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AMETEK Western Research

Model 933 UV Analyzer

User Manual

TQM
Process Instruments
COMMITTED TO TOTAL QUALITY

PN 903-8549, Rev. K
Western Research
2876 Sunridge Way N.E.
Calgary, Alberta, Canada T1Y 7H9
Offices

USA – HEADQUARTERS GERMANY


150 Freeport Road Postfach 2165
Pittsburgh, PA 15238 D-40644 Meerbusch
Phone: 412-828-9040 OR
Fax: 412-826-0399 Rudolf-Diesel Strasse 16
D-40670 Meerbusch
Phone: 49-21-59-9136-0
USA – Delaware Fax: 49-21-59-9136-80
455 Corporate Boulevard
Newark, Delaware 19702
Phone: 302-456-4400 FRANCE
Fax: 302-456-4444 4 Rue Edouard Branly
78190 Trappes
Phone: 33 1 30 68 69 20
USA – Texas Fax: 33 1 30 68 69 29
9750 Whithorn Drive
Houston, Texas 77095
Phone: 281-463-2820 CHINA
Fax: 281-463-2701 Room 406, Metro Tower
No. 30 Tian Yao Qiao Road
Shanghai, 200030
CANADA Phone: 8621 6426 7049
2876 Sunridge Way N.E. Fax: 8621 6426 7054
Calgary, Alberta T1Y 7H9
Phone: 403-235-8400
Fax: 403-248-3550

© 2004 AMETEK Process & Analytical Instruments Division Printed in Canada


This manual is a guide for the use of the Model 933 UV Analyzer. Data herein has been verified and validated and is believed adequate for the
intended use of this instrument. If the instrument or procedures are used for purposes over and above the capabilities specified herein, confirmation
of their validity and suitability should be obtained; otherwise, AMETEK does not guarantee results and assumes no obligation or liability. This
publication is not a license to operate under, or a recommendation to infringe upon, any process patents.

ii | Model 933 UV Analyzer


Contents
Offices ..................................................................................................................... ii
Safety Notes ........................................................................................................... x
Electrical Safety ..................................................................................................... x
Grounding ............................................................................................................. x
Personnel and Equipment Safety Measures.................................................... xi
Warnings ......................................................................................................... xi
Cautions ......................................................................................................... xii
Warning Labels .................................................................................................. xiii
Electromagnetic Compatibility (EMC) ........................................................... xiv
EQUIPMENT USED IN HAZARDOUS LOCATIONS ................................. xv
Declaration of Conformity ............................................................................... xvi
WARRANTY AND CLAIMS ............................................................................ xvii

CHAPTER 1 OVERVIEW
Theory of the Model 933 Analyzer ................................................................. 1-1
Features ............................................................................................................... 1-2
Application .......................................................................................................... 1-3
Implementation ................................................................................................. 1-4
Microcontroller Board and Host Controller Board ............................... 1-5
Sample Conditioning ................................................................................. 1-5
Discrete Wavelengths ................................................................................. 1-5
About the Analyzer Sampling System ........................................................... 1-8
Sample Conditioning Column Operation .............................................. 1-9
Relays ................................................................................................................. 1-10
Status Relays .............................................................................................. 1-10
Alarm Relays .............................................................................................. 1-11
Solid State Relays ...................................................................................... 1-11

CHAPTER 2 SPECIFICATIONS
Methodology ............................................................................................... 2-1
Full-Scale Ranges ......................................................................................... 2-1
Standard Range Measuring Cell (40 cm or smaller) .............................. 2-1
Low Range Measuring Cell (81.2 cm) ...................................................... 2-1
Response Time (excludes sampling system) ........................................... 2-1
Measurement Accuracy .............................................................................. 2-2
Repeatability ................................................................................................ 2-2
Calibration .................................................................................................... 2-2
Linearity ....................................................................................................... 2-2
Stability ......................................................................................................... 2-2
Sensitivity ..................................................................................................... 2-2
Cross-Talk ..................................................................................................... 2-3
Temperature Drift ....................................................................................... 2-3

Contents | iii
24-Hour Zero Drift ...................................................................................... 2-3
Analog Outputs ........................................................................................... 2-3
Digital Communication .............................................................................. 2-3
Electrical Requirements ............................................................................. 2-4
Maximum Start-Up Power .................................................................... 2-4
Electrical Requirements ......................................................................... 2-4
Status Relay Contacts ............................................................................ 2-4
Typical Sample Gas Flow Rate .................................................................. 2-4
Zero Gas ........................................................................................................ 2-4
Ambient Limits ............................................................................................ 2-5
Temperature ........................................................................................... 2-5
Humidity ............................................................................................... 2-5
Maximum Altitude ................................................................................ 2-5
Sample Pressure Requirement .................................................................. 2-5
Sample Stream Requirements ................................................................... 2-6
Physical Dimensions (on backpan) .......................................................... 2-6
Options ......................................................................................................... 2-6
Approvals and Certifications .................................................................... 2-7
ATEX (CENELEC) Certificate and Analyzer Marking ................................. 2-8
CSA Certificate and Analyzer Marking ........................................................ 2-11

CHAPTER 3 INSTALLATION & START-UP


Safety Considerations ....................................................................................... 3-2
Pre-Installation Requirements ......................................................................... 3-3
Storage Prior to Installation ....................................................................... 3-3
Uncrating and Inspecting the Analyzer .................................................. 3-3
General Installation Information .............................................................. 3-4
Tools and Equipment Required ................................................................ 3-4
Installation of the Mechanical Components ................................................. 3-5
Mounting the Analyzer .............................................................................. 3-5
Location and Environment .................................................................... 3-5
Installing the Optical Bench Assembly ................................................... 3-7
Installing the Sampling System .............................................................. 3-11
Zero Gas ...................................................................................................... 3-11
Electrical Installation ....................................................................................... 3-14
Input/Output Signal Connections ......................................................... 3-15
Digital Communication ............................................................................ 3-18
Hardware Configuration ..................................................................... 3-18
Multiple-Analyzer (Multi-Drop) System Configuration .................... 3-21
AC Power Connection and Fusing ......................................................... 3-23
North American Installation ............................................................... 3-24
European Installation .......................................................................... 3-25
Installing the System 200 Configurator Software....................................... 3-27
Minimum PC Requirements for Configurator Software .................... 3-27
Configurator Software Installation ........................................................ 3-28
Removing the Configurator Software ................................................... 3-30

iv | Model 933 UV Analyzer


Start-Up and Verification ................................................................................ 3-31
Powering Up the Analyzer ...................................................................... 3-31
Establishing Communication Between the Analyzer
and Computer ........................................................................................... 3-37
Configurator Software Troubleshooting ............................................... 3-41
Analyzer Start-Up Diagnostic Checklist ............................................. 3-43
Sampling System Leak Check ....................................................................... 3-45
Operating Parameters Verification/Configuration ..................................... 3-48
Temperature Setpoints ............................................................................. 3-48
Output Ranges .......................................................................................... 3-50
Modbus/Customer Data Acquisition Port ............................................. 3-51
Sample Conditioning System Optimization ............................................... 3-52
Column Switch Time Optimization ....................................................... 3-52
Hold Time Optimization.......................................................................... 3-57

CHAPTER 4 CONTROLLER / USER INTERFACE


Configuration Software Overview – Getting Started .................................. 4-3
Starting the Configurator Software ......................................................... 4-3
Closing the Configurator Software .......................................................... 4-5
General Tab .................................................................................................. 4-6
PC Communication Setup ..................................................................... 4-8
Device Communication Tab .................................................................... 4-10
User Interface............................................................................................. 4-11
Setting Up Your Screen ............................................................................ 4-12
View / Configure Analyzer Parameters and Data ................................ 4-12
Viewing Device Activities ........................................................................ 4-13
Saving Analyzer Configuration Parameters ......................................... 4-14
Restoring Analyzer Configuration Parameters .................................... 4-15
Modifying Analyzer Device Settings ............................................................ 4-16
Working From the Setup Tab ................................................................... 4-16
Saving Analyzer Configuration Parameters to an ASCII File ............. 4-18
Printing Analyzer Configuration Parameters ..................................... 4-18
Refreshing Configuration Parameters .................................................. 4-19
Saving Configuration Parameters to EEPROM .................................. 4-19
Setting Gas Calibration Parameters ..................................................... 4-20
Modbus Settings .................................................................................. 4-23
Temperature Control ............................................................................ 4-24
Optical Bench ................................................................................ 4-25
Measuring Cell ............................................................................. 4-26
Column Block ................................................................................ 4-26
Output Setup ....................................................................................... 4-27
Analyzer Information .......................................................................... 4-30
Optical Bench ...................................................................................... 4-31
Matrix ................................................................................................. 4-34
Column Timing ................................................................................... 4-35

Contents | v
Compensation Parameters .................................................................... 4-36
Advanced Options ............................................................................... 4-38
Custom Output (Custom Setup) ......................................................... 4-39
Status Tab .................................................................................................... 4-40
Optical Bench Data Tab ............................................................................ 4-42
Analyzer Data Tab ..................................................................................... 4-43
Scanning Data .................................................................................................. 4-45
Display Modes ........................................................................................... 4-45
Defining Scan Settings ............................................................................. 4-46
Starting a Scan ........................................................................................... 4-47
Stopping a Scan ......................................................................................... 4-47
Scheduling Scans ...................................................................................... 4-48
Working with Data Files ................................................................................. 4-49
Saving Data Files ....................................................................................... 4-49
Opening Data Files ................................................................................... 4-50
Scrolling Through Data Records ............................................................ 4-50
Converting Data Files ............................................................................... 4-51
Printing Data .............................................................................................. 4-51

CHAPTER 5 CALIBRATION
Manual Span Gas Calibration .......................................................................... 5-1
Analog Output Calibration .............................................................................. 5-4
Current Calibration .................................................................................... 5-4
Voltage Calibration ..................................................................................... 5-6

CHAPTER 6 MAINTENANCE & TROUBLESHOOTING


Safety Considerations ....................................................................................... 6-1
Maintenance ....................................................................................................... 6-2
Preventive Maintenance Schedule ........................................................... 6-2
Before Performing Maintenance .............................................................. 6-4
Locating a Plug in the Sampling System ............................................... 6-4
Detecting Plugs in the Sampling System .............................................. 6-4
Preventing Plugs in the Sampling System ............................................ 6-5
Changing Out Replaceable Parts .............................................................. 6-7
Measuring Cell Preventive Maintenance .............................................. 6-8
Disassembling and Cleaning the Measuring Cell ........................... 6-8
Replacing Parts and Resassembling the Measuring Cell ............... 6-14
Column Block Preventive Maintenance ............................................... 6-16
Removing and Replacing Parts in the Column Block .................... 6-17
Reassembling the Column Block and Inspecting Flow
Restrictors ..................................................................................... 6-20
Source Lamp Replacement ................................................................... 6-21
When Do Source Lamps Need to be Replaced? .............................. 6-21
About the Source Lamps ............................................................... 6-22
Replacing the Source Lamps ......................................................... 6-22

vi | Model 933 UV Analyzer


Auto-Setup .......................................................................................... 6-27
When is an Auto-Setup Required? ................................................ 6-27
When is an Auto-Setup Not Required .......................................... 6-27
PMT Level and PMT Balance ............................................................. 6-28
Auto-Setup Fault Message and Corrective Action ........................ 6-29
The Auto-Setup Sequence ............................................................. 6-29
Cancel Auto-Setup ........................................................................ 6-30
Manipulating the PMT Level and PMT Balance .......................... 6-31
Source Lamp Alignment ............................................................... 6-33
EEPROM Replacement ....................................................................... 6-35
Examining and Caring For the Flamepaths ......................................... 6-38
Upper/Lower Electronics Enclosure Flamepaths
(Mating Surfaces) ......................................................................... 6-38
Diagnostics and Troubleshooting .................................................................. 6-40
Host Controller Board Error Conditions and Corrective Action ...... 6-42
Microcontroller Board Error Conditions and Corrective Action ....... 6-51
Analyzer Reset ........................................................................................... 6-59

CHAPTER 7 SERVICE & PARTS


Technical Support .............................................................................................. 7-1
Returning Equipment ....................................................................................... 7-2
Recommended Spare Parts .............................................................................. 7-4
Optical Bench/Sampling System Spare Parts ......................................... 7-4
Spare Analyzer Fuses.................................................................................. 7-5
Printed Wiring Board Re-Ordering Part Numbers ............................... 7-6

APPENDIX A ADVANCED SOFTWARE OPERATION


Assigning Inputs to Channels for Display Modes ...................................... A-2
Modes of Operation ......................................................................................... A-3
Meter Mode ................................................................................................. A-3
Annunciator Mode ..................................................................................... A-5
Trend Mode ................................................................................................. A-7
Tabular Mode .............................................................................................. A-8
Custom Modes............................................................................................ A-9
Moving or Resizing a Window in Custom Mode ............................... A-10
Adding a Display Window in Custom Mode ...................................... A-10
Deleting a Window in Custom Mode ................................................. A-10
Saving Custom Mode Files ................................................................. A-11
Opening Custom Mode Files .............................................................. A-11
Adding Custom Mode Files to the Mode Menu .................................. A-11
Saving Tabular Mode Files ............................................................................ A-12
About Dynamic Data Exchange (DDE) ................................................ A-13
Copying Magnitudes .......................................................................... A-13
Copying Channels .............................................................................. A-13
Setting Up the Display ................................................................................... A-14
Setting Alarms ................................................................................................. A-17

Contents | vii
APPENDIX B OPTIONS
Natural Gas Filter (Field Upgradeable) – Filterblock .................................. B-1
Filtration Stages .......................................................................................... B-2
Vent Flow ..................................................................................................... B-3
Natural Gas Filter Maintenance .............................................................. B-4
Replacing O-rings and Flow Restrictors in the Filterblock ................... B-4
Reinstalling Fittings and Replacing the Coalescing
Cartridge and Membrane Filters .......................................................... B-6
Filterblock Assembly Spare Parts ............................................................. B-8
Environmental Purge Option (Field Upgradeable) .................................... B-9
Connection and Use .................................................................................. B-9
Pressure Compensation Option (Field Upgradeable) .............................. B-11
Setting Up the Pressure Compensation Option ................................. B-11
Using the Pressure Compensation Option .......................................... B-12
Diagnostics Feature ............................................................................ B-12
Loop-Powered Current Outputs (Field Upgradeable) ............................. B-13
Using the Loop-Powered Current Option ........................................... B-13
Low Range (White Cell) Measuring Cell (Field Upgradeable) ............... B-14
Calibrated Carbonyl Sulfide Output (Factory Upgradeable Only) ........ B-15
Using a Calibrated Carbonyl Sulfide Output ...................................... B-15
Calibrated Methyl Mercaptan Output (Factory Upgradeable Only) ..... B-16
Using a Calibrated Methyl Mercaptan Output ................................... B-16

APPENDIX C MODBUS COMMUNICATION INTERFACE


Overview ........................................................................................................... C-1
Modbus Interface Parameters ......................................................................... C-2
Modbus Address ........................................................................................ C-2
Communication Parameters ..................................................................... C-2
Modbus Functions ............................................................................................ C-3
Exception Code ................................................................................................. C-4
Digital Output Status ....................................................................................... C-4
Digital Input Status .......................................................................................... C-6
Holding Registers ............................................................................................. C-6
ID/Status Information .................................................................................... C-12

APPENDIX D DRAWINGS
Backpan Dimensions ........................................................................................D-2
Upper Enclosure ...............................................................................................D-3
Lower Enclosure ...............................................................................................D-4
Backpan Component Layout (North America) ...........................................D-5
Backpan Component Layout (Europe) .........................................................D-6
Column Block Assembly ..................................................................................D-7
AC Distribution PWB (P/N 100-1771) ............................................................D-8
Customer I/O Board (P/N 100-1758) ..............................................................D-9
Host Controller Board (P/N 100-1757) .........................................................D-10
Microcontroller Board (P/N 100-1781) .........................................................D-11
Micro-Interface Board (P/N 100-1759) .........................................................D-12

viii | Model 933 UV Analyzer


Optical Bench Service Electronics Board (P/N 100-1662) .........................D-13
Customer Connections Wiring Schematic (North America) ...................D-14
Customer Connections Wiring Schematic (Europe) .................................D-15
Conduit Entries and AC Power Connection Locations
(North America) ..............................................................................................D-16
Conduit Entries and AC Power Connection Locations
(Europe) ............................................................................................................D-17
RS-232 Cable Communications Connections .............................................D-18
Analyzer Wiring Diagram .............................................................................D-19
Natural Gas Filterblock Assembly – Optional (P/N 100-1782) .................D-20
Solenoid Block (North America) ..................................................................D-21
Solenoid Block (Europe) ................................................................................D-22
Standard Range Measuring Cell (100-1811) ...............................................D-23
Low Range (White) Measuring Cell (100-1780) .........................................D-24
Inlet and Vent Flame Arrestor Locations for Environmental
Purge Option ...................................................................................................D-25
PMT Buffer Board P/N 100-0140...................................................................D-26
Optical Bench Assembly ................................................................................D-27

APPENDIX E CONVERSION FACTORS AND CALCULATIONS


Conversion Factors ........................................................................................... E-1
Prefixes ............................................................................................................... E-4

Contents | ix
Safety Notes
WARNINGS, CAUTIONS, and NOTES contained in this manual emphasize critical instructions
as follows:

An operating procedure which, if not strictly observed, may result in personal injury or
! environmental contamination.
WARNING

An operating procedure which, if not strictly observed, may result in damage to the equipment.
!
CAUTION

Important information that should not be overlooked.



NOTE

Electrical Safety
High voltages are present in the analyzer housings. Always shut down power source(s) before
performing maintenance or troubleshooting. Only a qualified electrician should make electrical
connections and ground checks.

Any use of the equipment in a manner not specified by the manufacturer may impair the safety
protection originally provided by the equipment.

Grounding
Instrument grounding is mandatory. Performance specifications and safety protection are void if
instrument is operated from an improperly grounded power source.

Verify ground continuity of all equipment before applying power.


!
WARNING

x | Model 933 UV Analyzer


Personnel and Equipment Safety Measures
This section describes important safety information to avoid personal injury and damage to the
equipment while installing, operating, maintaining, or servicing the equipment. All safety
regulations, standards, and procedures at the analyzer location must be followed.

All personnel involved with the installation, start-up, operation, maintenance, service, or trou-
bleshooting of the Model 933 Analyzer must review and follow these Warnings and Cautions.

Warnings
Review and follow these Warnings to avoid personal injury or environmental contamination.

Always disconnect main AC power and/or alternate power sources (if used, i.e., for relay
! contacts) to the analyzer before removing any sampling system assemblies and components
WARNING from the analyzer, or before opening any covers on the analyzer.

If it is necessary to open the Upper/Lower Enclosures while the circuits are alive, test the area
for hazardous gases and proceed only when it is found to be safe. When the EEx d Electronics
Enclosures are open, take appropriate precautions to avoid electrical shock. Hazardous voltages
are present inside.

Any electrical connections, adjustments, or servicing of the analyzer should be performed only
! by properly trained and qualified personnel.
WARNING
All electrical connections, materials, and methods (plus all safety policies and procedures) must
be made in compliance with local wiring regulations and electrical code for the hazardous area,
and be approved by the Owner Company.

Before working on the sampling system, confirm that the system is purged with zero gas and is
! isolated (blocked in) from the process.
WARNING

Because ultraviolet radiation can harm your eyes, avoid direct viewing of the light emanating
! through the end window of the source lamp. If the source lamp must be viewed while energized,
WARNING wear safety glasses that absorb ultraviolet radiation.

If the analyzer uses the optional Measuring Cell heater, take precautions to avoid burning
! yourself; the Measuring Cell and Heater Assembly are hot.
WARNING

Contents | xi
Cautions
Review and follow these Cautions to avoid damaging the equipment.

The electronic circuit boards and other static-sensitive components should be stored and
! transported in static-shielding carriers or packages.
CAUTION

For electrical-shock protection, the analyzer must be operated from a grounded power source
! that has a securely connected protective-ground contact.
CAUTION

If it becomes necessary to handle any of the electronic circuit boards, do not subject the boards
! to static discharge. The ideal solution is a static-safe work area. Since such areas typically are
CAUTION
not available at field installation sites, the use of a wrist strap connected directly to a ground is
recommended. If a wrist strap is not available, you should at the very least touch the metal
chassis (to ground yourself) before handling or touching the boards.

When handling the source lamps, it is very important not to touch the lamp windows because
! residual oils from the fingers will absorb ultraviolet light. The window is the flat surface at the
CAUTION end of the narrow glass tube. The lamp assembly is fragile and should be handled with care.

Do not exceed the maximum working pressure rating of the sampling system – 21 000 KPAG
! (3000 PSIG) without optional Filterblock Assembly – under any circumstances.
CAUTION
For analyzers using the optional Filterblock Assembly, do not exceed the maximum working
pressure rating of the sampling system – 14 000 KPAG (2000 PSIG) with optional Filterblock
Assembly – under any circumstances.

If the Model 933 Analyzer is equipped with the Environmental Purge option, clean air or
! nitrogen can be supplied to the inlet flame arrester at a pressure of 7–70 KPAG (1–10 PSIG).
CAUTION

xii | Model 933 UV Analyzer


Warning Labels
These symbols may appear on the instrument in order to alert you of existing conditions.

PROTECTIVE CONDUCTOR TERMINAL

(BORNIER DE L’ECRAN DE PROTECTION)

Schutzerde

CAUTION – Risk of electric shock

(ATTENTION – RISQUE DE DÉCHARGE ÉLECTRIQUE)

Achtung – Hochspannung Lebensgefahr

CAUTION – (Refer to accompanying documents)

(ATTENTION – SE RÉFERER AUX DOCUMENTS JOINTS)

Achtung (Beachten Sie beiliegende Dokumente)

CAUTION – Hot Surface

(ATTENTION – SURFACE CHAUDE)

Achtung – Heiße Oberfläche

Contents | xiii
Electromagnetic Compatibility (EMC)

Read and follow the recommendations in this section to avoid performance variations or
! damage to the internal circuits of this equipment when installed in harsh electrical environ-
CAUTION ments.

The various configurations of the Model 933 Analyzer should not produce, or fall victim to,
electromagnetic disturbances as specified in the European Union’s EMC Directive. Strict compli-
ance to the EMC Directive requires that certain installation techniques and wiring practices are
used to prevent or minimize erratic behavior of the Analyzer or its electronic neighbors. Below
are examples of the techniques and wiring practices to be followed.

In meeting the EMC requirements, the various Analyzer configurations described in this manual
rely heavily on the use of metallic shielded cables used to connect to the customer’s equipment
and power. Foil and braid shielded I/O and DC power cables are recommended for use in other-
wise unprotected situations. In addition, hard conduit, flexible conduit, and armor around non-
shielded wiring also provides excellent control of radio frequency disturbances. However, use of
these shielding techniques is effective only when the shielding element is connected to the
equipment chassis/earth ground at both ends of the cable run. This may cause ground loop
problems in some cases. These should be treated on a case-by-case basis. Disconnecting one
shield ground may not provide sufficient protection depending on the electronic environment.
Connecting one shield ground via a 0.1 microfarad ceramic capacitor is a technique allowing
high frequency shield bonding while avoiding the AC-ground metal connection. In the case of
shielded cables the drain wire or braid connection must be kept short. A two-inch connection
distance between the shield’s end and the nearest grounded chassis point, ground bar or termi-
nal is highly recommended. An even greater degree of shield performance can be achieved by
using metallic glands for shielded cable entry into metal enclosures. Expose enough of the braid/
foil/drain where it passes through the gland so that the shield materials can be wrapped back-
wards onto the cable jacket and captured inside the gland, and tightened up against the metal
interior.

Inductive loads connected to the low voltage “Alarm Contacts” are not recommended. However,
if this becomes a necessity, adhere to proper techniques and wiring practices. Install an appro-
priate transient voltage suppression device (low voltage MOV, “Transzorb,” or R/C) as close as
possible to the inductive device to reduce the generation of transients. Do not run this type of
signal wiring along with other I/O or DC in the same shielded cable. Inductive load wiring must
be separated from other circuits in conduit by using an additional cable shield on the offending
cable.

In general, for optimum protection against high frequency transients and other disturbances, do
not allow installation of this Analyzer where its unshielded I/O and DC circuits are physically
mixed with AC mains or any other circuit that could induce transients into the Analyzer or the
overall system. Examples of electrical events and devices known for the generation of harmful
electromagnetic disturbances include motors, capacitor bank switching, storm related transients,
RF welding equipment, static, and walkie-talkies.

xiv | Model 933 UV Analyzer


SPECIAL WARNINGS AND INFORMATION
EQUIPMENT USED IN HAZARDOUS LOCATIONS
This Equipment is Suitable for Use in Hazardous Locations as follows:

Canadian Standards Association (CSA)


Class I, Division 1, Groups C and D, and/or Class I, Zone 1, Ex d IIB, T3.

ATEX (KEMA)
II 2 G EEx d IIB T3.

Explosion Hazard – Substitution of Components May Impair Suitability for Class I, Division 2.
!
WARNING
Risque d’explosion – La substitution de composants peut rendre ce materiel
! inacceptable pour les emplacements de Classe I, Division 2.
Avertissement

Explosion Hazard – Do Not Disconnect Equipment Unless Power Has Been Switched Off or
! the Area is Known to be Non-Hazardous.
WARNING
Risque d’explosion – Avant de déconnecter l’équipement, coupez le courant où vous
! assurez que l’emplacement est designé non dangereux.
Avertissement

All input and output wiring must be in accordance with Class I, Division 2 wiring methods (NEC
Sec 501.4(b) or CEC 18-152) and in accordance with the authority having jurisdiction.

Contents | xv
Declaration of Conformity

xvi | Model 933 UV Analyzer


WARRANTY AND CLAIMS
We warrant that any equipment of our own manufacture or manufactured for us pursuant to our specifi-
cations which shall not be, at the time of shipment thereof by or for us, free from defects in material or
workmanship under normal use and service will be repaired or replaced (at our option) by us free of
charge, provided that written notice of such defect is received by us within twelve (12) months from date
of shipment of portable analyzers or within eighteen (18) months from date of shipment or twelve (12)
months from date of installation of permanent equipment, whichever period is shorter. All equipment
requiring repair or replacement under the warranty shall be returned to us at our factory, or at such other
location as we may designate, transportation prepaid. Such returned equipment shall be examined by us
and if it is found to be defective as a result of defective materials or workmanship, it shall be repaired or
replaced as aforesaid. Our obligation does not include the cost of furnishing any labor in connection with
the installation of such repaired or replaced equipment or parts thereof, nor does it include the responsi-
bility or cost of transportation. In addition, instead of repairing or replacing the equipment returned to us
as aforesaid, we may, at our option, take back the defective equipment, and refund in full settlement the
purchase price thereof paid by Buyer.

Process photometric analyzers, process moisture analyzers, and sampling systems are warranted to
perform the intended measurement, only in the event that the customer has supplied, and AMETEK has
accepted, valid sample stream composition data, process conditions, and electrical area classification prior
to order acknowledgment. The photometric light sources are warranted for ninety (90) days from date of
shipment. Resale items warranty is limited to the transferable portion of the original equipment
manufacturer’s warranty to AMETEK. If you are returning equipment from outside Canada, a statement
should appear on the documentation accompanying the equipment being returned declaring that the
goods being returned for repair are Canadian goods, the name of the firm who purchased the goods, and
the shipment date.

The warranty shall not apply to any equipment (or part thereof) which has been tampered with or altered
after leaving our control or which has been replaced by anyone except us, or which has been subject to
misuse, neglect, abuse or improper use. Misuse or abuse of the equipment, or any part thereof, shall be
construed to include, but shall not be limited to, damage by negligence, accident, fire or force of the
elements. Improper use or misapplications shall be construed to include improper or inadequate protec-
tion against shock, vibration, high or low temperature, overpressure, excess voltage and the like, or
operating the equipment with or in a corrosive, explosive or combustible medium, unless the equipment
is specifically designed for such service, or exposure to any other service or environment of greater
severity than that for which the equipment was designed.

The warranty does not apply to used or secondhand equipment nor extend to anyone other than the
original purchaser from us. Should the Buyer ’s technical staff require the on-site assistance of AMETEK’s
agents or employees for service calls covered by this warranty clause, the Buyer shall pay travel time plus
actual travel and living expenses.

THIS WARRANTY IS GIVEN AND ACCEPTED IN LIEU OF ALL OTHER WARRANTIES, WHETHER
EXPRESS OR IMPLIED, INCLUDING WITHOUT LIMITATION AND WARRANTIES OF FITNESS OR OF
MERCHANTABILITY OTHER THAN AS EXPRESSLY SET FORTH HEREIN, AND OF ALL OTHER
OBLIGATIONS OR LIABILITIES ON OUR PART. IN NO EVENT SHALL WE BE LIABLE UNDER THIS
WARRANTY OR ANY OTHER PROVISION OF THIS AGREEMENT FOR ANY ANTICIPATED OR LOST
PROFITS, INCIDENTAL DAMAGES, CONSEQUENTIAL DAMAGES, TIME CHANGES OR ANY OTHER
LOSSES INCURRED BY THE ORIGINAL PURCHASER OR ANY THIRD PARTY IN CONNECTION
WITH THE PURCHASE, INSTALLATION, REPAIR OR OPERATION OF EQUIPMENT, OR ANY PART
THEREOF COVERED BY THIS WARRANTY OR OTHERWISE. WE MAKE NO WARRANTY, EXPRESS
OR IMPLIED, INCLUDING WITHOUT LIMITATION ANY WARRANTIES OF FITNESS OR OF MER-
CHANTABILITY, AS TO ANY OTHER MANUFACTURER’S EQUIPMENT, WHETHER SOLD SEPA-
RATELY OR IN CONJUNCTION WITH EQUIPMENT OF OUR MANUFACTURE. WE DO NOT AUTHO-
RIZE ANY REPRESENTATIVE OR OTHER PERSON TO ASSUME FOR US ANY LIABILITY IN CON-
NECTION WITH EQUIPMENT, OR ANY PART THEREOF, COVERED BY THIS WARRANTY.

Contents | xvii
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xviii | Model 933 UV Analyzer


OVERVIEW

The AMETEK Model 933 Analyzer uses photometric analysis to continu-


ously monitor H2S levels in pipeline quality natural gas. It uses AMETEK
Western Research’s proven sample conditioning system based on frontal
elution chromatography. This system separates and eliminates interfering
species to ensure an accurate analysis of the gas. The microprocessor-
based Model 933 minimizes the complexity of these tasks and simplifies
operation of the analyzer system.

The Model 933 Analyzer is certified Pollution Degree 2 (normally noncon-


ductive environmental pollution occurs with occasional condensation)
and Installation Category II (local level transients, less than those found at
power distribution level).

Theory of the Model 933 Analyzer


The Model 933 Analyzer measures the absorbance of ultraviolet light by a
gas species. It analyzes a maximum of six discrete wavelengths. The
concentrations of the species absorbing the light are determined from the
relationships through application of the ideal gas law in concert with the
laws of Bouguer, Beer and Lambert law extended by using a system of
linear equations. The measurements can be viewed using a laptop com-
puter connected to the analyzer and running AMETEK’s Configurator
Software.

The Beer-Lambert law, in combination with the ideal gas situation, states
that:

At a given wavelength the volumetric concentration of an


absorbing gas is directly proportional to the logarithm of
the transmittance and the temperature, and inversely pro-
portional to the Measuring Cell length and pressure.

The proportionality constant is determined according to the units chosen


for length, temperature, and pressure.

Overview | 1-1
In a situation where several species are absorbing light at several measur-
ing wavelengths, the total absorbance at any particular wavelength is the
sum of the absorbances for each of the species present. Using Beer’s law
for each measuring wavelength, a system of linear equations relating the
unknown concentration to the measured absorbance at each wavelength
is obtained. The total absorbance at each measuring wavelength is equal
to the proportionality constant multiplied by the molar absorptivity for
the first species times its concentration, plus the (molar absorptivity)
factor for the second species, times its concentration, and so on for all
species present in the Measuring Cell. Provided that there are more
measuring wavelengths than unknown concentrations, this system of
linear equations is solved using standard methods of linear algebra.

Features
Microprocessor-Based
The operation of the analyzer, calculations and data manipulations are
all controlled by two on-board microprocessors.

Multicomponent Analysis
The availability of six discrete wavelengths enables either single-
component analysis or multicomponent analysis, with the capability
of eliminating interferences from other gas species. All interfering
species except COS and MeSH are eliminated by a gas-conditioning
system based on frontal elution chromatography. The H2S concentra-
tion is mathematically corrected for the presence of COS and MeSH so
that H2S concentrations are presented free of interferences.

Auto Zero
Automatically updates the analyzer zero. You can initiate the Auto-
Zero function on command using the Configurator Software, at user-
specified time intervals, or by a remote (potential free) contact closure.

Serial Communications
One RS-485 serial communications port is dedicated to customer data
acquisition. The port uses Modicon Modbus® protocol.

A second serial communications channel is available for servicing or


reconfiguring of the analyzer using the System 200 Configurator
Software program running on a PC. The channel is jumper-selectable
between an RS-232 port and an RS-485 port. The RS-232 port is in-
tended for occasional connection while the RS-485 port is intended for
permanent connection.

1-2 | Model 933 UV Analyzer


Analog Outputs
There are eight independent output-signal channels. Four channels
consist of voltage outputs (1–5V full-scale) and the other four are
isolated 4–20 mA outputs. The standard configuration for the analyzer
is one 4–20 mA output which is set for the H2S concentration.

Temperature Control
The analyzer controls the temperature of two temperature-controlled
zones:

• Column Block

• Optical Bench

Independent over-temperature circuits protect the two zones.

Status Relays
There are five independent sets of SPDT (Form C) relay contacts (2 A,
250 V).

Low Maintenance
The robust analyzer and sample conditioning system design reduces
maintenance requirements.

Temperature-Controlled Enclosure (optional)


Used for applications requiring a temperature-controlled environ-
ment, to maintain the ambient temperature within 0–50 °C. The
Temperature-Controlled Enclosure uses cooling and heating systems
to maintain this ambient temperature range.

Pressure Compensation (optional)


See Appendix B – Options for more information about this feature.

Environmental Purge (optional)


See Appendix B – Options for more information about this feature.

Application
The principal application of the Model 933 Analyzer is the analysis of
hydrogen sulfide (H2S) in pipeline quality natural gas. The major compo-
nents of the gas are alkanes (e.g., methane), which are transparent to the
analyzer. However, in addition to H2S, the gas may contain a variety of
minor components that are non-transparent. These potential interferers
include sulfur species such as mercaptans (e.g., ethyl mercaptan), aromat-
ics (e.g., benzene), and various other chemicals that are indigenous to gas
“sweetening” plants. The Model 933 sample conditioning system removes
potential interferers (conditions) from the gas sample so an accurate
analysis can be performed.

Overview | 1-3
Implementation
The Model 933 Analyzer is comprised of the following (see Figure 1-1):

• Two ultraviolet light sources

• Filter wheel containing up to six interference filters

• Beam splitter

• Front surfaced mirrors

• Gas Measuring Cell

• Two matched photodetectors

Figure 1-1.
Analyzer analytical
block diagram.

1-4 | Model 933 UV Analyzer


Microcontroller Board and Host Controller Board
The operation of the analyzer is controlled by two microprocessors. One is
the Microcontroller board and is assigned to the Optical Bench interface,
data conversion, data preprocessing functions and temperature control of
the Optical Bench. The other is the Host Controller board and is assigned
to handling input/output, column temperature control, and final process-
ing of data from the Microcontroller board. The System 200 Configurator
Software is a proprietary AMETEK software package that is used to
interface with the analyzer.

Sample Conditioning
When a measurement is taken, the sample flows from the process stream
through to the Sample Conditioning System (SCS) where potentially
interfering gas species are removed using a form of gas chromatography.
The conditioned sample is then analyzed in the Measuring Cell and
finally vented to the atmosphere (see Figure 1-2).

Discrete Wavelengths
To achieve measurements at discrete wavelengths, the locations of the
filters in the filter wheel and the placement of the source lamps are cho-
sen so that, at any time, the photodetectors are exposed to light from only
one lamp and filter combination (i.e., a discrete wavelength).

For practical reasons related to timing and lamp control, two revolutions
of the filter wheel are required to collect a complete set of wavelength
data. During one revolution, consecutive pulses of light from Source
Lamp 1 arrive at the beam splitter. During the next revolution, consecu-
tive pulses of light arrive at the beam splitter from Source Lamp 2. Since
the nominal speed of the filter wheel is 400 RPM, pulses for any given
wavelength arrive at the beam splitter at a rate of 200 pulses per minute.

As each flash of light arrives, the beam splitter directs half the light to the
Reference photodetector and half through the gas sample to the Measure
photodetector. Because of the longer optical path and light losses at the
mirrors and through the Measuring Cell windows, the amount of light
received by the Measure photodetector is less than that received by the
Reference photodetector, even when there are no absorbers in the gas
sample. This is the reason that there is balance screen on the Reference
photodetector.

Overview | 1-5
LEGEND

Figure 1-2.
Sample Flow Diagram.

1-6 | Model 933 UV Analyzer


At each wavelength, for any given analyzer, these optical-path factors produce
a constant difference between the amounts of light received by the two photo-
detectors. When absorbers are present in the gas sample, the amount of light
received by the Measure photodetector is reduced further. The magnitude of
the reduction is dependant on the concentrations of the absorbers. Thus, for
each wavelength, the difference in the amounts of light received by the two
photodetectors (corrected for the optical-path factors) is used to determine the
absorbance of the gas sample. Then the concentration of the individual absorb-
ers (for which the analyzer is configured) is calculated.

For the Model 933 configuration, the concentrations of three absorbers are
determined:

• H2S
• COS
• MeSH

This application requires measurements at four discrete wavelengths:


214nm, 228nm, and 326nm from Source Lamp 1 (cadmium); 249nm and
326nm from Source Lamp 2 (copper).

Overview | 1-7
About the Analyzer Sampling System
The sampling system is mounted to the Model 933 backpan. The purpose
of the system is to maintain constant pressure and temperature, and to
condition the sample to obtain correct analysis. Refer to the Flow Diagram
(Figure 1-2) and the appropriate Backpan Component Layout drawing in
Chapter 3 (Figure 3-5, North America or Figure 3-6, Europe).

In addition to the components mounted to the backpan, an optional


Filterblock Assembly is available to remove condensables and particulates
from the sample gas. If the Filterblock Assembly option is not installed,
AMETEK recommends installing a coalescing or membrane filter.

The sampling system consists of the components listed below:

Component Function
Sample Probe Extends into the process stream to obtain a representative sample.

Contains a shut-off valve used to isolate the sample path from the
process stream.
Inlet Pressure Regulator The inlet pressure regulator adjusts the sample pressure to the
operating pressure (typically 80 PSIG/560 KPAG) specified in the
analyzer data sheet.
Pressure Gauge The pressure gauge is used to set the proper sample pressure in the
sampling system.
Solenoid Block The solenoid manifold block directs flow between the Zero solenoid,
Column A solenoid and Column B solenoid. There is also a pressure
relief valve to safeguard against over pressuring of any components
down stream of the solenoid manifold block or if the pressure regulator
fails. This pressure relief valve is factory-adjusted to open at
approximately 150 PSIG (1050 KPAG).
Column Switching Solenoids Solenoids are automatically turned on or off to initiate switching the
sample between columns.
Zero Solenoid The zero solenoid allows zero gas (or span gas) to flush the sampling
system during the auto-zero (or span) process. The column switching
solenoids are closed when the zero solenoid is open.
Column Block The Column Block is where the sample conditioning process takes
place. The Column Block incorporates a proprietary material to permit
correct sample analysis.
Heat Exchanger Block The heat exchanger block reduces the temperature of the conditioned
gas sample prior to it entering the Measuring Cell.
Measuring (Sample) Cell The Measuring Cell is a chamber of known length, with optical-grade
quartz windows, through which the radiation beam passes through the
gas sample. The windows are sealed by means of o-rings and
removable end caps.
Flow Indicator (Rotameter) The flow meter provides a visual indication of the sample flow rate in
liters/minute through the analyzer. Please note that the scaling on the
flow indicator is for air at standard temperature and pressure. Its
purpose is to indicate and ensure that appropriate flow conditions are
maintained and not to provide an absolute measure of the flow of
sample gas.
Filterblock Assembly See Appendix B – Options for a description of this assembly.

1-8 | Model 933 UV Analyzer


Sample Conditioning Column Operation
The sample conditioning column uses a unique form of gas chromatogra-
phy in which the sample flows continuously and acts as the “carrier” of
the component to be measured. When an equilibrium is reached between
the quantity of a given compound in the absorbing material and that in
the gas, the concentration of the compound in the column exit gas will
start to increase. This concentration increase is referred to as the com-
pound eluting from the column. The object of this process is to create an
elution spectrum of the sample by passing it through an absorber. The
spectrum is a series of plateaus – each plateau associated with the elution
of a detector-sensitive component. The absorbing material in the columns
has been selected so that hydrogen sulfide (H2S) is the first detector-
sensitive component that elutes from the column. The next detector-
sensitive components to elute are carbonyl sulfide (COS) and methyl
mercaptan (MeSH). You must also adjust the operating parameters so that
the first potential interferer, ethyl mercaptan (EtSH), does not interfere by
terminating the analytical cycle before it begins to elute from the absorb-
ing column and “replacing” it with a fresh column so that the analysis can
continue. This requires the use of two columns. While one column is
operating in the absorbing mode, the other is being regenerated. The
column is regenerated by reducing the pressure and backpurging with
purified sample from the outlet of the Measuring Cell. This process is
effective only when the analytical cycle is terminated before ethyl mercap-
tan begins to elute from the absorbing column.

The column is regenerated at a lower pressure than that at which absorp-


tion takes place, and so a short period of time is required for equilibrium
to be reestablished on the regenerated column when it is switched to the
absorbing mode. During this time period, the analyzer output signal is not
valid and so a track and hold function is used to maintain a consistent
output signal. At the time the columns are switched (analytical cycle
terminated), the output signal is held at the value immediately before
which the switch occurred. At the end of the equilibrium time, the hold
function is terminated. The column switching time and the hold time are
both user-adjustable functions. Refer to the Column Profile drawing
under “Sample Conditioning System Optimization” in Chapter 3.

Overview | 1-9
Relays

Status Relays
The Customer I/O Board contains three independent relays that indicate
the operational status of the analyzer. Each relay provides a set of SPDT
(form C) dry (potential free) contacts. The relays are configured for fail-
safe operation (i.e., energized for the non-alarm condition). Each relay
also has an associated green LED on the Customer I/O board, which
remains on steady to indicate a non-alarm (normal operating) condition.

• The Fault relay indicates that an error has been detected by the built-in
diagnostics system. If this relay is de-energized, the green LED (D404)
will turn off to indicate the analyzer requires servicing. If the relay is
configured to latch (default) it will not clear unless the user manually
resets the alarm; otherwise, it will reset automatically upon correction
of the fault alarm.

• The Warning relay indicates that the analyzer’s built-in diagnostics has
detected a warning alarm condition, that the analyzer is not operating
under normal automatic control, or that the analyzer is performing a
gas or analog output calibration. If this relay is de-energized, the green
LED (D405) will turn off to indicate the analyzer requires attention.

• The Alarm Valid relay indicates whether information from the Concen-
tration 1 and Concentration 2 relays is valid or whether the analyzer is
capable of alarming. The contacts automatically change state upon
correction of the condition which caused the alarm. If this relay is de-
energized, the green LED (D406) will turn off to indicate there is a
problem.

1-10 | Model 933 UV Analyzer


Alarm Relays
There are two independent relays, which indicate that the gas concentra-
tion has exceeded the alarm Concentration On (Conc. On) or Concentra-
tion Off (Conc. Off) setpoint. Each relay provides a set of SPDT (Form C),
dry (potential free) contacts. Each relay has an associated red LED (D407
and D408 on the Customer I/O board), which lights to indicate an alarm
condition.

• The Concentration 1 relay indicates that the assigned species has


exceeded the Alarm 1 Conc. On or Conc. Off setpoint. The relay con-
tacts will remain in the alarm state after the concentration returns to
normal if the relay configuration is set to be latching (default). If
desired, the concentration alarm can be configured to be non-latching.

• The Concentration 2 relay indicates that the assigned species has


exceeded the Alarm 2 Conc. On or Conc. Off setpoint. The relay con-
tacts will remain in the alarm state after the concentration returns to
normal if the relay configuration is set to be latching (default). If
desired, the concentration alarm can be configured to be non-latching.

Solid State Relays


There are three solid state relays which control AC power to the Column
A solenoid, Column B solenoid and the Zero Solenoid. Three digital
control lines are used to turn these solid-state relays on and off. Each
control line has an associated red LED (D411, D410 and D409 on the
Customer I/O board), which turns on to indicate that the solid state relay
has turned switched and the solenoid is activated. If all the LEDs are
turned off, this indicates that the analyzer is in Shut-in Mode.

Overview | 1-11
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1-12 | Model 933 UV Analyzer


SPECIFICATIONS

Methodology
Proprietary frontal elution sampling; non-dispersive ultraviolet analysis
for measurement of hydrogen sulfide (H2S), carbonyl sulfide (COS), and
methyl mercaptan (MeSH) in sales quality (pipeline quality) natural gas.
Frontal elution chromatography is used to remove interfering species
from the sample gas.

Full-Scale Ranges
PPM ranges are standard; mg/Nm 3 and other ranges are available.

Standard Range Measuring Cell (40 cm or smaller)


Maximum ranges are based on Measuring Cell length (expressed in cm).
Minimum ranges are one-fifth of maximum ranges.

H2S Standard Range: 5,000 / (Cell length)


COS Standard Range: 20,000 / (Cell length)
MeSH Standard Range: 10,000 / (Cell length)

Low Range Measuring Cell (81.2 cm)


H2S: 0–5 PPM minimum and 0–50 PPM maximum
COS: 0–25 PPM minimum and 0–250 PPM maximum
MeSH: 0–15 PPM minimum and 0–100 PPM maximum

Response Time (excludes sampling system)


H2S: Typically < 30 seconds to T90
COS: Typically < 60 seconds to T90
MeSH: Typically < 180 seconds to T90

Specifications | 2-1
Measurement Accuracy
± 2.0 % full-scale of standard ranges to a minimum of:

H2S: ± 0.25 PPM


COS: ± 1 PPM
MeSH: ± 0.75 PPM

Based on minimum ranges (e.g., 40 cm):

H2S: ± 0.5 PPM


COS: ± 2 PPM
MeSH: ± 1 PPM

Accuracy is determined by comparing analyzer response to a known


standard gas after a calibration has been performed.

Repeatability
< ± 2.0 % full-scale of standard ranges (including Column effects)

Calibration
Calibration gases in nitrogen or methane.

Linearity
< ± 2.0 % full-scale of standard ranges to a minimum of:

H2S: ± 0.25 PPM


COS: ± 1 PPM
MeSH: ± 0.75 PPM

Stability
Noise: < 1.0 % of standard ranges (excluding cross-talk effects)

Sensitivity
0.5 % of standard ranges

2-2 | Model 933 UV Analyzer


Cross-Talk
H 2S concentration measurement – less than 2 % of the sum of COS and
MeSH concentrations.

Cross-talk adjustments should be made by factory-trained service


 personnel only.
NOTE

Temperature Drift
H2S: 2 PPM / (Cell length) / °C
COS: 12 PPM / (Cell length) / °C
MeSH: 4 PPM / (Cell length) / °C

24-Hour Zero Drift


± 2.0 % full-scale of standard ranges to a minimum of:

H2S: ± 0.25 PPM


COS: ± 1 PPM
MeSH: ± 0.75 PPM

Analog Outputs
Up to 4 isolated 4–20 mA, loop or self-powered.
4 non-isolated 1–5 V.
5 independent sets of SPDT, Form C, potential free relay contacts, 2 A at
250 VAC.

Digital Communication
RS-485 Modbus® port
RS-232/RS-485 service port

Specifications | 2-3
Electrical Requirements

Maximum Start-Up Power

<500 W maximum start-up with continuous average, depending on


ambient temperature (excluding Sample and Vent line).

Electrical Requirements

ATEX/Hazardous Locations:
120 VAC, 50–60 Hz, 2 A Maximum
240 VAC, 50–60 Hz, 1 A Maximum

CSA:
104–132 VAC, 47–63 Hz, 3 A Maximum
207–264 VAC, 47–63 Hz, 2 A Maximum

Status Relay Contacts

250 VDC, 2 A Maximum

Digital Input Signals


For Auto-Cal and Alarm Enable/Clear
0–24 VDC, 30 VDC Maximum

Output Signal
4–20 mA DC, 30 VDC Maximum

Typical Sample Gas Flow Rate


2.5 L/minute (5 SCFH)

Zero Gas
Instrument zero purity carbon dioxide; UHP nitrogen, or UHP methane.
Minimum Auto-Zero interval is once per 24 hours. More frequent Auto-
Zeroing can be used to reduce temperature drift in installations with
widely varying ambient temperatures.

2-4 | Model 933 UV Analyzer


Ambient Limits

Temperature

From 0 °C to 50 °C (32 °F to 122 °F).

The surrounding ambient temperature must be at least 5 °C (9 °F) degrees


above the highest expected dewpoint temperature. It is also extremely
important to maintain a relatively stable ambient temperature in the
vicinity of the analyzer, with no rapid temperature fluctuations.

Humidity

0–95 % RH

Maximum Altitude

2000 m

Sample Pressure Requirement


Without optional Filterblock Assembly:
830–20 700 KPAG (120–3000 PSIG)

With optional Filterblock Assembly:


830–13 790 KPAG (120–2000 PSIG)

Refer to Article 3, Paragraph 3 in the Pressure Equipment Directive


 document titled “Directive 97/23/EC of the European Parliament and
NOTE of the Council.”

Specifications | 2-5
Sample Stream Requirements
> 80 % ethane plus methane
< 10 % ethane (for standard column application)
< 3 % propane
< 1.25 % total butanes
< 0.5 % C5+
< 0.6 %Water content (based on a 35 °C maximum water dewpoint tem-
perature at 120 PSIG/830 KPAG)

The surrounding ambient temperature must be at least 5 °C (9 °F)


 degrees above the highest expected dewpoint temperature.
NOTE

Physical Dimensions (on backpan)


Height: 1185 mm (46.65")

Width: 780 mm (30.7")

Depth: 232 mm (9.1")

Weight: Approximately 72 kg (160 lb), entire system and


backpan only (may vary, depending on system).

Options
• Gas/liquid (glycol) separating filter (Filterblock Assembly)
• Other measuring ranges
• COS and methyl mercaptan measurement
• Pressure compensation
• Up to 4 V/I outputs

2-6 | Model 933 UV Analyzer


Approvals and Certifications
The Model 933 Analyzer is certified Pollution Degree 2 (normally noncon-
ductive environmental pollution occurs with occasional condensation)
and Installation Category II (local level transients, less than those found at
power distribution level).

Other certifications and approvals include:

CSA: Class I, Zone 1 (Division 1), Groups C&D, Ex d IIB T3


NEC: Class I, Zone 1 (Division 1), Groups C&D, AEx d IIB T3
GOST: 1ExdIIBT3
Complies with all relevant European Directives,
GOST Pattern Approval
ATEX (KEMA): II 2 G EEx d IIB T3
PED: Pressure Equipment Directive (97/23/EC)
Article 3, Paragraph 3
EMC: Electromagnetic Compatibility Directive:
EN61326 Industrial
LVD: Low Voltage Directive:
EN61010-1

Specifications | 2-7
ATEX (CENELEC) Certificate and Analyzer Marking
For installation sites with potentially explosive atmospheres that require
ATEX certification, AMETEK’s ATEX certificate for the Model 933 Analyzer
is included in the following pages.

2-8 | Model 933 UV Analyzer


Specifications | 2-9
ATEX-certified Model 93X Analyzers are marked with the label shown
below.

0344

PROCESS INSTRUMENTS II 2 G

Western Research Model 933 Analyzer


Certificate No: KEMA 02ATEX2247, EEx d IIB T3 (T amb. 0°C...50°C)
Year. _______
Serial No. __________________

Caution
Do not open when an explosive gas atmosphere is present.

Power Dissipation Input


<210W 120VAC 50/60Hz 2A max.
<210W 240VAC 50/60Hz 1A max.

2-10 | Model 933 UV Analyzer


CSA Certificate and Analyzer Marking
For installation sites that require CSA certification, AMETEK’s CSA certifi-
cate for the Model 933 Analyzer is included in the following pages.

Specifications | 2-11
2-12 | Model 933 UV Analyzer
Specifications | 2-13
CSA-certified Model 933 Analyzers are marked with the label shown
below.

PROCESS INSTRUMENTS

Western Research Model: 933 ANALYZER


SN:

___104-132Vac, 3A ___207-264 Vac, 2A, 47-63 Hz, <500W


CLASS I, GROUPS C & D
CLASS I ZONE 1 Ex d IIB T3, AEx d IIB T3
Tamb. +50°C

Caution
Open circuit before removing cover.

2-14 | Model 933 UV Analyzer


INSTALLATION & START-UP

This chapter shows you how to install and start up the Model 933 UV
Analyzer. It includes the following:

• Where to find safety information in this guide before working with


the analyzer.

• General Installation and Maintenance Information

• Uncrating and Inspection

• Storage Prior to Installation

• Installation of Mechanical Components

• Electrical Installation

• Input / Output Signal Connections

• Installation of System 200 Configurator Software

• Sampling System Leak Check

• Operating Parameters Verification/Configuration

• Sample Conditioning System Optimization

The installation of the analyzer must be in accordance with all of the


! user and local regulatory standards and procedures. There are no
WARNING operator-serviceable components inside the analyzer. Refer servicing
to qualified personnel.

Installation & Start-Up | 3-1


Safety Considerations
Under normal operating conditions, dangerous concentrations of H2S and
other toxic gases from the process may be present within the sampling
system. The sampling system is defined as all components in the analyzer
system through which the process gas passes.

Before beginning the installation of the Model 933 Analyzer and


 before powering it up, review and follow all personnel and equipment
NOTE safety information under “Important Safety Notes, Warnings, and
Cautions” following the Table of Contents. This information describes
procedures to follow to avoid personal injury and/or damage to the
equipment. All regulatory agency and personnel safety procedures
for your jurisdiction must be followed.

3-2 | Model 933 UV Analyzer


Pre-Installation Requirements

Storage Prior to Installation


If the analyzer and its Optical Bench Assembly are stored for any period
of time prior to installation, store the equipment in an environment where
it is not subject to dripping liquids, splashing liquids, corrosive gases, high
humidity, or excessive heat or cold.

Uncrating and Inspecting the Analyzer


The analyzer, along with its associated sampling system, is shipped pre-
mounted on a backpan in a crate. Upon receiving the analyzer, remove
the analyzer from its shipping crate and check the exterior of the analyzer
for damage. Open the upper and lower enclosure (48 hex-socket screws)
and check that all of the components and wiring within the electronics
enclosures are secure and there is no physical damage.

Avoid damaging the analyzer’s piping and instrumentation by lifting


! it out of its shipping crate using only its backpan. DO NOT use any
CAUTION piping or instrument as a handle for lifting.

The analyzer and its backpan weighs approximately 72 kg (160 lb).


! Use caution when lifting it from its crate.
WARNING

After the inspection, replace and tighten at least one hex screw for
! each enclosure. This will keep the enclosures secure and will prevent
CAUTION damage to the mating surfaces (flamepaths) during installation.

The Optical Bench Assembly is shipped in a separate box. Remove the


shipping crate and check it for any physical damage.

Installation & Start-Up | 3-3


General Installation Information

The electronic circuit boards and other static-sensitive components


! should be stored and transported in static-shielding carriers or
CAUTION packages.

When handling the source lamps, it is very important not to touch the
! lamp windows because residual oils from the fingers will absorb
CAUTION ultraviolet light. The window is the flat surface at the end of the
narrow glass tube. The lamp assembly is fragile and should be handled
with care.

• Metric fasteners are used throughout the analyzer assembly. 2 mm,


2.5 mm, 3 mm, 4 mm, 5 mm, and 8 mm hexagonal wrenches are
required for servicing the analyzer.

• The torque specification for fastening M6 screws is 4.0 ± 0.7 Nm


(36 ±9 in-lb). The torque specification for fastening M10 screws is 9.0
±1.0 Nm (80 ± 9 in-lb).

Tools and Equipment Required


To install the analyzer, you need the following tools, equipment, and
supplies:
• Set of open-end wrenches for fittings.
• Set of metric hexagonal wrenches.
• Set of metric ball drivers.
• Wire Cutters, strippers, and crimpers.
• Flat blade instrument screwdriver.
• Electric Drill.
• Wrist Strap (for grounding).
• Detergent-based leak detector (Snoop® or another suitable leak detec-
tion agent is permissible).
• One power-disconnect explosion-proof switch (breaker), rated for at
least 250 VAC, 3 A and certified for the hazardous area. For safety
reasons during maintenance, this switch allows the main power to be
disconnected from the analyzer. This switch is to be supplied by the
customer/end user.
• Supply of 1/8" or 1/4" 316 stainless steel tubing for the sample line
(depends on required flow rate).

3-4 | Model 933 UV Analyzer


Installation of the Mechanical Components
The Model 933 Analyzer and the Optical Bench Assembly are shipped in
separate crates.

Do not mount the Optical Bench in the EEx d Upper Enclosure until
! after the analyzer has been mounted in its designated location.
CAUTION

All electrical connections to the Optical Bench Assembly are made via pre-
wired connector plugs. No hard wiring is required.

Follow the installation procedures in this chapter under the sections


“Mounting the Analyzer” and “Installing the Optical Bench.”

Mounting the Analyzer


The analyzer system comes mounted on a backpan. See Figure 3-1 for the
backpan and mounting hole locations and dimensions, plus necessary
clearances on all sides that are required for service.

Location and Environment

The Model 933 is designed for indoor operation (Pollution Degree 2) so it


must be shielded from the elements. The entire analyzer system (and its
backpan) can be mounted directly on a wall inside a building, in a spe-
cially designed cabinet, or in a custom-built shelter. In all cases, the ana-
lyzer system must be installed indoors to ensure it is shielded from harsh
environmental elements.

Regardless of which installation method is used, be sure to install the


 analyzer in a location that is as free as possible from vibrations.
NOTE

The surrounding ambient temperature of the analyzer must be between


0 °C and 50 °C (32 °F and 122 °F). The minimum ambient temperature
around the analyzer and sampling system should be at least 5 °C (9 °F)
above the maximum sample dew point temperature. If the analyzer
system is mounted within an AMETEK-designed shelter, these conditions
are taken into consideration in the design of shelter.

Locate the analyzer at an accessible location as close to the sample point


as possible in order to obtain minimum response time and, if the sample
line must be heated, minimize the heating requirements.

Installation & Start-Up | 3-5


PROCESS INSTRUMENTS

CAUTION:
RISK OF ELECTRIC SH OCK

ATTENTION:
CONSULT USER MAN UAL

0344

II 2 G
PROCESS INSTRUMENTS

Western Research Model 933 Analyzer


Certificate No: KEMA 02ATEX2247, EEx d IIB T3 (T amb. 0°C...50°C)
Year. _______
Serial No. __________________

Caution
Do not open when an explosive gas atmosphere is present.

Power Dissipation Input


<210W 120VAC 50/60Hz 2A max.
<210W 240VAC 50/60Hz 1A max.

SERIA L COMMUNICATIONS PORT


D O NOT OPEN IF A HAZARDOUS
GAS A TMOSPHER E IS PRESENT

MAY NOT BE EXACTLY AS SHOWN

Figure 3-1.
Model 933 backpan
dimensions (Europe).

3-6 | Model 933 UV Analyzer


Installing the Optical Bench Assembly
The Optical Bench Assembly is shipped separately from the analyzer. You
will need to mount it in the Upper Enclosure. Refer to the drawings in this
section for assistance in identifying the hardware components.

Ensure there is no power being supplied to the analyzer during the


! installation of the Optical Bench Assembly.
WARNING

While installing the Optical Bench Assembly in the EEx d Upper


! Enclosure, take care not to damage the mating areas (flamepath) of the
CAUTION EEx d Upper Enclosure.

To mount the Optical Bench Assembly:

1. Connect the Optical Bench AC power lines (via the connector plug) to
TB100 on the Optical Bench Service Electronics Board (Figure 3-2).

The cam pins must stay aligned while the Optical Bench Assembly is
 being mounted into the enclosure. The lined groove on the head of the
NOTE cam pin must stay parallel to the Measuring Cell until the Optical
Bench Assembly is in place.

2. Locate the cam pins, which are situated in the Optical Bench mount
(Figure 3-3). Confirm that the grooved lines in the cam pins are facing
inward.

3. Attach the Optical Bench Assembly by fitting the Optical Bench


mount over the Cell Window Housing mount.

4. Rotate the lower cam pin counter-clockwise and the upper cam pin
clockwise until they are tight.

5. Connect the green/yellow ground wire from the interior of the upper
enclosure (via the disconnect terminals) to the green/yellow wire
connected to the Optical Bench Assembly.

Installation & Start-Up | 3-7


Figure 3-2.
Optical Bench Service
Electronics Board
(P/N 100-1662, w/o
bracket).

3-8 | Model 933 UV Analyzer


LOOSE CLAMPED

OPTICAL BENCH REMOVAL/INSTALLATION

Figure 3-3.
Upper enclosure
layout and cam pin
locations.

6. Connect the Micro-Interface AC power lines (via the connector plug)


to J200 on the Micro-Interface board (Figure 3-4).

7. Connect the DC power lines (via the connector plug) to J103 on the
Micro-Interface board.

8. Connect the RS-422 communication lines (via the connector plug) to


J104 on the Micro-Interface board.

9. Connect the Measuring Cell RTD (via the connector plug) to J300 on
the Micro-Interface board.

Use a soft, nonabrasive cloth to gently clean the mating areas


! (flamepath) of the Upper Enclosure and its door. Close the door and
CAUTION replace at least one of the M10 screws while completing the installa-
tion. This will ensure the flamepath is not inadvertently damaged.

Installation & Start-Up | 3-9


Figure 3-4.
Micro-Interface board
(P/N 100-1759).

3-10 | Model 933 UV Analyzer


Installing the Sampling System
Refer to Figure 3-5 (North America) or Figure 3-6 (Europe) for Sample and
Vent Line tubing connection points. The analyzer is supplied with fittings
for sample line, vent line, and zero gas. The sample inlet fitting (1/8”
Swagelok® tubing fitting) is located on the inlet pressure regulator. The
vent outlet fitting (1/4” Swagelok tubing fitting) is located on the vent
rotameter. The optional Filterblock Assembly is included in Figure 3-5 and
Figure 3-6.

 If the Filterblock Assembly option is not installed, AMETEK recom-


mends that you install your own coalescing or membrane filter.
NOTE

 The inlet sample pressure should be 560 KPAG (80 PSIG) or higher.

NOTE

The vent line should be connected at atmospheric pressure or <0.5 PSI.



NOTE

Zero Gas
The zero gas fitting (1/4” Swagelok tubing fitting) is located on the sole-
noid manifold block. See Figure 3-5 (North America) or Figure 3-6 (Eu-
rope) for the Zero gas tubing connection point.

The recommended zero gas is carbon dioxide -99.99 %. If required, acti-


vated charcoal filters can be used to obtain:

• <15 PPM O2

• <10 PPM H2O

• <1 PPM Hydrocarbons

• <0.1 PPM Total Sulfur

at a pressure 10 % above the sample Measuring Cell pressure. Refer to


the specifications in Chapter 2 for substitutes.

Installation & Start-Up | 3-11


PROCESS INSTRUMENTS

SERIAL COMMUNICATIONS PORT


DO NOT OPEN IF A HAZARDOUS
GAS ATMOSPHERE IS PRESENT

MAY NOT BE EXACTLY AS SHOWN

Figure 3-5.
Backpan component
layout (North
America).

3-12 | Model 933 UV Analyzer


PROCESS INSTRUMENTS

CAUTION:
RISK OF ELECTRIC SHOCK

ATTENTION:
CONSULT USER MANUAL

0344

II 2 G
PROCESS INSTRUMENTS

Western Research Model 933 Analyzer


Certificate No: KEMA 02ATEX2247, EEx d IIB T3 (T amb. 0°C...50°C)
Year. _______
Serial No. __________________

Caution
Do not open when an explosive gas atmosphere is present.

Power Dissipation Input


<210W 120VAC 50/60Hz 2A max.
<210W 240VAC 50/60Hz 1A max.

SERIAL COMMUNICATIONS PORT


DO NOT OPEN IF A HAZARDOUS
GAS ATMOSPHERE IS PRESENT

MAY NOT BE EXACTLY AS SHOWN

Figure 3-6.
Backpan component
layout (Europe).

Installation & Start-Up | 3-13


Electrical Installation
The nominal operating voltage and power consumption is indicated on a
metal label riveted to the front of the EEx d Lower Enclosure and on the
backpan. Verify that the operating voltage indicated on the label agrees
with the operating voltage indicated on the documentation supplied with
the analyzer.

Where required, certified EEx d cable glands must be used and each
! unused cable entry port must be plugged with a certified EEx d plug.
WARNING
For AC electrical supply cable and conduit requirements, refer to and
comply with local wiring regulations and electrical codes for the
hazardous area.

Refer to the Electromagnetic Compatibility (EMC) page in the contents


 section of this manual for information that discusses the EMC Directive
NOTE regarding techniques and wiring practices to be followed.

To maintain EMC compliance in European installations, AMETEK


recommends using metal glands and shielded cable (shielded with at
least 85 % coverage) for both power and signal cable connections.

3-14 | Model 933 UV Analyzer


Input/Output Signal Connections
The analyzer can be configured with up to four (4) current output signals.
The following inputs/outputs are supplied with the analyzer as standard:
• One digital input for remote zero,
• One digital input for Alarm Enable/Disable Concentration Alarms (this
input must be terminated with a jumper or closed contact for the
alarms to be enabled),
• Four (4) non-isolated voltage outputs, and
• One isolated current output.

The analog input/output (and alarm relay) terminations are made on the
Customer I/O PWB, located in the Lower Enclosure.

North American Installation:


For North American installations, refer to Figure 3-7 for analog input/
output (and alarm relay) terminal assignments.

European Installation:
Signal wires, contained within cable that is approved locally for the
hazardous area, enter the EEx d Lower Enclosure through one of the
Signal Cable Entries on the bottom of the EEx d Lower Enclosure.

For European installations, refer to Figure 3-8 for analog input/output


(and alarm relay) terminal assignments.

Installation & Start-Up | 3-15


I/O BOARD CUSTOMER CONNECTIONS

120VAC POWER TERMINATIONS

HC BOARD CUSTOMER CONNECTIONS

Figure 3-7.
Customer connections
wiring schematic (North
American installations).

3-16 | Model 933 UV Analyzer


I/O BOARD CUSTOMER CONNECTIONS

220VAC POWER TERMINATIONS

HC BOARD CUSTOMER CONNECTIONS

Figure 3-8.
Customer connections
wiring schematic
(European installations).

Installation & Start-Up | 3-17


Digital Communication
The digital communication port configurations are made on the Host
Controller board. Refer to the Host Controller board (HC Board) Cus-
tomer Connections in Figure 3-7 (North American) or Figure 3-8 (Euro-
pean) for communication/termination options and Figure 3-9 for jumper
(JP) locations/settings.

Hardware Configuration

The Explosion-Proof Digital (Local Service) Communications Port (9-pin


D-sub connector), configured as RS-232, is located on the front of the
Lower Enclosure (see Figures 3-5 or 3-6). The port is principally intended
as a temporary connection for configuring and servicing the analyzer
while communicating with the analyzer via the AMETEK M933
Configurator Software.

Hazardous Locations:
! Before attempting to access the Digital Communications Port, test the area for
WARNING hazardous gases and proceed only when the area is found to be safe.

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure, do not connect the
computer’s serial cable to the analyzer’s serial communication port,
and do not power up the laptop computer if there is an explosive gas
atmosphere present.

There are also two other serial port connections available for permanent
connection: Remote Service Port and Customer Data Acquisition Port,
both RS-485.

To configure either port, refer to “Remote Service Port/Local Service Port


Configurations” (and “Remote Service Port RS-485, Full/Half Duplex,” if using
the Remote Service Port) or “Customer Data Acquisition Port RS-485, Full/
Half Duplex” in the following pages. The jumpers for these service ports are
located on the Host Controller board (see Figures 3-7 or 3-8 and Figure 3-9).

Remote Service Port/Local Service Port Configurations


Set these jumpers to
To configure the analyzer for: these positions:
JP300 = 1-2
Local Service Port RS-232 or Modem JP301 = 1-2
JP302 = 1-2
JP300 = 2-3
Remote Service Port RS-485 JP301 = 2-3
(* See Note.) JP302 = 2-3

*Note: Requires additional configuration, discussed under “Remote


Service Port RS-485, Full/Half Duplex” configurations.

3-18 | Model 933 UV Analyzer


Figure 3-9.
Host Controller board
(P/N 100-1757, Rev. B).

Installation & Start-Up | 3-19


If using the Remote Service Port (RS-485), you must configure it for Full-
Duplex (4-Wire) or Half-Duplex (2-Wire), as shown below in the “Remote
Service Port RS-485, Full/Half Duplex” configuration, and Figures 3-7 or
3-8 and Figure 3-9.

 The RS-485 Remote Service Port can also be used for customer
service, but not both at the same time as the RS-232 Digital Commu-
NOTE
nications Port.

Remote Service Port RS-485, Full/Half Duplex


(Service RS-485 JP304)
To configure Set jumper JP304 to
the analyzer for: this position:

Full-Duplex (4-Wire) 1-2

Half-Duplex (2-Wire) 2-3

The Customer Data Acquisition Port (Modbus Communication) is config-


ured as RS-485 and is accessed via J302 on the Host Controller board
inside the Lower Enclosure. This line can be configured as Full-Duplex
(4-Wire) or Half-Duplex (2-Wire), as shown below in the “Customer Data
Acquisition Port RS-485, Full/Half Duplex” configuration, and Figures 3-7
or 3-8 and Figure 3-9.

 If your system is configured to communicate through the RS-485


Customer Data Acquisition Port (Modbus Communication), you
NOTE
cannot communicate with the analyzer through the RS-232 Digital
Communications Port (on the front of the Lower Enclosure) unless
you stop polling from the Customer Data Acquisition Port.

Customer Data Acquisition Port RS-485, Full/Half Duplex


(Customer RS-485 JP303)
To configure Set jumper JP303 to
the analyzer for: this position:

Full-Duplex (4-Wire) 1-2

Half-Duplex (2-Wire) 2-3

3-20 | Model 933 UV Analyzer


If it is possible to do so during installation, cable the terminal connections
into a nonhazardous area. Ensure that all unused cable/conduit entries to
the enclosures are closed with appropriately certified plugs for the haz-
ardous area.

Use a soft, nonabrasive cloth to gently clean the mating areas


! (flamepath) of the Upper and Lower Enclosures before closing them.
CAUTION

Multiple-Analyzer (Multi-Drop) System Configuration

When using multiple analyzers wired together (called a Multi-Drop


system), the configuration may vary due to the overall setup of your
application.

This section describes various connection options available for configuring


Multi-Drop systems.

To configure analyzers in a Multi-Drop system:

1. Choose the appropriate port, either RS-232 or RS-485.

2. If using the RS-485 port, select either a 2- or 4-wire link for both Cus-
tomer Data Acquisition and Remote Service ports.

3. For termination and biasing of RS-485 links, refer to Figure 3-10. Refer to
Figures 3-7 or 3-8 and Figure 3-9 for communication/termination
options and jumper (JP) locations/settings.

The termination and biasing options will depend on the analyzer role
and location in the network (master or slave, located at the end of the
transmission line or at a drop point). It will also depend on whether a
2- or 4-wire line is used, and the transmission line conditions (e.g.,
length of cable, or termination and biasing on the other end of the cable).

Figures 3-9 and 3-10 apply only to Model 933 Analyzers with Host
 Controller Board, Rev. B and newer.
NOTE

Installation & Start-Up | 3-21


A
RX+
R J302 (Customer Data Acquisition) J303 (Remote Service Port)
B
RX- JP305 (RX RT) 2-3 JP307 (RX RT) 2-3
JP306 (TX RT) 2-3 JP308 (TX RT) 2-3
(a) JP309 (RX RB1) 2-3 JP311 (RX RB1) 2-3

Y JP310 (TX RB1) 2-3 JP312 (TX RB1) 2-3


TX+
D JP313 (RX RB2) 2-3 JP315 (RX RB2) 2-3
Z
TX- JP314 (TX RB2) 2-3 JP316 (TX RB2) 2-3

A
RX+
R J302 (Customer Data Acquisition) J303 (Remote Service Port)

130
RT
B
RX- JP305 (RX RT) 1-2 JP307 (RX RT) 1-2
JP306 (TX RT) 1-2 JP308 (TX RT) 1-2

(b) JP309 (RX RB1) 2-3 JP311 (RX RB1) 2-3

Y JP310 (TX RB1) 2-3 JP312 (TX RB1) 2-3


TX+
D JP313 (RX RB2) 2-3 JP315 (RX RB2) 2-3

130
RT
Z
TX- JP314 (TX RB2) 2-3 JP316 (TX RB2) 2-3

+5V
R B1

619

A
RX+
R J302 (Customer Data Acquisition) J303 (Remote Service Port)
B
RX- JP305 (RX RT) 2-3 JP307 (RX RT) 2-3
R B2

JP306 (TX RT) JP308 (TX RT)


619

2-3 2-3
(c) +5V JP309 (RX RB1) 1-2 JP311 (RX RB1) 1-2
JP310 (TX RB1) 1-2 JP312 (TX RB1) 1-2
R B1

619

Y JP313 (RX RB2) 1-2 JP315 (RX RB2) 1-2


TX+
D JP314 (TX RB2) 1-2 JP316 (TX RB2) 1-2
Z
TX-
R B2

619

+5V
R B1

619

A
RX+
R J302 (Customer Data Acquisition) J303 (Remote Service Port)
130
RT

B
RX- JP305 (RX RT) 1-2 JP307 (RX RT) 1-2
R B2

JP306 (TX RT) JP308 (TX RT)


619

1-2 1-2
(d) +5V JP309 (RX RB1) 1-2 JP311 (RX RB1) 1-2
JP310 (TX RB1) 1-2 JP312 (TX RB1) 1-2
R B1

619

Y JP313 (RX RB2) 1-2 JP315 (RX RB2) 1-2


TX+
D JP314 (TX RB2) 1-2 JP316 (TX RB2) 1-2
130
RT

Z
TX-
NOTES:
1. RB - BIAS RESISTOR
R B2

619

2. RT - TERMINATION RESISTOR
3. RESISTANCE VALUES IN OHMS
Figure 3-10.
Various RS-485 port
terminations and bias
options (Host
Controller board,
P/N 100-1757, Rev. B).

3-22 | Model 933 UV Analyzer


AC Power Connection and Fusing

Both the North American and European versions of the Model 933
 UV Analyzer require that a power-disconnect switch (breaker), rated
NOTE for at least 250 VAC, 3 A, must be connected to, and mounted near,
the analyzer (supplied by the customer). To satisfy local electrical
codes, the switch must be certified by the local authority for the
appropriate hazardous area.

For safety reasons during maintenance, this switch allows the main
AC power to be disconnected from the analyzer prior to performing
service on the analyzer.

The analyzer must be operated from a grounded power source; failure to


do so will void the warranty. Depending on analyzer configuration, the
supply voltage may be 115 VAC ± 10 % (47–63 Hz) or 230 VAC ± 10 %
(47–63 Hz). The nominal operating voltage and power consumption is
indicated on the metal nameplate that is secured to the front of the Lower
Enclosure. Verify that the operating voltage indicated on the label agrees
with the operating voltage indicated on the documentation supplied with
the analyzer. The analyzer is intended for use in Installation Category II
(Overvoltage Category) and AC power requirements for each analyzer
system are specified on the system electrical drawings.

Installation & Start-Up | 3-23


North American Installation

To make the AC power connections in the Lower Enclosure:

The power connection to the analyzer is made at TB1-1, TB1-2, and TB1-5
on the AC Terminal Strip in the lower enclosure (see Figure 3-11, Detail A).

LOWER ENCLOSURE

Figure 3-11.
Conduit entries and AC
power connection
locations, lower DETAIL A
enclosure (North
American installations).

3-24 | Model 933 UV Analyzer


European Installation

To maintain EMC compliance in European installations, AMETEK


 recommends using metal glands and shielded cable (shielded with at
NOTE least 85 % coverage) for both power and signal cable connections.

To make the AC power connections in the EEx d Lower Enclosure:

• The AC electrical supply cable, which must be approved by the local


wiring regulations and electrical codes for the hazardous area, enters
the EEx d Lower Enclosure through the Power Cable Entry on the
bottom of the EEx d Enclosure (see Figure 3-12).

• The AC power connections are made at the AC Terminal Strip to the


terminals designated “H”, “N”, and “PE” within the EEx d Lower
Enclosure (see Detail A in Figure 3-12).

Use certified EEx d cable glands.


!
WARNING Each unused cable entry port must be plugged with a certified EEx d
plug.

Installation & Start-Up | 3-25


LOWER ENCLOSURE

Figure 3-12.
Conduit entries and DETAIL A
AC power connection
locations, EEx d lower
enclosure (European
installations).

3-26 | Model 933 UV Analyzer


Installing the System 200 Configurator Software
AMETEK’s proprietary M933 Configurator Software is included with the
analyzer. The primary use of the software is to configure the analyzer’s
operating parameters and to control the functions of the analyzer. While
working from the Configurator Software you can view real-time and histori-
cal data, and modify configuration and calibration parameters. Details of
how to perform these tasks are described, primarily, in Chapter 4. The
software is also necessary while performing maintenance and while trouble-
shooting the analyzer. The majority of these functions are performed from
the M933 Properties dialog box of the software. Details of these tasks are
described in other chapters of this manual.

The software also provides advanced software features, such as graphing


and scanning data. Details of how to perform these tasks are described,
primarily, in Appendix A – Advanced Software Options.

Hazardous Locations:
 Before proceeding, test the area around the analyzer for hazardous
NOTE gases and proceed only when the area is found to be safe.

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is an explosive gas atmosphere present.

Minimum PC Requirements for Configurator Software


System 200 Configurator Software requires the following:

• CD-ROM drive (for installation); software is also available on 3.5 inch


floppy discs, upon request.

• Pentium 166 or faster.

• 16 MB RAM.

• 3 MB of available hard disk space.

• Sound Card (for alarms) recommended, not required.

• Windows 98 / ME / NT 4.0 / 2000 / XP.

• 800 x 600 resolution or higher recommended.

• 256-color display, 32767 colors (HiColor, 16-bit) recommended.

Installation & Start-Up | 3-27


Configurator Software Installation

 During installation, AMETEK recommends installing the software


and program icons in the default directories.
NOTE

To install the System 200 Configurator Software on your computer:

1. Insert the AMETEK Configurator Software CD in the CD-ROM drive.


The auto-setup program will run and begin the installation. The
Welcome to the InstallShield Wizard screen will appear.

2. Click Next to continue with the setup. The Readme Information


screen will appear.

3. Click Next to continue. The Destination Folder screen will appear


(Figure 3-13). Follow the on-screen instructions to install the software.

By default, the software will be installed in C:\AMETEK\M933.

AMETEK recommends using the default directory. Otherwise, click


Change to view the Change Current Destination Folder screen and
navigate to the folder you wish to install the software in. Or, create a
new directory.

Figure 3-13.
Destination Folder
screen.

3-28 | Model 933 UV Analyzer


4. Click Next to continue. The software will install and the InstallShield
Wizard Completed screen (Figure 3-14) will appear. If you plan to use
the Configurator Software immediately, enable Launch the program
(selected by default). Click Finish and then remove the CD from the
CD-ROM drive.

If the software prompts you to restart your computer, click No.



NOTE

You can also start the software by clicking M933 Configurator from
the Start\Programs\Ametek\933 Configurator menu.

The software will create a shortcut icon on the desktop to start the
 software (called 933 Configurator).
NOTE

For details about using System 200 Configurator Software to commu-


nicate with the analyzer, refer to “Establishing Communication Be-
tween the Analyzer and Computer,” later in this chapter.

Figure 3-14.
InstallShield Wizard
Completed screen.

Installation & Start-Up | 3-29


Removing the Configurator Software
To remove the System 200 Configurator Software from your computer:

1. From the Windows Start menu, select Settings, and then Control
Panel.

2. Double-click Add/Remove Programs.

3. Select AMETEK 933 Configurator and click Add/Remove to automati-


cally remove it.

4. In the C:\AMETEK\M933 folder, delete all remaining folders and files,


including the M933 folder.

3-30 | Model 933 UV Analyzer


Start-Up and Verification
This section describes equipment and controls on the analyzer system that
require adjustments and settings before, during, and after power-up.
Refer to Figure 3-5 (North America) or Figure 3-6 (Europe) for the loca-
tions of analyzer equipment or controls that require adjustments.

Powering Up the Analyzer


When powering up the analyzer, certain checks should be performed to
ensure the analyzer is operating properly. These checks are discussed in
the following power-up procedures. If there are problems encountered
during power-up, refer to the “Analyzer Start-Up Diagnostic Checklist,”
later in this chapter, for help in diagnosing and correcting problems.

Before powering up the analyzer, test the area for flammable gases. If
! an explosive gas atmosphere is present, do not apply power to the
WARNING analyzer or any alternate power sources that supply power to the
analyzer components. Proceed only when the area is found to be safe.

Before operating the analyzer for the first time, following a power-up
! or reset, or after maintenance, you must manually block in the sample
WARNING gas flow.

Also, for verification and troubleshooting purposes during power up,


it will be necessary to work with the Upper and Lower Enclosures
open. Before powering up the analyzer, the area first must be tested for
hazardous gases (and found to be safe).

When the Electronics Enclosures are open, take appropriate precau-


tions to avoid electrical shock. Hazardous voltages are present inside.

Do not apply power to the analyzer if any of its flamepaths appear to


! be scratched, dented, or worn. Applying power to an analyzer with a
WARNING damaged flamepath is dangerous and could result in serious injury or
death and/or serious damage to equipment.

Installation & Start-Up | 3-31


To power up the analyzer and verify it is operating properly:

1. Apply main AC power to the analyzer.

Establish communication between the analyzer and the Configurator


Software. (See “Establishing Communication with the Analyzer Using
a Computer,” following this section for information on how to estab-
lish communications.)

2. Perform the following checks to ensure the analyzer starts up properly


and is ready to be commissioned into operation.

If you cannot verify these checks, refer to “Analyzer Start-Up Diagnos-


tic Checklist,” later in this chapter, for corrective action to take. Resolve
any problems before proceeding to the next start-up stage.

a. Verify the operation of the status relays on the Customer I/O board
(Figure 3-15):

• The Alarm Valid Status Relay and the two Concentration


Alarm Relays will be in the de-energized state. Observe the
green LED D406 and the two red LEDs D407 and D408. Each
of these LEDs should be on to indicate normal operation.

• The state of the Fault Status Relay and the Warning Status
Relay depends on the current status of the analyzer. However,
it is most likely that both relays will be de-energized upon
initial power-up as the temperatures of the Column Block and
the Optical Bench have not yet reached their respective
setpoints, and are generating a fault (“Fault Column Temp Lo”)
and warning (“Warning Bench Temp”) alarm error message,
respectively. Verify this in the Error Condition list on the
Status tab of the M933 Properties dialog box. These green
LEDs D404 and D405 will be off in this case.

b. Upon power-up, all solenoids will remain de-energized for at least


five minutes. Verify this by viewing the red LEDs D411, D410 and
D409 on the Customer I/O board (Figure 3-15). These LEDs should
be off.

c. The Column Block heater will be turned on to heat up the Col-


umn Block. Verify this by viewing the red LED D401 on the Cus-
tomer I/O board (Figure 3-15). It should be on steady or pulsing.

3-32 | Model 933 UV Analyzer


Figure 3-15.
Customer I/O board
(P/N 100-1758).

Installation & Start-Up | 3-33


Figure 3-16.
Microcontroller board
(P/N 100-1781).

3-34 | Model 933 UV Analyzer


d. The green status LED (LED100) on the Host Controller board
(Figure 3-9) will stay on continuously for a few seconds before
pulsing at a rate of once per second. Verify this operation. The
pulsing indicates that communication is established between the
Microcontroller and the Host Controller.

You can also verify communication between the Host Controller


board and the Microcontroller board by viewing LEDs D201 and
D200 on the Microcontroller board (Figure 3-16). Both LEDs
should be pulsing in unison once per second.

e. Check the UV lamps to ensure they are firing (flashing) after


communication between the Host Controller and Microcontroller
boards is established.

f. The Optical Bench heater will turn on to heat up the Optical Bench.
You can verify this by observing that the red LED (LED201) on the
Micro-Interface board (Figure 3-4) is on continuously or pulsing.

g. While working from the Configurator Software, check the set points
and current temperature readings for each of the temperature-
controlled zones. This will help you to determine if the signal wiring
is properly terminated and if all of the circuitry is operating properly.
Record the set point and current (start-up) temperature value indi-
cated for each zone to use as a reference later while comparing the
temperature value (after the analyzer has warmed up).

To do this, click the Temp Control button from the Setup tab of the
M933 Properties dialog box. View and record the set points for
each temperature-controlled zone.

Next, select the Analyzer Data tab to view the current temperature
readings, under Temperature Zone. Record the set points for each
temperature-controlled zone. This will help you determine if the
signal wiring is properly installed and if all of the circuitry is
operating properly.

h. Check for any alarms (under Error Condition) by clicking and


viewing the Status tab. Temperature-related alarms should correct
themselves after the analyzer has warmed up to normal operating
temperature. If any alarms remain active, refer to “Analyzer Start-
Up Diagnostic Checklist” in this chapter or “Diagnostics and
Troubleshooting” in Chapter 6 for more information on how to
correct alarms.

After all alarms have cleared, recheck the temperature of each


zone. Compare the current temperatures to their respective set
point values and their start-up values. Normal operating tempera-
tures are values that are within 5 % of the Set Point values.

Installation & Start-Up | 3-35


3. If you cannot verify the observations listed in Step 2, refer to “Analyzer
Start-Up Diagnostic Checklist” or the “Diagnostics and Troubleshoot-
ing” section in Chapter 6 for more information on how to correct
alarms or persistent problems. Resolve any problems before proceed-
ing to the next start-up stage.

4. After all fault alarms have cleared, the analyzer will automatically
perform an Auto-Zero.

5. If all of the temperature zones have reached normal operating tem-


peratures and there are still no alarm conditions or other problems,
perform a pressure leak check on the analyzer sampling system to
ensure there are no leaks in the system.

To perform this test, follow the procedures listed under the section
titled “Pressure Leak Check,” later in this chapter. Then, return to this
section and complete the remaining steps.

6. After all of these checks have been made and verified, close the upper
and lower enclosures. However, the sample gas should remain
blocked in.

Use a soft, nonabrasive cloth to gently clean the mating areas


! (flamepath) of the Upper and Lower enclosures before closing the
CAUTION
Upper and Lower enclosures.

The torque specification for fastening M10 screws is 9 ±1 Nm (80 in-lb).



NOTE

Replace the parts immediately if damage or wear is apparent. Contact


! AMETEK immediately if there is any doubt about the integrity of any
WARNING flamepath.

7. Perform an Auto-Setup to optimize the PMT gains of the source


lamps. Information on how to do this is located in Chapter 6.

3-36 | Model 933 UV Analyzer


Establishing Communication Between the Analyzer
and Computer
You establish communications with the Model 933 Analyzer by using a
computer running AMETEK’s Configurator Software.

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up/
down the laptop computer if there is a hazardous gas atmosphere
present.

To connect a computer to the analyzer and establish communications with


the analyzer:

1. Connect the supplied Serial Communications Cable to the computer.

2. After the area has been tested for hazardous gases (and has been
found to be safe), loosen the hex screw on the cover of the Explosion-
Proof Serial Communications Port (RS-232) on the Lower Enclosure
enough to allow the cover to slide to the right and reveal the Digital
Communications Port.

3. Connect the other end of the Serial Communications Cable to the


Digital Communications Port, either the Local Service port (RS-232, on
the front of the Lower Enclosure) or the Remote Service port (RS-485,
accessed from connector J303 on the Host Controller board) connec-
tion.

4. Power up the computer and run the Configurator Software. To do this:

a. From the Start menu, click Properties, AMETEK, and then M933,
or double-click the M933 shortcut icon on the desktop (if one was
created). The software will start and the M933 Configurator screen
will appear (Figure 3-17).

Within this screen is the Devices & Log dialog box (see “Viewing
Device Activities” in Chapter 4 for details about this window).

Installation & Start-Up | 3-37


Figure 3-17.
M933 Configurator main
window, with Devices &
Log window active.

b. The Configurator Software automatically attempts to establish


communications with the analyzer. If the communication attempt
fails, the communication settings may be incorrect and/or the
communication cable may not be connected properly.

Check the communications settings to ensure they are set properly


to allow the analyzer to communicate with a PC via the
Configurator Software.

Also, confirm the instructions for setting up the Host Controller


board for service/customer digital communication by reviewing the
section “Digital Communication,” earlier in this chapter.

c. To change the communication settings, click Device Properties


from the Edit menu to view the M933 Properties dialog box
(Figure 3-18). This is your primary interface with the analyzer
when viewing live data, or when modifying the analyzer’s con-
figuration or calibration parameters.

Figure 3-18.
M933 Properties
dialog box (General
tab).

3-38 | Model 933 UV Analyzer


d. From the General tab, the Device Enabled and Live Data check
boxes should be checked. If the software prompts for proceeding
with auto-detect, answer NO.

e. Click the Setup button on the General tab to access the Serial Port
Configuration (Figure 3-19).

Figure 3-19.
Serial port
configuration.

Provide the following information:

• Port: Select the COM port used for communicating


with the analyzer.

• Baud Rate: Select the baud rate at which data will be


transferred.

• Port Type: RS-232 Port:


Click if using the analyzer’s Local Service port
(RS-232). This should be the default and recom-
mended setting at this stage.

RS-485 Port:
Click if using the Remote Service port (RS-485).
See “Modifying Analyzer Device Settings” in
Chapter 4 before attempting to configure the
RS-485 remote service port.

Installation & Start-Up | 3-39


Click OK to accept the settings and allow the Configurator Soft-
ware to establish communication with the analyzer. The Status
Information box on the General tab will display “Online” after
communication is established with the analyzer.

If communications still are not established, review “Digital Com-


munication,” earlier in this chapter.

If you will be working with the computer powered up for prolonged


! periods, periodically test the area around the analyzer for hazardous
WARNING gases, according to your company’s safety policies.

Before powering down the computer or disconnecting the serial


communications cable from the Explosion-Proof Digital Communica-
tions Port , test the area for hazardous gases and proceed only when
the area is safe.

5. After you have completed communicating with the analyzer, exit the
Configurator Software, power-down the computer, and disconnect the
Serial Communications Cable from the Explosion-Proof Digital Com-
munications Port on the Lower Enclosure.

6. Slide the cover of the Explosion-Proof Digital Communications Port to


the left and hand-tighten the hex screw to secure the cover in place.

3-40 | Model 933 UV Analyzer


Configurator Software Troubleshooting

This section describes problems (error messages) that may be encountered


while attempting to establish communication between the analyzer and
the computer, or when starting the software. Communication error mes-
sages can be displayed in the Status field on the General tab and in the
Devices & Log window. If this window is not displayed in the M933
Configurator main window (Figure 3-17), select Devices & Log from the
View menu or click to display it.

If communication problems occur, review this section and perform the


corresponding corrective action to fix any problems.

Problem Encountered
The “Wrong Device” message is displayed on the Devices & Log window.

Corrective Action
Check the analyzer markings to ensure it is a Model 933 Analyzer (the M933
Configurator Software cannot communicate with other models of analyzers,
such as a Model 900 ADA Analyzer).

The COM Port Parameter Settings may be incorrect. Review the settings in
the Serial Port Configuration dialog box and verify or set them to the proper
settings. The address must also match that of the analyzer – check the
analyzer Address on the Device Communication tab and change it if neces-
sary.

Problem Encountered
The “Connected” message is displayed on the Devices & Log window, but
the software is not communicating with the analyzer.

Corrective Action
Select the Live Data check box to establish communication.

Problem Encountered
The “DEMO Online” message is displayed in the Status field on the General
tab. This message will be displayed if the Live Data check box is not selected
(but the Device Enabled check box is).

Corrective Action
Select the Live Data check box to establish communication.

Installation & Start-Up | 3-41


Problem Encountered
The “OFFLINE” message is displayed in the Status field on the General tab.

Corrective Action
Observe the Device Enabled and Live Data check boxes on the General tab.
One or both of these check boxes may not be selected. Select both of them to
establish communication.

Check the Serial Communication Cable for proper connections and for
damage such as cuts, nicks, or burn marks. Also, check it to ensure the
internal wiring is still terminated at the connectors.

Problem Encountered
The “DISABLED” message is displayed in the Status field on the General
tab. This message will be displayed if the computer is connected to the
analyzer but is not communicating with it.

Corrective Action
Select the Device Enabled check box, if necessary, to establish communica-
tion.

Check the analyzer markings to ensure it is a Model 933 Analyzer (the M933
Configurator Software cannot communicate with other analyzer models).

Problem Encountered
The Device Properties command under the Edit menu is grayed out (access
to the M933 Properties dialog box is not available). If this occurs, the analyzer
configuration and calibration parameters cannot be viewed or modified. This
problem suggests that the “M933.dys” file has become corrupt.

Corrective Action
Delete the “M933.dys” file from the C:\Ametek\M933 folder. The software
will restore this file (and correct the problem) the next time it is started.

3-42 | Model 933 UV Analyzer


Analyzer Start-Up Diagnostic Checklist

This diagnostic checklist describes problems that may be encountered


while powering up the analyzer and/or preparing it for normal operation.
If the analyzer experiences problems during power-up, review this check-
list and perform the corresponding corrective action to fix any problems.

Problem Encountered
The LEDs for various analyzer operations are not operating properly, as
described in the procedures under “Powering Up the Analyzer.”

Corrective Action
Take appropriate safety precautions and check for proper I/O wiring and
power connections.

If the LEDs are still not operating properly, reset the analyzer. To do this, cycle
the AC power off a minimum of 15 seconds before cycling it on again.

Problem Encountered
One or both source lamps are not firing.

Corrective Action
Take appropriate safety precautions and check for proper wiring connections.

If the wiring is okay, check the connections of the lamps in their sockets.
Review the section titled “Source Lamp Replacement” in Chapter 6 to make
adjustments to the lamps. Perform an Auto-Setup if necessary to ensure the
lamps are operating at peak efficiency.

Problem Encountered
Temperature zone values do not increase.

Corrective Action
Take appropriate safety precautions and check for proper wiring terminations
for the appropriate temperature zone.

Installation & Start-Up | 3-43


Problem Encountered
A temperature-control zone value is equal to or greater than the maximum
temperature range being used (view the Temperature Control dialog box to
check the range). A high temperature value may indicate a faulty RTD for the
related temperature zone.

Corrective Action
Take appropriate safety precautions and check the related RTD for a short or
an open circuit. If necessary, replace the RTD with an AMETEK-approved
replacement part. Contact AMETEK for assistance.

Problem Encountered
Alarms remain active after the analyzer has warmed up to normal operating
temperature, as displayed under Error Condition on the Status tab.

The “Fault Column Temp Lo”, “Warning Bench Temp”, and “Warning Cell
Temp” alarm error messages will typically be displayed upon start-up due to
low temperatures in these temperature-controlled zones.

Corrective Action
If these or other alarms remain active, refer to the alarm conditions and
corrective action in Chapter 6.

3-44 | Model 933 UV Analyzer


Sampling System Leak Check
The analyzer has been checked at the factory for leaks. Since fittings can
loosen during transport, the sampling system should be checked for leaks
before any sample gas is applied to the analyzer. The sample line and vent
line should also be checked for leaks.

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up/
down the laptop computer if there is a hazardous gas atmosphere
present.

Follow these steps to leak check the sampling system:

1. If the sample line is connected, block in the sample to prevent sample


gas from flowing.

2. Connect the zero gas to the sample inlet port of the analyzer.

3. Disconnect the vent tubing from the analyzer and plug it with a cap
fitting.

4. Start the Configurator Software, if not already running.

a. From the Edit menu, click Device Properties.

b. Click the Setup tab of the M933 Properties dialog box (Figure
3-20), then click the Gas Calibration button to view the Gas
Calibration dialog box (Figure 3-21).

c. In the Flow Control drop-down list, select “Col A”. Click OK and
then Apply. Click NO when prompted to save parameters to
EEPROM.

Do not set the pressure higher than 689 KPA (100 PSIG) if the
! optional pressure transducer is installed.
CAUTION

Installation & Start-Up | 3-45


Figure 3-20.
Setup tab, Properties
dialog box.

Figure 3-21.
Gas Calibration dialog
box.

5. Bring the pressure on the zero gas to 550 KPA (80 PSIG). Use the
pressure gauge mounted on the backpan to observe the pressure. The
sample inlet regulator may need to be adjusted.

6. Shut off the zero gas flow at the cylinder. If the reading on the pres-
sure gauge starts to decrease, use a leak detection fluid on the sam-
pling system to find the problem area.

7. Repeat Steps 4-b through 6, but select “Col B” in Step 4-c.

Bleed down the sampling system from the vent port of the analyzer.
! Otherwise, damage to the Filterblock (if installed) may occur.
CAUTION

8. After the sampling system has been bled down, re-cap the vent outlet.
Unhook the zero gas from the sample inlet port and reconnect the
zero gas to the zero gas port of the analyzer.

3-46 | Model 933 UV Analyzer


9. Reconnect the sample line to the sample gas inlet port on the analyzer.
Keep the sample in the blocked condition.

10. Return to the Gas Calibration dialog box and select “Zero” from the
Flow Control drop-down list. Click OK then click Apply. Click NO
when prompted to save parameters to EEPROM.

11. Increase the pressure of the zero gas to 550 KPA (80 PSIG). Use the
pressure gauge mounted on the backpan to observe the pressure.

12. Repeat Step 6 (shut off zero gas).

13. Bleed down the sampling system and remove the cap fitting from the
vent outlet.

14. Reconnect the vent line to the analyzer vent outlet.

15. Return to the Gas Calibration dialog box and select “Auto” from the
Flow Control drop-down list. Click OK then click Apply. Click YES
when prompted to save parameters to EEPROM.

16. The sample gas can now be turned on. Set the pressure to 560 KPA
(80 PSIG) using the sample inlet regulator. The analyzer is ready to
analyze sample gas.

Installation & Start-Up | 3-47


Operating Parameters Verification/Configuration
This section provides instructions for verification and/or configuration of
the Model 933 Analyzer operating parameters prior to normal operation.

Temperature Setpoints
1. Click on the Setup tab of the M933 Properties dialog box.

2. Click on Temp Control to view the Temperature Control dialog box


(Figure 3-22).

Figure 3-22.
Temperature Control
dialog box.

The maximum usable Optical Bench temperature setpoint is 60 °C. Do


! not exceed this set point value.
CAUTION

3. Verify that the (Optical) Bench temperature setpoint and range are
correct. The Optical Bench temperature setpoint should be at least
8 °C to 10 °C above the maximum ambient temperature around the
analyzer. For applications with maximum ambient temperature of 30 °C
and below, a default setpoint temperature of 40 °C is normally used.
The temperature setpoint is set at the factory using the ambient
temperature data that is specific to the application and location. Refer
to Chapter 4 for additional information about how to alter the setpoint
or range.

To alter the set point or range in Step 3, and those set points or ranges
 in Steps 4–8, refer to Chapter 4 for additional information.
NOTE

3-48 | Model 933 UV Analyzer


4. Verify that the Too Hot setpoint for the Bench is correct. It should be
5 °C to 10 °C above the Optical Bench setpoint temperature. The Too
Hot setpoint that is used should not exceed 65 °C. The Too Hot set-
point is set at the factory using the ambient temperature data that is
specific to the application and location.

5. Verify that the Too Cold setpoint for the Bench is correct. It should be
5 °C to 10 °C below the Optical Bench setpoint temperature. The Too
Cold setpoint is set at the factory using the ambient temperature data
that is specific to the application and location.

6. Verify that the Column temperature setpoint is correct. The Column


temperature setpoint should be greater than or equal to, the maxi-
mum ambient temperature around the analyzer. The acceptable range
of setpoint temperatures is between 40 °C and 50 °C. For applications
with maximum ambient temperature of 40 °C and below, a default
setpoint temperature of 40 °C is used. For applications with maximum
ambient temperatures between 40 °C and 50 °C, the maximum ambi-
ent temperature should be used as the Column setpoint temperature.
Do not increase the Column setpoint temperature unless you are sure
that the ambient temperature will periodically exceed 40 °C. The
operation of the columns is optimal at 40 °C. As the temperature is
increased from 40 °C to 50 °C, the columns will have to be switched
more frequently. The temperature setpoint is set at the factory using
the ambient temperature data that is specific to the application and
location.

7. Verify that the Too Hot setpoint for the Column is correct. It should be
5 °C to 10 °C above the column setpoint temperature. The Too Hot
setpoint is set at the factory using the ambient temperature data that is
specific to the application and location.

8. Verify that the Too Cold setpoint for the Column is correct. It should
be 5 °C to 10 °C below the column setpoint temperature. The Too Cold
setpoint is set at the factory using the ambient temperature data that is
specific to the application and location.

9. To confirm the changes, click OK then click Apply; otherwise, click


Cancel. Click YES when prompted to save parameters to EEPROM.

Installation & Start-Up | 3-49


Output Ranges
1. Click the Setup tab of the M933 Properties dialog box.

2. Click Output to view the Output Setup dialog box (Figure 3-23).

3. Verify that each current and voltage output channel configured has
the correct range applied for the application. The ranges are set at the
factory using the data that is specific to the application.

• Below each configured channel, confirm that the Iout/Vout Low


Scale and Iout/Vout High Scale are the correct minimum and
maximum ranges required.

• To ensure the V/I result will not go below 4 mA, enable (check) the
V/I Low Limit 4 mA check box. This will ensure the actual output
clamps the result at 4 mA; the output cannot go below this value.

• Refer to the Chapter 4 for additional information about altering


the ranges. To confirm a change, click OK and then click Apply;
otherwise, click Cancel.

4. Verify that all concentration alarms are configured correctly for the
specific application. The alarm setpoints are set at the factory using
the data that is specific to the application. To alter the setpoints, refer
to Chapter 4 for additional information.

Figure 3-23.
Output Setup dialog
box.

3-50 | Model 933 UV Analyzer


Modbus/Customer Data Acquisition Port
The analyzer is capable of serial communications with a Customer Data
Acquisition system using Modbus protocol on a RS-485 link. Detailed
description of the Modbus implementation on the analyzer can be found
in Appendix C.

A few parameters need to be set up using the Configurator Software to


enable the Modbus port. Click the Setup tab of the M933 Properties
dialog box and click Modbus (Figure 3-24) to view the Modbus dialog box.
Provide the following information:

Address: Enter the Modbus network address assigned to the


analyzer.

Baud Rate: Select the baud rate of the Modbus network.

Stop Bits: Select the number of stop bits of the Modbus


network.

Parity: Select the parity of the Modbus network.

When you have finished entering the Modbus/Data Acquisition Port


parameters, click OK and then click Apply. Click YES when prompted to
save parameters to EEPROM.

Figure 3-24.
Modbus dialog box.

Installation & Start-Up | 3-51


Sample Conditioning System Optimization

The optimization procedure should be performed only after the Optical


! Bench and column temperatures have reached their respective
CAUTION setpoints.

Differences in sample stream composition in various applications can


affect the operation of the chromatographic columns that are used to
remove interfering species. As the quantity of ethane and heavier hydro-
carbons in the sample stream increases, the elution time of all gas species
through the columns tends to decrease.

This change in elution time affects the analyzer’s column switching time
interval and hold time period configuration parameters. These two param-
eters are set up at the factory using stream composition data that was
provided for the application. Check that the parameters are properly set
up for the application and adjust them if necessary.

Column Switch Time Optimization


The first UV-absorbing gas species that elute through the chromato-
graphic columns are hydrogen sulfide, carbonyl sulfide, and methyl
mercaptan. Because the Model 933 can measure the concentrations of all
three of these species, carbonyl sulfide and methyl mercaptan do not
interfere with the hydrogen sulfide measurement. The concentration
reading of each of these species is automatically corrected for the presence
of the other two compounds. Ethyl mercaptan is the first UV-absorbing
species to elute that interferes with the concentration measurement of the
first three species.

During normal analyzer operation, while sample gas is flowing through


one absorbing column and concentration measurements are being per-
formed, the other column is being regenerated. Periodically, the columns
are switched before interfering species can elute from the absorbing
column. The column switch time is the time interval of this switching
cycle. When this switch time is properly adjusted, the columns switch
before ethyl mercaptan elutes from the absorbing column.

3-52 | Model 933 UV Analyzer


Check that the column switch time is properly adjusted:

1. From the Setup tab of the M933 Properties dialog box, click Output
and then click Alarm Disable (Figure 3-23). Click OK.

2. From the Setup tab, click Gas Calibration (Figure 3-21).

Verify that “Auto” is selected from the Flow Control list. If not, select
“Auto”, click OK, and then click Apply. Click NO when prompted to
save parameters to EEPROM.

3. Close the M933 Properties dialog box by clicking OK or Cancel. From


the File menu click Open Configuration. Navigate to the M933 folder
and select the “ColumnSetup.dyc” file. Click Open. A graph will
appear that displays the concentration signals as a function of time.
From the M933 Configurator main window, click (on the Stan-
dard Toolbar) to start data scanning (see Figure 3-25).

Figure 3-25.
Column setup graph.

If the X-axis time interval on the ColumnSetup.dyc needs to be


 adjusted, right-click your mouse button on the graph, click Display
NOTE and change the time period in the Minutes text field.

Installation & Start-Up | 3-53


CONCENTRATION (PPM)

TIME (SECONDS)
MeSH, COS AND H2 S WITH EXCESSIVE COLUMN SWITCH TIME
REAL TIME CONCENTRATIONS
CONCENTRATION (PPM)

TIME (SECONDS)
MeSH, COS AND H 2 S WITH CORRECT COLUMN SWITCH TIME
REAL TIME CONCENTRATIONS
CONCENTRATION (PPM)

Figure 3-26. TIME (SECONDS)


Column profile. MeSH, COS AND H2 S WITH CORRECT COLUMN SWITCH TIME AND CORRECT TRACK & HOLD TIME

3-54 | Model 933 UV Analyzer


4. The sample should now be flowing through the analyzer and periodi-
cally, approximately every 120 seconds, should be switching the two
columns. The graph on the computer screen being displayed should
resemble one of the three graphs in Figure 3-26. Immediately after a
column switch, the real time concentrations of hydrogen sulfide (H2S),
carbonyl sulfide (COS), and methyl mercaptan (MeSH) should drop.

After a short time delay (usually 10–20 seconds) the concentration of


H2S should start to increase. This is the onset of H2S elution from the
column. A few seconds later, COS should also begin to elute from the
column. The concentrations should then stabilize into a plateau.

Eventually, if the column switch time is sufficiently long, the MeSH


will elute and also plateau. Typically, ethyl mercaptan (EtSH) elution
may begin soon after (10–30 seconds) the MeSH stabilizes into a
plateau.

5. Look at the graph of the concentrations being displayed and compare


it to the top graph in Figure 3-26. The column should be switching
before EtSH begins to elute. The EtSH elution time can be recognized
as the point after H2S, COS, and MeSH have all stabilized and where
H2S begins to drop and COS and MeSH begin to increase. If it appears
that EtSH is eluting, the column switch time is too long. Step 6 de-
scribes how to change the column switch time.

6. To change the column switch time, click Column Timing (Figure 3-27)
on the Setup tab. In the Switch Interval text field, enter the new
column switch time and click OK. Click Apply and save the change to
EEPROM.

Figure 3-27.
Column Timing dialog
box.

Installation & Start-Up | 3-55


7. If the analyzer is configured with only the standard H2S output, then
it is likely that the factory default column switch time setting will be
correct for the application. Check that the H2S concentration has
stabilized into a plateau before the columns switch. If the columns are
switching before the H2S concentration has stabilized, the column
switch time is too short. Change the Switch Interval time (see Step 6).

8. If the analyzer is configured with the COS output in addition to the


standard H2S output, then check that the COS concentration has
stabilized into a plateau before the columns switch. If the columns are
switching before the COS concentration has stabilized, the column
switch time is too short. Change the Switch Interval time (see Step 6).

9. If the analyzer is configured with the MeSH output in addition to the


standard H2S output, check that the MeSH concentration has stabi-
lized into a plateau before the columns switch. If the columns are
switching before the MeSH concentration has stabilized, the column
switch time is too short. Change the Switch Interval time (see Step 6).
Verify that the EtSH elution described in Step 5 is not occurring.

To avoid potential interference from EtSH elution, analyzers with the


MeSH output option should be set up to switch the columns as soon
as a reasonably stable MeSH reading is achieved.

3-56 | Model 933 UV Analyzer


Hold Time Optimization
Immediately after a column switch, the real time concentrations of H2S,
COS, and MeSH drop temporarily. During this period of time, the output
concentrations are held constant until the real time concentrations reach
stable values. The Hold Time for each species is the time duration that the
concentration is held constant after the columns are switched.

At the end of the hold period, the Hold Time for each species should be
adjusted so that the real time concentration of the gas in question is
between the T90 concentration (90 % of the stable plateau value) and the
stable value. Refer to the lower graph in Figure 3-26. Setting the Hold
Time to end at, or slightly after, the T90 point for the species, will result in
the fastest response time but will give the noisiest output signal. Setting
the Hold Time to end after the concentration has reached a stable plateau
will give the smoothest output signal, but will result in a longer response
time.

For the H2S output, the factory default Hold Time should be correct. It is
usually set up so that at the end of the hold time, the H2S output is be-
tween the T90 concentration and the stable value. If a slightly faster re-
sponse time is required, the Hold Time can be reduced slightly (see
procedure below). If there is too much noise on the output (the down-
ward spikes that occur between when the Hold Time ends and the con-
centration stabilizes) then the Hold Time can be increased by a few sec-
onds.

If the analyzer is equipped with the optional COS and MeSH Outputs,
then their hold times should have been set up at the factory. Before
adjusting them, check the column switch times as described in the previ-
ous section and, if necessary, adjust them. Because there is not usually a
requirement for fast response time on the COS and MeSH outputs, their
adjustment is usually less critical than that for the H2S.

The COS hold time should be long enough to hold the concentration
constant until the real time COS concentration has reached a stable
plateau. For most applications, the factory default setting should be
correct.

The MeSH hold time is usually adjusted so that the hold on the concen-
trations comes off several seconds before the columns are switched. If the
column switch time in the previous section is adjusted, then the MeSH
hold time will also need to be adjusted. Take the new column switch time
and subtract 2 seconds from it and then use that as the new MeSH hold
time.

Installation & Start-Up | 3-57


To change the hold times:

1. Click Output on the Setup tab to view the Output Setup dialog box
(Figure 3-23). Click Alarm Disable and then OK.

2. Click Column Timing on the Setup tab to view the Column Timing
dialog box (Figure 3-27).

In the Hold Time text field for the species of interest, enter the new
hold time. Click OK. Click Apply and save the changes to EEPROM.

3. Once the column switch time and the hold times have been properly
adjusted, click Output on the Setup tab. Click Alarm Enable. Click
OK.

Hold time for other species not mentioned above should be set to that
 of H2S.
NOTE

3-58 | Model 933 UV Analyzer


CONTROLLER / USER INTERFACE

If potentially flammable gases or vapors are present, do not open any


! covers without first disconnecting power to the analyzer.
WARNING

Before proceeding to connect devices or power up a computer in a


! hazardous area, test the area around the analyzer for hazardous gases
WARNING
and proceed only when the area is found to be safe.

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

The AMETEK M933 Configurator Software program provides a graphical


user interface to configure and control the functions of the analyzer.
Running under Windows 98, ME, NT4.0, 2000, or XP, it provides powerful
features and flexible operating modes.

While working from the Configurator Software you can view real-time
and historical data, and modify configuration and calibration parameters.
The software is also necessary while performing maintenance and while
troubleshooting the analyzer. The majority of these functions are per-
formed from the M933 Properties dialog box of the software. From this
window, all current operating and calibration parameter settings can be
viewed from the various dialog boxes that can be selected from the Setup
tab. Live data for different aspects of the analyzer can be viewed from the
Status, Analyzer Data, and Optical Bench Data tabs.

Controller / User Interface | 4-1


This chapter is divided into the following sections:

• Configurator Software/User Interface overview.

• Modifying analyzer device settings.

• Scanning data.

• Working with data files (saving, opening, scrolling, converting, and


printing).

Graphical and data logging interface, plus configuration and device


 setting operations and procedures not covered in this chapter can be
NOTE found in Appendix A – Advanced Software Operation.

4-2 | Model 933 UV Analyzer


Configuration Software Overview – Getting Started
This section reviews the Configurator Software setup required to begin
working with the software. Before beginning, you should have already set
up the appropriate hardware and software as explained in Chapter 3.

Hazardous Locations:
! Before proceeding, test the area around the analyzer for hazardous
WARNING gases and proceed only when the area is found to be safe.

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure and do not power up
the computer if there is a hazardous gas atmosphere present.

Starting the Configurator Software


To connect a computer to the analyzer and establish communication with
the analyzer:

1. Connect the supplied serial communication cable between the com-


puter and the analyzer (and power up and run the Configurator
Software), as described in Chapter 3.

2. The software will start and the Devices & Log window (Figure 4-5)
will appear in the M933 Configurator window. From here, select
Device Properties from the Edit menu to view the M933 Properties
dialog box (General tab, Figure 4-1).

The M933 Properties dialog box will be your main interface when
 working on the analyzer or viewing live data.
NOTE

By default, the Live Data check box is enabled. When Live Data is
selected, the Configurator Software automatically attempts to establish
communication with the analyzer. If the communication attempt fails,
the communication settings may be incorrect and/or the communica-
tion cable may not be connected properly (or it may be damaged), or
you may be attempting to communicate with the wrong model of
analyzer. Refer to “Configurator Software Troubleshooting” in Chap-
ter 3 for information about how to resolve communication problems.

Controller / User Interface | 4-3


Figure 4-1.
M933 Properties
dialog box (General
tab).

3. Confirm or configure communication settings by clicking Setup to


view the Serial Port Configuration dialog box. Enter or select the
appropriate communication parameters to establish communication
with the analyzer. Detailed descriptions about these communication
options are discussed in the following pages under “PC Communica-
tion Setup.” Then, return to this procedure.

After configuring analyzer communication parameters, click OK to


initiate communication with the analyzer. The software will revert to
the M933 Properties dialog box and the analyzer will be Online, as
indicated in the Status message box.

The M933 Properties dialog box is your primary interface with the
analyzer when viewing live data, or when modifying or viewing the
analyzer’s configuration or calibration parameters.

If at any time you close the M933 Properties dialog box (by clicking
 OK or Cancel), the software will revert to the M933 Configurator
NOTE Software screen. Return to the M933 Properties dialog box by
clicking Edit and then Device Properties.

4-4 | Model 933 UV Analyzer


Closing the Configurator Software

Hazardous Locations:
! Before proceeding, test the area around the analyzer for hazardous
WARNING gases and proceed only when the area is found to be safe.

After you have completed communicating with the analyzer, exit the
Configurator Software and disconnect the computer from the analyzer.

To exit the software:

1. From the M933 Properties dialog box, click OK or Cancel at the


bottom of the screen.

2. From the M933 Configurator window, select Exit from the File menu.

3. Power-down the computer, and disconnect the serial communication


cable from the Explosion-Proof Digital Communications Port on the
Lower Enclosure.

4. Slide the cover of the Explosion-Proof Digital Communications Port to


the left and hand-tighten the hex screw to secure the cover in place.

Controller / User Interface | 4-5


General Tab
When the analyzer is connected to the PC, the current Host Controller
Firmware Version Number and Serial Number of the analyzer will be
displayed in the analyzer information box to the right of PC Communica-
tions under the General tab.

Other parameters include:

PC Communications
Displays information that has been configured from the Serial Port
Configuration dialog box.

Setup
Allows you to set up the communication parameters required to
establish communication with the analyzer. Detailed descriptions
about these communication options are discussed in the following
pages under “PC Communication Setup.”

Device

Name
Enter a tag number or tag name.

Description
Enter a description to further define the analyzer, such as a loca-
tion or area where it is installed in the plant.

This can be useful if using a Multi-Drop system, where multiple


analyzers are wired together on the same line. In this case, you can
assign different names and descriptions for each analyzer.

Save Configuration button


Saves the current analyzer configuration parameters to a file that
can be used later to restore the analyzer configuration settings. See
“Saving Analyzer Configuration Parameters,” later in this chapter,
for details about how to save configuration settings to a file.

Restore Configuration button


Retrieves previously saved analyzer configuration parameters
from a “.dev” file on the computer. See “Restoring Analyzer Con-
figuration Parameters,” later in this chapter, for details about how
to restore configuration data to an analyzer.

4-6 | Model 933 UV Analyzer


Device Enabled

Checked (default) Allows communication with the analyzer,


and allows the user to set up system con-
figurations.

Not Checked Device communication is disabled.

Live Data

Checked (default) Software uses live data from the analyzer.

Not Checked Software uses demonstration data.

Status
Displays the status of the analyzer (device) you are communicating
with. Refer to “Configurator Software Troubleshooting” in Chapter 3
for information about how to correct the problem.

“OFFLINE” Displayed if the PC is not communicating


with the analyzer (one or both of the Device
Enabled and Live Data check boxes are not
selected).

“Online” Displayed if the PC is communicating with


the analyzer (Device Enabled and Live
Data check boxes are selected).

“DISABLED” Displayed if the PC is connected to the


analyzer but is not communicating with it
(Device Enabled and Live Data check boxes
are not selected).

“Device Not Found” Displayed if the analyzer’s Serial Port


Configurations do not match the
computer’s.

“DEMO Online” Displayed if the PC is not connected to the


analyzer (or the Live Data check box is not
selected and the Device Enabled check box
is selected).

Configurator Software version


Displays the version of Configurator Software running (located below
Status).

Controller / User Interface | 4-7


PC Communication Setup

The PC can communicate with the analyzer through either the Local
Service Port or the Remote Service Port , but not both at the same time.
The Local Service Port is located on the front of the Lower Enclosure and
it is configured as RS-232; the remote service port is configured as RS-485
and is accessed via connector J303 on the Host Controller board. See the
Host Controller board drawing under “Digital Communication” in Chap-
ter 3 for locations of jumpers and connectors.

Figure 4-2.
Serial Port
Configuration dialog
box.

Before accessing the local service port on the front of the Lower
! Enclosure, test the area around the analyzer for hazardous gases and
WARNING proceed only when the area is found to be safe.

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure and do not power up/
down the laptop computer if there is a hazardous gas atmosphere
present.

To set up PC serial communications parameters to allow the analyzer to


communication with the Configurator Software:

1. Start the Configurator Software. The M933 Properties dialog box


(General tab) will appear.

2. Click the Setup button to view the Serial Port Configuration dialog
box (Figure 4-2).

4-8 | Model 933 UV Analyzer


3. Enter or select the communications information:
Settings
Port
Select the COM port on the computer used to communicate
with the analyzer.

For more information about selecting a port, refer to the


“Digital Communication” in Chapter 3.

If you need to set up the analyzer to communicate via the Remote


 Service Port, configure the settings on the Device Communication
NOTE tab first, then return to this dialog box and select RS-485 Port.

If you need to set up the analyzer to communicate via the Remote Service
Port, configure the settings on the Device Communication tab first, then
return to this dialog box and select RS-485 Port.

Baud Rate
Baud rate at which data will be transferred. The baud rate is
fixed at 9600.

Port Type
Select RS-232 if using the analyzer’s local service port.

Select RS-485 if using the analyzer’s remote service port.


Configure the RS-485 port in the Device Communication tab
before selecting RS-485 here.

Address
If the RS-485 port is selected, enter the communications ad-
dress of the analyzer. If using multiple analyzers, be sure to
enter a different address for each unit.

4. Click OK to initialize communication with the analyzer. The software


will revert back to the M933 Properties dialog box and the analyzer
will be Online, as indicated in the Status message box.

If the computer cannot establish communication with the analyzer,


 refer to “Configurator Software Troubleshooting” in Chapter 3 for
NOTE information about how to correct the problem.

5. View the Status tab. Live data should begin updating within 10 sec-
onds.

Controller / User Interface | 4-9


Device Communication Tab
The Device Communication tab (Figure 4-3) contains the setup param-
eters specifically for the RS-485 Remote Service Port for the Model 933
Analyzer. If you need to set up the analyzer to communicate via the
Remote Service Port, configure the settings on this tab first, then return to
the Serial Port Configuration dialog box and select RS-485 Port.

Baud Rate This is the baud rate at which data will be transferred.
The baud is fixed at 9600.

RS-485 Address Enter the communications address of the analyzer. If


using multiple analyzers, be sure to enter a different
address for each unit.

Figure 4-3.
Device
Communication tab.

To set up the Remote Service Port (RS-485) communication parameters:

1. Ensure the device is Online. To check this, view the Status of the
system from the General tab: it should read “Online” (the Device
Enabled and Live Data check boxes must be enabled).

2. View the Device Communication tab and enter an address (a number


between 0 and 239) for the analyzer in the RS-485 Address text box.
You can either type a number in this box or use the arrows to select
one.

3. The baud rate defaults to 9600. There are no other options.

4. Click Apply. The software will prompt: “Would you like to save the
settings to EEPROM?”. Click Yes for the changes to take effect.

4-10 | Model 933 UV Analyzer


5. Return to the General tab and click Setup to display the Serial Port
Configuration dialog box again.

Note that the address you entered in the Address text box in the
Device Communication tab matches the Address setting on this
dialog box.

6. Click RS-485 Port to enable the Remote Service Port. Click OK to save
this change.

Check the Status of the system from the General tab again. It should
 now read “Online” if the communication port settings for both the
NOTE analyzer and the PC are correct.

7. If the error message “Communication Failure. Do you want to start


auto-detect?” appears click No then repeat Steps 2–7 and ensure the
proper settings are made.

User Interface
The software allows you to customize how data is viewed and to set up
your display. This is done from the main window (Figure 4-4).

Standard Toolbar
Custom Mode Toolbar
Data File Toolbar

Main Window

Figure 4-4.
Configurator Software
main window (Trend
mode display active). Status Bar

Controller / User Interface | 4-11


Setting Up Your Screen
Using the View menu, configure your screen by selecting the toolbars you
want displayed. If the option has a checkmark beside it, the toolbar is
active. To toggle these functions on/off, select the menu option again.
Toolbars that can be displayed on the Main Window (Figure 4-4) include:

• Standard Toolbar
Contains icons used most often including the main display modes.

• Custom Mode Toolbar


Contains icons that are used to create the Custom mode displays.

• Data File Toolbar


Contains icons relating to saving data files.

• Main Window
Displays the various mode windows used to view data. Also can
display the Devices & Log window, which is a system event log that
lists all devices and their status.

• Status Bar
Located at the bottom of the window, the Status Bar displays system
messages, including if the system is currently scanning.

View / Configure Analyzer Parameters and Data


The M933 Properties dialog box – which is your primary interface with
the analyzer – contains several tabs (screens of information) that allow
you to set up communications, view real-time and historical data, and
modify configuration and calibration parameters for the analyzer. When
the software is first started, this dialog box defaults to the General tab.
The descriptions of the parameters on this and other screens can be found
throughout this chapter.

The settings for your analyzer have been configured at the factory to
! meet specified customer requirements. Changing the factory-set
CAUTION configuration could cause the analyzer to operate incorrectly.

4-12 | Model 933 UV Analyzer


Viewing Device Activities
The Devices & Log window (Figure 4-5) displays the status of all analyz-
ers (devices), plus a system event log of all analyzer operations. This
window, which is displayed within the M933 Configurator main window
(Figure 4-4), can help you diagnose problems with the analyzer.

Figure 4-5.
Devices & Log
window.

To display the Devices & Log window:

1. From the View menu, select Devices & Log or click . A log is
displayed showing all active devices and their status.

 The system log is saved in a text file in the “Log” folder.


NOTE

2. From here you can view a log of all related activity for active devices
such as when scans were started or completed as well as any alarm
conditions. It also provides information on the data source for the
reading under the Source field (e.g., Dev1, or Device 1). The Status
field indicates the current status of the analyzer (e.g., Online). Demo
data can be used to simulate real data for testing purposes.

3. To remove the display, select View and then Devices & Log again or

click .

Controller / User Interface | 4-13


Saving Analyzer Configuration Parameters
The Configurator Software allows you to save current analyzer (device)
setup configuration parameters to a file that can be used later as a refer-
ence or to restore the parameters to their original settings (if they are
changed). This function is useful to create a backup copy of the analyzer
configuration parameter, or if you will be replacing the EEPROM.

If major changes are made to the analyzer configuration parameters, it


 is important to make a backup copy of these settings. This file can then
NOTE be used to restore all parameters to their original settings in the event
of an EEPROM failure.

To save configuration parameters:

1. Click the Save Configuration button from the General tab of the
M933 Properties dialog box. When you click Save Configuration, the
Save As dialog box will appear. Navigate to the Ametek\M933 folder
on the computer’s hard drive (AMETEK does not recommend saving
this file to another path).

2. Name the file and click Save. The file will be saved with a “.dev”
extension. This file can be used only by the Configurator Software.

4-14 | Model 933 UV Analyzer


Restoring Analyzer Configuration Parameters
The Configurator Software allows you to retrieve previously saved ana-
lyzer configuration parameters to restore the parameters to their original
settings. This function is useful if you wish to recover analyzer configura-
tion parameters if changes have been made that you do not wish to keep,
or to restore the settings after replacing the EEPROM. The configuration
parameters are stored in a “.dev” file on the computer.

To restore configuration parameters:

1. Click the Restore Configuration button from the General tab of the
M933 Properties dialog box. When you click Restore Configuration,
the Open dialog box will appear with a message box (“Preparing to
restore. Click OK to continue.”). Click OK if you wish to restore
configuration parameters.

2. Navigate to the location of the file (for example, C:\Ametek\M933),


select it, and click Open. To restore configuration parameters to the
analyzer you are communicating with, click YES to the prompt
“Would you like to save the settings EEPROM?”.

During the parameters restoration, the analyzer will temporarily go


OFFLINE. After the restoration is complete, the Name and Descrip-
tion will change to reflect those of the saved parameters.

Controller / User Interface | 4-15


Modifying Analyzer Device Settings

 Descriptions for the functions on the General tab can be found earlier
in this chapter, under “Starting the Configurator Software.”
NOTE

Working From the Setup Tab


The Setup tab (Figure 4-6) contains all functional parameters that control
the operation of the analyzer. These screens, which allow you to view all
information about the analyzer, are accessed by clicking the appropriate
Modify button.

The settings for your analyzer have been configured at the factory to
! meet specified customer requirements. Changing the factory-set
CAUTION configuration could cause the analyzer to operate incorrectly.

Figure 4-6.
Setup tab.

The Setup screens on this tab cannot be accessed unless communication


between the software and the analyzer has been established. If the
Modify (Setup) buttons on this tab are grayed out, check the status of the
system from the General tab. You will have to establish communication
with the analyzer before you can view or configure its parameters.

For all first-time analyzer setups, set up the analyzer from the M933
 Properties dialog box. From here, you must check the Device En-
NOTE
abled and Live Data text boxes to initiate communication. Then, you
must set up communication parameters by clicking the Setup button
from the General tab.

4-16 | Model 933 UV Analyzer


While changing parameters from individual Modify (Setup) Configura-
tion/Calibration dialog boxes, observe the following functions and rules:

• After changing any of the parameter values from any setup screen,
you must click the Apply button under the Setup tab to activate the
new settings. This will send the new parameters to the analyzer, but
will not save them to the analyzer’s EEPROM. The Configurator
Software will then prompt with “Would you like to save the settings
EEPROM?”. Click YES to save the new value(s) to the analyzer’s
EEPROM.

• You can change numerous parameter values in multiple setup screens


and dialog boxes before clicking Apply or saving the new value(s) to
the analyzer’s EEPROM.

• If you want the parameter changes to be valid only for the current
session, click NO when prompted with “Would you like to save the
settings EEPROM?”. The changes will revert to the previously saved
changes after the system is powered down and then powered up
again, or if the analyzer is reset.

Controller / User Interface | 4-17


Saving Analyzer Configuration Parameters to an ASCII File

When you select the Print to File button from the Setup tab, the Save As
dialog box appears (Figure 4-7). Select the path you wish to save the file
to, give the file a name, and then click Save. The software saves the
current analyzer configuration parameters to an ASCII file. Note that the
file will be saved with a “.dmp” extension.

Figure 4-7.
Save As dialog box
(Print to File button).

Printing Analyzer Configuration Parameters

When you select the Print button from the Setup tab, the Print dialog box
appears (Figure 4-8). Make sure a printer is connected to the PC or avail-
able through a network before printing these settings. Click OK to print a
hard copy of the current analyzer configuration parameters.

Figure 4-8.
Print dialog box (Print
button).

4-18 | Model 933 UV Analyzer


Refreshing Configuration Parameters

When you click the Refresh button from the Setup tab, the latest Calibra-
tion or Configuration changes made in the Configurator Software are
updated in the analyzer.

Saving Configuration Parameters to EEPROM

After changing any of the parameters or their values from any Setup
dialog box, click OK to exit the dialog box and return to the Setup tab (see
Figure 4-6). Then, click the Apply button at the bottom of the M933
Properties dialog box (under the Setup tab). The software will then
prompt “Would you like to save the settings to EEPROM?”. Click YES to
send the new value(s) to the analyzer and save them to EEPROM.

Controller / User Interface | 4-19


Setting Gas Calibration Parameters

The Gas Calibration dialog box (Figure 4-9) contains gas species informa-
tion and sampling system control parameters.

Figure 4-9.
Gas Calibration dialog
box.

Species
Displays the names of available, factory-set gas species/output set-
tings.

Span Conc
This is the concentration of the component (typically PPM) in the
calibration gas mixture. The concentration value must be entered
before initiating a calibrations sequence. The concentration is entered
in decimal notation. The maximum concentration which can be
entered is 999 999. If a calibration gas is not used, this value must be
set to zero. Concentrations are typically in PPM, but can be custom-
ized (refer to “Custom Output (Custom Setup),” later in this chapter.

SFactor
The Span (calibration) Factor for the calculated result (component
concentration) for each configured gas species. The analyzer’s Span
Factor is adjusted automatically whenever the analyzer is Spanned.

ZDriftSpec
At the end of every Auto-Zero or manual zero, the zero drift from the
previous Auto-Zero or manual zero result is calculated and displayed.
A “Warning Zero Drift” error message is displayed if the zero drift of
any species exceeds its Zero Drift Specification.

Span 1/Span 2/Span 3/Span 4 buttons


These buttons allow the user to manually span each individual gas
species. The analyzer span factors are adjusted automatically based on
the average reading during the Cal Int Time (sec) period after clicking
each Span button. The span gas must be introduced manually (see
Chapter 5), using the Flow Control selection “Zero”.

4-20 | Model 933 UV Analyzer


Flow Control

The analyzer gas flow control can operate in one of six “sampling”
modes. For normal operations, the analyzer is in the Auto mode.

Auto The analyzer is under automatic control. Sample gas is


continuously switched through Col A and Col B respec-
tively when the analyzer is operating normally. Upon
analyzer start-up and fault alarm condition, the flow
could be shut down automatically by the analyzer.

Col A The analyzer is under user control and sample is


continuously forced through Column A.

Col B The analyzer is under user control and sample is


continuously forced through Column B.

Sample The analyzer is under user control and sample is


continuously switched through Column A and Column
B respectively.

Shut-in The analyzer is under user control and no gas is al-


lowed to flow through the sampling system.

Zero The sampling system is continuously purged with zero


gas.

A-Z Interval (hr)


This timer controls the interval between timed Auto-Zero sequences.
The timer may be set to an interval from 0 to 999 hours in one-hour
increments (default is 24 hours). Setting the interval to zero turns the
timer off, disabling a timed start of the Auto-Zero sequence. The time
remaining until the next Auto-Zero (minutes) can be viewed in the
Analyzer Data tab.

A-Z Duration (min)


The Auto-Zero Duration is the amount of time that the zero solenoid
is active during an Auto Zero function. The time may be set from
0–255 minutes (default 4 minutes) in one-minute increments. Setting
the time to zero turns the timer off.

Cal Int Time (sec)


This timer sets the integration time (default 90 seconds) during which
the concentration reading for each of the species is averaged. The
timer may be set to a duration from 0–65535 seconds in one-second
increments. When the duration is set to zero, the timer defaults to a
30-second averaging time.

Controller / User Interface | 4-21


Auto Zero button
This button initiates an automatic Auto-Zero function that controls an
automatic adjustment of the analyzer zero. The zero gas solenoid is
turned on and off automatically during the sequence. The zero offset
is adjusted based on the average reading during the Cal Int Time at
the end of the Auto Zero Duration countdown.

An Auto-Zero sequence initiated on a timed basis or by a remote


 contact will not be executed if there is a fault alarm
NOTE

Zero button
This button permits a manual zeroing of the analyzer. The analyzer
zero is adjusted automatically based on the average reading during
the Calibration Integration time period. The zero gas must be intro-
duced manually (see Chapter 5), using the Flow Control command
(Zero).

Cancel Cal button


When a calibration (Manual Zero, Auto Zero, Span) is in progress,
clicking this button will stop it.

4-22 | Model 933 UV Analyzer


Modbus Settings

The Modbus dialog (Figure 4-10) box contains operational parameters for
the Customer Data Acquisition port.

A few parameters need to be set up using the Configurator Software to


enable the Modbus port. Select the Setup tab of the M933 Properties
dialog box and click Modbus.

Figure 4-10.
Modbus dialog box.

Provide the following information:

Address
Enter the Modbus network address assigned to the analyzer.

Baud Rate
Select the baud rate of the Modbus network.

Stop Bits
Select the number of stop bits of the Modbus network.

Parity
Select the parity of the Modbus network.

Controller / User Interface | 4-23


Temperature Control

The Temperature Control dialog box (Figure 4-11) contains temperature


control parameters for the two temperature-controlled zones: (Optical)
Bench and Column (Block).

The Measuring Cell temperature-controlled zone is not used with the


 Model 933 Analyzer. This temperature-controlled zone is typically
NOTE reserved for other variations of this analyzer.

Figure 4-11.
Temperature Control
dialog box.

Bench
The measure range (°C) for the Optical Bench. For more information,
refer to “Optical Bench” following these descriptions.

Cell
The measure range (°C) for the Measuring Cell. For more information,
refer to “Measuring Cell” following these descriptions.

Column
The parameters for the Column Block. For more information, refer to
“Column Block” following these descriptions.

Range
The measure range (°C) for each temperature zone.

Setpoint (°C)
The control setpoint (°C) for each temperature-controlled zone.

Because the Model 933 Analyzer only monitors (it does not control)
the temperature of the Measuring Cell, the Measuring Cell setpoint
should be set to zero (0).

Kp (band)
The proportional term of the PI temperature control algorithm for
each zone.

4-24 | Model 933 UV Analyzer


Ti (sec)
The integral term of the PI temperature control algorithm for each
zone.

Start-up (%)
The duty cycle used on start-up for each temperature-controlled zone.

Too Cold (°C)


Too Cold is an alarm temperature setpoint. If the current temperature
falls below Too Cold, it will cause the analyzer to default to an alarm
state.

Too Hot (°C)


Too Hot is an alarm temperature setpoint. If the current temperature
exceeds the Too Hot, it will cause the analyzer to default to an alarm
state.

Optical Bench

The Optical Bench temperature is controlled to maintain a stable condition


for the analysis of the target species and to ensure that no condensation
forms to obscure the light path of the analyzer. Control is accomplished by
using an RTD and heater embedded in the Optical Bench Assembly.

The Optical Bench temperature control is protected by an independent


over-temperature circuit with a trip temperature of 65 °C. The default
temperature setpoint for the Optical Bench is typically 40 °C but can be
modified through the Configurator Software. The setpoint should be
approximately 5 °C to 10 °C above the maximum ambient temperature, to a
maximum of 60 °C. If the temperature of the Optical Bench falls below the
Too Cold setpoint or exceeds the Too Hot setpoint, the Host Controller will
set the analyzer in a Fault situation.

The Optical Bench can be configured to measure in two different ranges


(see the “Optical Bench Temperature Range, JP301” configuration, below).
The ranges are selectable via a jumper on the Micro-Interface board (see
“Installing the Optical Bench Assembly” in Chapter 3) and changes in the
software. When the temperature of the Optical Bench is changed through
the software, jumpers on the Micro-Interface board must be changed
according to the “Optical Bench Temperature Range, JP301” configuration.

Optical Bench Temperature Range, JP301


(Micro-Interface Board)
Range Jumper Position Temperature Range

A (default) 2-3 31 °C to 47 °C

B 1-2 45 °C to 62 °C

Controller / User Interface | 4-25


Measuring Cell

The Measuring Cell operating temperature parameter is monitored and


used to calculate the analyzer results. The control option is currently not
available for the Model 933 Analyzer. The setpoint for the Measuring Cell
temperature control must be set to zero (0). If the Measuring Cell tem-
perature falls below the Too Cold setpoint or exceeds the Too Hot setpoint,
the Host Controller will generate a warning status (“Warning Cell Temp”
alarm error message will be displayed in the software).

The Measuring Cell can be configured to measure in four different ranges


(see “Measuring Cell Temperature Range, JP300” configuration). The
ranges are selectable via a jumper on the Micro-Interface board (see
“Installing the Optical Bench Assembly” in Chapter 3) and changes in the
software. When the temperature measuring range of the Measuring Cell
is changed through the software, jumpers on the Micro-Interface board
must be changed according to the “Measuring Cell Temperature Range,
JP300” configuration.

Measuring Cell Temperature Range, JP300


(Micro-Interface Board)
Range Jumper Position Temperature Range

A (default) 1-2 -3 °C to 66 °C
B 3-4 60 °C to 131 °C
C 5-6 121 °C to 194 °C
D 7-8 186 °C to 261 °C

Column Block

The Column Block temperature is controlled so that it maintains consis-


tent elution time. Control is accomplished using an RTD and heater
embedded in the Column Block. The Column Block temperature control is
protected by an independent over-temperature circuit, with a trip tem-
perature of 65 °C. The default temperature setpoint for the Column Block
is typically set at 40 °C but can be increased to a maximum of 50 °C
through the Configurator Software to allow for a higher ambient temperature.
AMETEK recommends that the setpoint be at maximum ambient temperature
or 40 °C, whichever is higher, but not more than 50 °C. If the temperature of
the Column Block falls below the Too Cold setpoint or exceeds the Too Hot
setpoint, the analyzer Host Controller will send the analyzer into a fault situa-
tion. The Column Block temperature measuring range is from 0 °C–120 °C.

4-26 | Model 933 UV Analyzer


Output Setup

The Output Setup dialog box (Figure 4-12) contains Current and Voltage
output assignments plus concentration alarms and setting parameters.

Figure 4-12.
Output Setup dialog
box.

There are four independent isolated 4 to 20 mADC outputs (see the


Customer I/O Board drawing under “Start-Up and Verification” in Chap-
ter 3). One self-powered output is standard. The other three outputs
(optional) can be either self-powered or loop-powered. The user must
provide the loop supply for the loop-powered output. There are also four
1 to 5 VDC outputs (see the Customer I/O Board drawing in Chapter 3).
The default signal assignment is configured to meet the specifications of
the end user. If either the current or voltage output assignments need to
be changed, click the drop-down arrow beside the output and select a
different assignment.

In addition to the usual capability of zeroing and spanning the V/I and
Voltage Outputs, you can also set them to a mid-scale level for diagnostic
purposes. The low end of each analog output range can be a nonzero
value.

Iout
Iout Assignment
Current output assignment with and without Track and Hold
(T&H).

Iout Low Scale


Current Low Scale point corresponding to 4 mADC.

Iout High Scale


Current High Scale point corresponding to 20 mADC.

Controller / User Interface | 4-27


Iout Zero (mA)
The measured current (mA) in the current output loop when the
output is set to zero during the calibration procedure.

Iout Span (mA)


The measured full-scale current (mA) in the current output loop
when output is set to full-scale during the calibration procedure.

Vout
Vout Assignment
Voltage output assignment with and without Track and Hold
(T&H).

Vout Low Scale


Voltage Low Scale point corresponding to 1 VDC.

Vout High Scale


Voltage High Scale point corresponding to 5 VDC.

Vout Zero
The measured voltage output when the analog output is set to
zero during the calibration procedure for a voltage output.

Vout Span
The measured voltage output when the analog output is set to
full-scale during the calibration procedure for a voltage output.

V/I Low Limit 4 mA check box

Checked The actual output clamps the result at 4 mA;


the output cannot go below this value.
Not Checked The output can go below 4 mA.

Normal button
Once analog output calibration is complete, this button will allow the
outputs to go back to normal operation.

Mid-Scale button
Places the outputs to mid scale.

Zero Cal button


Places the outputs to zero.

Span Cal button


Places the outputs to full-scale span.

4-28 | Model 933 UV Analyzer


Alarm 1 / 2

Alarm Enable button


This will enable concentration alarm.

Alarm Disable button


This will disable concentration alarm.

Toggling between Alarm Disable and Alarm Enable will clear the
 latched alarms.
NOTE

Conc. Assn.
Concentration alarm assignments.

Conc. On
This alarm will activate when the output value exceeds the Con-
centration On setpoint.

Conc. Off
This alarm will deactivate when the output value falls below the
Concentration Off setpoint.

Conc. Delay
The alarm activation will be delayed by the amount of time en-
tered in the Concentration Delay text field after the concentration
output has exceeded the Conc. On setpoint.

Conc. Latch (Alarm 1, Alarm 2)

Checked The activated alarm will not clear (latch)


until the user intervenes.
Not Checked The alarm will automatically return to the
non-alarm state once the concentration falls
below the Concentration Off value.

Controller / User Interface | 4-29


Analyzer Information

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

The Info dialog box (Figure 4-13) contains Microcontroller and Host
Controller information.

Figure 4-13.
Information dialog
box.

Host Version
Host Controller version number.

Micro Version
Microcontroller version number.

Serial #
Analyzer serial number.

EEPROM Writes
This indicates the number of times that data has been saved on the
EEPROM. The maximum number of saves that an EEPROM will allow
is 20,000. After this point, the EEPROM will need to be replaced (refer
to “EEPROM Replacement” in Chapter 6).

Reset M933
Resets the analyzer’s Host Controller board.

4-30 | Model 933 UV Analyzer


Optical Bench

The Optical Bench dialog box (Figure 4-14) allows optical bench control
and data acquisition parameters to be viewed and modified.

Figure 4-14.
Optical Bench dialog
box.

These parameters should only be modified by a trained technician.


!
CAUTION

Base (mV)
The minimum operating current control setpoint for each source lamp.

FltrPulse (mV)
Filter Pulse is the source lamp pulse current control signal for each
filter. The normal operating range is between base setting and Lamp
Max, with the control signal for the key filter being Lamp Max. If the
filter position is not used, the Filter Pulse value must be set to a
negative number. The recommended value is negative base setpoint.

Tzero
Transmittance Zero is the PMT signal transmittance value of the filters
with zero gas in the sampling system. It is adjusted automatically
whenever the analyzer is zeroed.

ALC SetPt (mV)


The Automatic Lamp Control (ALC) Setpoint is obtained from the
reference PMT for each filter after an Auto-Setup function is complete.
These values are updated automatically by an Auto-Setup function.

ALC On check box


ALC (Automatic Lamp Control) automatically becomes active at the
completion of an Auto-Setup function.

Checked The ALC is active.


Not Checked The ALC is disabled.

Controller / User Interface | 4-31


Lamp Conserve Mode check box
The lamps are not pulsed during the time period between a column
switch and 2 seconds before the first concentration output is tracked.
The default and recommended setting is the deactivated state.

Checked Lamp Conserve Mode is active.


Not Checked Lamp Conserve Mode is disabled.

Bench Type
The bench type code defines the Optical Bench orientation and the
filter positions assigned to each source lamp. The code is the decimal
equivalent of an 8 bit binary number. The definition for each bit is
shown below under “Bench Orientation,” “Filter Position Assign-
ment,” and “Standard Bench-Type Code.”

Bench Orientation
B0 Measure PMT Reference PMT

0 PMT 1 PMT 2
1 PMT 2 PMT 1

Filter Position Assignment (B3, B2,


B1)*
B3 B2 B1 Lamp 1 (Cd) Lamp 2 (Cu)

0 0 0 1 3 5 4 6 2
0 0 1 3 5 4 6 1 2
0 1 0 1 3 4 5 6 2
0 1 1 1 3 2 Motorless
1 0 0 1 3 5 4 6 1
* B7, B6, B5, and B4 are reserved for future use.

Standard Bench-Type Code (8)*


Code B3 (8) B2 (4) B1 (2) B0 (1)

8 1 0 0 0
* Values in brackets beside number is its decimal weighting.

Samples
This indicates the number of times the PMT signal is measured while a
filter is completely within the light path.

Delay
The time interval between when the filter becomes completely within
the light path and the first PMT signal measurement. The interval is
shown as multiples of 1.6 microseconds (µs).

4-32 | Model 933 UV Analyzer


Sigma
This is the adaptive filtering algorithm constant (default is 0.00025)
and should not be adjusted.

MaxT90 (sec)
Maximum T90 is the time (default is 60 seconds) required for the
output signal to reach 90 percent of the final value after a step change
in the concentration. Larger values reduce the noise level on the
output signal but, at the same time, increase the response time. Ad-
justing from default is not recommended.

Key Filter
Key Filter is the position of the filter which gives the weakest signal
for a given source lamp current.

PMT Level (mV)


PMT Level is a gain control signal, which is based on the signal from
the PMT when the key filter is in the light path.

PMT Balance (mV)


PMT Balance is a secondary control signal, which adjusts the PMT
gains to equalize the signals from the PMT when the filters with the
lowest and highest transmittances are in the light path.

Lamp Max (mV)


Lamp Maximum is the voltage to which the lamp pulse current
control-signal for the key filter location is set during the Auto-Setup
function. The default value is 7000 mV.

Signal Max (mV)


The Auto-Setup function uses this value as a target to adjust the PMT
gains so that either the reference or measure PMT signal for each filter
location attains that value.

Auto-Setup button
The Automatic-Setup function optimizes the PMT gains and source
lamp currents. This function combines automatic signal adjustment
with manual jumper positioning and should be executed after any
lamps, filters, or PMTs have been installed or replaced. The process
requires approximately three minutes. To determine when an Auto-
Setup is needed, refer to Chapter 6.

Cancel Auto-Setup button


Click this button and the Auto-Setup function will be cancelled.

Controller / User Interface | 4-33


Matrix

The Matrix dialog box (Figure 4-15) contains information that is respon-
sible for partially calculating the concentration output and negating the
effects of cross talk by interfering gas species.

These parameters should only be modified by a trained technician on


! advice from the factory.
CAUTION

Figure 4-15.
Matrix dialog box.

Species
This designates which gas species are currently configured.

Row/Filter
The value in each row (Row 1–6) and each column (Filter 1–6) in the
calculation matrix.

4-34 | Model 933 UV Analyzer


Column Timing

The Column Timing dialog box (Figure 4-16) contains column operational
parameters.

Figure 4-16.
Column Timing dialog
box.

Switch Interval (sec)


This is the time in seconds (3–1200 seconds) between column switches.

Species
These are the gas species that are currently configured for the ana-
lyzer.

Hold Time (sec)


Hold Time (seconds) is a user-adjustable parameter in which the
output is held after column switching occurs. This will allow the
output signal to appear steady. The time must be between 0 (zero)
seconds and the column switch time.

Controller / User Interface | 4-35


Compensation Parameters

The Compensations dialog box (Figure 4-17) contains compensation


parameters used in calculating the concentration. They account for tem-
perature, pressure, compressibility, and other variations that affect the
concentration reading computed by the analyzer.

Figure 4-17.
Compensations dialog
box.

These parameters should only be modified by a trained technician on


! advice from the factory.
CAUTION

Abs Offset
The absorbance offset vector for each filter location.

Gas 3 to Gas 1 Comp


Effects of Gas 3 on Gas 1 are mathematically negated. For standard
Model 933 Analyzer, Gas 3 is MeSH and Gas 1 is H2S. Gas 2 is COS.

Gas 3 to Gas 2 Comp


Effects of Gas 3 on Gas 2 are mathematically negated. For standard
Model 933 Analyzer, Gas 3 is MeSH and Gas 1 is H2S. Gas 2 is COS.

Compressibility
In addition to pressure and temperature compensations of the concen-
trations according to the ideal gas law, it is possible to enter an addi-
tional parameter, Z to account for the compressibility factor of the
sample gas. One value of Z is used for all species. The default value for
this parameter is 1, but can be any value between 0.5 and 1.5. The
correction is applied to the concentrations in the following manner:

<Conc>corr. = <Conc>uncorr. / Z

Cell Length (cm)


The axial length of the Measuring Cell gas space (cm).

4-36 | Model 933 UV Analyzer


Cell Temp. Default
The default temperature for the Measuring Cell (°C or °F). This value is
used in place of the measured Measuring Cell temperature when
measured temperature compensation is disabled.

Fixed The analyzer will refer to the default value.

Measured The analyzer will actively measure the temperature


reading.

Cell Pressure (optional)

Fixed The analyzer will refer to the default value.

Measured The analyzer will actively measure the absolute


pressure reading. Refer to “Cell Pressure JP301 and
JP302 Customer I/O Board,” below, for jumper
selectable pressure ranges.

Default
The default absolute pressure for the Measuring Cell (mmHg or
"Hg). This value is used in place of the measured Measuring Cell
pressure when active pressure compensation is disabled.

LowScale
The pressure transducer low value (mmHg or "Hg) corresponding
to 0.0 VDC. See “Cell Pressure JP301 and JP302 Customer I/O
Board” below.

HighScale
The pressure transducer high value (mmHg or "Hg) corresponding
to 5.0 VDC. See “Cell Pressure JP301 and JP302 Customer I/O
Board” below.

Cell Pressure JP301 and JP302 Customer I/O Board


Pressure Range JP301 JP302

0–5171.49 mmHg (0–100 PSIA) A A


0–1706.59 mmHg (0–33 PSIA) A B
1706.59–3413.19 mmHg (33–66 PSIA) B B
3413.19–5171.49 mmHg (66–100 PSIA) C B

Controller / User Interface | 4-37


Advanced Options

The Advanced Options dialog box (Figure 4-18) contains Auto-Zero


ReCheck Timer control parameters.

Figure 4-18.
Advanced Options
dialog box.

Startup Auto-Zero ReCheck (min)


When the Startup Auto-Zero Re-Check interval has a non-zero
positive value, the feature is enabled.

At recheck interval minutes from the start of the first Auto-Zero, another
Auto-Zero is performed and the drift-over-time value for each species
is computed. If one of the drift-over-time values is above its allowable
specified value, the Startup Auto-Zero ReCheck process is repeated
for up to four more times.

A maximum of five Auto-Zeros will be performed at the time interval


 entered in the Startup Auto-Zero ReCheck text field.
NOTE
For example, if the value entered is 60 minutes, an Auto-Zero will be
performed every 60 minutes to a maximum of five Auto-Zeros.

If all drift-over-time values are within their specified values or the


Auto-Zero ReCheck has been performed five times, the normal Auto-
Zero operation begins with the first one occurring at Auto-Zero
interval hours from the end of the last Startup Auto-Zero Re-Check.

Fault Relay Latching check box

Checked The activated fault alarm relay will latch


(will not clear) until the user disables the
Fault alarm by unchecking this check box.
Not Checked The relay will automatically return to its
non-alarm state once the fault condition has
been corrected.

4-38 | Model 933 UV Analyzer


Custom Output (Custom Setup)

The Custom Output dialog box (Figure 4-19) contains units information
and configuration parameters for custom setup.

Figure 4-19.
Custom Output dialog
box.

Conversion Factors
These are the units of measurement used for gas species concentra-
tions (PPMV is equal to 1). The analyzer always computes the concen-
tration in PPMV. To have the analyzer output concentration values in
other units, a conversion factor is required. See “Conversion Factors in
Custom Setup.”

The concentration result, the drift specification, the span concentra-


 tion and the alarm threshold of a species must be in the same unit of
NOTE measurement.

Conversion Factors in Custom Setup


Conversion from ppm to mg/Nm^3 Conversion from mg/Nm^3 to ppm

H2S: 1.416581 mg/Nm^3 per ppm H2S: 0.705925 ppm per mg/Nm^3

COS: 2.49747 mg/Nm^3 per ppm COS: 0.400405 ppm per mg/Nm^3

MeSH: 1.999695 mg/Nm^3 per ppm MeSH: 0.500076 ppm per mg/Nm^3

The coefficients listed in “Conversion Factors in Custom Setup” have


been calculated based on a 20 °C and 1 atmosphere standard. Conver-
sion numbers for 25 °C, 15 °C, 0 °C, or any other temperature and
pressure are available upon request.

Custom Results
Custom Result is the weighted sum of the first four species. A multipli-
cation factor is applied to each concentration before it is summed with
the next concentration.

For Example: Custom Result = Sum of the sulphur species


1 * H2S + 1 * COS + 1 * MeSH

Controller / User Interface | 4-39


Status Tab
The Status tab (Figure 4-20) displays live species concentration values.
Any Microcontroller or Host Controller error conditions can be viewed in
this tab.

Figure 4-20.
Status tab.

Status
This will indicate the communication status between the Configurator
and the Model 933 Analyzer (i.e., Online or DEMO).

Error Condition
There are two categories of alarm errors, Warning and Fault. Active
Warning and Fault errors are annunciated in the Error Condition list.

Warning errors indicate that the analyzer may require servicing.


Warning errors are also indicated by the Warning relay being de-
energized. However, the Warning relay can also be de-energized
during Auto-Zero, manual Zero, and other calibrations.

Fault errors indicate that a fault has occurred and the analyzer data
are not valid. Fault errors are also indicated by the Fault relay being
de-energized.

See Chapter 6 for a listing of the various warnings and faults and the
corrective actions.

Host Runtime
This indicates the amount of time the Host Controller has been opera-
tional.

Micro Runtime
This indicates the amount of time the Microcontroller has been opera-
tional.

4-40 | Model 933 UV Analyzer


Micro Wheel Speed
This shows the current Optical Bench filter wheel speed in rotation
per minute (RPM).

Micro State
This displays messages that indicate which step of the Auto-Setup
function is currently being performed:

• Setup - Prelim PMT Level


• Setup - Prelim Lamp Pulses
• Setup - PMT Balance
• Setup - Final PMT Level
• Setup - Final Lamp Pulse
• Setup - ALC
• Setup - Off/Completed

Host State
This displays messages that indicate the current operational status of
the analyzer:

Start-up shut-in/off The analyzer has shut off the flow of sample
gas through the sampling system during its
start-up sequence.
Start-up time delay This delay period, activated at analyzer
power-up or reset, allows time for the
analyzer to stabilize prior to operation. This
parameter is not user-adjustable.
Operational The analyzer is operating normally (sam-
pling gas).
Alarm clearing The analyzer is clearing an alarm after the
alarm has been corrected.
Calculated Results
The gas species, or parameters, calculated by the analyzer are dis-
played. The name of the result and its value will be displayed and
updated at one-second intervals. The custom parameter is a combina-
tion of calculated results (refer to “Custom Output (Custom Setup),”
earlier in this chapter).

Controller / User Interface | 4-41


Optical Bench Data Tab
The Optical Bench tab (Figure 4-21) displays live data from the Model 933
Optical Bench. To access the Optical Bench tab, select Edit from the main
menu and click Device Properties, and then click Optical Bench.

Figure 4-21.
Optical Bench Data
tab.

Transmittance
Displays the transmittance for each filter location.

PMT Measure (V)


Displays the signal from the measuring PMT for each filter location.

PMT Reference (V)


Displays the signal from the reference PMT for each filter location.

Absorbance
The absorbance for each filter location.

ALC Lamp Pulse (mV)


The current lamp pulse control for each filter location.

4-42 | Model 933 UV Analyzer


Analyzer Data Tab
The Analyzer Data tab (Figure 4-22) will display live data from the Model
933 Analyzer. To access the Analyzer Data tab, select Edit from the main
menu and click on Device Properties and then click Analyzer Data.

Figure 4-22.
Analyzer Data tab.

Concentration
This designates which gas species are currently configured and their
current values.
Analog Output Concentration Values
V-Output
The concentration value at each analog voltage output channel.
I-Output
The concentration value at each analog current output channel.
Timing
Next Auto-Zero (min)
The amount of time until the next Auto-Zero starts. Minus 1 (-1)
indicates timed Auto-Zero disabled.
Cal Ends (sec)
The amount of time left in the Calibration Integration Timer (see
Cal Int Time). Minus 1 (-1) indicates no gas calibration in progress.
Next Col Switch (sec)
The amount of time left until the regenerating column and absorb-
ing columns switch. Minus 1 (-1) indicates column switching
deactivated.
Temperature Zone
Temperature (°C)
The real time operating temperature for each temperature-con-
trolled zone (Bench/Cell/Column).
Duty Cycle (%)
The real time duty cycle of each temperature-controlled zone
(Bench/Cell/Column).

Controller / User Interface | 4-43


Scaled Analog Input
The analog input or scaled parameter.
Bench Temp (°C)
Displays the real time bench temperature.
Cell Temp (°C)
Displays the real time Measuring Cell temperature or the default.
Column Temp (°C)
Displays the real time column temperature.
Cell Pressure (mmHg)
Displays the real time Measuring Cell pressure (optional) or the
default.
Digital IO (input/output)
Digital In
The Model 933 Analyzer has two digital inputs (J101, Customer I/O
board), each of which is designed to accept a contact closure. Input
1 is used for the remote start of the Auto-Zero sequence. Input 2 is
used to enable or clear alarms. Close the contact to enable Concen-
tration 1 and Concentration 2 alarms. Toggle the contact to clear
any latched alarm. The contact must remain closed for at least 1
second. Refer to the Customer I/O board in the section “Start-Up
and Verification” in Chapter 3.
The digital inputs are isolated from the digital logic power supply
of the analyzer. The isolation can be analyzer-powered or cus-
tomer-powered. The selection is made through JP401 on the
Customer I/O board, as defined in “Digital Input Isolation Power
Supply.”

Digital Input Isolation Power Supply


Power Supply JP401 Position

Customer +15V to +24V 2-3 (default)

Analyzer +24V 1-2

Solenoid
This will indicate which solenoid (Zero, Column A, Column B) is
currently energized, if any.
Alarm
This will indicate which, if any alarms are currently active.

4-44 | Model 933 UV Analyzer


Scanning Data
This section contains information on how to scan data and how to link
data from a different display. Data that is scanned on the Model 933
Analyzer can be displayed on the screen in any of five formats or modes
based on your application. See Appendix A for detailed information on
setting up modes and defining their parameters.

A configuration file has been included with the Configurator Soft-


 ware.
NOTE

From the File menu, select Open Configuration to open the


DataLogSetup.dyc file. This should be in the same directory in which the
Configurator Software has been installed. This configuration file sets up
the screen to view the:
• Trend graph of real-time concentration
• Track and hold concentration
• Measure and reference PMT signals
• Analog inputs

Once the file is opened, click on the Standard Toolbar to start data
scanning.

Display Modes
• Meter Mode
Meter-type format. Alarms can be displayed to view current reading
relative to high- and low-alarm limits.
• Annunciator Mode
Track whether a measured parameter is within acceptable user-de-
fined limits using a simple color/text indication.
• Trend Mode
View trends of measured parameters.
• Tabular Mode
View information in a textual, table-type format.
• Custom Mode
Create custom setups to include a single mode display window or
multiple mode display windows.

Controller / User Interface | 4-45


Defining Scan Settings
Define the type of information you want to gather from the selected
device.

Right-click on the display window for the device you have selected
(Figure 4-23) and then click Scan from the context menu. The Trend
Properties dialog box appears with the Scan tab active (Figure 4-24).

For Trend and Tabular modes, you must first select a channel before
 you can define scan settings.
NOTE

Figure 4-23.
Mode context menu.

Figure 4-24.
Scan tab.

Data Source
Select the device from which to scan or temporarily disable the scan-
ning device.

Disabled
Select this option to disable the display of the selected channel.

Device
Select this option and use its list box to select the device from
which to scan.

4-46 | Model 933 UV Analyzer


Link from
Data can be linked from one window into another. This can save
scanning time since the system only needs to scan the data one
time. To do this:

1. Select the display window that will receive the linked data
from another data source.

2. Right-click over the display window and then click Scan from
the context menu that appears.

3. From the Data Source group, select the Link from button.

4. Select the data source to link from using the Link from list box.

 You cannot link data into a Bar mode window.


NOTE

Starting a Scan

To start a scan, click or select Scan from the Control menu. The
message “Scanning” and the scanning progress will appear in the Status
Bar at the bottom of the window (if it has been enabled).

If you have scheduled scans at timed intervals and the system has fin-
ished a scan and is waiting to start the next scan, the time remaining
before the start of the next scan is displayed.

“Idle” is displayed in the Status Bar when the system is not scanning.

Stopping a Scan

Click or select Scan from the Control menu to toggle off the scan.

Controller / User Interface | 4-47


Scheduling Scans

From the Control menu, select Schedule or click on the Standard


Toolbar to view the Schedule dialog box (Figure 4-25).

Figure 4-25.
Schedule scans dialog
box.

Single Scan radio button


Select this to command the software to run a single scan when you

click . The system will stop scanning after one scan.

Continuous radio button


Select this to command the software to run scans at timed intervals

when you click .

Scan Interval text field


Type a number to specify the time delay between scans. The unit this
number represents depends on whether the scans were scheduled
using seconds or minutes as the time interval.

Seconds Select this option to use seconds as the


interval between successive scans, as de-
fined by the number specified in the Scan
Interval text field.

Minutes Select this option to use minutes as the


interval between successive scans, as de-
fined by the number specified in the Scan
Interval text field.

4-48 | Model 933 UV Analyzer


Working with Data Files

Saving Data Files


Displayed information can be saved for later viewing or printing. Each
data record within a data file contains scan data from the display
window(s). Data records are created in serial format, as the data becomes
available from the system. A Custom mode, for example, will save each
display as a data record.

1. Select the display window or windows for which data will be saved.

• Hold down the shift key and click on each window to be included
when selecting multiple display windows.

• Selecting a highlighted display window deselects the display


window.

• If no display window is selected, the software saves data for all


display windows in the mode.

2. From the File menu, select Save Data or click on the Data File
Toolbar to view the Save As dialog box (Figure 4-26). From here, you
can specify data file attributes.

Figure 4-26.
Save As dialog box.

3. Once the attributes are set, enter a name for the data file in the File
name text field and save it in a folder using standard Windows tech-
niques. Select the following (as required):

Save Now radio button


Prompts the system to save the most recent scanned data and then
stop scanning. If there are multiple Trend modes within a Custom
mode setup, only one can be selected for which to save data.

Controller / User Interface | 4-49


Start Saving radio button
Prompts the system to start saving data with the next scan and to
continue saving data files.

When File Full


Chooses how to handle cases in which the data file becomes
greater than 1 megabyte. A disk icon appears in the windows that
are selected to have data saved.

Stop radio button


Stops scanning when the file is full.

Start new file radio button


Save the data to a new file. The system automatically appends
consecutively numbered digits at the end of each new file it
creates so it is easier to follow the order in which the files were
created. Each file will be one megabyte in size so the data can be
copied to a disk.

4. To stop saving data, select Stop Saving from the File menu or click

on the Data File Toolbar.

Opening Data Files

1. From the File menu, select Open Data or click on the Data File
Toolbar.

2. Navigate to the location of the data file and select it.

3. Select Open. The data file appears on the screen. From here it can
either be viewed or printed.

Scrolling Through Data Records


From the File menu, select Data File Position or use the Data File Toolbar
to scroll forward and backward through the data file using the standard
recording symbols such as rewind or fast forward.

4-50 | Model 933 UV Analyzer


Converting Data Files
Use this utility to convert the analyzer Configurator Software data files
into ASCII text.

1. From the File menu, select Convert Data File and select one or more
data files.

2. Click Convert to convert and save the file with a CSV extension.

Printing Data
The Configurator Software will print scanning information in a format
similar to how it is displayed on the screen using the display parameters
created for that mode. You can view a preview of what will be printed by
selecting Print Preview from the File menu.

In Custom mode, the system prints the currently selected display win-
dow. If you do not select a display window, the system prints information
for each display window using the required number of pages.

To print data:

1. Select the display window(s) to be printed. If a window is not selected,


the entire screen will be printed. To select multiple windows, hold
down the shift key while selecting each window.

2. From the File menu, select Print or click .

3. Type a print-header comment in the Display Print dialog box. This


information appears in the title of the printed pages. Click OK.

4. If you select Print from the File menu, a standard Windows Print
dialog box appears. Set the additional print information.

5. Click OK to print the scanning information.

Controller / User Interface | 4-51


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4-52 | Model 933 UV Analyzer


CALIBRATION

Before proceeding to connect a device or power up a computer in a


! hazardous area, test the area around the analyzer for hazardous gases
WARNING
and proceed only when the area is found to be safe.

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

Manual Span Gas Calibration


The Gas Calibration dialog box (Figure 5-1) contains gas species informa-
tion and sampling system control parameters. For more information on
setting up parameters, see the section on “Gas Calibration” in Chapter 4.

Figure 5-1.
Gas Calibration dialog
box.

Calibration | 5-1
To perform a span gas calibration follow these steps:

1. Perform an Auto Zero function on the analyzer to automatically adjust


the analyzer zero. To initiate the auto-zero function, click the Auto
Zero button. The zero gas solenoid is turned on and off automatically
during the sequence. The zero offset is adjusted based on the average
reading during the Cal Int Time at the end of the Auto Zero duration
(A-Z Duration) countdown.

2. Once the Auto Zero process is completed, turn off the zero gas.

3. Remove the Swagelok plug from the span gas connection inlet and
connect the span gas. See Figure 5-2.

PROCESS INSTRUMENTS

CAUTION:
RISK OF ELECTRIC SHOCK

ATTENTION:
CONSULT USER MANUAL

0344

PROCESS INSTRUMENTS II 2 G

Western Research Model 933 Analyzer


Certificate No: KEMA 02ATEX2247, EEx d IIB T3 (T amb. 0°C...50°C)
Year. _______
Serial No. __________________

Caution
Do not open when an explosive gas atmosphere is present.

Power Dissipation Input


<210W 120VAC 50/60Hz 2A max.
<210W 240VAC 50/60Hz 1A max.

SERIAL COMMUNICATIONS PORT


DO NOT OPEN IF A HAZARDOUS
GAS ATMOSPHERE IS PRESENT

MAY NOT BE EXACTLY AS SHOWN

Figure 5-2.
Span gas and zero
gas inlet locations
(Europe).

5-2 | Model 933 UV Analyzer


4. Adjust the span gas regulator to between 80 and 90 PSIG.

5. From the Flow Control list, select “Zero.” Click OK on the Gas Cali-
bration dialog box and then click Apply on the Setup tab. Click NO
when prompted to save parameters to EEPROM.

6. Adjust the span gas regulator so the pressure regulator on the Model
933 reads 80 PSI.

7. Change the span concentration value of the gas species to be cali-


brated in the Gas Calibration dialog box to the actual span gas value
that is being used. Then click OK and click Apply. Click NO when
prompted to save parameters to EEPROM.

8. View the Analyzer Data tab (Figure 5-3) and observe the concentra-
tion readings.

Figure 5-3.
Analyzer Data tab.

9. Once the Span Concentration readings have stabilized, return to the


Gas Calibration dialog box and click the Span button below the gas
species being calibrated. Observe the Host State under the Status tab
for a message indicating the completion of the span function. Confirm
that the Span Factor (SFactor on Gas Calibration dialog box) for the
species is updated. The default value for span factor is 1.0.

10. Bleed down the calibration gas and disconnect it from the span gas
connection point.

11. Connect the Swagelok plug to the span gas connection point.

12. Turn on the zero gas and confirm that the pressure is at 80 PSIG.

13. From the Flow Control list, select “Auto.” Click OK on the Gas Cali-
bration dialog box and then click Apply on the Setup tab. Click YES
when prompted to save the parameters to EEPROM.

Calibration | 5-3
Analog Output Calibration

When performing current or voltage calibration, do not enable (check)


 the V/I Low Limit 4 mA check box until after calibration is complete.
NOTE

Figure 5-4.
Output Setup dialog
box.

Current Calibration
The current outputs are calibrated at the factory. If a current output
module is replaced or added, then that output should be calibrated.
Calibration of a current output is performed by entering the measured
zero and full-scale (span) signals for each output (see Figure 5-4). These
values are used to offset the output to the correct values.

To calibrate the output (1, 2, 3, or 4), connect a current meter to the output
of interest (see J109 on the Customer I/O board, Figure 5-5) and then:

1. Click the Zero Cal button.

2. Measure the current at the output of interest.

3. Enter the value in the applicable Zero (mA) text field.

4. Once all desired output channels have been measured and data
entered, click Span Cal.

5. Measure the current at the output of interest.

6. Type the value into the applicable Span (mA) text field.

7. Once all desired output channels have been measured and data
entered, click OK and then click Apply. Click YES when prompted to
save the parameters to EEPROM.

8. To test the accuracy of the output channels, click Mid-Scale.

5-4 | Model 933 UV Analyzer


9. Measure and verify a Mid-Scale current at the output you are testing.

10. The current outputs are now calibrated.

11. Click Normal to return to normal operation.

Figure 5-5.
Customer I/O board
(Part No. 100-1758).

Calibration | 5-5
Voltage Calibration
The voltage outputs are calibrated at the factory. Most users will probably
use current outputs rather than the non-isolated voltage outputs. If the
I/O board is replaced, then the voltage outputs should be calibrated if
they are used for data acquisition. This is done from the Output Setup
dialog box (Figure 5-4). Calibration of a voltage output is performed by
entering the measured zero and full-scale (span) signals for each output.
These values are used to offset the output to the correct values.

To calibrate the output (1, 2, 3, or 4), connect a voltage meter to the output
of interest (see J108, Figure 5-5) and then:

1. Click Zero Cal.

2. Measure the voltage at the output of interest.

3. Type the value into the applicable Zero (V) text field.

4. Once all desired output channels have been measured and data
entered, click Span Cal.

5. Measure the voltage at the output of interest.

6. Type the value into the applicable Span (V) text field.

7. Once all desired output channels have been measured and data
entered, click OK and then click Apply. Click YES when prompted to
save the parameters to EEPROM.

8. To test the accuracy of the output channels, click Mid-Scale.

9. Measure and verify a Mid-Scale voltage at the output of interest.

10. The voltage outputs are now calibrated.

11. Click Normal to return to normal operation.

5-6 | Model 933 UV Analyzer


MAINTENANCE & TROUBLESHOOTING

The Maintenance & Troubleshooting chapter discusses preventive mainte-


nance to keep the analyzer system operating at peak efficiency, how to
check for plugging in the analyzer’s sampling system, and how to replace
internal parts. This chapter also discusses how to view error messages that
can be used to diagnose and troubleshoot problems with the analyzer.

Safety Considerations

Before performing any maintenance, service, or troubleshooting on the


 analyzer, review and follow all personnel and equipment safety
NOTE information under “Personnel and Equipment Safety Measures”
following the Table of Contents near the beginning of this manual.
This information describes procedures to follow to avoid personal
injury and/or damage to the equipment. All regulatory agency and
personnel safety procedures for your jurisdiction must be followed.

Personnel should be thoroughly familiar with the operation of the


analyzer before performing the maintenance procedures described in
this chapter.

To prevent an explosion, test the area around the analyzer for hazard-
! ous gases and proceed with maintenance only when the area is found
WARNING to be safe (nonhazardous).

Maintenance & Troubleshooting | 6-1


Maintenance
Generally, the Model 933 Analyzer requires limited maintenance. The
Preventive Maintenance Schedule lists general maintenance to follow to
ensure continued and proper operation of the analyzer. This section also
describes parts that require replacing and the frequency in which they
should be replaced, according to the Preventive Maintenance Schedule.

Preventive Maintenance Schedule


To reduce the occurrence of problems with the analyzer, AMETEK West-
ern Research recommends that you follow the Preventive Maintenance
Schedule as outlined in the following pages. Since most analyzer prob-
lems originate within the sampling system, the primary objective of the
Preventive Maintenance Schedule is proper care of the sampling system.

Preventing leaks in the sample handling system is critical to proper


! analyzer operation. The analyzer’s sampling system must be leak
CAUTION checked whenever it has been dismantled for maintenance or repair.

Refer to the “Preventive Maintenance Schedule” for suggested actions and


their frequency when caring for the analyzer. Details and assembly draw-
ings to assist you when changing out parts can be found in appropriate
sections later in this chapter.

6-2 | Model 933 UV Analyzer


Frequency Task
Every 6 Months Zero Gas Cylinder

Check the Zero Gas cylinder and replace it if empty or nearly


empty.
Every 6 Months Sheltered Systems

If your analyzer system is installed in a custom shelter, check the


air filters for the shelter purge and air conditioning systems and
replace them if necessary.

Depending on the location of the site and its environmental


conditions, it may be necessary to check and replace these filters
more frequently.
9–12 Months Source Lamps

Replace the source lamps. The source lamps may need to be


replaced sooner if information from the analyzer’s diagnostics
indicates related alarms (i.e., “Warning ALC”, “Warning PMT
Signal”, “Warning Zero Drift”, or “Fault Lamp Failure” errors).
For more information, refer to “Replacing the Source Lamps” and
“Diagnostics and Troubleshooting” in this chapter.
Every Year Measuring Cell

Clean the Measuring Cell and the rest of the analyzer’s sampling
system. This schedule is a minimum requirement. If other
conditions are found to be present, as outlined under the section
titled “Cleaning the Measuring Cell and Replacing O-Rings,”
cleaning may be required more frequently.

At the same time, replace the o-rings.


Every Year * Filterblock Assembly (Optional, if used)

Replace the o-rings, filter elements, and the membrane filters in


the Filterblock Assembly.

Replace the flow restrictors (one in each of the three filter stages)
and clean the assembly before reassembling it.

* In natural gas streams that are extremely dirty, the flow restrictor
in the first filter stage may need to be changed more often
because it removes most of the liquids and particulate from the
gas.

For more information, refer to “Natural Gas Filter Maintenance” in


Appendix B.
Every 2 Years Column Block Assembly

Replace the o-rings and the filter elements in the Column Block
Assembly. At the same time, observe the check valves for wear
and replace them if necessary. Clean the Column Assembly cavity
before reassembling the Column Block.

Replace the flow restrictors if system flow rates have decreased to


unacceptable levels.

For more information, refer to “Column Block Preventative


Maintenance” in this chapter.

Maintenance & Troubleshooting | 6-3


Before Performing Maintenance

Under normal operating conditions, lethal concentrations of H2S and


! other toxic gases from the process may be present within the
WARNING analyzer’s sampling system.

Before working on the sampling system, manually force the analyzer


to backpurge the sampling system with Zero Gas (force its Flow
Control Mode to “Zero” from the Gas Calibration dialog box),
isolate it (block it in) from the process, and disconnect the power.
Follow this procedure prior to changing out any analyzer components
or replacing any replaceable parts (as part of regular preventive
maintenance), or performing leaks checks following the replacement of
instrument air or other adjustments to any of the connections points
in the analyzer’s sampling system. If this is not possible, a breathing
apparatus must be worn while servicing the sampling system.

The sampling system is defined as all components in the analyzer


system through which sample gas passes.

Locating a Plug in the Sampling System

If analyzer problems occur, they are most likely related to improper


sampling system operation, such as plugs or leaks. Plugs in the sample
system cause problems in analyzer response time, either to changing
process conditions or to Zero Gas. Leaks are potentially dangerous and
will eventually lead to corrosion problems.

Detecting Plugs in the Sampling System

Detecting plugs in the sampling system is best done by observing the


analyzer’s measurement response time immediately following a Zero
function. A typical response is in the range of 15–30 seconds. Observe
your analyzer and learn what a normal response time is. Use the recorded
response time as a reference for detecting the formation of plugs in the
sampling system.

If the sample response time is longer than normal, it is most likely due to
plugging somewhere in the sampling system. The next step is to locate
and remove the plug. The portion of the sampling system with the high-
est risk of plugging is the sample inlet and the section of the sample inlet
most prone to plugging is the Sample Probe Valve. One way to confirm
that a plug is in the sample inlet is to cap the Vent Line (or, optionally,
close the Vent Valve’s isolation valve) and Zero the analyzer.

6-4 | Model 933 UV Analyzer


If the Pressure Compensation option is installed, observe the Cell Pres-
sure reading on the Analyzer Data tab, and if the reading approaches the
Zero Gas supply pressure, a plug is present somewhere in the sample
inlet.

To avoid damaging the pressure transducer, do not set the pressure


! higher than the pressure transducer rating, either 105 KPAA (15
CAUTION PSIA) or 0–700 KPAA (0–100 PSIA).

After confirming that the plug is somewhere in the sample inlet, take
 all appropriate safety precautions and dismantle the sample system,
NOTE starting at the Sample Probe.

Plugs in the sample outlet (or vent side) of the sample system are rare. If
an aspirator is used to transport the sample gas (i.e., part of a Heated
Sample Gas Probe, if used), a plug in the vent system can cause the aspira-
tor drive air to flow back into the Measuring Cell and, essentially, simulate
a Zero Gas Flow or Backpurge condition.

Preventing Plugs in the Sampling System

This is done by maintaining the necessary operating temperatures for


each temperature-controlled zone. Check the real time temperature for
each Temperature Zone (on the Analyzer Data tab) and compare it to its
Setpoint temperature (on the Temperature Control dialog box).

To check the analyzer’s sampling system for possible plugging:

1. While working from the Configurator Software, manually force the


analyzer to backpurge the sampling system with Zero Gas.

To do this, click the Gas Calibration button from the Setup tab to view
the Gas Calibration dialog box. From the Flow Control list, select
“Zero.”

2. The rotameter should be active with flow indication.

3. Close the isolation valve on the Sample Probe Valve. Observe the flow
on the rotameter. If the flow reduces to a stop, a large plug has oc-
curred somewhere in the sampling system.

Open the isolation valve on the Sample Probe Valve.

Maintenance & Troubleshooting | 6-5


4. Close the isolation valve on the Vent Valve.

If your application disperses the used sample gas to atmosphere via a


 stack or low pressure flare header, disconnect the Vent Pipe at the Vent
NOTE port on the Measuring Cell and temporarily install an NPT plug.

Observe the flow on the rotameter. If the flow reduces to a stop, a


large plug has occurred somewhere in the sampling system.

5. After locating the cause of the restriction or plug (and after cleaning or
replacing the part or line), leak test the fittings or connections that
were loosened or replaced. To do this, follow the procedures under
“Sampling System Leak Check” in Chapter 3.

6. Return the isolation valve on the Vent Valve to the open position (or
remove the NPT plug and reconnect the Vent Pipe to the Vent port on
the Measuring Cell). Both isolation valves should be open.

7. While working from the Configurator Software, return the analyzer


Flow Control setting to “Auto” (Analyzer Control Mode).

To do this, click the Gas Calibration button from the Setup tab to view
the Gas Calibration dialog box. From the Flow Control list, select
“Auto.”

8. Check the sample response time. Record the response time. The
recorded value can be used later as a reference while testing response
time.

6-6 | Model 933 UV Analyzer


Changing Out Replaceable Parts
The following sections discuss the parts that should be changed out,
according to the schedule listed in the “Preventive Maintenance Sched-
ule.” These descriptions focus mainly on the AMETEK sampling system.

Preventing leaks in the sample handling system is critical to proper


! analyzer operation. If sample gas migrates into the Reflector Block or
CAUTION
Optical Bench Assembly (uncommon) due to a leak in the Measuring
Cell Assembly, the optics will become damaged and most likely require
replacement. Most leaks are preventable with regular cleaning and
replacement of the Measuring Cell o-rings.

If the Configurator Software displays Warning or Fault alarm error


! messages that indicate a faulty component requires replacement [as
CAUTION described in the “Microcontroller Board Error Conditions and Correc-
tive Action” table or “Host Controller Board Error Conditions and
Corrective Action” later in this chapter], review this manual for
replacement procedures.

For complex maintenance procedures not discussed in this manual,


such as replacing heaters, RTDs, or electronic boards, consult with
your AMETEK distributor or representative. Or, contact the factory
for assistance and information about returning the assembly/analyzer
to the factory for repair.

Maintenance & Troubleshooting | 6-7


Measuring Cell Preventive Maintenance

The preventive maintenance procedure discussed in this section is for a


Standard Range Measuring Cell (Figure 6-2a) and a Low Range/White Cell
(Figure 6-2b). For other types of Measuring Cells, refer to the “Supplemen-
tal Information” tab of this manual, or the Documentation Package
shipped with the analyzer.

If your application uses a Measuring Cell other than the two men-
 tioned in this manual, refer to the Supplemental Information tab of
NOTE this manual, or the Documentation Package shipped with the analyzer
for the appropriate assembly drawing.

Disassembling and Cleaning the Measuring Cell

The o-rings in the Measuring Cell should be replaced every year to avoid
a leak in the sampling system. While the Measuring Cell is disassembled,
clean its chambers and parts, including the windows.

Refer to Figures 6-1, 6-2a, and 6-2b for assistance in locating and identify-
ing the parts that make up the Measuring Cell.

Clean the Measuring Cell and its windows:

• If the analyzer responds slowly to zero when the sampling system is


free of restrictions, or

• If evidence of contamination is present in the sampling tubing, or

• Every year as indicated in the “Preventive Maintenance Schedule.”

Replace the o-rings in the Measuring Cell:

• If the parts are found to be damaged while performing an unsched-


uled cleaning (see cleaning requirements above). For example, the
Measuring Cell Windows are scratched, cracked, or chipped, or the
o-rings are damaged.

• Every year as indicated in the “Preventive Maintenance Schedule.”

6-8 | Model 933 UV Analyzer


Figure 6-1.
Optical Bench Assembly,
with Standard Range
Measuring Cell.

Maintenance & Troubleshooting | 6-9


To disassemble and clean the Measuring Cell:

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

1. Connect a laptop computer to the analyzer via the Explosion-Proof


Digital Communications Port on the front of the Lower Enclosure.

Start the Configurator Software and from the Edit menu, click Device
Properties, view the Setup tab, and then click the Gas Calibration
button. Refer to “Establishing Communications With the Analyzer
Using a Laptop Computer,” in Chapter 3.

From the Flow Control list, select “Zero”. Click OK and then click
Apply. Click NO when prompted to save parameters to EEPROM.

2. If the analyzer is using measured pressure compensations (optional),


put pressure compensations in fixed mode so that a low sample
pressure fault does not occur. To do this, click Compensations from
the Setup tab to view the Compensations dialog box. Set the Cell
Pressure (pressure compensations) to Fixed Mode so that a “Fault
Sample Pres Lo” error does not occur. Refer to “Compensations” in
Chapter 4 for more information.

Close the sample inlet valve. Allow the analyzer sampling system to
backpurge with Zero gas for 2–3 minutes.

3. Return to the Gas Calibration dialog box and select “Shut-In” from
the Flow Control list. Click OK and then click Apply.

Allow the sampling system pressure to bleed down to atmospheric


pressure (check the pressure gauge). If there is a valve on the Vent
Line, close it (or cap the Vent Line outlet).

If a Filterblock is used, never bleed down the sampling system pres-


! sure from the sample inlet side of the Filterblock Assembly. Pressure
CAUTION differentials of more than 210 KPA (30 PSI) in this direction can tear
the filter membranes.

4. Disconnect AC power to the analyzer by opening the power-discon-


nect switch (external to the analyzer). Power down the computer, too,
while maintenance is being performed.

6-10 | Model 933 UV Analyzer


5. Disconnect the tubing from the Measuring Cell and follow the remain-
ing procedures for the Measuring Cell used by the analyzer, either
STANDARD RANGE (Figure 6-2a) or the optional LOW RANGE/
WHITE CELL (Figure 6-2b).

6. STANDARD RANGE
Remove the three M4 x 35 mm screws that secure the Measuring Cell to
the Window Cover. Grasp the edge of the window and carefully re-
move it. Remove the o-ring (P/N 300-9060).

LOW RANGE
Remove the three M4 x 35 mm screws that secure the Measuring Cell
to the Window Cover. Remove the three M4 x 8 mm screws that
secure the aperture plate to the Measuring Cell. Grasp the edge of the
window/mirror combination and carefully remove it. Remove both
o-rings (P/N 300-9060).

7. STANDARD RANGE
Hold the Measuring Cell vertically so that the Reflector Block is on top
and remove the three screws that secure the Reflector Block to the
Measuring Cell. Remove the Reflector Block.

Grasp the edge of the window and carefully remove it. Remove the
two o-rings (P/N 300-9060). Inspect all the o-rings for flexibility and for
any signs of wear or contamination.

LOW RANGE
Hold the Measuring Cell vertically so that the Reflector Block is on top
and remove the three screws that secure the Reflector Block to the
Measuring Cell. Remove the Reflector Block. Remove the o-ring
(P/N 300-9060).

Remove the three M3 x 10 mm screws that secure the window mount-


ing plate to the window holder. Grasp the edge of the window and
carefully remove it. Remove the o-rings (P/N 300-9060). Inspect the
o-rings for flexibility and for any signs of wear or contamination.

8. Using Kimwipes® EX-L or an equivalent extra low-lint tissue, clean the


front and back side of the windows. A high purity solvent, such as
isopropanol, can also be used. Rinse with pharmaceutical-grade
distilled water. Chipped or cracked windows should be replaced.

9. Inspect the interior of the Measuring Cell for foreign material. If you
need to clean the interior, use a nonabrasive detergent and water
solution, isopropanol, or reagent-grade acetone followed by a rinse
with pharmaceutical-grade distilled water.

10. Allow all components to dry thoroughly before reassembling.

Maintenance & Troubleshooting | 6-11


Figure 6-2a.
Standard Range Cell
(P/N 100-1811).

6-12 | Model 933 UV Analyzer


Figure 6-2b.
Low Range/White Cell
(P/N 100-1780).

Maintenance & Troubleshooting | 6-13


Replacing Parts and Resassembling the Measuring Cell

It is critical to reassemble the Reflector Block in the exact orientation


! as it was assembled at the factory.
CAUTION

To replace the o-rings and reassemble the Measuring Cell:

1. STANDARD RANGE
Hold the Measuring Cell vertically with the Reflector Block end up and
install two new o-rings (P/N 300-9060) and the window.

LOW RANGE
Install a new o-ring (P/N 300-9060) in the end of the Measuring Cell
that connects to the window holder. Install one new o-ring
(P/N 300-9060) in the window holder. Replace the window in the
window holder. Place the window mounting plate on the window
holder and secure it using the three M3 x 10 mm screws.

Hold the Measuring Cell vertically with the Reflector Block end up.
Connect the Reflector Block and window holder to the Measuring Cell
using the three screws removed earlier.

2. STANDARD RANGE ONLY


Place the Reflector Block on the Measuring Cell, with the “peak-line”
of the mirror block at 90 degrees to a line through the fittings. Ensure
that the Measuring Cell window does not slide out of position when
the Measuring Cell is initially placed against the Reflector Block.

Using the three screws removed earlier, secure the Reflector Block to
the Measuring Cell. Tighten the screws evenly.

3. STANDARD RANGE
Invert the Measuring Cell and install a new o-ring (P/N 300-9060) and
the window.

LOW RANGE
Invert the Measuring Cell and install a new o-ring (P/N 300-9060) and
the window/mirror combination. Orient the window/mirror combination
so that the mirror side is not in contact with the sample gas. Install a new
o-ring (P/N 300-9060) on the aperture plate. Orient the aperture plate so
that the outside countersink hole is aligned with the sample fitting.
Secure the aperture plate to the Measuring Cell using the three
M4 x 8 mm screws removed earlier. Tighten the screws evenly.

6-14 | Model 933 UV Analyzer


4. STANDARD RANGE
Align the two larger-diameter holes in the Window Cover with the two
larger-diameter holes in the Measuring Cell. Using the three screws
removed earlier, secure the Measuring Cell to the Window Cover on the
Optical Bench. Tighten the screws evenly.

LOW RANGE
Hold the Measuring Cell so that the sample fitting near the aperture
plate is up. Use the three screws removed earlier to secure the Measur-
ing Cell to the window cover. Tighten the screws evenly.

5. Reconnect the sampling tubing to the Measuring Cell.

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not power up the analyzer or laptop computer if there is a hazard-
ous gas atmosphere present.

6. Restore power to the analyzer. Power up the computer, if it was pow-


ered down while maintenance was being performed.

7. Perform a leak (pressure) check on the sampling system fittings that


were disconnected/reconnected. These procedures are described in
Chapter 3 under the section titled “Sampling System Leak Check.”

8. Open the valves isolating the analyzer from the sampling stream
and/or remove the cap from the Vent Line outlet.

9. Allow the analyzer to warm up then click Gas Calibration from the
Setup tab. Select “Zero” from the Flow Control list. Click OK and then
click Apply. When prompted to save parameters to EEPROM, answer
click NO.

10. Click Optical Bench from the Setup tab and perform an Auto-Setup
function by clicking Auto-Setup.

11. When the Auto-Setup is complete, return to the Gas Calibration


dialog box and perform a manual zero calibration by clicking the Zero
button.

12. When the zero calibration is complete, return the Flow Control setting
in the Gas Calibration dialog box to “Auto”. Click OK, and then click
Apply. Click YES when prompted to save the parameters to EEPROM.

The procedure is complete.

Maintenance & Troubleshooting | 6-15


Column Block Preventive Maintenance

The mating surfaces of the Column Block Assembly housing and cover
! is a flamepath.
CAUTION
Take care to avoid damaging this flamepath when disassembling and
reassembling the Column Block.

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING

Do not apply power to the analyzer if any of its flamepaths appear to


! be scratched, dented, or worn. Applying power to an analyzer with a
WARNING damaged flamepath is dangerous and could result in serious injury or
death and/or serious damage to equipment.

Certain parts in the Column Block must be replaced according to the


“Preventive Maintenance Schedule,” or sooner if system flow rates have
decreased or if sampling system contamination is evident. While the
Column Block is disassembled, clean the Column Assembly parts and the
Column Assembly chamber. Refer to Figure 6-3 for assistance in locating
and identifying the parts that make up the Column Block.

Replace the o-rings:

• In the Column Assembly if the parts are found to be damaged while


performing an unscheduled maintenance, or

Every 2 years as indicated in the “Preventive Maintenance Schedule.”

• In the Check Valve if the parts are found to be damaged while per-
forming an unscheduled maintenance, or

Every 2 years as indicated in the “Preventive Maintenance Schedule.”

Replace the Column Block filter elements:

• If the Measuring Cell was inspected and white particulate was re-
moved from it.

• Every 2 years as indicated in the “Preventive Maintenance Schedule.”

6-16 | Model 933 UV Analyzer


Replace the flow restrictors in the Column Block if:

• The system flow rates have decreased. Typical flow on the rotameter
should be approximately 2 litres/min with 80 PSIG (550 KPAG) supply
pressure.

The spare parts for this assembly can be found under “Recommended
Spare Parts” in Chapter 7.

 If the RTD is found to be faulty and must be replaced, contact


AMETEK to verify operation before attempting to replace the RTD,
NOTE
and to order replacement parts.

Removing and Replacing Parts in the Column Block

The parts that are removed and replaced in this procedure correspond
with Item #s in Figure 6-3.

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

To disassemble, clean, and replace parts in the Column Block:

1. Connect your laptop computer to the Model 933 Analyzer via the
Explosion-Proof Digital Communications Port on the front of the
Lower Enclosure.

Start the Configurator Software and from the Edit menu, click Device
Properties, view the Setup tab, and then click the Gas Calibration
button.

From the Flow Control list, select “Zero”. Click OK and then click
Apply. Click NO when prompted to save parameters to EEPROM.

2. Close the sample inlet valve. Allow the analyzer sampling system to
backpurge with Zero gas for 2–3 minutes.

Maintenance & Troubleshooting | 6-17


3. Return to the Gas Calibration dialog box and select “Shut-In” from
the Flow Control list. Click OK and then click Apply.

Allow the sampling system pressure to bleed down to atmospheric


pressure (check the pressure gauge). If there is a valve on the Vent
Line, close it (or cap the Vent Line outlet).

If a Filterblock is used, never bleed down the sampling system pres-


! sure from the sample inlet side of the Filterblock Assembly. Pressure
CAUTION differentials of more than 210 KPA (30 PSI) in this direction can tear
the filter membranes.

4. Disconnect AC power to the analyzer by opening the power-discon-


nect switch (external to the analyzer). Power down the computer, too,
while maintenance is being performed.

5. Disconnect the tubing from the Column Block and follow the remain-
ing procedures.

6. Remove the three M6 X 12 mm screws (Item 28) that secure the Col-
umn Block valve cover (Item 27) to the Column Block (Item 25).

7. Remove the check valves (Item 26) from the Column Block with a pair
of needle nose pliers. Remove the o-ring (Item 29). Inspect the check
valves and o-ring for any signs of wear. Install a new o-ring. Replace
the check valves or install new check valves, if necessary.

8. With the check valves and o-ring in place, replace the Column Block
valve cover in the Column Block and tighten the three M6 X 12 mm
screws.

9. Remove both column assemblies (Item 10).

10. Inspect the o-ring (Item 9) on each column assembly and replace if
necessary.

11. Remove the M6 nut (Item 8) from the filter spool assembly (Item 4).
Remove the seal washer (Item 11), o-rings (Items 5 and 7), and filter
(Item 6).

12. Inspect filter for signs of saturation (yellowing) and replace if neces-
sary. If there is particulate on either black filter spool, clean it with
isopropanol or distilled water.

6-18 | Model 933 UV Analyzer


1. Internal Tooth 3 mm SS Washer (300-0642) – 4 places 15. Column Block Mounting Tube (300-9123)
2. Ground Terminal (300-0511) 16. Mounting Tube Locknut (300-9135) – 2 places
3. Ground Wire (300-8306) 17. M6 x 20 Socket HD SS Hex Screw (300-4492) – 10 places
4. Filter Spool (300-9149) 18. M3 x 6 Button HD SS Hex Screw (300-4865) – 6 places
5. O-Ring, Aflas, #113 (300-9147) 19. Warning Label (300-9169)
6. Coalescing Filter Element (300-6217) 20. Column Block Flange (300-9159)
7. O-Ring, Viton, #010 (300-2375) 21. 1/8" O-Ring Seal Fitting (300-9139) – 3 places
8. M6 Nut (300-0263) 22. Cartridge Heater 120 VAC (300-9038)
9. O-Ring, Viton, #121 (300-8719) 240 VAC (300-9039)
10. Column Assembly 23. Flow Restrictor (100-1794) – 2 places
2-Turn Column Assembly (100-1789) 24. O-Ring, Aflas, #008 (300-6241) – 2 places
4-Turn Column Assembly (100-1857) 25. Column Block (300-9156)
11. Seal Washer (300-6151) 26. Check Valve (100-1788) – 2 places
12. RTD (300-4924) 27. Column Block Valve Cover (300-9160)
13. Overtemp Switch (300-9062) 28. M6 x 12 Socket HD SS Hex Screw (300-4496) – 3 places
14. Overtemp Switch Mounting Hardware 29. O-Ring, HSN, #125 (300-9060)

Figure 6-3.
Column Block assembly.

Maintenance & Troubleshooting | 6-19


Reassembling the Column Block and Inspecting Flow Restrictors

To replace the flow restrictors and reassemble the Column Block:

1. Reassemble the filter spool assembly (Item 4) and tighten the M6 nut
(Item 8) by hand.

2. For each column assembly (Item 10), replace new o-rings (Items 5
and 7) and filter element (Item 6) on the filter spool and then replace
the column assembly in the Column Block (Item 25).

3. Remove the ten M6 X 20 mm screws (Item 17) that secure the Column
Block flange (Item 20) to the Column Block and remove the two flow
restrictors (Item 23).

4. Inspect the flow restrictors for signs of plugging from column material
particulate and replace them with new ones if necessary.

5. Install the flow restrictors using new o-rings (Item 24). The o-rings are
rolled over the threads onto the flow restrictor.

6. Replace the ten M6 X 20 mm screws (Item 17) that secure the Column
Block flange (Item 20) to the Column Block (Item 25).

7. Reconnect the sampling tubing to the Column Block.

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not power up the analyzer or laptop computer if there is a hazard-
ous gas atmosphere present.

8. Restore power to the analyzer. Power up the computer, if it was pow-


ered down while maintenance was being performed.

9. Perform a leak (pressure) check on the sampling system fittings that


were disconnected/reconnected. These procedures are described in
Chapter 3 under the section titled “Sampling System Leak Check.”

10. Open the valves isolating the analyzer from the sampling stream
and/or remove the cap from the Vent Line outlet.

11. Allow the analyzer to warm up then click Gas Calibration from the
Setup tab. Select “Zero” from the Flow Control list. Perform a manual
zero calibration by clicking the Zero button.

12. When the zero calibration is complete, return the Flow Control setting
to “Auto”. Click OK, and then click Apply. Click YES when prompted
to save the parameters to EEPROM.

The procedure is complete.

6-20 | Model 933 UV Analyzer


Source Lamp Replacement

The typical life span of the source lamps is approximately 9–12 months of
continuous operation. However, a source lamp can exhibit signs of degra-
dation after 5 to 6 months.

When Do Source Lamps Need to be Replaced?

Possible signs of degradation or indications of Source Lamp failures are:


• Unstable lamp voltage (check voltage levels on the Optical Bench
Data tab – see Figure 6-4), or
• Unstable analyzer output under Zero Gas conditions (“Excessive Zero
Drift” warning error is displayed in Error Condition list in the Status
tab of the Configurator Software – see Figure 6-5), or
• The “Warning ALC” (Automatic Warning PMT Signal) Microcontroller
error is displayed in the Error Condition list in the Status tab of the
Configurator Software (Figure 6-5).

Figure 6-4.
Optical Bench Data
tab.

Figure 6-5.
Error Condition on
Status tab.

Maintenance & Troubleshooting | 6-21


About the Source Lamps

• Source Lamp 1 is closest to the Measuring Cell.

• The cathode of the source lamp must be centered on the optical axis of
the beam splitter for optimal operation of the analyzer. The cathode
and the outer envelope of the lamp are not necessarily concentric or
consistent from lamp to lamp.

• A new source lamp must be aligned to ensure optimal operation of the


analyzer.

• This procedure is based on the standard Model 933, bench code 8.

Do not interchange the source lamps. Lamp 1 must be cadmium (Cd)


! – P/N 300-2070. Lamp 2 must be copper (Cu) – P/N 300-8707.
CAUTION

Replacing the Source Lamps

Refer to Figure 6-1 for assistance in locating and identifying the hardware
components encountered while replacing the source lamps.

To replace Source Lamps:

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING

1. Disconnect power from the analyzer by opening the power-discon-


nect switch (external to the analyzer).

2. After the area has been tested for hazardous gases (and found to be
safe), remove the 24 M10 screws from the EEx d Upper Enclosure door
and open it.

3. Loosen – but do not remove – the two M3 x 8 screws on the Optical


Bench Microcontroller mounting bracket.

Swing the Microcontroller/Micro-Interface board assembly outward.

4. Loosen the Lamp Retaining Screw on the bottom of the lamp socket
and rotate the Lamp Adjustment Plate 90 degrees. Remove the Lamp
Socket Assembly.

6-22 | Model 933 UV Analyzer


5. Loosen the Lamp Clamping Screw on the Lamp Compression Bar and
remove each lamp by rotating and sliding it downward.

Do not rotate or pull on the base of the source lamp because this may
! cause it to separate from the glass envelope. Grasp the glass envelope
CAUTION when rotating or pulling the source lamp.

6. Install the new lamps. Make sure that the narrow end of each lamp is
pushed completely into the holder. Do not touch the (flat) window at
the end of the lamp.

7. Lightly tighten each Lamp Clamping Screw to secure each lamp. Do


not overtighten; the spring should not be collapsed.

8. Reinstall each Lamp Socket Assembly by rotating the Lamp Adjust-


ment Plate 90 degrees (to its original position) and tighten the Lamp
Retaining Screw to secure the Lamp Socket Assemblies. Do not over-
tighten; the springs should not be collapsed. The lamp must be al-
lowed to move so it can be adjusted later in this procedure.

It is necessary to work with the EEx d Upper Enclosure door open


! after replacing source lamps so that adjustments can be made to the
WARNING lamps.

Before proceeding, test the area around the analyzer for hazardous
gases and proceed only when the area is found to be safe.

9. After the area has been tested for hazardous gases (and found to be
safe), restore power to the analyzer. Allow the analyzer to warm up
before continuing.

Do not remove the cover of the Explosion-Proof Digital Communica-


! tions Port on the front of the Lower Enclosure and do not power up
WARNING
the laptop computer if there is a hazardous gas atmosphere present.

Maintenance & Troubleshooting | 6-23


10. Power up the laptop computer and connect the serial cable to the
Explosion-Proof Digital Communications Port on the Lower Enclo-
sure.

Start the Configurator Software and establish communications with


the analyzer.

a. From the Setup tab, click Output to view the Output Setup dialog
box. Click Alarm Disable and then OK.

Allow the analyzer to stabilize for approximately 10 minutes before


continuing.

b. Perform an Auto-Setup and then return to this procedure.

For detailed information about performing an Auto-Setup, refer to


“The Auto-Setup Sequence” later in this chapter.

c. From the Setup tab, click the Gas Calibration button to view the
Gas Calibration dialog box (Figure 6-6).

From the Flow Control list, select “Zero”. Click OK and then click
Apply from the Setup tab. When prompted to save the parameters
to EEPROM, click NO. Allow the zero gas to flow for 2–3 minutes.

Figure 6-6.
Gas Calibration dialog
box.

11. Return to the Output Setup dialog box and click Alarm Enable and
then OK.

Return to the Gas Calibration dialog box and change the Flow Con-
trol setting back to “Auto”.

6-24 | Model 933 UV Analyzer


12. From the Optical Bench dialog box (Figure 6-7), click the Alc On check
box to turn off the Automatic Lamp Control enable function (off =
unchecked). The Alc On function must be off to ensure the analyzer is
not making automatic adjustments while you are setting the Measure
and Reference signals to operate at optimum ratios to each other, as
described in the following steps.

Click OK and then click Apply from the Setup tab. Click NO when
prompted to save parameters to EEPROM.

Figure 6-7.
Optical Bench dialog
box.

13. Open the Configurator file “LampSetup.dyc” by clicking the Open


Configuration icon on the Standard Toolbar. Two Trend graphs will
appear on the screen (see Figure 6-8):

• One for Measure PMT signals.

• One for Reference PMT signals.

Figure 6-8.
Configurator screen
after opening
LampSetup.dyc.

Maintenance & Troubleshooting | 6-25


14. Click on the Standard Toolbar to start scanning of the Measure
and Reference PMT signals.

• Observe PMT signals of filter positions 1, 3, and 5 if Lamp 1 was


replaced.

• Observe PMT signals of filter positions 2, 4, and 6 if Lamp 2 was


replaced.

To change the Y-axis voltage scale, move the mouse pointer to the
 graph and right-click. Click Display and change the Upper and
NOTE Lower Limits.

If the lamp pulse current-control value for a filter location is negative,


that filter location is not used.

15. Align the Source Lamps (described under “Source Lamp Alignment,”
later in this chapter) to ensure optimal operation and then perform
another Auto-Setup. Return to these procedures after the Auto-Setup
is complete.

16. After the lamp replacement and alignment process is complete, the
analyzer is ready to operate.

If you have additional work to do from the Configurator Software,


complete your work and then disconnect the computer from the
analyzer. Do this by exiting the Configurator Software, powering
down the laptop computer, and disconnecting the Serial Communica-
tions Cable from the Explosion-Proof Digital Communications Port on
the Lower Enclosure.

Close the cover of the Explosion-Proof Digital Communications Port


and tighten the hex screw to secure it in place.

17. Using a soft, nonabrasive cloth, gently clean the mating areas
(flamepath) of the Upper Enclosure and its door and replace the 24
M10 screws. Tighten the M10 screws to 9.0 Nm, ±1.0 Nm (80 in.-lb,
±9 in.-lb).

6-26 | Model 933 UV Analyzer


Auto-Setup

The Auto-Setup function optimizes PMT (photomultiplier tube) gains and


the source lamp currents after the source lamps have been replaced or
adjusted. Always initiate an Auto-Setup after any lamps, optical filters, or
PMTs have been installed or replaced.

When the Auto-Setup is initialized, the Automatic Lamp Control (Alc On)
function is automatically turned on. To view the current status of this
function, press the Optical Bench button from the Setup tab. The Alc On
check box will be checked when this function is on.

When is an Auto-Setup Required?

Auto-Setup is required when:

• The “Warning PMT Signal” error is displayed under Error Condition


on the Status tab.

• One or both source lamps are replaced.

• Any optical filter is replaced.

• One or both PMTs are replaced.

• The Optical Bench Service Electronics board is replaced.

• The Measuring Cell windows and/or optics are cleaned.

When is an Auto-Setup Not Required

Auto-Setup is not required as part of a preventive maintenance schedule


(i.e., do not perform an Auto-Setup every month).

Maintenance & Troubleshooting | 6-27


PMT Level and PMT Balance

PMT Level and PMT Balance are adjusted only during the Auto-Setup
sequence. The range of operation for both these parameters is 0–10 VDC.
Normal values for both, after a successful Auto-Setup, is from 2.5–7.5
VDC. The analyzer will function with values outside this range, but it is a
sign that a change has likely occurred in the transmission of light within
the Optical Bench.

At the end of every Auto-Setup, always check the PMT Level and PMT
Balance. Take note of severe changes in PMT Level and PMT Balance
because they are as important as the absolute value.

The PMT Level signal adjusts the gain of both PMTs simultaneously in
the same direction. PMT Balance adjusts the gain of the two PMTs in
opposite directions by controlling a virtual ground circuit on the Optical
Bench Service Electronics Board.

If the PMT signals are outside their normal range of operation after the
Auto-Setup function is complete, check for the following:

• Was the Auto-Setup done with zero gas flowing through the sampling
system?

• Are the Measuring Cell windows clean?

• Are the PMTs in their original sockets (i.e., is the higher gain PMT in
the Measure path)?

• Do the source lamps need replacement? If not, are the source lamps
aligned?

• Have there been any leaks from the Measuring Cell? If so, check the
condition of the optical filters, beamsplitter, mirrors, windows, lenses,
and o-rings in the Optical Bench and in the Measuring Cell (including
Reflector Block). Contact AMETEK for procedures not discussed in
this manual.

6-28 | Model 933 UV Analyzer


Auto-Setup Fault Message and Corrective Action

If during the Auto-Setup the error message “Warning Auto Setup” is


displayed next to Micro State on the Status tab, it may indicate a problem
with the PMT Level or PMT Balance signal. Refer to “Microcontroller
Board Error Conditions and Corrective Action” later in this chapter for
corrective action to take to reset this alarm. Restart the Auto-Setup func-
tion after this alarm has been corrected.

The Auto-Setup Sequence

To perform an Auto-Setup:

1. From the Setup tab, click the Gas Calibration button to view the Gas
Calibration dialog box.

From the Flow Control list, select “Zero.” Click OK and then click
Apply from the Setup tab. When prompted to save the parameters to
EEPROM, click NO. Allow the zero gas to flow for 1–3 minutes.

2. From the Setup tab, click Output to view the Output Setup dialog box.
Click Alarm Disable and then OK.

Allow the analyzer to stabilize for approximately 10 minutes before


continuing.

3. From the Setup tab, click the Optical Bench button to view the Opti-
cal Bench dialog box.

Check and record the PMT Level and PMT Balance.

4. Click the Auto-Setup button to initiate the Auto-Setup function and


then click OK. The process takes about 3 minutes to complete.

5. From the Status tab, observe the status of the Micro State. The follow-
ing messages are displayed to indicate which step of the Auto-Setup
process is being performed:

• Setup - Prelim PMT Level


• Setup - Prelim Lamp Pulses
• Setup - PMT Balance
• Setup - Final PMT Level
• Setup - Final Lamp Pulse
• Setup - ALC
• Setup - Off/Completed

Maintenance & Troubleshooting | 6-29


6. When the message “Setup - Off/Completed” is displayed, the Auto-
Setup function is complete.

P300 may have up to four jumpers installed (when changing jumpers,


 at least one must be present at all times).
NOTE
P301 may have up to two jumpers installed (when changing jumpers,
at least one must be present at all times). However, P301 must have
only one jumper during normal operation.

7. From the Optical Bench dialog box, check the PMT Level and PMT
Balance again. The voltage should be between 2.5 and 9.84 VDC.

Cancel Auto-Setup

To cancel the Auto-Setup function, click the Cancel Auto-Setup button on


the Optical Bench dialog box.

6-30 | Model 933 UV Analyzer


Manipulating the PMT Level and PMT Balance

If a PMT is replaced, it may be necessary to change the P300 and P301


jumper settings on the Optical Bench Service Electronics board.
Changing the jumper positions provides coarse gain adjustment of the
Reference PMT and therefore changes the PMT Level and PMT Balance.

There are six jumper positions (four in P300 and two in P301) that can
accommodate one jumper each. At least one jumper is required in P300
and P301 at all times. Adding jumpers increases the supply voltage avail-
able to the Reference path PMT. This increases the PMT Balance and, to a
small degree, decreases the PMT Level. The opposite occurs if jumpers are
removed.

Figure 6-9 describes the effect on the PMT Balance and PMT Gain in
relation to different jumper positions.

To achieve an acceptable PMT Balance and PMT Level:

1. If jumpers have been reconfigured, perform an Auto-Setup.

2. After an acceptable PMT Balance and PMT Level has been achieved,
initiate a zero function.

To do this, click Gas Calibration from the Setup tab to view the Gas
Calibration dialog box. Click the Zero button to initiate a zero calibra-
tion and then click OK.

Click the Status tab and observe the Host State status to determine
the current operation being performed.

3. When the zero calibration is complete, return to the Gas Calibration


dialog box and select “Auto” from the Flow Control list. Click OK and
then click Apply from the Setup tab. Click YES when prompted to
save parameters to EEPROM.

4. From the Setup tab, click Output. Click Alarm Enable and then OK.

Maintenance & Troubleshooting | 6-31


Jumper Positions
P300 P301
1 2 3 4 5 6
X X X X X
Higher PMT
Balance X X X X
X X X X
X X X X
X X X
X X X
X X X
X X X X
X X
X X X
X X X
X X X
X X X X X
X X X X
X X X X
X X X X
X X X
X X X
X X X
X X
X X X X
X X
X X X
X X
X X X
X X X
Figure 6-9. X X
Optical Bench Service
Electronics board P300 X X
Lower PMT
jumper position vs PMT Balance
X X
balance. X X

When changing jumpers, at least one must be present in P300 and


 P301 at all times.
NOTE

6-32 | Model 933 UV Analyzer


Source Lamp Alignment

If either of the Measure or Reference PMT voltages becomes equal to or


greater than 10,000 mV at any time during the alignment manipulations
(while rotating a lamp), decrease the PMT Level, allow the analyzer to
stabilize for approximately 10 minutes, and perform an Auto-Setup before
continuing.

To align the source lamps:

1. Loosen – but do not remove – the two M3 x 8 screws on the Optical


Bench Microcontroller mounting bracket.

Swing the Microcontroller/Micro-Interface board assembly outward.

2. Slightly loosen the Lamp Clamping and Lamp Retaining screws.

3. While viewing the signals on the LampSetup screen in the


Configurator Software (see Figure 6-8), slowly rotate the new lamp to
obtain the maximum voltage signal from the Measure PMT. Since the
software is updated at one-second intervals use slow, small movements,
pausing each turn to view the new value. See “Scheduling Scans” in
Chapter 4 for more information about scan intervals.

Because the Automatic Lamp Control (Alc On function) is turned off,


 the displayed signal may not be completely steady.
NOTE

4. Loosen the Locking Screw located between the two source lamps.

5. To obtain the maximum signal from the Measure PMT voltage, adjust
the Lamp Adjusting Screw for the lamp that is being adjusted.

6. If the other lamp was also replaced, repeat Steps 2–5.

7. Tighten the Locking Screw located between the two source lamps.

8. Tighten the Lamp Clamping Screw to secure the lamps. Do not over-
tighten; the spring should not be collapsed.

9. Tighten the Lamp Retaining Screw to secure the lamp socket. Do not
overtighten; the spring should not be collapsed.

10. Swing the Microcontroller/Micro-Interface board assembly back into


its original position.

Tighten the two M3 X 8 screws on the Optical Bench Microcontroller


mounting bracket.

Maintenance & Troubleshooting | 6-33


11. Allow the analyzer to operate for 15 minutes and then initiate an
Auto-Setup function, which automatically turns on the Alc Enable
function. Continue with these procedures only after the Auto-Setup is
complete.

For detailed information about performing an Auto-Setup, refer to


“The Auto-Setup Sequence,” earlier in this chapter.

12. After the Auto-Setup is complete, initiate a zero function. To do this,


click Gas Calibration from the Setup tab to view the Gas Calibration
dialog box. If not already done (i.e., as part of another procedure),
select “Zero” from the Flow Control list.

Click the Zero button to initiate the zero calibration and then click OK.

Click the Status tab and observe the Host State status for a message
indicating the completion of the zero calibration.

Allow the analyzer to operate for 2–3 minutes with the zero gas still
flowing.

13. When the zero calibration is complete, return to the Output Setup
dialog box and click Alarm Enable and then OK.

Return to the Gas Calibration dialog box and change the Flow Con-
trol setting back to “Auto” (to return the analyzer to Analyzer Control
Mode). Click OK and then click Apply from the Setup tab. Click YES
when prompted to save parameters to EEPROM.

The lamp replacement and alignment process is complete and the ana-
lyzer is ready to operate.

6-34 | Model 933 UV Analyzer


EEPROM Replacement

The EEPROM must be replaced when the Host Controller “Warning


EEPROM Full” error message is displayed by the Configurator Software
under Error Condition in the Status tab (see Figure 6-11).

This warning condition indicates the number of times that configuration


data has been rewritten to the EEPROM (nonvolatile memory) has ex-
ceeded the safe number (95 % of the acceptable 20K writes is used). The
EEPROM should be replaced as soon as possible.

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

To replace the EEPROM:

1. Connect a laptop computer to the Model 933 Analyzer to communi-


cate with the analyzer. To do this:

a. Connect a Serial Communications Cable to the laptop computer.

b. Loosen the hex screw on the cover of the Explosion-Proof Digital


Communications Port on the Lower Enclosure just enough to allow
the cover to slide to the right. This will reveal the digital Serial Com-
munications Port.

c. Connect the other end of the Serial Communications Cable to the


Serial Communications Port on the analyzer.

d. Power up the laptop computer, start the Configurator Software,


and establish communications with the analyzer.

2. From the Edit menu, click Device Properties to view the Model 933
Properties screen.

3. From the General tab, click Save Configuration to save the current
Model 933 Analyzer configuration parameter values to a file on the
PC.

Record the location and name of this file; it will be necessary to use
this file to restore the analyzer configuration parameter values after
replacing the EEPROM.

Maintenance & Troubleshooting | 6-35


4. Exit the Configurator Software. Power down the analyzer and the
computer. Remove the 24 M10 screws from the Lower Enclosure door
and open it.

If it becomes necessary to handle any of the electronic circuit boards,


! do not subject the boards to static discharge. The ideal solution is a
CAUTION
static-safe work area. Since such areas typically are not available at
analyzer installation sites, the use of a wrist strap connected directly
to a ground is recommended. If a wrist strap is not available, you
should at the very least touch the metal chassis (to ground yourself)
before handling or touching the boards.

5. While wearing a static wrist strap, use an IC extraction tool to remove


the EEPROM (U106) from the Host Controller Board (see Figure 6-10).
If an extraction tool is not available, use a small flathead screwdriver
instead but be careful not to bend any pins while removing it.

6. Properly orient the new EEPROM and place it on the IC socket. Make
sure all of the pins are seated in their pin sockets before pushing the
EEPROM gently and completely into the socket.

7. Using a soft, nonabrasive cloth, gently clean the mating areas


(flamepath) of the Lower Enclosure and its door.

Close the Lower Enclosure door and replace the 24 M10 screws.
Tighten the M10 screws to 9.0 Nm, ±1.0 Nm (80 in.-lb, ±9 in.-lb).

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING

Do not power up the analyzer or laptop computer if there is a hazard-


ous gas atmosphere present.

8. Power up the analyzer and the computer, start the Configurator


Software, and establish communications with the analyzer.

9. From the Edit menu, click Device Properties to view the Model 933
Properties screen.

10. From the General tab, click Restore Configuration. Locate and open
the file saved in Step 3.

11. Click YES when prompted to save the parameters to EEPROM. The
software will transfer saved Model 933 Analyzer configuration param-
eter values to the new EEPROM. The EEPROM replacement process is
now complete.

6-36 | Model 933 UV Analyzer


Figure 6-10.
Host Controller board
(P/N 100-1757, Rev. B).

Maintenance & Troubleshooting | 6-37


Examining and Caring For the Flamepaths

The Model 933 Analyzer is designed with flamepaths that will prevent
flame propagation from within the analyzer’s EEx d Electronics Enclo-
sures to the outside, should an internal explosion occur.

The flamepaths on the Model 933 Analyzer consist of:

• The EEx d Upper and Lower Enclosures’ mating surfaces (enclosure


doors and enclosure housings), cable entry ports, and the Digital
Communications Port.

• All separable joints in the Heated Column Block Assembly. These parts
include the mating surfaces of the Column Block Assembly housing
and its cover, and the connecting tube to the analyzer.

Upper/Lower Electronics Enclosure Flamepaths (Mating Surfaces)

Any time either EEx d (Upper or Lower) Electronics Enclosure is opened


for maintenance, inspect the flamepath for scratches, indentations, or
other damage. Carefully clean the flamepaths (mating surfaces) with a
soft, nonabrasive cloth just prior to closing it.

If it is necessary to use a cleaning agent, make sure the power to the


! analyzer is off. Also, the agent must be nonabrasive and must not
CAUTION attack aluminum (example, a suitable agent is Isopropanol). Following
any maintenance and/or cleaning – and after the cleaning fluid has
evaporated completely – immediately close the EEx d Upper/Lower
Enclosure.

When performing equipment maintenance in hazardous areas, all


! safety standards and procedures must be followed, as specified by the
WARNING Owner Company, local electrical-inspection authority, and National/
EU regulations.

6-38 | Model 933 UV Analyzer


When the EEx d Upper/Lower Enclosure is opened for maintenance or
! repair, take extreme care to avoid scratching or damaging its
WARNING flamepaths.

If at any time the enclosure door is open and service personnel are not
working on the EEx d Upper/Lower Enclosure, close the door and
secure it with at least one screw. This will reduce the risk of inadvert-
ently scratching or damaging the flamepath.

Before closing the door, gently clean the flamepath with a soft, non-
abrasive cloth and make sure the surfaces are free of debris.

Do not apply power to the analyzer if any of its flamepaths appear to


! be scratched, dented, or worn. Applying power to an analyzer with a
WARNING damaged flamepath is dangerous and could result in serious injury or
death and/or serious damage to equipment.

Replace the parts immediately if damage or wear is apparent. Contact


AMETEK immediately if there is any doubt about the integrity of any
flamepath.

Before opening the analyzer’s EEx d Upper/Lower Enclosure, follow


! all necessary safety procedures to ensure the area is nonhazardous
WARNING (main power to the Model 933 Analyzer is off, explosive gas atmo-
sphere is not present, etc.).

Before performing maintenance on the Model 933 Analyzer, shut off


the power to the analyzer and all alternate power supplies (if used).

Maintenance & Troubleshooting | 6-39


Diagnostics and Troubleshooting

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

The Model 933 Analyzer has a built-in error detection system that con-
tinuously monitors the operation of key parameters. An error can be
detected by either the Host Controller or the Microcontroller and can be
of two types: Fault and Warning. An error is annunciated by the Fault
Status relay or the Warning Status relay. If the analyzer is communicating
with the Configurator Software, the particular condition that causes an
error and the type of error are shown in the Error Condition display box
under the Status tab (Figure 6-11).

Figure 6-11.
Analyzer Status tab.

6-40 | Model 933 UV Analyzer


A Warning indicates that the analyzer may require servicing and the data
may be suspect. Though all warning errors cause the Warning Status relay
to de-energize, the Warning Status relay can also indicate one of these
analyzer operating conditions:

• Performing a gas calibration (e.g., Auto-Zero, Zero, Span).

• Performing an analog output calibration.

• Performing Optical Bench setup.

• Non-Auto Flow Control.

The Warning Status relay returns to the normal energized state automati-
cally when the offending error condition is corrected and/or the analyzer
completes one of the above operations.

A Fault indicates that a failure has been detected and the analyzer data is
invalid. Under the Fault situation, the analyzer de-energizes the Fault
Status relay and switches the sampling system into the shut-in mode, if
the Flow Control setting is “Auto.” If the Fault Status relay is configured as
non-latching, the relay returns to its normal energized state and the
sampling system is switched back to sampling state when the offending
error condition is corrected. However, if the Fault Status relay is config-
ured as latching, the operator must unlatch the relay in one of the follow-
ing ways:

• If the Alarm Enable digital input is permanently wired to the Enable


state, click the Alarm Disable button once on the Output Setup dialog
box and then click Alarm Enable once.

• If the Alarm Enable digital input is wired to a customer’s data acquisi-


tion system, have the system toggle that line from Enable to Disable
and then back to Enable at least one second later.

Maintenance & Troubleshooting | 6-41


Host Controller Board Error Conditions and Correc-
tive Action
Figure 6-12 lists valid alarm error messages that originate from the Host
Controller Board, alarm type (Fault or Warning), descriptions of the
errors, and suggested corrective actions.

Host Controller error conditions are displayed automatically by the


Configurator Software under Error Condition in the Status tab (see Figure
6-11). The error is displayed if the error condition exists; otherwise noth-
ing is displayed.

Alarm Type / Error Condition Description & Suggested Corrective Action


Warning EEPROM Full The EEPROM (nonvolatile memory) has exceeded the safe
number of times that configuration data has been rewritten to it
(95 % used).
Corrective Action:
• Replace the EEPROM as soon as possible. Refer to the
section titled “EEPROM Replacement” in this chapter.
Warning Output Range One or more of the output channels exceeds its normal operating
full-scale range by more than 5 %.
Corrective Action:
• From the Setup tab, click Output to view the Output
Setup dialog box and check that the full-scale ranges are
correct for the current sample. If this warning persists
during normal operation, contact AMETEK. If necessary,
adjust the range and recalibrate the analyzer from the
Output Setup dialog box. See also “Analog Output
Calibration” in Chapter 5.

Figure 6-12.
Host Controller error
conditions/diagnostics.

6-42 | Model 933 UV Analyzer


Alarm Type / Error Condition Description & Suggested Corrective Action
Warning Column Temp Hi The Column Block temperature has exceeded the column
temperature Too Hot setpoint.
Corrective Action:
• From the Setup tab, click Temp Control to view the
Temperature Control dialog box and check the Column
Setpoint and Too Hot setpoint.
• Check the ambient temperature around the analyzer; if it
is higher than the Too Hot setpoint, adjust the
surrounding temperature to within the Column Block
measuring range (see “Temperature Control” in Chapter 4
for details).
Take appropriate safety precautions before opening the
Electronics Enclosure covers, and:
• Check the heater control circuit:
- Check fuse F3 on the AC Distribution PWB in the
Lower Enclosure – see Figure 6-13. Replace if
necessary.
- Check the thermo-switch (OverTemp) on the Optical
Bench Assembly in the upper enclosure (see Figure
6-1). If the plunger has popped out, press it to reset it.
• Check the Column Block temperature sensor (RTD) for a
short or an open circuit.
• Replace the Customer I/O board. Contact AMETEK to
verify operation before removing this board.
Warning Zero Drift This Warning condition indicates excessive Zero Drift. Excessive
Zero Drift is indicated if Zero Gas transmission values attained
after a Zero function have exceeded user-specified values.
Corrective Action:
• Perform a zero calibration. See Chapter 5 for calibration
information.
• From the Analyzer Data tab, check the Bench
Temperature under Temperature Zone to ensure it has
stabilized.
• From the Status tab, check the Error Condition list for
error messages that indicate contaminated Measuring
Cell, optics, and/or sampling system.
If necessary, clean the appropriate component(s) of the
sampling system that require cleaning.
• From the Setup tab, click Gas Calibration to view the
Gas Calibration dialog box and check that the ZDrift
parameters are appropriate and have not been changed.
• This Warning condition may also indicate that one or both
lamps need to be replaced, especially if a “Warning ALC”
error message is also displayed on the Status tab.
For information on how to change out source lamps, refer
to “Source Lamp Replacement,” earlier in this chapter.

Figure 6-12.
Host Controller error
conditions/diagnostics.

Maintenance & Troubleshooting | 6-43


Alarm Type / Error Condition Description & Suggested Corrective Action
Warning Zero Pressure The zero gas pressure is outside of 1 % to 99% of full-scale range.
Note: This Warning error is used only by analyzers with the
pressure transducer option.
Corrective Action:
• Check the zero gas regulator on the zero gas bottle and
ensure it has an adequate supply.
• Check the zero gas pressure gauge and ensure that the
zero gas is at an appropriate pressure. Refer to “Zero
Gas” in Chapter 3. Adjust the pressure regulator until the
pressure is at an appropriate level.
• Check the LowScale and HighScale Cell Pressure
readings on the Compensations dialog box. If the
HighScale reading is > 100 PSIA (5171.49 mmHg) or the
LowScale reading is < 66 PSIA (3413.19 mmHg), this
indicates the pressure transducer is saturated; it won’t
allow the analyzer to perform an Auto-Zero.
Adjust the pressure to 80 PSIG and re-start the Auto-
Zero.
• Check the pressure transducer.
• Check the zero solenoid.
• From the Setup tab, click Output to view the Output
Setup dialog box and confirm that the Low Scale and
High Scale pressure settings are correct.
• Confirm that the pressure transducer jumpers on the
Customer I/O Board are configured correctly. For more
information about Measuring Cell pressure jumper
configurations, refer to “Compensations” in Chapter 4.
• Replace the Customer I/O board. Contact AMETEK to
verify operation before removing this board.
Warning Sample Pressure Hi The sample pressure is above 99 % of the full-scale range.
Note: This Warning error is used only by analyzers with the
pressure transducer option.
Corrective Action:
• Check the sample gas pressure gauge and ensure that
the sample gas is at an appropriate pressure (80 PSIG).
Adjust the sample gas pressure regulator until the sample
gas is at an appropriate flow and pressure.
• Check the pressure transducer.
• From the Setup tab, click Output to view the Output
Setup dialog box and confirm that the Low Scale and
High Scale pressure settings are correct.
• Confirm that the pressure transducer jumpers on the
Customer I/O Board are configured correctly. For more
information about Measuring Cell pressure jumper
configurations, refer to “Compensations” in Chapter 4.

Figure 6-12.
Host Controller error
conditions/diagnostics.

6-44 | Model 933 UV Analyzer


Alarm Type / Error Condition Description & Suggested Corrective Action
Fault Internal Comm This serious system fault indicates the Host Controller board
cannot establish reliable communications with the Microcontroller
board.
Corrective Action:
• Reset the analyzer.
If the Lower Electronics Enclosure door is closed, take
appropriate safety precautions and cycle the analyzer AC
power off for a minimum of 15 seconds before cycling it
on again.
If this doesn’t correct the error, click Info from the Setup
tab to view the Analyzer Information dialog box and click
the Reset M933 button.
If this still doesn’t correct the error, take appropriate
safety precautions, open the Electronics Enclosure
covers and:
- Reset the Host Controller board (SW100, Lower
Enclosure – see Figure 6-10).
- Reset the Microcontroller board (SW400, Upper
Enclosure – see Figure 6-14).
• Check the connections of the 4-wire cable between the
Host Controller (J300) and Micro-Interface (J104) boards.
Also, inspect it for damage (cuts, nicks, burn marks, etc.).
• Replace the Microcontroller board. Contact AMETEK to
verify operation before removing this board.
• Replace the Host Controller board. Contact AMETEK to
verify operation before removing this board.
• Replace the Micro-Interface board. Contact AMETEK to
verify operation before removing this board.

Figure 6-12.
Host Controller error
conditions/diagnostics.

Maintenance & Troubleshooting | 6-45


Alarm Type / Error Condition Description & Suggested Corrective Action
Fault Analytical Data This serious system fault indicates the Host Controller board is not
receiving analytical data from the Microcontroller board.
Corrective Action:
• Reset the analyzer.
If the Lower Electronics Enclosure door is closed, take
appropriate safety precautions and cycle the analyzer AC
power off for a minimum of 15 seconds before cycling it
on again.
If this doesn’t correct the error, click Info from the Setup
tab to view the Analyzer Information dialog box and click
the Reset M933 button.
If this still doesn’t correct the error, open the Electronics
Enclosure covers and:
- Reset the Host Controller board (SW100, Lower
Enclosure – see Figure 6-10).
- Reset the Microcontroller board (SW400, Upper
Enclosure – see Figure 6-14).
• Check the connections of the 4-wire cable between the
Host Controller (J300) and Micro-Interface (J104) boards.
Also, inspect it for damage (cuts, nicks, burn marks, etc.).
• Replace the Microcontroller board. Contact AMETEK to
verify operation before removing this board.
• Replace the Host Controller board. Contact AMETEK to
verify operation before removing this board.
• Replace the Micro-Interface board. Contact AMETEK to
verify operation before removing this board.
Fault Sample Pres Lo The sample pressure is below 1 % of the full-scale range.
Note: This Warning error is used only by analyzers with the
pressure transducer option.
Corrective Action:
• Check the sample gas pressure gauge and ensure that
the sample gas is at an appropriate pressure (80 PSIG).
Adjust the sample gas pressure regulator until the sample
gas is at an appropriate flow and pressure.
• From the Setup tab, click Output to view the Output
Setup dialog box and confirm that the Low Scale and
High Scale pressure settings are correct.
• Check the solenoids.
• Check for leaks in the sampling system. For more
information, refer to “Sampling System Leak Check” in
Chapter 3.
• Check the pressure transducer.
• Inspect the check valves in the Column Block Assembly
for signs of wear. Refer to the section titled “Column
Block Preventative Maintenance,” earlier in this chapter.
• Replace the Customer I/O board. Contact AMETEK to
verify operation before removing this board.

Figure 6-12.
Host Controller error
conditions/diagnostics.

6-46 | Model 933 UV Analyzer


Alarm Type / Error Condition Description & Suggested Corrective Action
Fault Chip ADC The Host Controller Board’s internal analog-to-digital converter (ADC)
is not responding.
Corrective Action:
• Replace the Host Controller board. Contact AMETEK to
verify operation before removing this board.
Fault Column Temp Lo The Column Block temperature is below the column temperature
Too Cold setpoint.
Corrective Action:
• From the Setup tab, click Temp Control to view the
Temperature Control dialog box and check the Column
Setpoint and Too Cold setpoint.
• Check the ambient temperature around the analyzer; if it
is lower than the Too Cold setpoint, adjust the
surrounding temperature to within the Column Block
measuring range (see “Temperature Control” in Chapter 4
for details).
Take appropriate safety precautions before opening the
Electronics Enclosure covers, and:
• Check the heater control circuit:
- Check fuse F3 on the AC Distribution PWB in the
Lower Enclosure (see Figure 6-13). Replace if
necessary.
- Check the thermo-switch (OverTemp) on the Optical
Bench Assembly in the upper enclosure (see Figure
6-1). If the plunger has popped out, press it to reset it.
• Check the Column Block temperature sensor (RTD) –
inside the Column Block – for a short or an open circuit.
See “Column Block Preventive Maintenance,” earlier in
this chapter for more information. Replace the RTD, if
necessary. Contact AMETEK to verify operation before
removing this component..

Figure 6-12.
Host Controller error
conditions/diagnostics.

Maintenance & Troubleshooting | 6-47


Figure 6-13.
AC Distribution PWB
(P/N 100-1771).

6-48 | Model 933 UV Analyzer


Figure 6-14.
Microcontroller Board
(P/N 100-1781).

Maintenance & Troubleshooting | 6-49


LOOSE CLAMPED

OPTICAL BENCH REMOVAL/INSTALLATION

Figure 6-15.
Upper enclosure
Overtemp switch
(thermo-switch)
location.

6-50 | Model 933 UV Analyzer


Microcontroller Board Error Conditions and Correc-
tive Action
Figure 6-16 lists valid alarm error messages that originate from the
Microcontroller Board, error type (Fault or Warning), descriptions of the
errors, and suggested corrective actions .

Microcontroller error conditions are displayed automatically by the


Configurator Software under Error Condition in the Status tab (see Figure
6-11). The error is displayed if the error condition exists; otherwise noth-
ing is displayed.

Alarm Type / Error Condition Description & Suggested Corrective Action


Warning PMT Signal The highest signal from either the Measure or Reference PMT
(photomultiplier tube) is outside its normal range (2.5–9.84 VDC).
View these signals from the Optical Bench Data tab.
Corrective Action:
• Check the flat cables between the Optical Bench Service
Electronics Board and Optical Bench for proper
connections and inspect them for damage (cuts, nicks,
burn marks, etc.).
• Initiate an Auto-Setup function. Refer to “The Auto-Setup
Sequence,” earlier in this chapter for information on how
to do this.
• Replace the lamp(s), if necessary. For information on how
to determine if the lamps need to be replaced and how to
change out source lamps, refer to “Source Lamp
Replacement,” earlier in this chapter.
• Replace the Optical Bench Service Electronics board.
Contact AMETEK to verify operation before removing
this board.
• Replace the PMT Buffer board. Contact AMETEK to
verify operation before removing this board.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

Maintenance & Troubleshooting | 6-51


Alarm Type / Error Condition Description & Suggested Corrective Action
Warning ALC One or both lamp pulse current-control signals has exceeded its
Lamp Maximum signal set point. The default Lamp Maximum is
7.0 VDC. When this alarm occurs, the analyzer will initiate an
Auto-Zero and then an Auto-Setup, to a maximum of three times.
If the lamps are within range after the Auto-Setup, the counter
resets to zero. If not, the alarm will remain on to indicate there is a
problem with the lamps, which may need replacing.
This error may occur during a cold start, but should clear after the
source lamps have stabilized.
Corrective Action:
• Check that the lamp sockets are attached securely to the
lamps and that the Lamp Adjustment Plate is in place.
• Check that the lamps are inserted completely into the
detector assembly.
• Check the flat cables between the Optical Bench Service
Electronics Board and Optical Bench for proper
connections and inspect them for damage (cuts, nicks, burn
marks, etc.).
• The light levels may be too low as a result of natural aging
of the lamps. This is an indication that the lamps are nearing
the end of their useful lives and likely should be replaced.

Eventually, a “Fault Lamp Failure” alarms will be activated.


Refer to the description of this alarm for more details.

As a temporary solution, initiate an Auto-Setup to increase


the PMT gain to compensate for the reduced light levels.
Refer to “The Auto-Setup Sequence,” earlier in this
chapter for information on how to do this.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

6-52 | Model 933 UV Analyzer


Alarm Type / Error Condition Description & Suggested Corrective Action
Warning Cell Temp The Measuring Cell temperature has exceeded its Too Hot
setpoint or has fallen below its Too Cold setpoint, or the Measuring
Cell temperature range is not set properly.
Corrective Action:
From the Setup tab, click Temp Control to view the
Temperature Control dialog box and check the Cell Too Hot
and Too Cold setpoints. Also, check the Cell temperature
Range – it should be set to Range A (“-3 °C to 66 °C”). See
“Temperature Control” in Chapter 4 for more details.
Perform the following checks:
• Check the ambient temperature around the analyzer; if it
is higher than the Too Hot setpoint or lower than the Too
Cold setpoint, adjust the surrounding temperature to
within the Cell temperature measuring Range.
Take appropriate safety precautions before opening the
Electronics Enclosure covers, and:
• Check the jumpers at JP300 on the Micro-Interface board
for proper temperature range setting. The typical default
jumper setting is Range A (jumpers 1-2). See
“Temperature Control” in Chapter 4 for details.
• Check the Measuring Cell temperature sensor (RTD) in
the upper enclosure – see Figure 6-1 for location – for a
short or an open circuit. Replace the RTD, if necessary.
Contact AMETEK to verify operation before removing
this component.
• Replace the Micro-Interface board. Contact AMETEK to
verify operation before removing this board.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

Maintenance & Troubleshooting | 6-53


Alarm Type / Error Condition Description & Suggested Corrective Action
Warning Bench Temp The Optical Bench temperature has exceeded its Too Hot setpoint
or has fallen below its Too Cold setpoint, or the Optical Bench
temperature range is not set properly.
Corrective Action:
From the Setup tab, click Temp Control to view the
Temperature Control dialog box and check the Bench Too
Hot and Too Cold setpoints. Also, check the Bench
temperature Range – it should be set to Range A (“31 °C to
47 °C”). See “Temperature Control” in Chapter 4 for more
details.
Perform the following checks:
• Check the ambient temperature around the analyzer; if it
is higher than the Too Hot setpoint or lower than the Too
Cold setpoint, adjust the surrounding temperature to
within the Bench temperature measuring Range.
Take appropriate safety precautions before opening the
Electronics Enclosure covers, and:
• Check the jumpers at JP301 on the Micro-Interface board
for proper temperature range setting. The typical default
jumper setting is Range A (jumpers 2-3). See
“Temperature Control” in Chapter 4 for details.
• Check the Optical Bench temperature sensor (RTD) in
the upper enclosure – see Figure 6-1 for location – for a
short or an open circuit. Replace the RTD, if necessary.
Contact AMETEK to verify operation before removing
this part.
• Check the heater control circuit:
- Check fuse F4 on the AC Distribution PWB in the
Lower Enclosure – see Figure 6-13. Replace if
necessary.
- Check the thermo-switch (Over-Temp) on the Optical
Bench Assembly. If the plunger has popped out, press
it to reset it.
• Replace the Micro-Interface board. Contact AMETEK to
verify operation before removing this board.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

6-54 | Model 933 UV Analyzer


Alarm Type / Error Condition Description & Suggested Corrective Action
Warning Auto Setup This Warning condition indicates problems with the operation of
the Optical Bench Assembly during an Auto-Setup function.
This alarm will also be set if any of the FltrPulse values are
greater than the Lamp Max signal or less than the (Lamp) Base
signal.
This alarm will also be set if the PMT Level or PMT Balance value
is greater than 9840 mV or less than 2500 mV.
Corrective Action:
View the Optical Bench dialog box and check for deviations
outside of these ranges.
Perform the following checks, correct any faults, and restart
the Auto-Setup function:
• Ensure that the Measuring Cell was zeroed.
• Make sure the source lamps are not burned out.
• Ensure the lamp sockets are attached securely to the
lamps.
• Ensure the lamps are inserted completely into the detector
assembly.
• Make sure the lamp power supply cables are connected
and not damaged.
• Ensure the PMT high-voltage (JP100, JP101) and flat
(J103) cables are connected and not damaged.
• Align the source lamps and restart the Auto-Setup.
• Adjust the jumper positions located at P300 and P301 on
the Optical Bench Service Electronics Board. Refer to
“Manipulating the PMT Level and PMT Balance” and
Figure 6-11, earlier in this chapter, for a description of the
effects on the PMT Balance and PMT Level in relation to
different jumper positions.
• Ensure the Measuring Cell windows are clean and not
damaged.
• Ensure the Measuring Cell is clean.
• Check and clean, if necessary, the steering mirror in the
PMT Block). Contact AMETEK to verify operation
before checking.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

Maintenance & Troubleshooting | 6-55


Alarm Type / Error Condition Description & Suggested Corrective Action
Fault Wheel Speed There is no signal from the filter wheel opto-interruptor, or the filter
wheel speed is outside the normal range of 240–600 RPM.
Corrective Action:
• Check the power (15 V) on the opto-coupler cable to
ensure there is power being supplied to the filter wheel
motor.
• Check the power on the filter wheel motor. Contact
AMETEK to verify operation before checking.
• Check the opto-coupler cable to the Chopper Assembly for
proper connections and inspect it for damage (cuts, nicks,
burn marks, etc.).
• Check the clip-ring for the filter wheel shaft and ensure it
is snug against the bushing. Contact AMETEK to verify
operation before checking.
• Check the filter wheel bearings. Contact AMETEK to
verify operation before checking.
• Replace the Microcontroller board. Contact AMETEK to
verify operation before removing this board.
Fault Board ADC One or both of the Microcontroller board’s discrete analog-to-
digital converters (ADC) is not responding.
Corrective Action:
• Replace one or both of the A/D converters. Contact
AMETEK to verify operation before removing these
components.
• Replace the Microcontroller board. Contact AMETEK to
verify operation before removing this board.
Fault Chip ADC The Microcontroller board’s internal analog-to-digital converter (ADC)
is not responding.
Corrective Action:
• Replace the Microcontroller board. Contact AMETEK to
verify operation before removing this board.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

6-56 | Model 933 UV Analyzer


Alarm Type / Error Condition Description & Suggested Corrective Action
Fault Comm The Microcontroller board cannot establish reliable
communications with the Host Controller board.
Corrective Action:
• Reset the analyzer.
If the Lower Electronics Enclosure door is closed, take
appropriate safety precautions and cycle the analyzer AC
power off for a minimum of 15 seconds before cycling it
on again.
If this doesn’t correct the error, click Info from the Setup
tab to view the Analyzer Information dialog box and click
the Reset M933 button.
If this still doesn’t correct the error, open the Electronics
Enclosure covers and:
- Reset the Host Controller board (SW100, Lower
Enclosure – see Figure 6-10).
- Reset the Microcontroller board (SW400, Upper
Enclosure – see Figure 6-14).
• Check the connections of the 4-wire cable between the
Host Controller (J300) and Micro-Interface (J104) boards.
Also, inspect it for damage (cuts, nicks, burn marks, etc.).
• Replace the Microcontroller board. Contact AMETEK to
verify operation before removing this board.
• Replace the Host Controller board. Contact AMETEK to
verify operation before removing this board.
• Replace the Micro-Interface board. Contact AMETEK to
verify operation before removing this board.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

Maintenance & Troubleshooting | 6-57


Alarm Type / Error Condition Description & Suggested Corrective Action
Fault Cell Temp The Measuring Cell temperature has exceeded its Too Hot
setpoint or has fallen below its Too Cold setpoint, or the Measuring
Cell temperature range is not set properly.
Note: This Warning error is used only by analyzers using the
optional Measuring Cell Heater.
Corrective Action:
From the Setup tab, click Temp Control to view the
Temperature Control dialog box and check the Cell Too Hot
and Too Cold setpoints. Also, check the Cell temperature
Range – it should be set to Range A (“-3 °C to 66 °C”). See
“Temperature Control” in Chapter 4 for more details.
Perform the following checks:
• Check the ambient temperature around the analyzer; if it
is higher than the Too Hot setpoint or lower than the Too
Cold setpoint, adjust the surrounding temperature to
within the Cell temperature measuring Range.
Take appropriate safety precautions before opening the
Electronics Enclosure covers, and:
• Check the jumpers at JP300 on the Micro-Interface board
for proper temperature range setting. The typical default
jumper setting is Range A (jumpers 1-2). See
“Temperature Control” in Chapter 4 for details.
• Check the Measuring Cell temperature sensor (RTD) in
the upper enclosure – see Figure 6-15 for location – for a
short or an open circuit. Replace the RTD, if necessary.
Contact AMETEK to verify operation before removing
this component.
• Replace the Micro-Interface board. Contact AMETEK to
verify operation before removing this board.
Fault Lamp Failure If a PMT Reference signal falls below 0.75 V for 5 minutes, it
indicates the lamp has failed and requires replacement.
Corrective Action:
From the Optical Bench Data tab, check the PMT Reference
value for each filter. If any of these signals are below 0.75 V,
take appropriate safety precautions, open the Electronics
Enclosure covers, and replace the Source Lamp(s)
immediately. See “Source Lamp Replacement” earlier in this
chapter for details.

Figure 6-16.
Microcontroller error
conditions/diagnostics.

6-58 | Model 933 UV Analyzer


Analyzer Reset
Should a situation arise where the Host Controller board or the
Microcontroller board must be reset, take appropriate safety precautions
and cycle the AC power to the analyzer off for a minimum of 15 seconds
before cycling it on again.

If this doesn’t correct the error, click Info from the Setup tab to view the
Analyzer Information dialog box and click the Reset M933 button.

If this still doesn’t correct the error, open the Electronics Enclosure covers
and:

• Reset the Host Controller board (SW100, Lower Enclosure – see Figure
6-10).

• Reset the Microcontroller board (SW400, Upper Enclosure – see Figure


6-14).

Do not randomly reset the analyzer during normal operation. Typi-


! cally, the only resets required are in cases where the Host Controller or
CAUTION Microcontroller boards have been replaced. In this case, it is necessary
to shut down the analyzer. The analyzer will reset upon normal
power-up.

Maintenance & Troubleshooting | 6-59


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6-60 | Model 933 UV Analyzer


SERVICE & PARTS

The Service & Parts chapter discusses what to do if you need technical
support from AMETEK, or if you are returning parts for service. This
chapter also lists the recommended spare parts to have on hand to ensure
all consumable and replaceable parts are replaced according to the “Pre-
ventive Maintenance Schedule” included in Chapter 6.

Technical Support
AMETEK Western Research is committed to providing you the best
technical support in the industry. If you need service or application
assistance, contact your local or nearest AMETEK Service Centre or the
AMETEK factory AMETEK at (403) 235-8400 or 1-800-661-9198, or contact
your local AMETEK Western Research representative.

Before contacting AMETEK with questions regarding the installation,


operation, or maintenance/troubleshooting of your analyzer system,
carefully review the contents of this manual. If you are unable to find an
explanation for your problem in this manual, please gather the following
information prior to contacting AMETEK:

• Model number of the analyzer.

• Serial number of the analyzer experiencing problems.

• Purchase order number.

• AMETEK part number for the specific component you are enquiring
about, if known.

• Information describing the problem.

• Billing address, shipping address, and telephone number.

Service & Parts | 7-1


Returning Equipment
If you need to return parts or equipment for repair, you will need a Re-
turn Material Authorization (RMA) number. This will ensure your equip-
ment is serviced and returned to you in a prompt and efficient manner. To
obtain an RMA number, contact your local or nearest AMETEK Service
Centre and have the following information available:

• Model number of the analyzer.

• Serial number of the analyzer.

• Purchase order number.

• Billing address, shipping address, and telephone number.

7-2 | Model 933 UV Analyzer


?? ANSWERS TO YOUR QUESTIONS ??
The choice is yours...
Whether by phone or in person, we can meet the needs required to keep
your analyzer running at peak performance. Our factories are located in
Calgary, Alberta and Newark, Delaware with a Sales & Service Centre in
Houston, Texas. Depending on the programs you select, we will have a
factory-trained representative talking to you within minutes – 24 hours
a day, 365 days a year or on-site within 24 hours. We stock parts at all
MINUTES OR HOURS, three locations.
WE'RE THERE FOR YOU
ANYTIME / ANYWHERE
AMETEK SERVICE & AFTERMARKET SALES SUPPORT
• PRE-lNSTALLATlON INSPECTIONS • ASAP
To ensure you order the correct analyzer with the AMETEK SERVICE ASSISTANCE PROGRAM.
options your operation requires, schedule a fac- AMETEK’s exclusive ASAP program lets you se-
tory-trained Service Engineer to inspect the pro- lect a service package from a menu of service
posed analyzer location. The on-site charge for options. ASAP options include 24 hour phone
this visit can be deducted from the start-up charge support, 24 hour on-site guarantee, rapid parts
if you select that option. shipment, and many more service benefits. ASAP
plans may be written to provide coverage for a
• START UPS
single analyzer, or all of the AMETEK process
Your decision to buy an AMETEK analyzer is
analyzers at your facility.
greatly appreciated. After the time and money
spent on your analyzer, wouldn’t you expect a fast • AFTERMARKET SALES
and successful start up? We can ensure that will Our Aftermarket Sales group will keep you sup-
happen! Schedule us to be there before you power plied with the parts to maintain your analyzer to
up the system. We will guarantee a satisfactory factory specifications. This is also the group that
commissioning of your analyzer. will keep your analyzer current with upgrades
and retrofits.
• WARRANTY VALIDATION
Upon start-up, we will validate your 1 year war-
ranty. AMETEK’s warranty policy covers all parts • TECHNICAL SUPPORT
and on-site time. Incurred costs will be the respon- Just call AMETEK and a factory trained Service
sibility of the customer. Engineer will be there to answer your questions.
With over 200 years of combined field service
• WARRANTY EXTENSIONS
experience, our engineers are available to provide
AMETEK offers a 2 or 3 year warranty extension
operational support or troubleshooting expertise.
for your analyzers. The warranty is identical to the
original policy supplied with the analyzer. Con- • TRAINING
tact AMETEK Service for more details. We will train your service technicians at our Tech-
nology Transfer Centres located in Calgary, New-
• SPARE PARTS KITS
ark, or at your facility. Our TTCs have equipment
These parts allow each customer to properly main-
similar to yours for hands-on training. A diploma
tain their analyzers according to the recommended
will be presented upon completion of the course.
Preventive Maintenance Schedule (listed in the
manual), to ensure optimal operations.

PROCESS INSTRUMENTS
Canada: 1-800-661-9198 U.S.A.: 1-800-537-6044

Service & Parts | 7-3


Recommended Spare Parts
This section lists the recommended spare parts to have readily available
for the Model 933 Analyzer.

Optical Bench/Sampling System Spare Parts


AMETEK recommends having the following spare parts available to
ensure your analyzer will operate at peak efficiency. The replacement of
these parts is required as part of the Preventive Maintenance Schedule. It
is also necessary to have these parts on hand in case the parts become
damaged or contaminated, and need to be replaced.

Refer to appropriate assembly drawings in Chapter 6 (in the correspond-


ing maintenance procedures) for the locations of these recommended
spare parts to have on-site.

If your analyzer uses the optional Filterblock Assembly (for Natural


 Gas applications), refer to Appendix B (Options) for additional
NOTE
recommended spare parts.

IMPORTANT SPARE PARTS INFORMATION


 Spare Parts for your analyzer may vary from those included in this
NOTE section. This can be due to non-standard Measuring Cells or optional
equipment used for your specific application.

Before ordering spare parts, always refer to the “Supplemental Infor-


mation” tab of this manual or the Documentation Package included
with the analyzer for a Supplemental Spare Parts. If a Supplemental
Spare Parts list is found, use those Part Numbers; if not, use the Part
Numbers listed in this section.

Measuring Cell Windows – Recommended Parts to Have On-Site


Description Part No. 1 Year Qty Warranty
Standard Measuring Cell (5 cm, 10 cm, 15 cm, 20 cm, 40 cm, etc.)
Cell Window, Fused Silica 300-0281 2 3 Months
Low Range (White) Cell (81.2 cm)
Cell Window, Fused Silica 300-0281 1 3 Months
Cell Window, Fused Silica 300-6288 1 3 Months

7-4 | Model 933 UV Analyzer


General Maintenance – Recommended Parts to Have On-Site
Description (Location) Part No. 1 Year Qty 2 Year Qty Warranty
Check Valve (Column Block Assy) 100-1788 0 2 None
Flow Restrictor (Column Block Assy) 100-1794 0 2 None
Source Lamp, Cadmium, SCD9MB 300-2070 1 2 3 Months
(Upper Enclosure)
O-ring, Viton, 2-010 (Column Block Assy) 300-2375 0 2 None
Coalescing Filter Element (Column Block Assy) 300-6217 0 2 None
O-ring, Aflas, 0008 (Column Block Assy) 300-6241 0 2 None
Source Lamp, Copper, Hollow Cathode 300-8707 1 2 3 Months
(Upper Enclosure)
O-ring, Aflas, #121 (Column Block Assy) 300-8719 0 2 None
O-ring, HSN, #125 (Column Block Assy; 300-9060 4 10 None
Low Range Cell; Standard Range Cell)
O-ring, Aflas, #113 (Column Block Assy) 300-9147 0 2 None
Bearing, Chopper Wheel (Chopper Assembly) 300-9437 0 2 1 Year
Conditions: Content is valid from June 15, 2002 and is subject to change without notice.

Spare Analyzer Fuses


AMETEK also recommends to have on-site spare fuses for the fuses used
in the analyzer. These fuses do not need to be changed out at regular
intervals, but AMETEK recommends that these fuses be available in case a
fuse blows and a replacement is needed. Recommended fuses include:

Model 933 Analyzer – Recommended Fuses to Have On-Site


120 V 240 V
Description (Location*) Part No. Fuse Type Part No. Fuse Type
Upper Enclosure (F4) 300-9244 1A 300-6291 0.5 A
Column Heater (F3) 300-9244 1A 300-6291 0.5 A
DC Power Supply (F2) 300-9244 1A 300-9244 1A
Main (F1) 300-9245 3.15 A 300-6292 1.6 A
* These fuses are located on the AC Distribution PWB in the Lower Enclosure.

Optical Bench Service Electronics Board (100-1662) – Recommended Fuses to Have On-Site
120 V 240 V
Description (Location*) Part No. Fuse Type Part No. Fuse Type
Main Board (F200) 300-8778 125 mA 300-8777 63 mA
Photomultiplier Tube (F300) 300-3214 0.2 A 300-3214 0.2 A
Lamp (F201) 300-9524 32 mA 300-9524 32 mA
* These fuses are located on the Optical Bench Service Electronics PWB in the Upper Enclosure.

Service & Parts | 7-5


Printed Wiring Board Re-Ordering Part Numbers
If you require replacement boards for the Model 933 Analyzer, use the
following part numbers to order the board(s) you need.

Printed Wiring Boards


Description (Location) Part No. Qty Warranty
Customer I/O Board (Lower Enclosure) 100-1758 1 1 Year
Host Controller Board (Lower Enclosure) 100-1757 1 1 Year
Microcontroller Board (Upper Enclosure) 100-1781 1 1 Year
Micro-Interface Board (Upper Enclosure) 100-1759 1 1 Year
Optical Bench Service Electronics Board c/w bracket 100-1841 1 1 Year
(Upper Enclosure)
PMT Buffer Board (Lower Enclosure) 100-0140 1 1 Year

7-6 | Model 933 UV Analyzer


APPENDIX A – ADVANCED
SOFTWARE OPERATION

If potentially flammable gases or vapors are present, do not open any


! covers without first disconnecting power to the analyzer.
CAUTION

Before proceeding to connect devices or power-up a computer in a


! hazardous area, test the area around the analyzer for hazardous gases
WARNING and proceed only when the area is found to be safe.

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure and do not power-up
the laptop computer if there is a hazardous gas atmosphere present.

Advanced Software Operation | A-1


Assigning Inputs to Channels for Display Modes
To define the parameters to be monitored by a display mode you select
one or more input channels. These input channels are accessed from the
Scan context menu and are limited only by the number of settings able to
be defined in the display window for that mode. The most commonly
used input channels are those for the species or gases that are monitored.
Most of the other inputs that can be selected are used for diagnostic
purposes.

Follow the steps below to select one or more input channels to display on
your screen.

1. Select a mode in which to display the parameters that you will ob-
serve.

2. Right-click with your mouse on the area to be defined. When the


context menu appears, click Scan.

3. Select your device by clicking Device and choosing a device from the
list box.

4. From the Input Channel list box, select the species or parameter that
you want to display in the selected area on your mode display win-
dow by clicking on it.

5. Click OK. The species or parameter that you have selected now
appears on your mode display screen. You can repeat this procedure
up to the number of times defined by the display mode, or create a
custom mode display that contains a greater number of parameters to
be monitored. Figure A-1 list the parameters that can be monitored.

Parameter Defined Areas


Species Concentration e.g., H2S and/or COS
Transmittance for each filter
PMT Measure Signal for each filter
PMT Reference Signal for each filter
Absorbance for each filter (ABS 1–6)
Lamp Current for each filter (ALC LP 1–6)
Voltage Output for each analog channel
Current Output for each analog channel
Temperature Zone 1–3 Bench, Cell, Column
Duty Cycle for each temperature zone
Scaled Analog Inputs Bench Temp
Figure A-1. Cell Temp
Possible parameters Column Temp
Cell Pressure
monitored for each
mode. Link from another Data Source

A-2 | Model 933 UV Analyzer


Modes of Operation
Any settings you define for a mode will be retained by the system when
you change the mode or exit the program.

Any display or scan parameters that you define for a mode will not be
transferred to a new mode when you switch modes. However, the system
will continue to scan when you change modes.

Meter Mode
Meter mode allows you to view information in a meter-type format
(Figure A-2). You can assign the parameters in Figure A-1 to any one of 12
meters. Alarms can be set up and displayed on the meter to view the
current reading in relation to the High and Low alarm limits defined. You
can also define unique scan, display, and alarm output settings.

While working in Meter mode:

• Each meter has a bar representing a measured value. Text under the
meter displays the numeric value of the measured parameter.

• Each meter can be set to display alarm limits. As long as the measured
value is within the high and low alarm limits, the meter bar appears in
green.

A yellow meter bar indicates an alarm warning condition.

A red meter bar indicates an alarm fault condition.

• Any other actions associated with alarms are activated if the limit is
exceeded (e.g., running an information file, or setting off a digital or
analog output).

• Before changing meter properties, you must select the meter by


clicking on it. The meter will be highlighted with a yellow border when
selected.

Advanced Software Operation | A-3


To set up a Meter mode display:

1. Select Meter from the Mode menu or select the icon from the
Standard Toolbar.

2. Select a meter by clicking on one. A yellow border around the meter


indicates it is active.

3. Right-click the active meter and define the Scan, Display, and/or
Alarm settings for the meter.

4. Repeat Steps 2 and 3 for additional meters.

Figure A-2.
Meter mode display.

A-4 | Model 933 UV Analyzer


Annunciator Mode
Annunciator mode (Figure A-3) allows you to track whether a measured
parameter is within acceptable user-defined limits using a simple color/
text indication. You can assign the parameters in Figure A-1 to any one of
12 annunciator display windows.

If the level is:

WITHIN the alarm limits defined = GREEN = OK

ABOVE the High alarm warning level = YELLOW = HIGH

ABOVE the High alarm limit = RED = HIGH

BELOW the Low alarm warning level = YELLOW = LOW

BELOW the Low alarm limit = RED = LOW

Annunciator mode also allows you to set up multiple indicators, each


corresponding to a different gas species. You can also define unique scan,
display, and alarm output settings.

While working Annunciator mode:

• Annunciator mode is normally used to define alarm limits so that you


can view – using visual indicators – whether the selected value is
within the alarm limits.

• For each channel, a green display indicates the value is within accept-
able limits.

A yellow display indicates an alarm warning condition.

A red display indicates an alarm fault condition.

• Before changing the display properties, you must select the display by
clicking on it. The display will be highlighted with a yellow border
when selected.

Advanced Software Operation | A-5


To set up an Annunciator mode display:

1. Select Annunciator from the Mode menu or select the icon


from the Standard Toolbar.

2. Select a display by clicking on one. A yellow border around the dis-


play indicates it is active.

3. Right-click the active display and define the Scan, Display, and/or
Alarm settings for the display.

4. Repeat Steps 2 and 3 for additional displays.

Figure A-3.
Annunciator mode
display.

A-6 | Model 933 UV Analyzer


Trend Mode
Trend mode allows you to view trends of measured parameters in a
graphical format (Figure A-4). You can assign the parameters in Figure A-1
to any one of 8 channels in Trend Mode. You can also define unique scan,
display, and alarm output settings.

While working in Trend mode:


• The main Trend mode window displays each channel as a colored
line. The Y-axis displays partial pressure or measured value; the X-axis
displays time.

• You can view the exact value of a trend line by holding down the left
mouse button in the trend graphical display area. Display the Data
File Toolbar to view the time of each data point.

To set up a Trend mode graph:

1. Select Trend from the Mode menu or select the icon from the
Standard Toolbar.

2. Select a display by clicking on one. A yellow border around the dis-


play indicates it is active.

3. Right-click the graph and define the Scan, Display, and/or Alarm
settings for the graph.

Figure A-4.
Trend mode (graph)
display.

Advanced Software Operation | A-7


Tabular Mode
Tabular mode allows you to view information in a textual, table-type
format (Figure A-5). You can assign the parameters in Figure A-1 to up to
four tables. You can also define unique scan, display, and alarm output
settings.

While working in Tabular mode:


• If an alarm was defined and the alarm has been exceeded, an alarm
indicator will appear to the right of the main table.

• You can copy any of the columns from a Tabular display window to
the clipboard. For more information, see also “Copying Magnitudes”
and “Copying Channels” under “About Dynamic Data Exchange
(DDE),” later in this Appendix.

• Before changing the display properties, you must select the display by
clicking on it. The display will be highlighted with a yellow border
when selected.

To set up the software for Tabular mode:

1. Select Tabular from the Mode menu or select the icon from the
Standard Toolbar.

2. Select a display by clicking on one. A yellow border around the dis-


play indicates it is active.

3. Right-click the active display and define the Scan, Display, and/or
Alarm settings for the display.

4. Repeat Steps 2 and 3 for additional displays.

Figure A-5.
Tabular mode display.

A-8 | Model 933 UV Analyzer


Custom Modes
Custom mode allows you to create custom setups that can include all
scanning, display, and alarm output options. This is done from the Set
Custom Mode Menu dialog box (Figure A-6). Custom mode setups can
include either a single mode display window or multiple mode display
windows. Using Custom mode, you can create a unique mode display by
mixing and matching the best features of various modes.

For example, you can customize the window to show one Meter mode
display window, one Trend mode window, and two Annunciator win-
dows. Or, you could set up two Trend mode display windows, or two
Tabular mode windows.

Three default custom mode setups are included with the Configurator
Software and more can be added as needed. For each display window
added in Custom mode, the scanning, displays, and alarm output options
are set as if in that mode.

For example, if adding a Meter mode window within the Custom mode,
all settings for that window are defined as if in Meter mode.

Figure A-6.
Set Custom Mode
Menu dialog box.

To create a custom mode:

1. From the File menu, select New or click on the Standard


Toolbar.

2. From the Edit menu, select Add Display and select the type of display
you want to add from the list of standard mode types. Or, use the
Custom mode icons on the Custom Mode Toolbar to add different
displays.

3. Specify the data source. Select the applicable source of data from the
Data Source group by clicking Device and then selecting the device
you want to enable.

Advanced Software Operation | A-9


4. Repeat Steps 3 and 4 to add others displays, if desired.

5. From the File menu, select Save As to save the Custom mode. Or

select one of the icons on the Standard Toolbar to save


the Custom mode to one of the predefined Custom mode file names
(custom1.dyc, custom2.dyc, or custom3.dyc). Custom mode files are
given a .dyc file extension.

6. To retrieve the Custom mode file at a later time, select Open Configu-
ration from the File menu. If you used one of the predefined icons,
double-click one of the files to retrieve it.

Moving or Resizing a Window in Custom Mode

Select the display window to move or resize. The window is highlighted


with a yellow border.

• To move the window, press and hold down the mouse button (just an
outline of the window is visible) while moving the display window,
then release the mouse button.

• To resize the window, use standard Windows methods.

Adding a Display Window in Custom Mode

1. From the Edit menu, select Add Display. Choose the type of display
window to add.

2. Select the data source for the display window.

3. The system adds a display window to the Custom mode window.

Deleting a Window in Custom Mode

1. Click on the window to delete. The window is highlighted with a


yellow border.

2. From the Edit menu, select Delete Display, press the Del key on the

keyboard, or select from the Custom Mode Toolbar to delete the


display window.

A-10 | Model 933 UV Analyzer


Saving Custom Mode Files

1. From the File menu, select Save As. You can save the Custom mode
setup under a new name or use one of the predefined icons.

2. Select the Save button to save the file.

3. By default, the system places these files in the folder where the
Configurator Software is installed and gives the file a .dyc extension.

If you save a Custom mode file in the install folder with the name
“startup.dyc” it will automatically be opened when the program starts.

Opening Custom Mode Files

1. From the File menu, select Open Configuration or select from


the Custom Mode Toolbar.

2. Navigate to the location of the Custom mode file to open.

3. Select the Custom mode file and click Open.

Adding Custom Mode Files to the Mode Menu

1. From the Mode menu, select Set Menu to view the Set Custom Mode
Menu dialog box (Figure A-6). You can associate a Custom mode file to
appear at the bottom of the Mode menu.

You can also provide a menu/button name to appear instead of the file
name at the bottom of the menu.

2. Navigate to the location of the Custom mode file using the Browse
button.

3. To enter a name that will appear at the bottom of the Mode menu,
enter a name in the Menu/Button Name text field.

4. To recall any of these files, click one of the icons.

Advanced Software Operation | A-11


Saving Tabular Mode Files
The Preferences dialog box (Figure A-7) allows you to set up parameters
that define how the Tabular mode files will be saved.

Figure A-7.
Preferences dialog
box.

To set preferences, select Preferences from the Edit menu.

• DDE Item Separator


Select the character that will separate multiple data items in a Dy-
namic Data Exchange (DDE) message.

• Trend Colors
Set the default trend channel colors.

• Data file size


Set the maximum size for a data file. This can be an integer between 1
and 16. The normal value is 1 megabyte. Setting the data file size to a
higher value will increase the size of your data files as well as the size
of the trend graph buffer. As a result of this increase, it will require
more disk space and memory.

You can copy any of the columns from a Tabular display window to
the clipboard.

A-12 | Model 933 UV Analyzer


About Dynamic Data Exchange (DDE)

Copying Magnitudes

You can copy any of the columns from a Tabular display window to the
clipboard.

1. Select Tabular mode.

2. Right-click on the mouse and select Copy Magnitudes from the


context menu. This places the DDE data onto the clipboard.

3. From the Edit menu, select Paste Special (or Paste Link, depending on
the version of Windows running) to create the DDE link and continu-
ously update the data in real time.

Copying Channels

1. Select Tabular mode.

2. Right-click and select Copy Channels. This places the name of the
channel onto the clipboard.

3. From the Edit menu, select Paste Special (or Paste Link, depending on
the version of Windows running) to create the DDE link and continu-
ously update the channel names in real time.

If you are importing data into Microsoft Excel, select Preference from
 the Edit menu. To place the numbers into separate columns, select
NOTE Return from the DDE Item Separator group. To place the numbers
in rows, select Tab.

Advanced Software Operation | A-13


Setting Up the Display
To set up the display for a mode, right-click on a display window and then
click Display from the context menu that appears. The Properties dialog
box is displayed (Figure A-8), with the Display tab active. For modes using
channels – Trend and Tabular modes – you must first select a channel
before you can define the scan settings.

Figure A-8.
Defining Display
Parameters screen.

Title
Type the title for the display window. It will then appear in the title
bar for that window and in other areas of the software to identify the
display window.

Autoscale check box


Applies to Meter mode only. When selected, the system automatically
sets the Y-axis based on the highest value from the previous scan. This
will also override the Y-axis. As the highest peak increases or de-
creases, the display scale is changed to accommodate the changing
highest peak.

Logarithmic check box


Applies to Trend and Meter modes only.

Checked The software uses a logarithmic scale to


display readings.

Not Checked The software uses a linear scale to display


readings.

A-14 | Model 933 UV Analyzer


Upper limit
Applies to Trend and Meter modes only. This value is used only when
the Autoscale check box is not checked. Enter the upper limit to
display on the Y-axis.

Lower limit
Applies to Trend and Meter modes only. This value is used only when
the Autoscale check box is not checked. If the Logarithmic check box
is selected, use this text field to enter the number of logarithmic
decades to display on the Y-axis using the upper limit as the top of the
display range. If the Logarithmic is not checked, enter a value into this
text box for the lower limit.

Units
This is the value in which your results will be displayed.

• In the Units text field, type in the units on which you want the
scanned information displayed.

• Precision
Defines the number of digits after the decimal point to be shown.
For example, if the precision is set to 2, a reading might be 5.22.

Channel name
Applies to Trend and Tabular modes only. Names the displayed
channel. See Figure A-9. Select one of the Channels buttons and enter
a name for it in the Channel name text field.

Figure A-9.
Trend Mode Display
Parameters screen.

Advanced Software Operation | A-15


Channel color
Applies to Trend mode only. Defines a different color for the displayed
channel. A custom color can also be chosen by clicking on the Custom
button and selecting a color.

Minutes
Applies to Trend mode only. Defines the time interval to include on
the display.

Display Values
If checked, displays channel values in Trend mode.

Hide check boxes


Applies to Trend mode only. If checked, the data channel will not be
displayed but will continue to track the data. This is useful when
viewing a scan that overlaps another scan.

A-16 | Model 933 UV Analyzer


Setting Alarms
To set alarms, right-click on a display window and then click Alarms from
the context menu. The Properties dialog box is displayed (Figure A-10),
with the Alarm tab active.

The alarms discussed in this chapter are used by the Configurator


 Software only. They are not the same as the concentration alarms on
NOTE the analyzer. The analyzer concentration alarms operate indepen-
dently of the Configurator Software.

Figure A-10.
Alarm setup.

For Trend and Tabular modes, first select the channel as the source of the
alarms before you define the alarm values. Setting alarms includes defin-
ing alarm limits and defining the actions that should be taken when an
alarm limit is reached. Alarm limits also appear on the main display for
the current mode. High and Low limit alarms appear in red; High and
Low warning alarms appear in yellow.

Enable all alarms

Checked Enables all high and low alarms.

Not Checked Deactivated – alarms can be deactivated


when, for example, your system is not
operating.

Advanced Software Operation | A-17


High Limit
When checked, enables the High Limit alarm.

Name Enter a name for the alarm that will be used to identify
the alarm to the system.

Value Enter the high (upper) limit value for the alarm.

Count Defines the number of consecutive readings that must


be above the high alarm limit before the alarm is
triggered. Higher count values decrease the possibility
that a transient or noise signal will set off a false alarm.

High Warning
When checked, enables the High Warning alarm.

Name Enter a name for the alarm that will be used to identify
the alarm to the system.

Value Enter the high (upper) limit value for the alarm. Must
be lower than the high alarm value.

Count Defines the number of consecutive readings that must


be above the high alarm warning limit before the alarm
is triggered. Higher count values decrease the possibil-
ity that a transient or noise signal will set off a false
alarm.

Low Limit
When checked, enables the Low Limit alarm.

Name Enter a name for the alarm that will be used to identify
the alarm to the system.

Value Enter the low limit value for the alarm.

Count Defines the number of consecutive readings that must


be below this limit before the alarm is triggered. Higher
count values decrease the possibility that a transient or
noise signal will set off a false alarm.

A-18 | Model 933 UV Analyzer


Low Warning
When checked, enables the Low Warning alarm.

Name Enter a name for the alarm that will be used to identify
the alarm to the system.

Value Enter the low limit value for the alarm. Must be higher
than the low alarm value. For analog mode, any mass
values that fall below this limit are counted even if they
are from the same scan.

Count Defines the number of consecutive readings that must


be below this limit before the alarm is triggered. Higher
count values decrease the possibility that a transient or
noise signal will set off a false alarm.

Auto Set button


When selected, this button automatically sets the alarm levels as
follows:

High Limit 10 times the current scan value


High Warning 5 times the current scan value
Low Warning 5 times less than the current scan value
Low Limit 10 times less than the current scan value

Action button
Choose the Action button to view the Alarm Action dialog box (Fig-
ure A-11), where you can specify what action the system should take
when the specified alarm is set. This can be used for all four alarms.

Figure A-11.
Alarm Action dialog
box.

Advanced Software Operation | A-19


Dialog Box
Specify a message to display when the alarm is set.

Message Enter a message that will be displayed in the Alarm


dialog box when the alarm is set.

Info File Enter the name and path of a help file or use the
Browse button to navigate to the location of a help
file and select the file.

This file will be launched when you click the Infor-


mation button in the Alarm message box that
appears when an alarm is set. For example, the file
could suggest what action to take when the alarm is
triggered. This function is currently not available.

Sound
Enter the name and path of a sound file or use the Browse button to
navigate to the location of the sound files and select a file. This allows
you to include warning sound (in addition to text instructions) to alert
the operator when the alarm is set.

Script (Configurator multi only)


Select a script that will perform some automated system instructions
when the alarm is triggered. You create the scripts in the Model 933
Configurator Software to perform predetermined actions.

Digital Output
Define how to send the alarm information to a digital output. Select
the device to which you want to send the digital output by using the
Device list box. Select the digital output module using the Module list
box.

Test Dialog button


Click this button to test the alarm. The Alarm message box will appear
(Figure A-12). Click Acknowledge or Disable to close this dialog box.

Figure A-12.
Alarm message dialog
box.

A-20 | Model 933 UV Analyzer


APPENDIX B – OPTIONS

Natural Gas Filter (Field Upgradeable) – Filterblock


The Natural Gas Filter (Filterblock) is used to filter pipeline natural gas for
critical instrumentation applications. Under normal operating conditions,
this gas often contains small quantities of liquids in the form of aerosol
droplets or liquids travelling along the walls of the pipe. Depending on
the processes upstream of the sample point, the liquids may be water,
glycols, amines, alcohols, heavy process hydrocarbons, or compressor oils.
Some typical locations where the liquids are found are given below:

• Small quantities of glycol droplets are often present immediately


downstream of glycol dehydration units.

• During process upsets, certain processes for removing heavy hydro-


carbons from natural gas, such as lean oil enrichment processes, are
prone to small quantities of residual liquid.

• Small quantities of compressor oil are periodically present at plant or


compressor outlets.

• In some cold climates, methanol is occasionally added to gas during


the winter. Methanol is also sometimes used for gas dehydration.
Occasionally, residual droplets may result.

• During sweetening processes in amine contactors, small quantities of


amine liquids are often entrained in gas.

• Natural gas produced from formations that are rich in heavy hydro-
carbons is usually processed. The processing reduces the hydrocarbon
dew point temperature to the required pipeline specifications. At these
installations, process upsets can result in high dew point temperatures
and hydrocarbon liquids in the gas.

Some instrumentation, such as pressure transmitters, does not react to


small quantities of liquids, while others, such as some flow measurement
devices, can be temporarily affected. Once the upset is over, these instru-
ments will return to normal.

Options | B-1
When accurate and reliable operation is needed for instruments such as
gas chromatographs, lead acetate tape or UV H2S analyzers, dew point
analyzers, some BTU analyzers, and intermittently-operated equipment
such as the manual dew point testers, the requirement of a liquid and
particulate-free sample is more critical. You will significantly reduce
maintenance of this instrumentation by using the appropriate filtration in
the sampling system.

For reliable analyzer operation, we recommend that you install a properly


designed filtration system in the Model 933 sampling system. If the
Natural Gas Filter option is not installed, then you should install a mem-
brane or coalescing-type filter.

The Natural Gas Filterblock Assembly is designed to filter natural gas in


the most critical instrumentation applications. The assembly has three
filtration stages. Each stage has its own drain/fast loop. The Filterblock
Assembly is shown in Figure B-1.

Filtration Stages
1. The first filtration stage is a coarse membrane filter. A membrane filter
is a thin membrane with small holes of a controlled size. Gases will
pass through the pores in the membrane with only a small pressure
drop. Liquid droplets will stay on the upstream side because their
surface tension is too high to allow them to pass through the pores.
This filter removes particulate and high surface-tension liquids such as
water, alcohols, glycols, and some amines. Most of the low-surface
tension liquids such as hydrocarbons will also be eliminated. Since this
membrane has a low surface area and volume, the filter will not
absorb volatile liquids. In contrast to the membrane filter, a single-
stage, coalescing filter can have problems, because during upset
conditions, these single stage filters become saturated with volatile
liquids and these liquids can only be evaporated slowly over time.

2. The second filtration stage is another membrane filter. This filter has
smaller pores than the first stage. In this stage, small quantities of low
surface tension liquids, such as hydrocarbons, that are not extracted
by the first filter are removed. Most of the pressure drop through the
entire Filterblock assembly occurs across the second filter stage.

3. The third and final filtration stage is a small coalescing filter. This filter
will remove trace quantities of liquid aerosols as small as 0.1 microns.
Should the membranes in the first two stages become ruptured, this
stage will temporarily act as the main particulate and liquid filter.

B-2 | Model 933 UV Analyzer


Vent Flow
• The total vent flow in the Model 933 is the sum of the flow through
the analyzer plus the flow from the drain flow restrictors in the three
filter stages.

• Flow through the analyzer is approximately 2.5 l/min (5.3 SCHF).

• Combined flow through the three drain flow restrictors is roughly


proportional to the pressure at the filter inlet.

• Total flow from the drain flow restrictors will increase by about 50
SCCM (0.05 l/min or 0.1 SCHF) for each 30 PSI (210 KPA) increase in
the inlet pressure. Typical values for this combined drain flow are:

- 0.165 l/min (0.35 SCHF) at 100 PSIG (690 KPAG) inlet pressure.

- 0.825 l/min (1.75 SCHF) at 500 PSIG (3450 KPAG) inlet pressure.

Preventive maintenance should be done on the Filterblock Assembly at


least once a year. During the maintenance, the filter elements and o-rings
should be changed. The housing components should also be cleaned. The
flow restrictors in each filter stage of the drain/fast loop should be
changed once a year. With very dirty natural gas streams, the flow
restrictor for the drain in the first filter stage may need to be changed
more often, because the first stage removes most of the liquids and par-
ticulate from the gas.

When depressurizing the system for any reason, always bleed off the
! pressure on the downstream side of the filter. If the pressure is dropped
CAUTION on the inlet side first, damage to the membrane filter elements may
result. Should the outlet pressure be higher than the inlet pressure by
as little as 210 KPA (30 PSI or 2 BAR), the membranes will rupture.
When one or both membranes have ruptured, replace them as soon as
possible.

Options | B-3
Natural Gas Filter Maintenance

Replacing O-rings and Flow Restrictors in the Filterblock

The parts that are removed and replaced in these procedures correspond
with Item #s in Figure B-1.

1. Depressurize the sampling system by shutting off the gas supply to


the inlet of the Filterblock Assembly. Bleed down the pressure on the
downstream side of the filter.

2. Using appropriate wrenches, disconnect all tubing connections to the


Filterblock Assembly and loosen the two mounting screws. Once the
screws are loose, slide the two mounting slots in the Filterblock assem-
bly out from the screw heads. Carry the Filterblock assembly to a
convenient work area.

3. Use a 5 mm ball-driver or hex wrench to remove the six M6 X 50 mm


stainless steel hex-socket cap screws (Item 11). Carefully separate the
assembly into three sections.

4. Visually inspect both membrane filters (Items 12 & 14) for damage,
particulate, and liquid films before removing the filters. Remove the
two small o-rings (Item 5) from the flat faces of the housings.

5. Use a 5 mm ball-driver or hex wrench to remove the three M6 X 20


mm hex-socket cap screws (Item 17). Remove the Filterblock Core
(Item 16) and inspect the Back Filterblock compartment (Item 24) for
signs of particulate or waxy films.

6. Remove the M6 nut (Item 23), washer (Item 22), o-ring (Item 21), and
then the coalescing filter element (Item 20).

7. To remove the drain/fast loop flow restrictor inserts (Item 3) in each of


the three filter stages, use appropriate wrenches to remove the fitting
from the bottom of each housing section. Use a 2.5 mm ball-driver or
hex wrench to remove the flow restrictor from the inside of each of the
three housing sections. Be careful not to damage the 1/8" NPT threads.
Remove the o-rings (Item 4) from each restrictor.

8. Clean all the metal parts in the assembly by immersing them in a clean
solvent. The solvent should not attack aluminum or stainless steel.
Remove the parts from the solvent and allow them to fully dry before
replacing. Isopropanol or acetone are both acceptable solvents for this
purpose.

B-4 | Model 933 UV Analyzer


1. M6 x 16 SS Hex Socket 14. Center Filterblock (300-6149)
Flat Head Screw (300-4600) – 2 places 15. Type-5 Membrane Filter (300-8594)
2. Mounting Bracket (300-9271) c/with separate #216 O-Ring (300-8643)
3. Flow Restrictor (100-1219) – 3 places 16. Sintered Disk (300-6257) – 2 places
4. O-Ring, Aflas, #008 (300-6241) – 3 places 17. Filterblock Core (300-6148)
5. O-Ring, Aflas, #006 (300-6244) – 2 places 18. M6 x 20 SS Hex Socket Cap Screw
6. 1/8-NPT Plug (300-5774) (300-4492) – 3 places
7. Front Filterblock (300-6147) 19. Male Connector (300-1236)
8. Male Connector (300-1239) 20. O-Ring, Aflas, #115 (300-6242)
9. 1/8-NPT Plug (300-5774) 21. Filter Cartridge (300-6217)
10. Male Connecter (300-1236) 22. O-Ring, Viton, #010 (300-2375)
11. M6 x 50 SS Hex Socket Cap Screw 23. Filterblock Seal Washer (300-6151)
(300-6216) – 6 places 24. M6 Nut (300-0263)
12. Button Plug (300-5010) – 2 places 25. Back Filterblock (300-6152)
13. High-Flow Membrane Filter (300-5862) 26. Tube Adapter (300-1400)
c/with attached #216 O-Ring (300-8643)

Figure B-1.
Filterblock Assembly.

Options | B-5
9. If the previous sample gas flow rates through the sampling system
suggest possible plugging of the internal flow restrictors (Item 3), the
restrictors should be replaced with new ones. If there was an excessive
amount of liquid in the first membrane filter stage, then the first drain
flow restrictor should be replaced.

10. Carefully install new o-rings (Item 4) on the internal flow restrictors.
Roll the o-rings over the threads making sure not to crack or scratch
the o-rings. In the bottom hole of each housing section, install a new
flow restrictor. Hand-tighten the restrictor using a 2.5 mm ball driver
or hex wrench.

Reinstalling Fittings and Replacing the Coalescing Cartridge


and Membrane Filters

The parts that are removed and replaced in these procedures correspond
with Item #s in Figure B-1.

1. Reinstall the flow restrictor fittings (Item 3) into the bottom of each
housing section. Use Teflon tape on the NPT threads.

2. Install two new small o-rings (Item 5) on the flat faces of the housing
sections.

3. Install a new o-ring (Item 19) in the Filterblock Core (Item 16). Do not
use any lubricants on the o-rings.

4. Install a new coalescing filter cartridge (Item 20). Secure the filter
cartridge with the washer (Item 22) and M6 nut (Item 23). Use a new
o-ring (Item 21), in the washer. Lightly tighten the M6 nut. Place the
coalescing filter assembly into its housing. You might have to rotate
the filter assembly as you push it into the housing (Item 24). Tighten
the M6 X 20 mm screws (Item 17) with a 5 mm ball driver or an hex
wrench until the Filterblock Core sits on the housing.

5. Place the Back Filterblock (Item 24) on a flat surface with the mem-
brane side facing up. Install one sintered stainless steel disk (Item 15)
into its recess.

6. Retrieve a new Type-5 flow membrane (membrane color white) and


o-ring (Item 14) from the plastic bag. Be extremely careful not to
damage the membrane. The Type-5 membrane and o-ring are not
bonded together, proceed to Step 8.

B-6 | Model 933 UV Analyzer


7. If the membrane and o-ring are bonded together, then place the
membrane/o-ring assembly over the o-ring groove, with the o-ring
side up. Gently press the o-ring to approximately half the groove
depth in one location. Likewise, depress the rest of the o-ring to half
its depth, beginning with the section across from the first location. The
membrane should now be tightly stretched.

8. If the membrane and o-ring are separate, then carefully centre the
membrane over the sintered disk. Use one finger to hold the mem-
brane in place. Place the o-ring over the membrane. Carefully push
the o-ring halfway into its groove in one location. Likewise, press the
rest of the o-ring to half its depth, beginning with the section across
from the first location. The membrane should now be tightly
stretched.

9. Place the Center Filterblock (Item 13) on a flat surface with the mem-
brane side facing up. Install the sintered disk (Item 15). Retrieve a new
high-flow membrane (membrane color white) and o-ring (Item 12)
from the clear plastic bag. Since the o-ring is usually bonded to the
High-Flow membrane, review Step 7 for instructions on installing it.

10. In all the housing sections, ensure that the o-rings are still in place.
Stack the three housings together by aligning the screw holes. Install
the M6 X 50 mm screws (Item 11). Tighten the screws in a cross-
pattern.

11. Install the Filterblock Assembly on the mounting screws. Attach and
tighten all tubing connections.

12. Open the valve at the inlet of the sampling system. With a suitable
leak detection liquid, leak check the Filterblock Assembly and fittings.

Although disassembling the Filterblock assembly to inspect the filters


 is possible, the o-rings and filter elements should be changed whenever
NOTE there is any doubt about the cleanliness or integrity of these parts.

Options | B-7
Filterblock Assembly Spare Parts
The recommended spare parts list for the Filterblock Assembly are listed
below.

General Maintenance – Recommended Parts to Have On-Site


Description Part No. 1 Year Qty 2 Year Qty Warranty
Flow Restrictor 100-1219 1 4 None
O-ring, Viton, #010 300-2375 1 2 None
High-Flow Membrane Filter 300-5862 1 2 None
comes with attached #216 O-Ring (300-8643)
Coalescing Filter Element 300-6217 1 2 None
O-ring, Aflas, #008 300-6241 1 4 None
O-ring, Aflas, #115 300-6242 1 2 None
O-ring, Aflas, #006 300-6244 2 4 None
Type-5 Membrane Filter 300-8594 1 2 None
comes with separate #216 O-Ring (300-8643)
O-ring, Viton, Filter 300-8643 1 2 None

B-8 | Model 933 UV Analyzer


Environmental Purge Option (Field Upgradeable)
The Environmental Purge option is used to reduce the humidity and
corrosive gas concentrations within the analyzer’s Upper and Lower
Enclosures through inlet and vent flame arrestors added to both enclo-
sures. Environmental purging is recommended in any location where the
relative humidity exceeds 70 % for long periods of time, or where the
surrounding atmosphere contains high trace concentrations of gases that
can corrode optics or electronics (e.g., sulfur dioxide, hydrogen sulfide).

This is an environmental purging option and should not be confused


! with purging actions taken for hazardous area classifications.
CAUTION

Connection and Use


The inlet and vent flame arrestors are located on the left side of the Upper
and Lower Enclosures (see Figure B-2).

• Use a 1/8” NPT female thread connector on the inlet flame arrestors.

• Use stainless steel fittings and tubing to connect clean and dry air or
nitrogen to both inlet flame arrestors at a pressure of between 1 and 10
PSIG (6.9 and 69 KPAG).

• The purge gas should have a water dew point temperature of less
than -30 °C and be contaminant free.

Do not attempt to make a connection to the vent flame arrestor


! fittings.
WARNING

The purge gas consumption will be approximately proportional to the


supply pressure at the inlet flame arrestors. At a supply pressure range of
1 to 10 PSIG (6.9 to 69 KPAG), the purge gas flow rate range should be
between 10 and 100 SCCM (0.01 and 0.1 l/min or 0.02 and 0.2 SCFH). A
large cylinder of air or nitrogen can last as long as 1 1/2 years or as short a
time as two months, depending on the supply pressure. The low flow rate
created by 1 PSIG (6.9 KPAG) supply pressure is sufficient to purge the
enclosures, so there is no advantage to using higher supply pressures; this
only leads to increased purge-gas consumption.

Options | B-9
UPPER ENCLOSURE

Figure B-2.
Inlet and vent flame
arrestor locations for
Environmental Purge
Option. LOWER ENCLOSURE

B-10 | Model 933 UV Analyzer


Pressure Compensation Option (Field Upgradeable)
The Pressure Compensation option provides pressure correction and
diagnostics to the analyzer by adding a 0–100 PSIA (0–700 KPA; 0–5171.49
mmHg) pressure transducer to the lower enclosure. The pressure trans-
ducer location and plumbing is shown in the Backpan Layout and Lower
Enclosure drawings located in Chapter 3.

Setting Up the Pressure Compensation Option


This option is enabled using the Configurator Software. If your analyzer
was ordered with this option, it was set up and tested at the factory – no
further adjustment is required. If you are adding this option to your
analyzer, proceed as follows:

Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING

Do not remove the cover of the Explosion-Proof Digital Communica-


tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.

1. Connect your laptop computer to the analyzer via the Explosion-Proof


Digital Communications Port on the front of the Lower Enclosure.
Start the computer and the Configurator Software.

2. From the Edit menu, click Device Properties.

3. From the M933 Properties dialog box, click the Setup tab and then
click Compensations to view the Compensations dialog box (Figure
B-3).

Figure B-3.
Compensations tab
using the Pressure
Compensation option.

Options | B-11
4. Click Measured under Cell Pressure and then enter the LowScale and
HighScale values to activate the measurement (refer to Chapter 4 for
more information).

 Jumpers on the Customer I/O Board are set up for a default pressure
measurement range of 3413.19–5171.49 mm Hg absolute (66–100
NOTE
PSIA).

Using the Pressure Compensation Option


The analyzer will use the measured cell pressure to compensate for the
effect of pressure on the species concentrations. Adjust the pressure gauge
on the analyzer to use 80 PSIG cell pressure. Small deviations in pressure
due to regulator/gauge drift will be corrected automatically.

Diagnostics Feature

In addition to compensating for concentration measurements, the ana-


lyzer also uses the pressure measurements for diagnostics. If the sample
gas pressure drops to the Low Scale value, the analyzer activates a Fault
alarm to indicate that the sample gas has been shut off. If you are per-
forming an Auto-Zero calibration and the zero gas pressure drops to the
Low Scale value, the analyzer activates a Warning alarm to indicate that
the zero gas cylinder is empty or has been shut off. See the “Diagnostics
and Troubleshooting” section in Chapter 6 for more information.

B-12 | Model 933 UV Analyzer


Loop-Powered Current Outputs (Field Upgradeable)
The standard analyzer comes with one self-powered current (V/I) output
configured for hydrogen sulfide concentration. This self-powered current
output can be replaced with an optional Loop-Powered Current Output.
Additional current outputs can be added as well (see the “Calibrated
Carbonyl Sulfide Output” and “Calibrated Methyl Mercaptan Output”
options in this appendix for more details).

Using the Loop-Powered Current Option


Loop-Powered Current Outputs are typically specified only when you
want to power the current output loop rather than using the analyzer to
do it.

• The user must supply an external power supply (15–30 VDC) capable
of supplying 25 mA per loop.

• The wiring of both types of current output is shown in the Customer


Connections Wiring Schematic in Chapter 3.

Options | B-13
Low Range (White Cell) Measuring Cell (Field Upgradeable)
The standard analyzer is equipped with a 2-pass measuring cell with a
total path length of 40 cm. The Low Range (White) Cell and path length
combination is suitable for hydrogen sulfide minimum full-scale concen-
tration ranges of 0–25 PPM. As an option, the 40 cm cell can be replaced
with a 4-pass Measuring Cell with 81.2 cm path length. This longer, Low
Range measuring cell is suitable for hydrogen sulfide minimum full-scale
concentration ranges as low as 0–5 PPM.

Review the specifications in Chapter 2 for more details on the specifica-


tions of the Low Range (White) Cell as compared to the standard cell.

When cleaning the Measuring Cell as part of your preventive mainte-


nance program, use the instructions for the Low Range option when
specified. The Standard Range Cell is mounted somewhat differently and
some instructions vary. Review Chapter 6 for details and assembly draw-
ings for both Measuring Cells.

B-14 | Model 933 UV Analyzer


Calibrated Carbonyl Sulfide Output (Factory Upgradeable Only)
The standard analyzer comes with one self-powered current (V/I) output
configured for hydrogen sulfide concentration. The standard analyzer
measures carbonyl sulfide (COS) and methyl mercaptan (MeSH) concen-
trations and compensates the Hydrogen Sulfide (H2S) reading for their
presence. The hydrogen sulfide output from the analyzer is tested and
calibrated at the factory so that the interference of the other two species is
minimized.

Using a Calibrated Carbonyl Sulfide Output


Choose the Calibrated Carbonyl Sulfide Output option when the carbonyl
sulfide reading is used for process control or diagnostic purposes.

• This option installs an additional self-powered current output that is


configured for carbonyl sulfide concentration.

• Extra gas runs are performed at the factory to minimize the interfer-
ence of hydrogen sulfide and methyl mercaptan on the carbonyl
sulfide reading. These additional calibration tests ensure that the
carbonyl sulfide output meets the accuracy specifications as stated in
Chapter 2. These accuracy specifications also depend on whether the
analyzer is equipped with a Standard or Low Range (White Cell)
Measuring Cell.

• The wiring connections for the extra current output are shown in the
Customer Connections Wiring Schematic in Chapter 3.

Options | B-15
Calibrated Methyl Mercaptan Output (Factory Upgradeable Only)
The standard analyzer comes with one self-powered current (V/I) output
configured for hydrogen sulfide concentration. The standard analyzer
measures carbonyl sulfide (COS) and methyl mercaptan (MeSH) concen-
trations and compensates the hydrogen sulfide (H2S) reading for their
presence. The hydrogen sulfide output from the analyzer is tested and
calibrated at the factory so that the interference of the other two species is
minimized.

Using a Calibrated Methyl Mercaptan Output


Choose the Calibrated Methyl Mercaptan Output option when the me-
thyl mercaptan reading is used for process control or diagnostic purposes.

• This option installs an additional self-powered current output that is


configured for methyl mercaptan concentration.

• Extra gas runs are performed at the factory to minimize the interfer-
ence of hydrogen sulfide and carbonyl sulfide on the methyl mercap-
tan reading. These additional calibration tests ensure that the methyl
mercaptan output meets the accuracy specifications as stated in
Chapter 2. These accuracy specifications also depend on whether the
analyzer is equipped with a Standard or Low Range (White Cell)
Measuring Cell.

• The wiring connections for the extra current output are shown in the
Customer Connections Wiring Schematic in Chapter 3.

B-16 | Model 933 UV Analyzer


APPENDIX C – MODBUS
COMMUNICATION INTERFACE

 The Modbus register buffer in an analyzer will have all system’s


configuration parameters refreshed at analyzer start up and after each
NOTE
calibration (CAL) action. When updating any parameters using the
Model 933 Configurator Software, the changes will not be available in
Modbus polling until after a CAL action is complete or after the
analyzer has been reset. Ensure this condition is met before using the
Modbus communication.

Overview
This Appendix (Model 933 Analyzer Customer Modbus Communication
Interface, Revision 1.3, November 17, 2003) describes the customer serial
communication interface on the Model 933 Analyzer. The communication
protocol implemented is Modicon Modbus as defined in “Modicon Modbus
Protocol Reference Guide” (PI-MBUS-300 Rev. C). The Modbus protocol
transmission mode implemented is Remote Terminal Unit (RTU) with the
analyzer operating as a slave device.

The physical communication connection between a Model 933 Analyzer


and a customer DCS\SCADA\PLC\DAS is RS-485. The analyzer RS-485
connection supports both 4-wire and 2-wire multi-drop systems. Refer to
the section titled “Digital Communication” in Chapter 3 (see the “Cus-
tomer Data Acquisition Port” configuration). A 4-wire full-duplex system is
the preferred and recommended choice. When designing a Modbus
RS-485 multi-drop communication system with the Model 933 Analyzer,
the system designer should consider the following:

• Analyzer primary outputs are concentrations of gas species being


analyzed and analyzer status codes. The register values are updated
once a second. Polling of these registers more frequently than once a
second is not recommended.

Modbus Communications Interface | C-1


• Analyzer secondary and diagnostic output registers are intended for
mid-term (e.g., minutes, hours) and long-term (e.g., days, months)
trending purpose. The register values are mostly updated once a few
seconds. Frequent polling of these registers is not required and not
recommended.

• Analyzer operation setup-related registers are modified only through


the service port or the Modbus port. The register values remain
unchanged unless service work has been performed on the analyzer
or the settings in the Modbus master have been changed. Polling of
these registers should be done occasionally as needed.

• The maximum polling rate of a Modbus multi-drop system is deter-


mined by a number of factors including the number of devices on the
system, the number of registers being polled from each device, the
baud rate and half- or full-duplex operation. Calculations, and possi-
bly experimentation, are needed to attain optimal system operation.

Modbus Interface Parameters


A number of analyzer Modbus interface parameters needs to be set up in
order to establish communication with the Modbus master. These param-
eters are accessed via the service port on the analyzer using the
Configurator Software program running on a computer.

Modbus Address
The analyzer needs to be assigned a Modbus slave address, which can be
a number from 0–247 with ‘0’ disabling the analyzer Modbus interface
altogether.

Communication Parameters
While the number of data bits is always 8, the baud rate, number of stop
bits and parity of the analyzer Modbus serial communication port are
selectable. The default communication parameter settings are 9600 baud,
1 stop bit and no parity.

Default Communication Parameter Settings


Value Baud Rate Stop Bits Parity
0 9600 1 None
1 4800 2 Odd
2 2400 — Even
3 1200 — —

C-2 | Model 933 UV Analyzer


Modbus Functions
As the Modbus protocol is designed for communication among Program-
mable Logic Controllers (PLCs), not all Modbus function codes supported
by a slave PLC are applicable to the Model 933 Analyzer. Only the rel-
evant function codes are implemented:

Modbus Function Codes


Code Description
01 read multiple digital outputs\coils (0x references)
02 read multiple digital inputs (1x references)
03 read multiple holding registers (4x references)
05 write one digital output\coils (0x references)
06 write one holding register (4x references)
08 loop-back test
15 write multiple digital outputs\coils (0x references)
16 write multiple holding registers (4x references)
17 read slave ID and status information

• Accordant to Modbus protocol specification, all address references in


Modbus messages are numbered relative to zero. For example, the first
holding register in a Modbus slave being referenced as “40001” would
be addressed as “0”. Similarly, output\coil 00010 would be addressed
as “9”.

• As for the loop-back test function, only one diagnostic code, Return
Query Data (00), is supported by the Model 933 Analyzer for verifica-
tion of correct communication connection. Illegal function exception
code is returned for unsupported loop-back test diagnostic codes.

Modbus Communications Interface | C-3


Exception Code
The Model 933 Analyzer Modbus protocol implementation supports these
exception codes:

Modbus Exception Codes


Code Description Condition

01 Illegal Function Unsupported function requests from Modbus master.


02 Illegal Address Requested address is outside the allowed range, or
writing to a read-only location.
03 Illegal Value Values written to holding registers are outside the
appropriate ranges.
06 Busy, Rejected Message Analyzer is unable to proceed with the calibration action
requested by the Modbus master.

Unsupported function requests from the Modbus master result in excep-


tion code 01 being returned. Illegal address exception code is returned
when the requested address is outside the allowed range or writing to a
read-only location. When the values to be written to holding registers are
outside the appropriate ranges, exception code 03 is returned. Busy
response is returned if the analyzer is unable to proceed with the calibra-
tion action requested by the Modbus master.

Digital Output Status


The analyzer digital output bits can be read as a group via Modbus func-
tion code 01 and each bit can be written to via Modbus function code 05 or
15. The bit definitions are:

Digital Output Status – Bit Definitions


Bit Definition Access

0 Reserved —
1 Auto-Zero r,w
2–7 Reserved —
8 Manual Zero r,w
9 Manual Span r,w
10–22 Reserved —
23 Concentration Alarm Soft Enable (0 = disable; 1 = enable) r,w
24 Fault Relay (0 = fault; 1 = normal) r
25 Warning Relay (0 = warning; 1 = normal) r
26 Concentration Alarm Invalid Relay (0 = invalid; 1 = valid) r
27 Concentration Alarm1 (0 = off; 1 = on) r

C-4 | Model 933 UV Analyzer


Bit Definition Access

28 Concentration Alarm2 (0 = off; 1 = on) r


29 Column A Solenoid (0 = off; 1 = on) r
30 Column B Solenoid (0 = off; 1 = on) r
31 Zero Gas Solenoid (0 = off; 1 = on) r

• Bits #0 to #22 indicate the current analyzer calibration action status.

- One (1) indicates the associated action is in progress

- Zero (0) indicates that the action is inactive.

Writing a “1” using Modbus function code 05 or 15 to one of bits #0 to


#22 starts the addressed calibration action. The bit stays set for as long
as the calibration action is in progress so that the Modbus master can
read the bit to determine if the action has been completed.

If the Modbus master initiates the same action before that action is
completed, the message is acknowledged but the action does not
restart. Since only one calibration action can be active at any given
time, if function code 15 is used to request more than one action, the
lowest action bit in the request takes precedence.

• Writing a “0” while the addressed calibration action is in progress


cancels the action.

However, only a calibration action initiated from the Modbus interface


can be cancelled from the Modbus interface. A calibration action
started at the analyzer using the service communication port, on a
timed basis or by remote digital input, cannot be cancelled using the
Modbus.

Before initiating a calibration action, the Modbus master must read


bits #0 to #22 to ensure that no action is in progress at that time. If a
calibration action is already in progress, a busy message is returned.
When the analyzer encounters fault conditions as indicated by bit
#24, FAULT Relay, a calibration action cannot be started by the
Modbus master and a busy message is also returned.

• Writing a “0” or “1” using Modbus function code 05 or 15 to bit #23


disables or enables the concentration alarms only when these alarms
are enabled by the Hard-Wired Concentration Alarm Enable Input.
Refer to the Customer Connections Wiring Schematic in Chapter 3 or
Appendix D. Status bits #24 to #21 are set and cleared according to
the conditions described under the section “Diagnostics and Trouble-
shooting” in Chapter 6.

Modbus Communications Interface | C-5


Digital Input Status
There are two digital inputs on the Model 933 Analyzer. They can be read
via Modbus function code 02 and the bit definitions are:

Digital Input Status – Bit Definitions


Bit Definition Value

0 Remote Auto-Zero Input 1 = enable (closed)


0 = disable (open)
1 Hard-Wired Concentration Alarm Enable Input 1 = start (closed)
0 = normal (open)

Holding Registers
RAM space on the Model 933 Analyzer is limited and not every
customer’s data acquisition system supports Modbus floating point value
transfer. These floating point values, accessed on a Model 933 Analyzer,
are scaled up and converted into integer values to load into Modbus
registers for transmission. The register values must be scaled back at the
receiving end to yield the actual values. The size of a Modbus holding
register is 16-bit. It can assume a value from -32768 to +32767 in two’s
complement. The holding register definitions, units of measurement and
scaling factors are listed in the following pages.

The references to ‘*’, ‘**’, ‘***’, and ‘#’ in the Holding Register Defini-
tions are:

* Each concentration result is the product of the concentration value generated


internally by the analyzer and multiplied by its corresponding Unit Conversion Factor
in registers 134 to 145.

The unit of measurement for concentration result is PPMV when the Unit Conversion
Factor is the default value of 1.0. However, the concentration result unit can be
changed, for example to mg/Nm3 or lb/mmscf, using a different Unit Conversion
Factor. See “Custom Output” in Chapter 4.

The concentration result, the drift specification, the span concentra-


 tion, and the alarm threshold of a species must be in the same unit of
NOTE measurement.

** The unit for Unit Conversion Factor is desired result unit/PPMV.

C-6 | Model 933 UV Analyzer


*** The scaling factors of concentration result are in registers 154 to 159, in the default
value of 100. They are applicable to the concentration results, the drift specification,
the span concentration, and the alarm threshold of a species. A scaling factor value of
100 means that the corresponding result-related value in the Modbus register is 100
times larger than its real value, and its scaled-back floating-point value will have two
digits after the decimal point. On the contrary, a scaling factor value of -100 means
that the corresponding result-related value in the Modbus register is 100 times smaller
than its real value, and its scaled-back floating-point value will have two zero digits
before the decimal point. Scaling factor values of 0 and -1 are not practical and will be
treated as 1.
# The default Custom Result Factor is 1.0 and the custom concentration result equation
is:

Custom Result = CustomResultFactor1 * ConcentrationResult1


+ CustomResultFactor2 * ConcentrationResult2
+ CustomResultFactor3 * ConcentrationResult3
+ CustomResultFactor4 * ConcentrationResult4

REG DEFINITION UNITS SCALING ACCESS


* ***
0 Concentration Result 1: H2S r
* ***
1 Concentration Result 2: COS r
* ***
2 Concentration Result 3: MeSH r
* ***
3 Concentration Result 4: Reserved r
* ***
4 Concentration Result 5: NDr2 r
* ***
5 Concentration Result 6: NDr1 r
*
6 Concentration Result 7: custom result# 100 r

7–9 Reserved – – –
10–19 Track & Hold Results of Registers 0 to 9 Reg0 to Reg9 Reg0 to Reg9 Reg0 to Reg9

20 Cell Pressure mmHg 1 r


21 Column Temperature °C 10 r
22 Bench Temperature °C 10 r
23 Cell Temperature °C 10 r
24 Reserved – – –
25 Reserved – – –
26 Analyzer Status: OBMC Warning Bit Image – – r
27 Analyzer Status: OBMC Fault Bit Image – – r
28 Analyzer Status: HC Warning Bit Image – – r
29 Analyzer Status: HC Fault Bit Image – – r
30 Time to Next Auto Zero min 1 r
-1 = auto-zero disabled
31 Time to End of Calibration sec 1 r
-1 = no calibration in progress

Modbus Communications Interface | C-7


REG DEFINITION UNITS SCALING ACCESS

32 Time to Next Column Switch sec 1 r


-1 = column switching not active
33 Reserved – – –
34 Reserved – – –
35 Column Heater Duty Cycle % 1 r
36 Bench Heater Duty Cycle % 1 r
37 Cell Heater Duty Cycle % 1 r
38 Reserved – – –
39 Reserved – – –
40 Optical Filter Wheel Speed RPM 1 r
41–46 Lamp Pulses for Optical Filters 1 to 6 mV 1 r
47 Reserved – – –
48 Reserved – – –
49 Digital Input Bit Image – – r
50 Digital Output Bit Image: lower 16-bit – – r,w
51 Digital Output Bit Image: upper 16-bit – – r,w
52–57 Zero Transmittance of Optical Filters 1 to 6 – 1000 r,w
*
58–63 Zero Drift Spec of Concentration Results 1 to 6 /day 100 r,w
*
64–69 Span Gas Concentration of Results 1 to 6 100 r,w

70–75 Span Factor of Concentration Results 1 to 6 – 1000 r,w


76–81 Concentration Hold Time for Result 1 to 6 sec 1 r,w
82 Concentration Alarm1: Result Assignment – – r,w
0 = disable
83 Concentration Alarm2: Result Assignment – – r,w
0 = disable
* ***
84 Concentration Alarm1: ON Threshold r,w
* ***
85 Concentration Alarm2: ON Threshold r,w
* ***
86 Concentration Alarm1: OFF Threshold r,w
* ***
87 Concentration Alarm2: OFF Threshold r,w

88 Concentration Alarm1: Delay sec 1 r,w


89 Concentration Alarm2: Delay sec 1 r,w
90 Concentration Alarm1: Latching – – r,w
0 = non-latching, 1 = latching
91 Concentration Alarm2: Latching – – r,w
0 = non-latching, 1 = latching
92 Bench Auto Setup Status – – r,w
Read:
0 = off/completed
1 = adjust PMT level
2 = adjust lamp pulses
3 = adjust PMT balance
4 = adjust PMT level
5 = adjust lamp pulses,
6 = set-up ALC
Write:
0 = stop, 1 = start

C-8 | Model 933 UV Analyzer


REG DEFINITION UNITS SCALING ACCESS

93 Gas Flow Control – – r,w


0 = auto
1 = column-A
2 = column-B,
3 = zero
4 = shut-in
5 = sample
94 Auto-Zero Interval hr 1 r,w
95 Auto-Zero Duration min 1 r,w
96 Calibration Duration sec 1 r,w
97 Column Switch Interval sec 1 r,w
98 Reserved – – –
99 Exclude Cal-condition in activation of warning alarm – – r,w
0 = include
1 = exclude
100 Bench Temperature Range Selection – – r,w
1 = 30 to 45 °C
2 = 45 to 60 °C
101 Cell Temperature Range Selection – – r,w
1 = -5 to 65 °C
2 = 60 to 130 °C
3 = 125 to 195 °C
4 = 190 to 260°C
102 Reserved – – –
103 Reserved – – –
104 Column Heater Temperature Set-Point °C 10 r,w
105 Bench Heater Temperature Set-Point °C 10 r,w
106 Cell Heater Temperature Set-Point °C 10 r,w
107 Reserved – – –
108 Reserved – – –
109 Column Heater Control: Kp – proportional factor °C 10 r,w
110 Bench Heater Control: Kp – proportional factor °C 10 r,w
111 Cell Heater Control: Kp – proportional factor °C 10 r,w
112 Reserved – – –
113 Reserved – – –
114 Column Heater Control: Ti – integral factor sec 1 r,w
115 Bench Heater Control: Ti – integral factor sec 1 r,w
116 Cell Heater Control: Ti – integral factor sec 1 r,w
117 Reserved – – –
118 Reserved – – –
119 Column Heater Control: Start-Up Duty Cycle % 1 r,w
120 Bench Heater Control: Start-Up Duty Cycle % 1 r,w
121 Cell Heater Control: Start-Up Duty Cycle % 1 r,w
122 Reserved – – –
123 Reserved – – –
124 Column Temperature: Too-Cold Threshold °C 10 r,w

Modbus Communications Interface | C-9


REG DEFINITION UNITS SCALING ACCESS

125 Bench Temperature: Too-Cold Threshold °C 10 r,w


126 Cell Temperature: Too-Cold Threshold °C 10 r,w
127 Reserved – – –
128 Reserved – – –
129 Column Temperature: Too-Hot Threshold °C 10 r,w
130 Bench Temperature: Too-Hot Threshold °C 10 r,w
131 Cell Temperature: Too-Hot Threshold °C 10 r,w
132 Reserved – – –
133 Reserved – – –

134–145 Unit Conversion Factor 1 to 6* ** Floating Point Value


r,w
# Floating Point Value
146–153 Custom Result Factor 1 to 4 #
r,w

154–159 Result Scaling Factor 1 to 6*** – 1 r,w

Holding registers #0 to #29 are the primary registers the Modbus master
should monitor regularly. Their values are updated once a second.
• Registers #0 to #19 are concentration results calculated by the ana-
lyzer.
• Registers #20 to #25 are analog inputs measured by the analyzer.
• Registers #26 to #29 are analyzer status codes.

The gas species assigned to concentration results listed in the “Hold-


 ing Registers” table assume default configuration. They are subject to
NOTE reassignment to customize the analyzer to an application.

Holding registers #30 to #51 are mainly for diagnostic purpose.


• Registers #30 to #34 are analyzer action countdown timers.
• Registers #35 to #39 are various heater duty cycles.
• Optical bench health is indicated by registers #40 to #48.
• Digital I/O bit images are duplicated in registers #49, #50 and #51 for
the convenience of customers whose Modbus communication system
only supports holding register read and write functions. The content
of these three registers is updated once a second. The layout and
definition of the bits in these registers are the same as those defined in
the corresponding sections in this document. The only difference is
that no busy message is returned if the analyzer is unable to proceed
with the requested action as the Modbus protocol does not permit
unsolicited message to be sent from a slave to a master.

C-10 | Model 933 UV Analyzer


Holding registers #52 to #133 are variables the Modbus master can alter
either to customize the analyzer calibration process or to alert the analyzer
of changing process operating conditions.

Holding registers #134 to #153 are used for customizing analyzer concen-
tration result outputs. They are normally set up at the factory and do not
require modification by the customer. They are accessed as floating point
values and are included here for completeness.

Registers #154 to #159 are used for programming the scaling factors of
analyzer concentration result-related values.

Modbus Communications Interface | C-11


ID/Status Information
The Modbus master can poll the analyzer periodically for status informa-
tion via Modbus function 17. The information returned has the following
format:

1 Byte Slave ID = 33h for Model 933 Analyzer

1 Byte Run Light = FFh for On\Normal


= 00h for Off\Fault

1 Dword Run Time = analyzer run time in seconds


(4 bytes)

2 Word OBMC Status = Optical Bench Microcontroller


warning status and fault status

Description (first word)


Bit 0 = Normal; 1 = Warning

0 PMT Signals Out of Range

1 ALC Out of Range

2 Cell Temperature Out of Range

3 Bench Temperature Out of Range

4 Bench Auto Setup Problem

5–15 Reserved

Description (second word)


Bit 0 = Normal; 1 = Fault

0 Filter Wheel Speed Out of Range

1 On-Board A/D Not Responding

2 On-Chip ADC Not Responding

3 OBMC-HC Communication Problem

4 Cell Temperature Out of Range

5 Lamp Failure

6–15 Reserved

C-12 | Model 933 UV Analyzer


2 Word HC Status = Host Controller warning status
and fault status

Description (first word)


Bit 0 = Normal; 1 = Warning

0 EEPROM Full

1 Analog Output Out of Range

2 Column Temperature Too High

3 Excessive Zero Drift

4 Zero Gas Pressure Out of Range

5 Sample Gas Pressure Too High

6–15 Reserved

Description (second word)


Bit 0 = Normal; 1 = Fault

0 HC-MC Communication Problem

1 Analytical Data Not Received

2 Sample Pressure Too Low

3 On-Chip A/D Not Responding

4 Column Temperature Too Low

5–15 Reserved

Modbus Communications Interface | C-13


This page intentionally left blank.

C-14 | Model 933 UV Analyzer


APPENDIX D – DRAWINGS

This appendix contains drawings included in the main body of this


manual, additional assembly drawings that can be used for advanced
maintenance purposes, and extra drawings that are not included in the
main body of this manual.

If advanced maintenance procedures are not included in this manual,


contact AMETEK for assistance on changing out replaceable parts.

Drawings that are customer-specific are included in the “Supplemen-


 tal Information” tab of this manual, and in the Documentation
NOTE Package shipped with the analyzer. For installation and maintenance/
diagnostic purposes, use these drawings in place of the associated
drawings in the manual.

Drawings | D-1
Backpan Dimensions

PROCESS INSTRUMENTS

CAUTION:
RIS K OF ELECTRIC SHOCK

ATTENTION:
CONSULT USER MANUAL

0344

II 2 G
PROCESS INSTRUMENTS

Western Research Model 933 Analyzer


Certificate No: KEMA 02ATEX2247, EEx d IIB T3 (T amb. 0°C...50°C)
Year. _______
Serial No. __________________

Caution
Do not open when an explosive gas atmosphere is present.

Power Dissipation Input


<210W 120VAC 50/60Hz 2A max.
<210W 240VAC 50/60Hz 1A max.

SERIAL COMMUNICATIONS PORT


DO NOT OP EN IF A HAZARDOUS
GAS ATMOSPHERE IS PRESENT

MAY NOT BE EXACTLY AS SHOWN

D-2 | Model 933 UV Analyzer


Upper Enclosure

LOOSE CLAMPED

OPTICAL BENCH REMOVAL/INSTALLATION

Drawings | D-3
Lower Enclosure

D-4 | Model 933 UV Analyzer


Backpan Component Layout (North America)

PROCESS INSTRUMENTS

SERIAL COMMUNICATIONS PORT


DO NOT OPEN IF A HAZARDOUS
GAS ATMOSPHERE IS PRESENT

MAY NOT BE EXACTLY AS SHOWN

Drawings | D-5
Backpan Component Layout (Europe)

PROCESS INSTRUMENTS

CAUTION:
RISK OF ELECTRIC SHOCK

ATTENTION:
CONSULT USER MANUAL

0344

PROCESS INSTRUMENTS II 2 G

Western Research Model 933 Analyzer


Certificate No: KEMA 02ATEX2247, EEx d IIB T3 (T amb. 0°C...50°C)
Year. _______
Serial No. __________________

Caution
Do not open when an explosive gas atmosphere is present.

Power Dissipation Input


<210W 120VAC 50/60Hz 2A max.
<210W 240VAC 50/60Hz 1A max.

SERIAL COMMUNICATIONS PORT


DO NOT OPEN IF A HAZARDOUS
GAS ATMOSPHERE IS PRESENT

MAY NOT BE EXACTLY AS SHOWN

D-6 | Model 933 UV Analyzer


Column Block Assembly

1. Internal Tooth 3 mm SS Washer (300-0642) – 4 places 15. Column Block Mounting Tube (300-9123)
2. Ground Terminal (300-0511) 16. Mounting Tube Locknut (300-9135) – 2 places
3. Ground Wire (300-8306) 17. M6 x 20 Socket HD SS Hex Screw (300-4492) – 10 places
4. Filter Spool (300-9149) 18. M3 x 6 Button HD SS Hex Screw (300-4865) – 6 places
5. O-Ring, Aflas, #113 (300-9147) 19. Warning Label (300-9169)
6. Coalescing Filter Element (300-6217) 20. Column Block Flange (300-9159)
7. O-Ring, Viton, #010 (300-2375) 21. 1/8" O-Ring Seal Fitting (300-9139) – 3 places
8. M6 Nut (300-0263) 22. Cartridge Heater 120 VAC (300-9038)
9. O-Ring, Viton, #121 (300-8719) 240 VAC (300-9039)
10. Column Assembly 23. Flow Restrictor (100-1794) – 2 places
2-Turn Column Assembly (100-1789) 24. O-Ring, Aflas, #008 (300-6241) – 2 places
4-Turn Column Assembly (100-1857) 25. Column Block (300-9156)
11. Seal Washer (300-6151) 26. Check Valve (100-1788) – 2 places
12. RTD (300-4924) 27. Column Block Valve Cover (300-9160)
13. Overtemp Switch (300-9062) 28. M6 x 12 Socket HD SS Hex Screw (300-4496) – 3 places
14. Overtemp Switch Mounting Hardware 29. O-Ring, HSN, #125 (300-9060)

Drawings | D-7
AC Distribution PWB (P/N 100-1771)

D-8 | Model 933 UV Analyzer


Customer I/O Board (P/N 100-1758)

Drawings | D-9
Host Controller Board (P/N 100-1757)

D-10 | Model 933 UV Analyzer


Microcontroller Board (P/N 100-1781)

Drawings | D-11
Micro-Interface Board (P/N 100-1759)

D-12 | Model 933 UV Analyzer


Optical Bench Service Electronics Board (P/N 100-1662)

Optical Bench Service Electronics Board (P/N 100-1662) is without


 bracket; P/N 100-1841 is with bracket. When ordering a replacement
NOTE Optical Bench Service Electronics Board, use P/N 100-1841.

Drawings | D-13
Customer Connections Wiring Schematic (North America)

I/O BOARD CUSTOMER CONNECTIONS

120VAC POWER TERMINATIONS

HC BOARD CUSTOMER CONNECTIONS

D-14 | Model 933 UV Analyzer


Customer Connections Wiring Schematic (Europe)

I/O BOARD CUSTOMER CONNECTIONS

220VAC POWER TERMINATIONS

HC BOARD CUSTOMER CONNECTIONS

Drawings | D-15
Conduit Entries and AC Power Connection Locations (North
America)

LOWER ENCLOSURE

DETAIL A

D-16 | Model 933 UV Analyzer


Conduit Entries and AC Power Connection Locations (Europe)

LOWER ENCLOSURE

DETAIL A

Drawings | D-17
RS-232 Cable Communications Connections

D-18 | Model 933 UV Analyzer


Analyzer Wiring Diagram

Drawings | D-19
Natural Gas Filterblock Assembly – Optional (P/N 100-1782)

1. M6 x 16 SS Hex Socket 14. Center Filterblock (300-6149)


Flat Head Screw (300-4600) – 2 places 15. Type-5 Membrane Filter (300-8594)
2. Mounting Bracket (300-9271) c/with separate #216 O-Ring (300-8643)
3. Flow Restrictor (100-1219) – 3 places 16. Sintered Disk (300-6257) – 2 places
4. O-Ring, Aflas, #008 (300-6241) – 3 places 17. Filterblock Core (300-6148)
5. O-Ring, Aflas, #006 (300-6244) – 2 places 18. M6 x 20 SS Hex Socket Cap Screw
6. 1/8-NPT Plug (300-5774) (300-4492) – 3 places
7. Front Filterblock (300-6147) 19. Male Connector (300-1236)
8. Male Connector (300-1239) 20. O-Ring, Aflas, #115 (300-6242)
9. 1/8-NPT Plug (300-5774) 21. Filter Cartridge (300-6217)
10. Male Connecter (300-1236) 22. O-Ring, Viton, #010 (300-2375)
11. M6 x 50 SS Hex Socket Cap Screw 23. Filterblock Seal Washer (300-6151)
(300-6216) – 6 places 24. M6 Nut (300-0263)
12. Button Plug (300-5010) – 2 places 25. Back Filterblock (300-6152)
13. High-Flow Membrane Filter (300-5862) 26. Tube Adapter (300-1400)
c/with attached #216 O-Ring (300-8643)

D-20 | Model 933 UV Analyzer


Solenoid Block (North America)

Do not perform maintenance on this assembly without first contact-


 ing AMETEK to verify operation. AMETEK will provide assistance
NOTE on how to perform maintenance on this assembly .

Drawings | D-21
Solenoid Block (Europe)

Do not perform maintenance on this assembly without first contact-


 ing AMETEK to verify operation. AMETEK will provide assistance
NOTE on how to perform maintenance on this assembly .

D-22 | Model 933 UV Analyzer


Standard Range Measuring Cell (100-1811)

Drawings | D-23
Low Range (White) Measuring Cell (100-1780)

D-24 | Model 933 UV Analyzer


Inlet and Vent Flame Arrestor Locations for Environmental
Purge Option

UPPER ENCLOSURE

LOWER ENCLOSURE

Drawings | D-25
PMT Buffer Board P/N 100-0140

D-26 | Model 933 UV Analyzer


Optical Bench Assembly

Drawings | D-27
This page intentionally left blank.

D-28 | Model 933 UV Analyzer


APPENDIX E – CONVERSION FACTORS AND
CALCULATIONS

Conversion Factors
PARAMETER TO CONVERT FROM: TO: MULTIPLY BY:
AMOUNT of SUBSTANCE lb mol kmol 0.453 592 4
g mol kmol 0.001
(for Ideal gas) m of gas (0 °C, 101.325 kPa)
3
kmol 0.044 615 8
m3 of gas (15 °C, 101.325 kPa) kmol 0.042 493 2
ft3 of gas (60 °F, 1.0 atm) kmol 0.001 195 30

AREA ft2 m2 0.092 903 04


in2 mm2 645.16
in2 cm2 6.451 6
yd 2
m 2
0.836 172 4

CAPACITY bbl (42 gal US) m3 0.158 987 3


fl oz (UK) cm 3
28.413 05
fl oz (US) cm 3
29.573 53
gal (UK) m 3
0.004 546 092
gal (UK) L 4.546 092
gal (US) m3 0.003 785 412
gal (US) L 3.785 412

CONCENTRATION grains/100 ft3 mg/m3 22.883 51


lb mol/ft 3
kmol/m 3
16.018 46
ppm percent 0.000 1
ppm by volume cm /m 3 3
1.0
ppm by weight mg/kg 1.0
weight percent kg/kg 0.01

Conversion Factors and Calculations | E-1


PARAMETER TO CONVERT FROM: TO: MULTIPLY BY:
DENSITY (Gases) lb/ft3 kg/m3 16.018 46

DENSITY (Liquids) lb/gal (UK) kg/L 0.099 776 44


lb/gal (US) kg/L 0.119 826 4
lb/ft 3
kg/L 0.016 018 46
g/cm3 kg/L 1.0

DENSITY (Solids) lb/ft3 kg/L 0.016 018 46

ENERGY BTU kJ 1.055 056


cal kJ 0.004 184
kcal kJ 4.184
kWh kJ 3600.0

FLOW RATE bbl/d t/a 58.030 36


bbl/h mh 3
0.158 987 3
gal (UK)/min m 3h 0.272 765 5
gal (US)/min mh 3
0.227 124 7
ft /h
3
mh 3
0.028 316 85
ft /h
3
L/min 0.471 947 5
ft3/min L/s 0.471 947 5
lb/h t/d 0.010 886 22
lb mole/h kmol/h 0.453 592 4
ton (2240 lb)/d kg/h 42.335 290 7
ton (2000 lb)/d kg/h 37.799 366 7

LENGTH ft m 0.304 8
in mm 25.4
yd m 0.914 40

MASS grain mg 64.798 91


lb kg 0.453 592 4
oz (avoirdupois) g 28.349 52
oz (troy) g 31.103 48
ton (2240 lb) t 1.016 047
ton (2000 lb) t 0.907 184 7

POWER BTU/min kW 0.017 584 27


BTU/s kW 1.055 056
hp kW 0.746
million BTU/h MW 0.293 071 1

E-2 | Model 933 UV Analyzer


PARAMETER TO CONVERT FROM: TO: MULTIPLY BY:
PRESSURE ATM kPa 101.325
bar kPa 100.0
cm of H2O (4 °C) kPa 0.098 063 8
in of Hg (32 °F) kPa 3.386 388 157
in of Hg (60 °F) kPa 3.376 85
in of H2O (39.2 °F) kPa 0.249 082
in of H2O (60 °F) kPa 0.248 84
mm of Hg = torr (0 °C) kPa 0.133 322 4
psi kPa 6.984 757

SPECIFIC HEAT CAPACITY BTU/lb * °F kJ/kg * °C 4.186 8


kcal/kg * °C kJ/kg * °C 4.184
kW * h/kg * °C kJ/kg * °C 3 600.0
BTU/lb mol * °F kJ/kmol * °C 4.186 8
cal/g mol * °C kJ/kmol * °C 4.184

SPEED ft/s m/s 0.304 8


in/s mm/s 2.54
mile/h km/h 1.609 344

TEMPERATURE °R K 0.555 555 555


°F-32 °C 0.555 555 555
Fahrenheit degree Celsius degree 0.555 555 555

VOLUME ft3 m3 0.02831685


in 3
cm 3
16.387 06
yd3 m3 0.764 554 9

Conversion Factors and Calculations | E-3


Prefixes
FACTOR
(by which unit is multiplied) PREFIX SYMBOL EXAMPLE
One million million (billion) 10 12
tera T
One thousand million 109 giga G gigahertz (GHz)
One million 106 mega M megawatt (MW)
One thousand 103 kilo k kilometre (km)
One hundred 102 hecto* h
Ten 101 deca* da decagram (dag)
UNITY 1
One tenth 10-1 deci* d decimetre (dm)
One hundredth 10 -2
centi* c centimetre (cm)
One thousandth 10-3 milli m milligram (mg)
One millionth 10-6 micro µ microsecond (µs)
One thousand millionth 10 -9
nano n nanosecond (ns)
One million millionth 10-12 pico p picofarad (pF)
One thousand million millionth 10-15 femto f
One million million millionth 10-18 atto a
* To be avoided wherever possible.

E-4 | Model 933 UV Analyzer

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