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Using a specially constructed and instrumented machine, the friction welding character-
istics of four thermoplastics: nylon 66, acetal, polymethylmethacrylate and polyvinyl
chloride (PVC) were investigated. It was found that during the frictioning stage the inter-
facial torque and burn-off rate are both constant, but dependent on the axial pressure and
rubbing velocity. The rate of heat generation was found to be greatest in nylon 66 and
least in PVC and this is discussed in terms of the thermal properties and coefficients of
friction of each material. It was found that the conditions required to produce good
welds in each of the four thermoplastics are quite critical.
Actuator
Tacho - Generator
Bearing T~ f H----H
Housing Arm Plan View
*Acetal homopolymer was supplied by Polypenco Ltd, Gate House, Welwyn Garden City, Hertfordshire, UK.
~fNylon 66 was supplied by Polypenco Ltd, Gate House, Welwyn Garden City, Hertfordshire, UK.
SExtruded PMMA was supplied by Richard Daleman Ltd, 325 Latimer Road, London, UK.
82Grey PVC was supplied by Plastics Constructions Ltd, Seeleys Road, Birmingham, UK.
3276
was a steady decrease in the length of the test sam-
~ ~ cylinder ples (Section AB on Fig. 3). In the subsequent
analysis the slope of AB, i.e. the burn-off rate, was
studied as a function of the process variables.
~ P r e s s u re gauge After a pre-set time the welding process was
stopped by either switching off the motor or
allowing the stationary chuck to slip off the
Two pos,t on/'
three port- valve \ ]'t[/J \~'tJ Two position torque arm. This latter effect was studied because
normally closed t:3
r'-'~,L.L_L~
tl t ~ five port valve it was felt that simply switching off the motor
would result in weld shearing which could have
Boost pressure L___
i[ deleterious effects on weld strength particularly in
~eguloto,-~r---F-~]
r ~---1 cases where the material solidifies rapidly (e.g.
semicrystalline plastics). When the stationary
chuck slipped off the torque arm, the shear stresses
L
at weld interface immediately dropped to zero and
pressure a boost, or forging, pressure could be applied.
eSso~r regulator
Welding This caused a further axial shortening of the sam-
Compr ples as the softened material at the interface was
forced out as flash.
Figure 2 Pneumatic circuit for friction welding rig.
In order to analyse the results, the mean
rubbing velocity, Vm, was calculated from
came into contact there was a slight drop in motor V m : COs (1)
speed which had to be allowed for in the initial
speed setting. During the welding process the where ~ is the angular velocity and rm is the mean
speed was perfectly constant. As the axial pressure radius. This velocity is approximately equal to the
quickly increased to its pre-set value, there was a average point velocity [2] and was used because of
proportionate increase in the resisting torque at the simple form of the expression in Equation 1.
the interface. During welding the torque remained Fig. 4 shows how the torque at the weld inter-
constant although there was generally a slight fall face between PMMA samples, varied when the
off of axial pressure, as shown in Fig. 3. The burn- average rubbing velocity was changed. The axial
off transducer showed that when the samples first pressure in each case was constant at 6.2 MPa and,
came into contact, and during the period that the as would be expected, the torque is less at the
axial pressure was building up, there was very higher rubbing velocities. However, the effect is
little shortening of the samples. However, once the not as large as one might expect. A six-fold increase
axial pressure reached its maximum value there in rubbing velocity, with the proportional increase
..._ . . . .
Burn - off B f
Speed
Axial pressure
/
I
L
Torque
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0'8 0'8
I
I
0'6__ Axial pressure : 6.2MPc 0'6
0'4 o- 0'4
z
cr 0 ' 3 _ _ 0.3
0'2 0.2
0.1 F I 0.1
0 0'4 0 '8 1'2 1.6 2'0 2"4 0'4 0'8 1-2 1'6 2-0 2"4
rubbing v e l o c i t y (rnsec-1) rubbing velocity (msec-1)
Figure 4 Variation of torque with rubbing velocity for Figure 5 Variation of torque with rubbing velocity for a
PMMA. range of thermoplastics.
in frictional heating, only caused a decrease in weld temperature whereas the nylon 66 samples
resisting torque from 0.32 to 0.22 Nm. Although attained the highest weld temperature (over twice
the rate of heat generation in the material is the value for PVC under the same welding con-
related to the product of angular velocity and ditions). The temperature rise in each of the
torque [14], it may be seen that for a fixed value materials will depend on their thermal properties
of axial pressure, the heat build up is almost and also on the coefficient of friction, which will
directly proportional to the rubbing velocity. be considered later. Of the four materials, nylon 66
Fig. 5 compares, for a range of rubbing veloci- has the highest coefficient of thermal conductivity
ties, the torque variations in the four thermo- and specific heat capacity, (0.43 Wm -1 K -1 and
plastics investigated. To avoid unnecessary com- 1.68kJkg -1 K - ' , respectively) and PVC has the
plexity on the diagram, the experimental points lowest values of these properties (0.16 W m -1 K -1
have been omitted. For nylon 66, acetal and PVC and 0.93 kJ kg -~ K -1 , respectively).
the reductions in torque are greater then those Fig. 6 illustrates how the torque at the weld
observed in PMMA. The effect is most pronounced interface in PMMA varies with axial pressure.
for nylon 66 although it is interesting to note that There are two distinct sections to the character-
for PVC the torque is essentially independent of istic. For axial pressures up to about 3 MPa the
rubbing velocity for speeds greater than torque increases rapidly, in a linear fashion, as the
0.8 m sec -~. Fig. 5 also illustrates that, of the four axial pressure is increased. For axial pressures in
materials, nylon 66 has the greatest rate of heat the region of 3 to 4 MPa there is a transition and
generation whereas PVC is the worst in this beyond 4MPa, although the torque increases
respect. In a series of tests to determine the tem- linearly with pressure, the rate of increase is only
perature rise at the weld interface this trend was about one-tenth of that experienced at low pres-
confirmed. A non-contacting infra-red radiation sures. This same type of behaviour was observed at
thermometer was directed at the weld zone two rubbing speeds in PMMA and, as shown in
during the frictioning period and although there Fig. 7, the other three thermoplastics also dis-
may have been some error in the measurement of played similar characterisitcs. Once again nylon 66
the absolute value of temperature, in relative exhibited the greatest rate of heat generation and
terms the PVC samples exhibited the lowest PVC exhibited the lowest rate.
3278
0'40 TABLE I Derived coefficients of friction during weld-
ing using a rubbing velocity of 1.21 m sec-1
0.35 Material PVC PMMA Acetal Nylon 66
Pressure = 1MPa 0.21 0.16 0.21 0.28
0'30 - - Rubbing velocity = 1"21msec-1 Pressure = 10MPa 0.04 0.065 0 . 0 7 2 0.086
E
z
v 0,25 This was done using a simple inclined plane
(u O- I --
o- apparatus. The value of/~ was calculated by noting
? --~---r--- ___
2 0.20
0,15
/// \
- - R u b b i n g velocity = 2msec-1-
the angle of tilt necessary to cause each material to
slide on a surface of the same material. A range of
normal loads was used for each material and the
following results were obtained.
0.10 / Material PVC PMMA Acetal Nylon66
Coefficient of 0.35 0.41 0.52 0.76
0,05 friction,/1
It will be noted that these values increase in the
6 8 10 12
same order as the observed rate of heat generation
axial pressure (MPo)
during friction welding. However, the coefficients
Figure 6 Variation o f torque with axial pressure for of friction will be dependent on temperature and
PMMA. will change, therefore, during the welding process.
No information could be found on the tempera-
As mentioned earlier, the coefficient of friction, ture dependence of/~, so, in order to get some idea
/J, of each of the materials has a considerable effect of the variation involved, the ratio of the torque to
on the rate of heat generation during friction the applied pressure was studied for a range of
welding. As the values of # were not readily avail- welding conditions. By including a factor to allow
able for the materials being investigated, it was for the cross-sectional area of the test-pieces and
necessary to determine the values in each case.- the average radius it was possible to estimate a
value for the coefficient of friction during welding.
0'4C From Figs 5 and 7 the values in Tables I and II
may be derived.
0.35 f - ~ ' ~ " ' ~ y Ion 6 , ' ~ " " For all materials, therefore, the derived values
for the coefficient of friction show a significant
decrease with temperature. However, it should be
remembered that the values in Tables I and II are
"~ 0.2!
z ///~_-.--f
not true coefficients of friction because as the
materials heat up a viscous film is formed at the
interface. The values in the tables are, therefore,
13" o.2c probably more akin to a coefficient of shear
viscosity.
0.15 , ~ During welding the viscous film which forms is
generally squeezed out from the weld interface
due to the application of the axial pressure. The
0.10
material squeezed out forms a weld bead, the
extent of which depends on--the welding para-
0-05 Rubbing Velocity= 1-21msee-~ - -
TABLE II Derived coefficients of friction during weld-
ing using an axial pressure of 6.2 Mpa
0 2 4 6 8 10 12
Material PVC PMMA Acetal N yl on 66
Axial pressure (MPa)
V e l oc i t y = 0 . 2 m s e c -~ 0.085 0.12 0.14 0.22
Figure 7 V a r i a t i o n
of t o r q u e with axial ptessttre for
V e l oc i t y = 2 m s e c -~ 0.063 0.084 0.08 0.12
several thermoplastics.
3279
3'0 3,0
/
2,5 Axiol pressure = 6.2MPo IU 2,5 PVC /
A
It#
E
E
/ Nylon 66
/
r
E
2,C 2'0
E
{b o
O
C ~."" A'~cAcetoI
1"5 1,5
~6 rn
i
c
D
m 1.C
/ 1'0 /
o
0 0"4 0"8 1"2 1-G
Rubbing
II
2.0 2'4
velocity (m sec-~)
o/ 0 0'4
I
0'8 1"2
Rubbing
1'6 2"0
velocity (msec -t)
2.4
meters (i.e. rubbing speed and axial pressure). cess of having to reform the film may explain
During the friction welding of the four thermo- partially why the overall burn-off rate is relatively
plastics considered it was found that the rate of slow.
axial shortening (bum-off), which is associated When the rubbing velocity was kept constant
with bead formation, was constant for any parti- and the axial pressure was varied it was found that,
cular set of welding conditions. However, the rate for PMMA, the burn-off rate increased relatively
changed as the welding variables were altered. quickly for pressures up to 2MPa (Fig. 10). For
Fig. 8 shows how the bum-off rate for PMMA pressures in excess of 4MPa the burn-off rate
varied for rubbing velocities up to 2 m sec-1. In increased linearly once again but the relative
Fig. 9, where the experimental points have been increase, for each increment of axial pressure, was
omitted for clarity, the burn-off rates for the four much less. Fig. 11 shows that for each of the other
materials may be compared. As would be expected, thermoplastics the same general shape of character-
in all cases the rate of axial shortening increases as istic was observed, with PVC once again exhibiting
the rubbing velocity (and hence the heat gener- the highest burn-off rate under all welding
ation rate) increases. However, it is apparent that conditions.
some complex interaction of material properties Although the primary objective of the present
must influence the amount of burn-off because study was to investigate the inter-relationships
PVC, which heats up more slowly than the other between the main welding variables, clearly the
materials and is generally regarded as having a high long-term aim would be to optimize the weld
melt viscosity, does in fact exhibit a much greater strength in terms of these variables. This aspect of
burn-off rate than any of the other materials. One the work is continuing. Tensile tests on t h e
possible explanation for this is that the PVC weld samples welded in this initial programme showed
bead forms uniformly whereas with the other that the weld strengths obtained in all four
materials the low viscosity film is formed quickly thermoplastics were relatively low. For the range
at the interface but is then immediately squeezed of welding variables considered in Figs 4 to 11, the
out so that two relatively cooler surfaces come best tensile strength which could be achieved in
together and must generate more frictional heat to the welds was about 50% of the strength of the
form a new viscous film. Therefore although the parent materials, even with the weld beads
viscous film is formed quickly the continual pro- removed.
3280
3,2 , 3"2
2~ / 2"4~
j-
E
Rubbing velocity = 2msec-1/
o 1'6 ,.,~~,"~:~
c
3
m 1.2 ~ o ~ c 1.2
m
0.4 0'4
0
0 2 4 6 8 10
I 12
0
o 2 6 8 10 12
Axiol pressure (MPo) Axial pressure (MPa)
Figure 10 Variation of burn-off rate with axial pressure Figure 11 Variation of burn-off rate with axial pressure
for PMMA. for several thermoplastics.
In recent years there has been some research through molecular chain entanglement, is squeezed
interest in butt-fusion welding of plastics. Since out of the weld area and causes high transverse
the principles of the two processes are similar, it orientation in the weld.
could well be that some of the information which Although there was no mechanism on the
has been accumulated in this field may be of use in friction welding machine for controlling the melt
optimizing the strength of friction welded joints. displacement independently of the other pro-
The first interesting point is that, in agreement cessing variables it was decided that it might be
with the results obtained in this investigation, possible to reproduce some of the optimum con-
Barber and Atkinson [15] found that the optimum ditions suggested for butt-welding. Therefore, a
conditions for welding are very critical. In com- few explanatory trials were conducted on PMMA.
mon with other workers [16, 17] they found that In order to keep the temperature high and the
long heating times are better than short. De Courcy heating period as long as possible, combinations of
and Atkinson [16] reported that with a range of low axial pressures (0.5-+ 2MPa) and relatively
different grades of polyethylene it was more harm- high rubbing velocities (1.8 -~ 2 m s e c -1) were
ful to have the weld temperature below the opti- explored. It was found that under these conditions
mum than above it. Their results suggested that the weld strength was in fact improved.
weld strength was not very sensitive to axial Using a rubbing velocity of 2msec -1 and an
pressures in the range 0.1 to 0.6MPa although axial pressure of 0.TMPa, the weld strength in
low pressure (< 0.1 MPa) was detrimental. Buck- PMMA was found to be 80% of the strength of the
nall etal. [17] have summarized most of the early unwelded material. Using a boost (or forging)
findings by reporting that during butt-welding, the pressure of 2 MPa after the frictioning stage it was
weld strength depends on the temperature at the found that the weld strength was improved to
interface, the duration of the heating period and 87%. In each case it was found that the weld
the extent of the melt displacement during weld- strength was much better when the stationary
ing. They also make the point that low pressures chuck was allowed to slip off the torque arm
produce poor welds but add that high pressures (thereby avoiding any shearing of the bond when
are equally undesirable. This is because the viscous the motor was switched off). Also, in order to
film, which offers the potential of a good weld reduce the notch effect caused by the weld bead
3281
[15], the latter was always removed prior to combination of low axial pressures, high rubbing
testing. velocities and a final boost pressure gave a weld
It is considered that the weld strength in each factor of 0.87.
of the plastics can be improved in the same way
and the next phase of the work will be to deter- References
mine optimum welding conditions and joint 1. J. O'RINDA TRAUERNICHT, Plastics Technology
designs for each of the materials. 16 (1970) 43.
2. J.A. NEUMANN and F. J. BOCKHOFF, "Welding
of Plastics", (Reinhold Publishing Co., New York,
Conclusions 1959).
From this series of friction welding trials on nylon 3. R.M. STEMMLER, Plastics Technology 9 (1963)
66, acetal, polymethylmethacrylate (PMMA) and 42.
polyvinyl chloride (PVC), the following con- 4. Anon, Technical Service Note K105, "Welding and
clusions may be drawn. Jointing Kematal", Amcel Ltd., Wafford, England
(1974).
(1) The resisting torque, between the fixed and 5. E. D. NICHOLAS, "Friction Welding Plastics",
rotating samples to be welded, remains essentially Welding lnst. Res. Bull. 17 (1976) 211.
constant throughout the frictioning stage. 6. A.J. CHENEY and W. E. EBELING, SPE J. March
(2) The values of the resisting torque increase (1958) 31.
as the axial pressure and the rubbing velocity 7. S.J. KAMINSKY and J.A. WILLIAMS, "Welding
and Fabricating of Thermoplastics", (Kamweld
increase. Products Co., Norwood, 1964).
(3) The rate of heat generation was greatest in 8. H. R. STILTON, in "Fabricating Plastics" edited by
nylon 66 followed by acetal, PMMA and PVC in J. D. Beadle, (MacMillan, London, 1972) Ch. 4.
descending order. 9. E.E. SPROW,Machine Design 27 (1972) 72.
(4)The rate at which the plastic samples 10. J.N. MATHER, Eng. Mater. Design 23 (1979) 45.
11. H. POTENTE, Industr. Prod. Eng. 3 (1980) 67.
become shorter during friction welding remains 12. S. NAKAHARA, Y. AOYAGI, M. YANO and K.
constant during the frictioning stage. NAKAMURA, J. Mech. Eng. Lab. 28 (1974) 224.
(5) The burn-off rate increases as the axial pres- 13. S. NOCKEL, ZISMitteilungen 16 (1974) 1264.
sure and rubbing velocity increase. 14. T. RICH and R. ROBERTS, MeL Construct. Brit.
(6)The burn-off rate was greatest in PVC WeldingJ. 50 (1971) 93.
15. P. BARBER and J. R. ATKINSON, J. Mater. ScL
followed by nylon66, PMMA and acetal in 9 (1974) 1546.
descending order. 16. D.R. DE COURCY and J. R. ATKINSON, ibid. 12
(7) It was found that satisfactory welds in these (1977) 1535.
four thermoplastics are not easy to achieve because 17. C. B. BUCKNALL, I.C. DRINKWATER and G. R.
the optimum conditions appear to be quite crucial. SMITH, Polymer Eng. Sci. 20 (1980) 432.
A set of explanatory tests on PMMA showed that a Received 13 March and accepted 29 April 1981.
3282