / Pecoroni, Dr. S.: Trübe Frucht- 21 Schobinger, U.: Frucht- und Gemüsesäfte:
säfte und fruchtsafthaltige Getränke, Technologie, Chemie, Mikrobiologie, Analytik,
Getränkeindustrie 10, 1993, S. 788-748. Bedeutung, Recht, Verlag E. Ulmer, 2001.
9 Günnewig, W. / Pecoroni, Dr. S.: Citrus Technology – 22 Shaw, Ph. E. / Velthuis, M. K.: Volume 1 + 2.
Improved Quality and Economics Through the Use 23 Verband der deutschen Fruchtsaft-Industrie e.V.
of High Performance Centrifuges, Fruit Processing 2, (VdF), Bonn / Canadean Ltd., London u. a., 2008.
2001, S. 46-48.
10 Hellmann, Prof. Dr. E.
11 Hemfort, H.: Separatoren, Zentrifugen für
Klärung, Trennung, Extraktion, Technisch-
wissenschaftliche Dokumentation Nr.1, 1983,
Westfalia Separator AG.
39
GEA Westfalia Separator
We live our values.
Excellence • Passion • Integrity • Responsibility • GEA-versity
GEA Group is a global engineering company with multi-billion euro sales and operations in more than
50 countries. Founded in 1881, the company is one of the largest providers of innovative equipment and
process technology. GEA Group is listed in the STOXX® Europe 600 Index.
Westfalia, Westfalia Separator, varipond, hydry, and hyvol are registered trademarks of GEA Westfalia Separator GmbH.
GEA Mechanical Equipment US, Inc.
GEA Westfalia Separator Division
Headquarters: West Coast:
100 Fairway Court Western Region Customer Support Center
Northvale, NJ 07647 555 Baldwin Road
201-767-3900 Patterson, CA 95363
209-895-6300
Midwest:
725 Tollgate Road, Suite B
Elgin, IL 60123 GEA Mechanical Equipment Canada, Inc.
630-503-4700
GEA Westfalia Separator Canada Division
South:
4725 Lakeland Commerce Parkway, Suite 4 835 Harrington Court
Lakeland, FL 33805 Burlington, ON L7N 3P3
863-603-8900 289-288-5500
Southwest:
2408 Timberloch Place, Suite C-4 Toll-Free: 800-722-6622
The Woodlands, TX 77380 24-Hour Technical Help: 800-509-9299
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281-465-7900 www.wsus.com