Beruflich Dokumente
Kultur Dokumente
User Manual
TQM
Process Instruments
COMMITTED TO TOTAL QUALITY
PN 903-8549, Rev. K
Western Research
2876 Sunridge Way N.E.
Calgary, Alberta, Canada T1Y 7H9
Offices
CHAPTER 1 OVERVIEW
Theory of the Model 933 Analyzer ................................................................. 1-1
Features ............................................................................................................... 1-2
Application .......................................................................................................... 1-3
Implementation ................................................................................................. 1-4
Microcontroller Board and Host Controller Board ............................... 1-5
Sample Conditioning ................................................................................. 1-5
Discrete Wavelengths ................................................................................. 1-5
About the Analyzer Sampling System ........................................................... 1-8
Sample Conditioning Column Operation .............................................. 1-9
Relays ................................................................................................................. 1-10
Status Relays .............................................................................................. 1-10
Alarm Relays .............................................................................................. 1-11
Solid State Relays ...................................................................................... 1-11
CHAPTER 2 SPECIFICATIONS
Methodology ............................................................................................... 2-1
Full-Scale Ranges ......................................................................................... 2-1
Standard Range Measuring Cell (40 cm or smaller) .............................. 2-1
Low Range Measuring Cell (81.2 cm) ...................................................... 2-1
Response Time (excludes sampling system) ........................................... 2-1
Measurement Accuracy .............................................................................. 2-2
Repeatability ................................................................................................ 2-2
Calibration .................................................................................................... 2-2
Linearity ....................................................................................................... 2-2
Stability ......................................................................................................... 2-2
Sensitivity ..................................................................................................... 2-2
Cross-Talk ..................................................................................................... 2-3
Temperature Drift ....................................................................................... 2-3
Contents | iii
24-Hour Zero Drift ...................................................................................... 2-3
Analog Outputs ........................................................................................... 2-3
Digital Communication .............................................................................. 2-3
Electrical Requirements ............................................................................. 2-4
Maximum Start-Up Power .................................................................... 2-4
Electrical Requirements ......................................................................... 2-4
Status Relay Contacts ............................................................................ 2-4
Typical Sample Gas Flow Rate .................................................................. 2-4
Zero Gas ........................................................................................................ 2-4
Ambient Limits ............................................................................................ 2-5
Temperature ........................................................................................... 2-5
Humidity ............................................................................................... 2-5
Maximum Altitude ................................................................................ 2-5
Sample Pressure Requirement .................................................................. 2-5
Sample Stream Requirements ................................................................... 2-6
Physical Dimensions (on backpan) .......................................................... 2-6
Options ......................................................................................................... 2-6
Approvals and Certifications .................................................................... 2-7
ATEX (CENELEC) Certificate and Analyzer Marking ................................. 2-8
CSA Certificate and Analyzer Marking ........................................................ 2-11
Contents | v
Compensation Parameters .................................................................... 4-36
Advanced Options ............................................................................... 4-38
Custom Output (Custom Setup) ......................................................... 4-39
Status Tab .................................................................................................... 4-40
Optical Bench Data Tab ............................................................................ 4-42
Analyzer Data Tab ..................................................................................... 4-43
Scanning Data .................................................................................................. 4-45
Display Modes ........................................................................................... 4-45
Defining Scan Settings ............................................................................. 4-46
Starting a Scan ........................................................................................... 4-47
Stopping a Scan ......................................................................................... 4-47
Scheduling Scans ...................................................................................... 4-48
Working with Data Files ................................................................................. 4-49
Saving Data Files ....................................................................................... 4-49
Opening Data Files ................................................................................... 4-50
Scrolling Through Data Records ............................................................ 4-50
Converting Data Files ............................................................................... 4-51
Printing Data .............................................................................................. 4-51
CHAPTER 5 CALIBRATION
Manual Span Gas Calibration .......................................................................... 5-1
Analog Output Calibration .............................................................................. 5-4
Current Calibration .................................................................................... 5-4
Voltage Calibration ..................................................................................... 5-6
Contents | vii
APPENDIX B OPTIONS
Natural Gas Filter (Field Upgradeable) – Filterblock .................................. B-1
Filtration Stages .......................................................................................... B-2
Vent Flow ..................................................................................................... B-3
Natural Gas Filter Maintenance .............................................................. B-4
Replacing O-rings and Flow Restrictors in the Filterblock ................... B-4
Reinstalling Fittings and Replacing the Coalescing
Cartridge and Membrane Filters .......................................................... B-6
Filterblock Assembly Spare Parts ............................................................. B-8
Environmental Purge Option (Field Upgradeable) .................................... B-9
Connection and Use .................................................................................. B-9
Pressure Compensation Option (Field Upgradeable) .............................. B-11
Setting Up the Pressure Compensation Option ................................. B-11
Using the Pressure Compensation Option .......................................... B-12
Diagnostics Feature ............................................................................ B-12
Loop-Powered Current Outputs (Field Upgradeable) ............................. B-13
Using the Loop-Powered Current Option ........................................... B-13
Low Range (White Cell) Measuring Cell (Field Upgradeable) ............... B-14
Calibrated Carbonyl Sulfide Output (Factory Upgradeable Only) ........ B-15
Using a Calibrated Carbonyl Sulfide Output ...................................... B-15
Calibrated Methyl Mercaptan Output (Factory Upgradeable Only) ..... B-16
Using a Calibrated Methyl Mercaptan Output ................................... B-16
APPENDIX D DRAWINGS
Backpan Dimensions ........................................................................................D-2
Upper Enclosure ...............................................................................................D-3
Lower Enclosure ...............................................................................................D-4
Backpan Component Layout (North America) ...........................................D-5
Backpan Component Layout (Europe) .........................................................D-6
Column Block Assembly ..................................................................................D-7
AC Distribution PWB (P/N 100-1771) ............................................................D-8
Customer I/O Board (P/N 100-1758) ..............................................................D-9
Host Controller Board (P/N 100-1757) .........................................................D-10
Microcontroller Board (P/N 100-1781) .........................................................D-11
Micro-Interface Board (P/N 100-1759) .........................................................D-12
Contents | ix
Safety Notes
WARNINGS, CAUTIONS, and NOTES contained in this manual emphasize critical instructions
as follows:
An operating procedure which, if not strictly observed, may result in personal injury or
! environmental contamination.
WARNING
An operating procedure which, if not strictly observed, may result in damage to the equipment.
!
CAUTION
Electrical Safety
High voltages are present in the analyzer housings. Always shut down power source(s) before
performing maintenance or troubleshooting. Only a qualified electrician should make electrical
connections and ground checks.
Any use of the equipment in a manner not specified by the manufacturer may impair the safety
protection originally provided by the equipment.
Grounding
Instrument grounding is mandatory. Performance specifications and safety protection are void if
instrument is operated from an improperly grounded power source.
All personnel involved with the installation, start-up, operation, maintenance, service, or trou-
bleshooting of the Model 933 Analyzer must review and follow these Warnings and Cautions.
Warnings
Review and follow these Warnings to avoid personal injury or environmental contamination.
Always disconnect main AC power and/or alternate power sources (if used, i.e., for relay
! contacts) to the analyzer before removing any sampling system assemblies and components
WARNING from the analyzer, or before opening any covers on the analyzer.
If it is necessary to open the Upper/Lower Enclosures while the circuits are alive, test the area
for hazardous gases and proceed only when it is found to be safe. When the EEx d Electronics
Enclosures are open, take appropriate precautions to avoid electrical shock. Hazardous voltages
are present inside.
Any electrical connections, adjustments, or servicing of the analyzer should be performed only
! by properly trained and qualified personnel.
WARNING
All electrical connections, materials, and methods (plus all safety policies and procedures) must
be made in compliance with local wiring regulations and electrical code for the hazardous area,
and be approved by the Owner Company.
Before working on the sampling system, confirm that the system is purged with zero gas and is
! isolated (blocked in) from the process.
WARNING
Because ultraviolet radiation can harm your eyes, avoid direct viewing of the light emanating
! through the end window of the source lamp. If the source lamp must be viewed while energized,
WARNING wear safety glasses that absorb ultraviolet radiation.
If the analyzer uses the optional Measuring Cell heater, take precautions to avoid burning
! yourself; the Measuring Cell and Heater Assembly are hot.
WARNING
Contents | xi
Cautions
Review and follow these Cautions to avoid damaging the equipment.
The electronic circuit boards and other static-sensitive components should be stored and
! transported in static-shielding carriers or packages.
CAUTION
For electrical-shock protection, the analyzer must be operated from a grounded power source
! that has a securely connected protective-ground contact.
CAUTION
If it becomes necessary to handle any of the electronic circuit boards, do not subject the boards
! to static discharge. The ideal solution is a static-safe work area. Since such areas typically are
CAUTION
not available at field installation sites, the use of a wrist strap connected directly to a ground is
recommended. If a wrist strap is not available, you should at the very least touch the metal
chassis (to ground yourself) before handling or touching the boards.
When handling the source lamps, it is very important not to touch the lamp windows because
! residual oils from the fingers will absorb ultraviolet light. The window is the flat surface at the
CAUTION end of the narrow glass tube. The lamp assembly is fragile and should be handled with care.
Do not exceed the maximum working pressure rating of the sampling system – 21 000 KPAG
! (3000 PSIG) without optional Filterblock Assembly – under any circumstances.
CAUTION
For analyzers using the optional Filterblock Assembly, do not exceed the maximum working
pressure rating of the sampling system – 14 000 KPAG (2000 PSIG) with optional Filterblock
Assembly – under any circumstances.
If the Model 933 Analyzer is equipped with the Environmental Purge option, clean air or
! nitrogen can be supplied to the inlet flame arrester at a pressure of 7–70 KPAG (1–10 PSIG).
CAUTION
Schutzerde
Contents | xiii
Electromagnetic Compatibility (EMC)
Read and follow the recommendations in this section to avoid performance variations or
! damage to the internal circuits of this equipment when installed in harsh electrical environ-
CAUTION ments.
The various configurations of the Model 933 Analyzer should not produce, or fall victim to,
electromagnetic disturbances as specified in the European Union’s EMC Directive. Strict compli-
ance to the EMC Directive requires that certain installation techniques and wiring practices are
used to prevent or minimize erratic behavior of the Analyzer or its electronic neighbors. Below
are examples of the techniques and wiring practices to be followed.
In meeting the EMC requirements, the various Analyzer configurations described in this manual
rely heavily on the use of metallic shielded cables used to connect to the customer’s equipment
and power. Foil and braid shielded I/O and DC power cables are recommended for use in other-
wise unprotected situations. In addition, hard conduit, flexible conduit, and armor around non-
shielded wiring also provides excellent control of radio frequency disturbances. However, use of
these shielding techniques is effective only when the shielding element is connected to the
equipment chassis/earth ground at both ends of the cable run. This may cause ground loop
problems in some cases. These should be treated on a case-by-case basis. Disconnecting one
shield ground may not provide sufficient protection depending on the electronic environment.
Connecting one shield ground via a 0.1 microfarad ceramic capacitor is a technique allowing
high frequency shield bonding while avoiding the AC-ground metal connection. In the case of
shielded cables the drain wire or braid connection must be kept short. A two-inch connection
distance between the shield’s end and the nearest grounded chassis point, ground bar or termi-
nal is highly recommended. An even greater degree of shield performance can be achieved by
using metallic glands for shielded cable entry into metal enclosures. Expose enough of the braid/
foil/drain where it passes through the gland so that the shield materials can be wrapped back-
wards onto the cable jacket and captured inside the gland, and tightened up against the metal
interior.
Inductive loads connected to the low voltage “Alarm Contacts” are not recommended. However,
if this becomes a necessity, adhere to proper techniques and wiring practices. Install an appro-
priate transient voltage suppression device (low voltage MOV, “Transzorb,” or R/C) as close as
possible to the inductive device to reduce the generation of transients. Do not run this type of
signal wiring along with other I/O or DC in the same shielded cable. Inductive load wiring must
be separated from other circuits in conduit by using an additional cable shield on the offending
cable.
In general, for optimum protection against high frequency transients and other disturbances, do
not allow installation of this Analyzer where its unshielded I/O and DC circuits are physically
mixed with AC mains or any other circuit that could induce transients into the Analyzer or the
overall system. Examples of electrical events and devices known for the generation of harmful
electromagnetic disturbances include motors, capacitor bank switching, storm related transients,
RF welding equipment, static, and walkie-talkies.
ATEX (KEMA)
II 2 G EEx d IIB T3.
Explosion Hazard – Substitution of Components May Impair Suitability for Class I, Division 2.
!
WARNING
Risque d’explosion – La substitution de composants peut rendre ce materiel
! inacceptable pour les emplacements de Classe I, Division 2.
Avertissement
Explosion Hazard – Do Not Disconnect Equipment Unless Power Has Been Switched Off or
! the Area is Known to be Non-Hazardous.
WARNING
Risque d’explosion – Avant de déconnecter l’équipement, coupez le courant où vous
! assurez que l’emplacement est designé non dangereux.
Avertissement
All input and output wiring must be in accordance with Class I, Division 2 wiring methods (NEC
Sec 501.4(b) or CEC 18-152) and in accordance with the authority having jurisdiction.
Contents | xv
Declaration of Conformity
Process photometric analyzers, process moisture analyzers, and sampling systems are warranted to
perform the intended measurement, only in the event that the customer has supplied, and AMETEK has
accepted, valid sample stream composition data, process conditions, and electrical area classification prior
to order acknowledgment. The photometric light sources are warranted for ninety (90) days from date of
shipment. Resale items warranty is limited to the transferable portion of the original equipment
manufacturer’s warranty to AMETEK. If you are returning equipment from outside Canada, a statement
should appear on the documentation accompanying the equipment being returned declaring that the
goods being returned for repair are Canadian goods, the name of the firm who purchased the goods, and
the shipment date.
The warranty shall not apply to any equipment (or part thereof) which has been tampered with or altered
after leaving our control or which has been replaced by anyone except us, or which has been subject to
misuse, neglect, abuse or improper use. Misuse or abuse of the equipment, or any part thereof, shall be
construed to include, but shall not be limited to, damage by negligence, accident, fire or force of the
elements. Improper use or misapplications shall be construed to include improper or inadequate protec-
tion against shock, vibration, high or low temperature, overpressure, excess voltage and the like, or
operating the equipment with or in a corrosive, explosive or combustible medium, unless the equipment
is specifically designed for such service, or exposure to any other service or environment of greater
severity than that for which the equipment was designed.
The warranty does not apply to used or secondhand equipment nor extend to anyone other than the
original purchaser from us. Should the Buyer ’s technical staff require the on-site assistance of AMETEK’s
agents or employees for service calls covered by this warranty clause, the Buyer shall pay travel time plus
actual travel and living expenses.
THIS WARRANTY IS GIVEN AND ACCEPTED IN LIEU OF ALL OTHER WARRANTIES, WHETHER
EXPRESS OR IMPLIED, INCLUDING WITHOUT LIMITATION AND WARRANTIES OF FITNESS OR OF
MERCHANTABILITY OTHER THAN AS EXPRESSLY SET FORTH HEREIN, AND OF ALL OTHER
OBLIGATIONS OR LIABILITIES ON OUR PART. IN NO EVENT SHALL WE BE LIABLE UNDER THIS
WARRANTY OR ANY OTHER PROVISION OF THIS AGREEMENT FOR ANY ANTICIPATED OR LOST
PROFITS, INCIDENTAL DAMAGES, CONSEQUENTIAL DAMAGES, TIME CHANGES OR ANY OTHER
LOSSES INCURRED BY THE ORIGINAL PURCHASER OR ANY THIRD PARTY IN CONNECTION
WITH THE PURCHASE, INSTALLATION, REPAIR OR OPERATION OF EQUIPMENT, OR ANY PART
THEREOF COVERED BY THIS WARRANTY OR OTHERWISE. WE MAKE NO WARRANTY, EXPRESS
OR IMPLIED, INCLUDING WITHOUT LIMITATION ANY WARRANTIES OF FITNESS OR OF MER-
CHANTABILITY, AS TO ANY OTHER MANUFACTURER’S EQUIPMENT, WHETHER SOLD SEPA-
RATELY OR IN CONJUNCTION WITH EQUIPMENT OF OUR MANUFACTURE. WE DO NOT AUTHO-
RIZE ANY REPRESENTATIVE OR OTHER PERSON TO ASSUME FOR US ANY LIABILITY IN CON-
NECTION WITH EQUIPMENT, OR ANY PART THEREOF, COVERED BY THIS WARRANTY.
Contents | xvii
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The Beer-Lambert law, in combination with the ideal gas situation, states
that:
Overview | 1-1
In a situation where several species are absorbing light at several measur-
ing wavelengths, the total absorbance at any particular wavelength is the
sum of the absorbances for each of the species present. Using Beer’s law
for each measuring wavelength, a system of linear equations relating the
unknown concentration to the measured absorbance at each wavelength
is obtained. The total absorbance at each measuring wavelength is equal
to the proportionality constant multiplied by the molar absorptivity for
the first species times its concentration, plus the (molar absorptivity)
factor for the second species, times its concentration, and so on for all
species present in the Measuring Cell. Provided that there are more
measuring wavelengths than unknown concentrations, this system of
linear equations is solved using standard methods of linear algebra.
Features
Microprocessor-Based
The operation of the analyzer, calculations and data manipulations are
all controlled by two on-board microprocessors.
Multicomponent Analysis
The availability of six discrete wavelengths enables either single-
component analysis or multicomponent analysis, with the capability
of eliminating interferences from other gas species. All interfering
species except COS and MeSH are eliminated by a gas-conditioning
system based on frontal elution chromatography. The H2S concentra-
tion is mathematically corrected for the presence of COS and MeSH so
that H2S concentrations are presented free of interferences.
Auto Zero
Automatically updates the analyzer zero. You can initiate the Auto-
Zero function on command using the Configurator Software, at user-
specified time intervals, or by a remote (potential free) contact closure.
Serial Communications
One RS-485 serial communications port is dedicated to customer data
acquisition. The port uses Modicon Modbus® protocol.
Temperature Control
The analyzer controls the temperature of two temperature-controlled
zones:
• Column Block
• Optical Bench
Status Relays
There are five independent sets of SPDT (Form C) relay contacts (2 A,
250 V).
Low Maintenance
The robust analyzer and sample conditioning system design reduces
maintenance requirements.
Application
The principal application of the Model 933 Analyzer is the analysis of
hydrogen sulfide (H2S) in pipeline quality natural gas. The major compo-
nents of the gas are alkanes (e.g., methane), which are transparent to the
analyzer. However, in addition to H2S, the gas may contain a variety of
minor components that are non-transparent. These potential interferers
include sulfur species such as mercaptans (e.g., ethyl mercaptan), aromat-
ics (e.g., benzene), and various other chemicals that are indigenous to gas
“sweetening” plants. The Model 933 sample conditioning system removes
potential interferers (conditions) from the gas sample so an accurate
analysis can be performed.
Overview | 1-3
Implementation
The Model 933 Analyzer is comprised of the following (see Figure 1-1):
• Beam splitter
Figure 1-1.
Analyzer analytical
block diagram.
Sample Conditioning
When a measurement is taken, the sample flows from the process stream
through to the Sample Conditioning System (SCS) where potentially
interfering gas species are removed using a form of gas chromatography.
The conditioned sample is then analyzed in the Measuring Cell and
finally vented to the atmosphere (see Figure 1-2).
Discrete Wavelengths
To achieve measurements at discrete wavelengths, the locations of the
filters in the filter wheel and the placement of the source lamps are cho-
sen so that, at any time, the photodetectors are exposed to light from only
one lamp and filter combination (i.e., a discrete wavelength).
For practical reasons related to timing and lamp control, two revolutions
of the filter wheel are required to collect a complete set of wavelength
data. During one revolution, consecutive pulses of light from Source
Lamp 1 arrive at the beam splitter. During the next revolution, consecu-
tive pulses of light arrive at the beam splitter from Source Lamp 2. Since
the nominal speed of the filter wheel is 400 RPM, pulses for any given
wavelength arrive at the beam splitter at a rate of 200 pulses per minute.
As each flash of light arrives, the beam splitter directs half the light to the
Reference photodetector and half through the gas sample to the Measure
photodetector. Because of the longer optical path and light losses at the
mirrors and through the Measuring Cell windows, the amount of light
received by the Measure photodetector is less than that received by the
Reference photodetector, even when there are no absorbers in the gas
sample. This is the reason that there is balance screen on the Reference
photodetector.
Overview | 1-5
LEGEND
Figure 1-2.
Sample Flow Diagram.
For the Model 933 configuration, the concentrations of three absorbers are
determined:
• H2S
• COS
• MeSH
Overview | 1-7
About the Analyzer Sampling System
The sampling system is mounted to the Model 933 backpan. The purpose
of the system is to maintain constant pressure and temperature, and to
condition the sample to obtain correct analysis. Refer to the Flow Diagram
(Figure 1-2) and the appropriate Backpan Component Layout drawing in
Chapter 3 (Figure 3-5, North America or Figure 3-6, Europe).
Component Function
Sample Probe Extends into the process stream to obtain a representative sample.
Contains a shut-off valve used to isolate the sample path from the
process stream.
Inlet Pressure Regulator The inlet pressure regulator adjusts the sample pressure to the
operating pressure (typically 80 PSIG/560 KPAG) specified in the
analyzer data sheet.
Pressure Gauge The pressure gauge is used to set the proper sample pressure in the
sampling system.
Solenoid Block The solenoid manifold block directs flow between the Zero solenoid,
Column A solenoid and Column B solenoid. There is also a pressure
relief valve to safeguard against over pressuring of any components
down stream of the solenoid manifold block or if the pressure regulator
fails. This pressure relief valve is factory-adjusted to open at
approximately 150 PSIG (1050 KPAG).
Column Switching Solenoids Solenoids are automatically turned on or off to initiate switching the
sample between columns.
Zero Solenoid The zero solenoid allows zero gas (or span gas) to flush the sampling
system during the auto-zero (or span) process. The column switching
solenoids are closed when the zero solenoid is open.
Column Block The Column Block is where the sample conditioning process takes
place. The Column Block incorporates a proprietary material to permit
correct sample analysis.
Heat Exchanger Block The heat exchanger block reduces the temperature of the conditioned
gas sample prior to it entering the Measuring Cell.
Measuring (Sample) Cell The Measuring Cell is a chamber of known length, with optical-grade
quartz windows, through which the radiation beam passes through the
gas sample. The windows are sealed by means of o-rings and
removable end caps.
Flow Indicator (Rotameter) The flow meter provides a visual indication of the sample flow rate in
liters/minute through the analyzer. Please note that the scaling on the
flow indicator is for air at standard temperature and pressure. Its
purpose is to indicate and ensure that appropriate flow conditions are
maintained and not to provide an absolute measure of the flow of
sample gas.
Filterblock Assembly See Appendix B – Options for a description of this assembly.
Overview | 1-9
Relays
Status Relays
The Customer I/O Board contains three independent relays that indicate
the operational status of the analyzer. Each relay provides a set of SPDT
(form C) dry (potential free) contacts. The relays are configured for fail-
safe operation (i.e., energized for the non-alarm condition). Each relay
also has an associated green LED on the Customer I/O board, which
remains on steady to indicate a non-alarm (normal operating) condition.
• The Fault relay indicates that an error has been detected by the built-in
diagnostics system. If this relay is de-energized, the green LED (D404)
will turn off to indicate the analyzer requires servicing. If the relay is
configured to latch (default) it will not clear unless the user manually
resets the alarm; otherwise, it will reset automatically upon correction
of the fault alarm.
• The Warning relay indicates that the analyzer’s built-in diagnostics has
detected a warning alarm condition, that the analyzer is not operating
under normal automatic control, or that the analyzer is performing a
gas or analog output calibration. If this relay is de-energized, the green
LED (D405) will turn off to indicate the analyzer requires attention.
• The Alarm Valid relay indicates whether information from the Concen-
tration 1 and Concentration 2 relays is valid or whether the analyzer is
capable of alarming. The contacts automatically change state upon
correction of the condition which caused the alarm. If this relay is de-
energized, the green LED (D406) will turn off to indicate there is a
problem.
Overview | 1-11
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Methodology
Proprietary frontal elution sampling; non-dispersive ultraviolet analysis
for measurement of hydrogen sulfide (H2S), carbonyl sulfide (COS), and
methyl mercaptan (MeSH) in sales quality (pipeline quality) natural gas.
Frontal elution chromatography is used to remove interfering species
from the sample gas.
Full-Scale Ranges
PPM ranges are standard; mg/Nm 3 and other ranges are available.
Specifications | 2-1
Measurement Accuracy
± 2.0 % full-scale of standard ranges to a minimum of:
Repeatability
< ± 2.0 % full-scale of standard ranges (including Column effects)
Calibration
Calibration gases in nitrogen or methane.
Linearity
< ± 2.0 % full-scale of standard ranges to a minimum of:
Stability
Noise: < 1.0 % of standard ranges (excluding cross-talk effects)
Sensitivity
0.5 % of standard ranges
Temperature Drift
H2S: 2 PPM / (Cell length) / °C
COS: 12 PPM / (Cell length) / °C
MeSH: 4 PPM / (Cell length) / °C
Analog Outputs
Up to 4 isolated 4–20 mA, loop or self-powered.
4 non-isolated 1–5 V.
5 independent sets of SPDT, Form C, potential free relay contacts, 2 A at
250 VAC.
Digital Communication
RS-485 Modbus® port
RS-232/RS-485 service port
Specifications | 2-3
Electrical Requirements
Electrical Requirements
ATEX/Hazardous Locations:
120 VAC, 50–60 Hz, 2 A Maximum
240 VAC, 50–60 Hz, 1 A Maximum
CSA:
104–132 VAC, 47–63 Hz, 3 A Maximum
207–264 VAC, 47–63 Hz, 2 A Maximum
Output Signal
4–20 mA DC, 30 VDC Maximum
Zero Gas
Instrument zero purity carbon dioxide; UHP nitrogen, or UHP methane.
Minimum Auto-Zero interval is once per 24 hours. More frequent Auto-
Zeroing can be used to reduce temperature drift in installations with
widely varying ambient temperatures.
Temperature
Humidity
0–95 % RH
Maximum Altitude
2000 m
Specifications | 2-5
Sample Stream Requirements
> 80 % ethane plus methane
< 10 % ethane (for standard column application)
< 3 % propane
< 1.25 % total butanes
< 0.5 % C5+
< 0.6 %Water content (based on a 35 °C maximum water dewpoint tem-
perature at 120 PSIG/830 KPAG)
Options
• Gas/liquid (glycol) separating filter (Filterblock Assembly)
• Other measuring ranges
• COS and methyl mercaptan measurement
• Pressure compensation
• Up to 4 V/I outputs
Specifications | 2-7
ATEX (CENELEC) Certificate and Analyzer Marking
For installation sites with potentially explosive atmospheres that require
ATEX certification, AMETEK’s ATEX certificate for the Model 933 Analyzer
is included in the following pages.
0344
PROCESS INSTRUMENTS II 2 G
Caution
Do not open when an explosive gas atmosphere is present.
Specifications | 2-11
2-12 | Model 933 UV Analyzer
Specifications | 2-13
CSA-certified Model 933 Analyzers are marked with the label shown
below.
PROCESS INSTRUMENTS
Caution
Open circuit before removing cover.
This chapter shows you how to install and start up the Model 933 UV
Analyzer. It includes the following:
• Electrical Installation
After the inspection, replace and tighten at least one hex screw for
! each enclosure. This will keep the enclosures secure and will prevent
CAUTION damage to the mating surfaces (flamepaths) during installation.
When handling the source lamps, it is very important not to touch the
! lamp windows because residual oils from the fingers will absorb
CAUTION ultraviolet light. The window is the flat surface at the end of the
narrow glass tube. The lamp assembly is fragile and should be handled
with care.
Do not mount the Optical Bench in the EEx d Upper Enclosure until
! after the analyzer has been mounted in its designated location.
CAUTION
All electrical connections to the Optical Bench Assembly are made via pre-
wired connector plugs. No hard wiring is required.
CAUTION:
RISK OF ELECTRIC SH OCK
ATTENTION:
CONSULT USER MAN UAL
0344
II 2 G
PROCESS INSTRUMENTS
Caution
Do not open when an explosive gas atmosphere is present.
Figure 3-1.
Model 933 backpan
dimensions (Europe).
1. Connect the Optical Bench AC power lines (via the connector plug) to
TB100 on the Optical Bench Service Electronics Board (Figure 3-2).
The cam pins must stay aligned while the Optical Bench Assembly is
being mounted into the enclosure. The lined groove on the head of the
NOTE cam pin must stay parallel to the Measuring Cell until the Optical
Bench Assembly is in place.
2. Locate the cam pins, which are situated in the Optical Bench mount
(Figure 3-3). Confirm that the grooved lines in the cam pins are facing
inward.
4. Rotate the lower cam pin counter-clockwise and the upper cam pin
clockwise until they are tight.
5. Connect the green/yellow ground wire from the interior of the upper
enclosure (via the disconnect terminals) to the green/yellow wire
connected to the Optical Bench Assembly.
Figure 3-3.
Upper enclosure
layout and cam pin
locations.
7. Connect the DC power lines (via the connector plug) to J103 on the
Micro-Interface board.
9. Connect the Measuring Cell RTD (via the connector plug) to J300 on
the Micro-Interface board.
The inlet sample pressure should be 560 KPAG (80 PSIG) or higher.
NOTE
Zero Gas
The zero gas fitting (1/4” Swagelok tubing fitting) is located on the sole-
noid manifold block. See Figure 3-5 (North America) or Figure 3-6 (Eu-
rope) for the Zero gas tubing connection point.
• <15 PPM O2
Figure 3-5.
Backpan component
layout (North
America).
CAUTION:
RISK OF ELECTRIC SHOCK
ATTENTION:
CONSULT USER MANUAL
0344
II 2 G
PROCESS INSTRUMENTS
Caution
Do not open when an explosive gas atmosphere is present.
Figure 3-6.
Backpan component
layout (Europe).
Where required, certified EEx d cable glands must be used and each
! unused cable entry port must be plugged with a certified EEx d plug.
WARNING
For AC electrical supply cable and conduit requirements, refer to and
comply with local wiring regulations and electrical codes for the
hazardous area.
The analog input/output (and alarm relay) terminations are made on the
Customer I/O PWB, located in the Lower Enclosure.
European Installation:
Signal wires, contained within cable that is approved locally for the
hazardous area, enter the EEx d Lower Enclosure through one of the
Signal Cable Entries on the bottom of the EEx d Lower Enclosure.
Figure 3-7.
Customer connections
wiring schematic (North
American installations).
Figure 3-8.
Customer connections
wiring schematic
(European installations).
Hardware Configuration
Hazardous Locations:
! Before attempting to access the Digital Communications Port, test the area for
WARNING hazardous gases and proceed only when the area is found to be safe.
There are also two other serial port connections available for permanent
connection: Remote Service Port and Customer Data Acquisition Port,
both RS-485.
The RS-485 Remote Service Port can also be used for customer
service, but not both at the same time as the RS-232 Digital Commu-
NOTE
nications Port.
2. If using the RS-485 port, select either a 2- or 4-wire link for both Cus-
tomer Data Acquisition and Remote Service ports.
3. For termination and biasing of RS-485 links, refer to Figure 3-10. Refer to
Figures 3-7 or 3-8 and Figure 3-9 for communication/termination
options and jumper (JP) locations/settings.
The termination and biasing options will depend on the analyzer role
and location in the network (master or slave, located at the end of the
transmission line or at a drop point). It will also depend on whether a
2- or 4-wire line is used, and the transmission line conditions (e.g.,
length of cable, or termination and biasing on the other end of the cable).
Figures 3-9 and 3-10 apply only to Model 933 Analyzers with Host
Controller Board, Rev. B and newer.
NOTE
A
RX+
R J302 (Customer Data Acquisition) J303 (Remote Service Port)
130
RT
B
RX- JP305 (RX RT) 1-2 JP307 (RX RT) 1-2
JP306 (TX RT) 1-2 JP308 (TX RT) 1-2
130
RT
Z
TX- JP314 (TX RB2) 2-3 JP316 (TX RB2) 2-3
+5V
R B1
619
A
RX+
R J302 (Customer Data Acquisition) J303 (Remote Service Port)
B
RX- JP305 (RX RT) 2-3 JP307 (RX RT) 2-3
R B2
2-3 2-3
(c) +5V JP309 (RX RB1) 1-2 JP311 (RX RB1) 1-2
JP310 (TX RB1) 1-2 JP312 (TX RB1) 1-2
R B1
619
619
+5V
R B1
619
A
RX+
R J302 (Customer Data Acquisition) J303 (Remote Service Port)
130
RT
B
RX- JP305 (RX RT) 1-2 JP307 (RX RT) 1-2
R B2
1-2 1-2
(d) +5V JP309 (RX RB1) 1-2 JP311 (RX RB1) 1-2
JP310 (TX RB1) 1-2 JP312 (TX RB1) 1-2
R B1
619
Z
TX-
NOTES:
1. RB - BIAS RESISTOR
R B2
619
2. RT - TERMINATION RESISTOR
3. RESISTANCE VALUES IN OHMS
Figure 3-10.
Various RS-485 port
terminations and bias
options (Host
Controller board,
P/N 100-1757, Rev. B).
Both the North American and European versions of the Model 933
UV Analyzer require that a power-disconnect switch (breaker), rated
NOTE for at least 250 VAC, 3 A, must be connected to, and mounted near,
the analyzer (supplied by the customer). To satisfy local electrical
codes, the switch must be certified by the local authority for the
appropriate hazardous area.
For safety reasons during maintenance, this switch allows the main
AC power to be disconnected from the analyzer prior to performing
service on the analyzer.
The power connection to the analyzer is made at TB1-1, TB1-2, and TB1-5
on the AC Terminal Strip in the lower enclosure (see Figure 3-11, Detail A).
LOWER ENCLOSURE
Figure 3-11.
Conduit entries and AC
power connection
locations, lower DETAIL A
enclosure (North
American installations).
Figure 3-12.
Conduit entries and DETAIL A
AC power connection
locations, EEx d lower
enclosure (European
installations).
Hazardous Locations:
Before proceeding, test the area around the analyzer for hazardous
NOTE gases and proceed only when the area is found to be safe.
• 16 MB RAM.
Figure 3-13.
Destination Folder
screen.
You can also start the software by clicking M933 Configurator from
the Start\Programs\Ametek\933 Configurator menu.
The software will create a shortcut icon on the desktop to start the
software (called 933 Configurator).
NOTE
Figure 3-14.
InstallShield Wizard
Completed screen.
1. From the Windows Start menu, select Settings, and then Control
Panel.
Before powering up the analyzer, test the area for flammable gases. If
! an explosive gas atmosphere is present, do not apply power to the
WARNING analyzer or any alternate power sources that supply power to the
analyzer components. Proceed only when the area is found to be safe.
Before operating the analyzer for the first time, following a power-up
! or reset, or after maintenance, you must manually block in the sample
WARNING gas flow.
a. Verify the operation of the status relays on the Customer I/O board
(Figure 3-15):
• The state of the Fault Status Relay and the Warning Status
Relay depends on the current status of the analyzer. However,
it is most likely that both relays will be de-energized upon
initial power-up as the temperatures of the Column Block and
the Optical Bench have not yet reached their respective
setpoints, and are generating a fault (“Fault Column Temp Lo”)
and warning (“Warning Bench Temp”) alarm error message,
respectively. Verify this in the Error Condition list on the
Status tab of the M933 Properties dialog box. These green
LEDs D404 and D405 will be off in this case.
f. The Optical Bench heater will turn on to heat up the Optical Bench.
You can verify this by observing that the red LED (LED201) on the
Micro-Interface board (Figure 3-4) is on continuously or pulsing.
g. While working from the Configurator Software, check the set points
and current temperature readings for each of the temperature-
controlled zones. This will help you to determine if the signal wiring
is properly terminated and if all of the circuitry is operating properly.
Record the set point and current (start-up) temperature value indi-
cated for each zone to use as a reference later while comparing the
temperature value (after the analyzer has warmed up).
To do this, click the Temp Control button from the Setup tab of the
M933 Properties dialog box. View and record the set points for
each temperature-controlled zone.
Next, select the Analyzer Data tab to view the current temperature
readings, under Temperature Zone. Record the set points for each
temperature-controlled zone. This will help you determine if the
signal wiring is properly installed and if all of the circuitry is
operating properly.
4. After all fault alarms have cleared, the analyzer will automatically
perform an Auto-Zero.
To perform this test, follow the procedures listed under the section
titled “Pressure Leak Check,” later in this chapter. Then, return to this
section and complete the remaining steps.
6. After all of these checks have been made and verified, close the upper
and lower enclosures. However, the sample gas should remain
blocked in.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up/
down the laptop computer if there is a hazardous gas atmosphere
present.
2. After the area has been tested for hazardous gases (and has been
found to be safe), loosen the hex screw on the cover of the Explosion-
Proof Serial Communications Port (RS-232) on the Lower Enclosure
enough to allow the cover to slide to the right and reveal the Digital
Communications Port.
a. From the Start menu, click Properties, AMETEK, and then M933,
or double-click the M933 shortcut icon on the desktop (if one was
created). The software will start and the M933 Configurator screen
will appear (Figure 3-17).
Within this screen is the Devices & Log dialog box (see “Viewing
Device Activities” in Chapter 4 for details about this window).
Figure 3-18.
M933 Properties
dialog box (General
tab).
e. Click the Setup button on the General tab to access the Serial Port
Configuration (Figure 3-19).
Figure 3-19.
Serial port
configuration.
RS-485 Port:
Click if using the Remote Service port (RS-485).
See “Modifying Analyzer Device Settings” in
Chapter 4 before attempting to configure the
RS-485 remote service port.
5. After you have completed communicating with the analyzer, exit the
Configurator Software, power-down the computer, and disconnect the
Serial Communications Cable from the Explosion-Proof Digital Com-
munications Port on the Lower Enclosure.
Problem Encountered
The “Wrong Device” message is displayed on the Devices & Log window.
Corrective Action
Check the analyzer markings to ensure it is a Model 933 Analyzer (the M933
Configurator Software cannot communicate with other models of analyzers,
such as a Model 900 ADA Analyzer).
The COM Port Parameter Settings may be incorrect. Review the settings in
the Serial Port Configuration dialog box and verify or set them to the proper
settings. The address must also match that of the analyzer – check the
analyzer Address on the Device Communication tab and change it if neces-
sary.
Problem Encountered
The “Connected” message is displayed on the Devices & Log window, but
the software is not communicating with the analyzer.
Corrective Action
Select the Live Data check box to establish communication.
Problem Encountered
The “DEMO Online” message is displayed in the Status field on the General
tab. This message will be displayed if the Live Data check box is not selected
(but the Device Enabled check box is).
Corrective Action
Select the Live Data check box to establish communication.
Corrective Action
Observe the Device Enabled and Live Data check boxes on the General tab.
One or both of these check boxes may not be selected. Select both of them to
establish communication.
Check the Serial Communication Cable for proper connections and for
damage such as cuts, nicks, or burn marks. Also, check it to ensure the
internal wiring is still terminated at the connectors.
Problem Encountered
The “DISABLED” message is displayed in the Status field on the General
tab. This message will be displayed if the computer is connected to the
analyzer but is not communicating with it.
Corrective Action
Select the Device Enabled check box, if necessary, to establish communica-
tion.
Check the analyzer markings to ensure it is a Model 933 Analyzer (the M933
Configurator Software cannot communicate with other analyzer models).
Problem Encountered
The Device Properties command under the Edit menu is grayed out (access
to the M933 Properties dialog box is not available). If this occurs, the analyzer
configuration and calibration parameters cannot be viewed or modified. This
problem suggests that the “M933.dys” file has become corrupt.
Corrective Action
Delete the “M933.dys” file from the C:\Ametek\M933 folder. The software
will restore this file (and correct the problem) the next time it is started.
Problem Encountered
The LEDs for various analyzer operations are not operating properly, as
described in the procedures under “Powering Up the Analyzer.”
Corrective Action
Take appropriate safety precautions and check for proper I/O wiring and
power connections.
If the LEDs are still not operating properly, reset the analyzer. To do this, cycle
the AC power off a minimum of 15 seconds before cycling it on again.
Problem Encountered
One or both source lamps are not firing.
Corrective Action
Take appropriate safety precautions and check for proper wiring connections.
If the wiring is okay, check the connections of the lamps in their sockets.
Review the section titled “Source Lamp Replacement” in Chapter 6 to make
adjustments to the lamps. Perform an Auto-Setup if necessary to ensure the
lamps are operating at peak efficiency.
Problem Encountered
Temperature zone values do not increase.
Corrective Action
Take appropriate safety precautions and check for proper wiring terminations
for the appropriate temperature zone.
Corrective Action
Take appropriate safety precautions and check the related RTD for a short or
an open circuit. If necessary, replace the RTD with an AMETEK-approved
replacement part. Contact AMETEK for assistance.
Problem Encountered
Alarms remain active after the analyzer has warmed up to normal operating
temperature, as displayed under Error Condition on the Status tab.
The “Fault Column Temp Lo”, “Warning Bench Temp”, and “Warning Cell
Temp” alarm error messages will typically be displayed upon start-up due to
low temperatures in these temperature-controlled zones.
Corrective Action
If these or other alarms remain active, refer to the alarm conditions and
corrective action in Chapter 6.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up/
down the laptop computer if there is a hazardous gas atmosphere
present.
2. Connect the zero gas to the sample inlet port of the analyzer.
3. Disconnect the vent tubing from the analyzer and plug it with a cap
fitting.
b. Click the Setup tab of the M933 Properties dialog box (Figure
3-20), then click the Gas Calibration button to view the Gas
Calibration dialog box (Figure 3-21).
c. In the Flow Control drop-down list, select “Col A”. Click OK and
then Apply. Click NO when prompted to save parameters to
EEPROM.
Do not set the pressure higher than 689 KPA (100 PSIG) if the
! optional pressure transducer is installed.
CAUTION
Figure 3-21.
Gas Calibration dialog
box.
5. Bring the pressure on the zero gas to 550 KPA (80 PSIG). Use the
pressure gauge mounted on the backpan to observe the pressure. The
sample inlet regulator may need to be adjusted.
6. Shut off the zero gas flow at the cylinder. If the reading on the pres-
sure gauge starts to decrease, use a leak detection fluid on the sam-
pling system to find the problem area.
Bleed down the sampling system from the vent port of the analyzer.
! Otherwise, damage to the Filterblock (if installed) may occur.
CAUTION
8. After the sampling system has been bled down, re-cap the vent outlet.
Unhook the zero gas from the sample inlet port and reconnect the
zero gas to the zero gas port of the analyzer.
10. Return to the Gas Calibration dialog box and select “Zero” from the
Flow Control drop-down list. Click OK then click Apply. Click NO
when prompted to save parameters to EEPROM.
11. Increase the pressure of the zero gas to 550 KPA (80 PSIG). Use the
pressure gauge mounted on the backpan to observe the pressure.
13. Bleed down the sampling system and remove the cap fitting from the
vent outlet.
15. Return to the Gas Calibration dialog box and select “Auto” from the
Flow Control drop-down list. Click OK then click Apply. Click YES
when prompted to save parameters to EEPROM.
16. The sample gas can now be turned on. Set the pressure to 560 KPA
(80 PSIG) using the sample inlet regulator. The analyzer is ready to
analyze sample gas.
Temperature Setpoints
1. Click on the Setup tab of the M933 Properties dialog box.
Figure 3-22.
Temperature Control
dialog box.
3. Verify that the (Optical) Bench temperature setpoint and range are
correct. The Optical Bench temperature setpoint should be at least
8 °C to 10 °C above the maximum ambient temperature around the
analyzer. For applications with maximum ambient temperature of 30 °C
and below, a default setpoint temperature of 40 °C is normally used.
The temperature setpoint is set at the factory using the ambient
temperature data that is specific to the application and location. Refer
to Chapter 4 for additional information about how to alter the setpoint
or range.
To alter the set point or range in Step 3, and those set points or ranges
in Steps 4–8, refer to Chapter 4 for additional information.
NOTE
5. Verify that the Too Cold setpoint for the Bench is correct. It should be
5 °C to 10 °C below the Optical Bench setpoint temperature. The Too
Cold setpoint is set at the factory using the ambient temperature data
that is specific to the application and location.
7. Verify that the Too Hot setpoint for the Column is correct. It should be
5 °C to 10 °C above the column setpoint temperature. The Too Hot
setpoint is set at the factory using the ambient temperature data that is
specific to the application and location.
8. Verify that the Too Cold setpoint for the Column is correct. It should
be 5 °C to 10 °C below the column setpoint temperature. The Too Cold
setpoint is set at the factory using the ambient temperature data that is
specific to the application and location.
2. Click Output to view the Output Setup dialog box (Figure 3-23).
3. Verify that each current and voltage output channel configured has
the correct range applied for the application. The ranges are set at the
factory using the data that is specific to the application.
• To ensure the V/I result will not go below 4 mA, enable (check) the
V/I Low Limit 4 mA check box. This will ensure the actual output
clamps the result at 4 mA; the output cannot go below this value.
4. Verify that all concentration alarms are configured correctly for the
specific application. The alarm setpoints are set at the factory using
the data that is specific to the application. To alter the setpoints, refer
to Chapter 4 for additional information.
Figure 3-23.
Output Setup dialog
box.
Figure 3-24.
Modbus dialog box.
This change in elution time affects the analyzer’s column switching time
interval and hold time period configuration parameters. These two param-
eters are set up at the factory using stream composition data that was
provided for the application. Check that the parameters are properly set
up for the application and adjust them if necessary.
1. From the Setup tab of the M933 Properties dialog box, click Output
and then click Alarm Disable (Figure 3-23). Click OK.
Verify that “Auto” is selected from the Flow Control list. If not, select
“Auto”, click OK, and then click Apply. Click NO when prompted to
save parameters to EEPROM.
Figure 3-25.
Column setup graph.
TIME (SECONDS)
MeSH, COS AND H2 S WITH EXCESSIVE COLUMN SWITCH TIME
REAL TIME CONCENTRATIONS
CONCENTRATION (PPM)
TIME (SECONDS)
MeSH, COS AND H 2 S WITH CORRECT COLUMN SWITCH TIME
REAL TIME CONCENTRATIONS
CONCENTRATION (PPM)
6. To change the column switch time, click Column Timing (Figure 3-27)
on the Setup tab. In the Switch Interval text field, enter the new
column switch time and click OK. Click Apply and save the change to
EEPROM.
Figure 3-27.
Column Timing dialog
box.
At the end of the hold period, the Hold Time for each species should be
adjusted so that the real time concentration of the gas in question is
between the T90 concentration (90 % of the stable plateau value) and the
stable value. Refer to the lower graph in Figure 3-26. Setting the Hold
Time to end at, or slightly after, the T90 point for the species, will result in
the fastest response time but will give the noisiest output signal. Setting
the Hold Time to end after the concentration has reached a stable plateau
will give the smoothest output signal, but will result in a longer response
time.
For the H2S output, the factory default Hold Time should be correct. It is
usually set up so that at the end of the hold time, the H2S output is be-
tween the T90 concentration and the stable value. If a slightly faster re-
sponse time is required, the Hold Time can be reduced slightly (see
procedure below). If there is too much noise on the output (the down-
ward spikes that occur between when the Hold Time ends and the con-
centration stabilizes) then the Hold Time can be increased by a few sec-
onds.
If the analyzer is equipped with the optional COS and MeSH Outputs,
then their hold times should have been set up at the factory. Before
adjusting them, check the column switch times as described in the previ-
ous section and, if necessary, adjust them. Because there is not usually a
requirement for fast response time on the COS and MeSH outputs, their
adjustment is usually less critical than that for the H2S.
The COS hold time should be long enough to hold the concentration
constant until the real time COS concentration has reached a stable
plateau. For most applications, the factory default setting should be
correct.
The MeSH hold time is usually adjusted so that the hold on the concen-
trations comes off several seconds before the columns are switched. If the
column switch time in the previous section is adjusted, then the MeSH
hold time will also need to be adjusted. Take the new column switch time
and subtract 2 seconds from it and then use that as the new MeSH hold
time.
1. Click Output on the Setup tab to view the Output Setup dialog box
(Figure 3-23). Click Alarm Disable and then OK.
2. Click Column Timing on the Setup tab to view the Column Timing
dialog box (Figure 3-27).
In the Hold Time text field for the species of interest, enter the new
hold time. Click OK. Click Apply and save the changes to EEPROM.
3. Once the column switch time and the hold times have been properly
adjusted, click Output on the Setup tab. Click Alarm Enable. Click
OK.
Hold time for other species not mentioned above should be set to that
of H2S.
NOTE
While working from the Configurator Software you can view real-time
and historical data, and modify configuration and calibration parameters.
The software is also necessary while performing maintenance and while
troubleshooting the analyzer. The majority of these functions are per-
formed from the M933 Properties dialog box of the software. From this
window, all current operating and calibration parameter settings can be
viewed from the various dialog boxes that can be selected from the Setup
tab. Live data for different aspects of the analyzer can be viewed from the
Status, Analyzer Data, and Optical Bench Data tabs.
• Scanning data.
Hazardous Locations:
! Before proceeding, test the area around the analyzer for hazardous
WARNING gases and proceed only when the area is found to be safe.
2. The software will start and the Devices & Log window (Figure 4-5)
will appear in the M933 Configurator window. From here, select
Device Properties from the Edit menu to view the M933 Properties
dialog box (General tab, Figure 4-1).
The M933 Properties dialog box will be your main interface when
working on the analyzer or viewing live data.
NOTE
By default, the Live Data check box is enabled. When Live Data is
selected, the Configurator Software automatically attempts to establish
communication with the analyzer. If the communication attempt fails,
the communication settings may be incorrect and/or the communica-
tion cable may not be connected properly (or it may be damaged), or
you may be attempting to communicate with the wrong model of
analyzer. Refer to “Configurator Software Troubleshooting” in Chap-
ter 3 for information about how to resolve communication problems.
The M933 Properties dialog box is your primary interface with the
analyzer when viewing live data, or when modifying or viewing the
analyzer’s configuration or calibration parameters.
If at any time you close the M933 Properties dialog box (by clicking
OK or Cancel), the software will revert to the M933 Configurator
NOTE Software screen. Return to the M933 Properties dialog box by
clicking Edit and then Device Properties.
Hazardous Locations:
! Before proceeding, test the area around the analyzer for hazardous
WARNING gases and proceed only when the area is found to be safe.
After you have completed communicating with the analyzer, exit the
Configurator Software and disconnect the computer from the analyzer.
2. From the M933 Configurator window, select Exit from the File menu.
PC Communications
Displays information that has been configured from the Serial Port
Configuration dialog box.
Setup
Allows you to set up the communication parameters required to
establish communication with the analyzer. Detailed descriptions
about these communication options are discussed in the following
pages under “PC Communication Setup.”
Device
Name
Enter a tag number or tag name.
Description
Enter a description to further define the analyzer, such as a loca-
tion or area where it is installed in the plant.
Live Data
Status
Displays the status of the analyzer (device) you are communicating
with. Refer to “Configurator Software Troubleshooting” in Chapter 3
for information about how to correct the problem.
The PC can communicate with the analyzer through either the Local
Service Port or the Remote Service Port , but not both at the same time.
The Local Service Port is located on the front of the Lower Enclosure and
it is configured as RS-232; the remote service port is configured as RS-485
and is accessed via connector J303 on the Host Controller board. See the
Host Controller board drawing under “Digital Communication” in Chap-
ter 3 for locations of jumpers and connectors.
Figure 4-2.
Serial Port
Configuration dialog
box.
Before accessing the local service port on the front of the Lower
! Enclosure, test the area around the analyzer for hazardous gases and
WARNING proceed only when the area is found to be safe.
2. Click the Setup button to view the Serial Port Configuration dialog
box (Figure 4-2).
If you need to set up the analyzer to communicate via the Remote Service
Port, configure the settings on the Device Communication tab first, then
return to this dialog box and select RS-485 Port.
Baud Rate
Baud rate at which data will be transferred. The baud rate is
fixed at 9600.
Port Type
Select RS-232 if using the analyzer’s local service port.
Address
If the RS-485 port is selected, enter the communications ad-
dress of the analyzer. If using multiple analyzers, be sure to
enter a different address for each unit.
5. View the Status tab. Live data should begin updating within 10 sec-
onds.
Baud Rate This is the baud rate at which data will be transferred.
The baud is fixed at 9600.
Figure 4-3.
Device
Communication tab.
1. Ensure the device is Online. To check this, view the Status of the
system from the General tab: it should read “Online” (the Device
Enabled and Live Data check boxes must be enabled).
4. Click Apply. The software will prompt: “Would you like to save the
settings to EEPROM?”. Click Yes for the changes to take effect.
Note that the address you entered in the Address text box in the
Device Communication tab matches the Address setting on this
dialog box.
6. Click RS-485 Port to enable the Remote Service Port. Click OK to save
this change.
Check the Status of the system from the General tab again. It should
now read “Online” if the communication port settings for both the
NOTE analyzer and the PC are correct.
User Interface
The software allows you to customize how data is viewed and to set up
your display. This is done from the main window (Figure 4-4).
Standard Toolbar
Custom Mode Toolbar
Data File Toolbar
Main Window
Figure 4-4.
Configurator Software
main window (Trend
mode display active). Status Bar
• Standard Toolbar
Contains icons used most often including the main display modes.
• Main Window
Displays the various mode windows used to view data. Also can
display the Devices & Log window, which is a system event log that
lists all devices and their status.
• Status Bar
Located at the bottom of the window, the Status Bar displays system
messages, including if the system is currently scanning.
The settings for your analyzer have been configured at the factory to
! meet specified customer requirements. Changing the factory-set
CAUTION configuration could cause the analyzer to operate incorrectly.
Figure 4-5.
Devices & Log
window.
1. From the View menu, select Devices & Log or click . A log is
displayed showing all active devices and their status.
2. From here you can view a log of all related activity for active devices
such as when scans were started or completed as well as any alarm
conditions. It also provides information on the data source for the
reading under the Source field (e.g., Dev1, or Device 1). The Status
field indicates the current status of the analyzer (e.g., Online). Demo
data can be used to simulate real data for testing purposes.
3. To remove the display, select View and then Devices & Log again or
click .
1. Click the Save Configuration button from the General tab of the
M933 Properties dialog box. When you click Save Configuration, the
Save As dialog box will appear. Navigate to the Ametek\M933 folder
on the computer’s hard drive (AMETEK does not recommend saving
this file to another path).
2. Name the file and click Save. The file will be saved with a “.dev”
extension. This file can be used only by the Configurator Software.
1. Click the Restore Configuration button from the General tab of the
M933 Properties dialog box. When you click Restore Configuration,
the Open dialog box will appear with a message box (“Preparing to
restore. Click OK to continue.”). Click OK if you wish to restore
configuration parameters.
Descriptions for the functions on the General tab can be found earlier
in this chapter, under “Starting the Configurator Software.”
NOTE
The settings for your analyzer have been configured at the factory to
! meet specified customer requirements. Changing the factory-set
CAUTION configuration could cause the analyzer to operate incorrectly.
Figure 4-6.
Setup tab.
For all first-time analyzer setups, set up the analyzer from the M933
Properties dialog box. From here, you must check the Device En-
NOTE
abled and Live Data text boxes to initiate communication. Then, you
must set up communication parameters by clicking the Setup button
from the General tab.
• After changing any of the parameter values from any setup screen,
you must click the Apply button under the Setup tab to activate the
new settings. This will send the new parameters to the analyzer, but
will not save them to the analyzer’s EEPROM. The Configurator
Software will then prompt with “Would you like to save the settings
EEPROM?”. Click YES to save the new value(s) to the analyzer’s
EEPROM.
• If you want the parameter changes to be valid only for the current
session, click NO when prompted with “Would you like to save the
settings EEPROM?”. The changes will revert to the previously saved
changes after the system is powered down and then powered up
again, or if the analyzer is reset.
When you select the Print to File button from the Setup tab, the Save As
dialog box appears (Figure 4-7). Select the path you wish to save the file
to, give the file a name, and then click Save. The software saves the
current analyzer configuration parameters to an ASCII file. Note that the
file will be saved with a “.dmp” extension.
Figure 4-7.
Save As dialog box
(Print to File button).
When you select the Print button from the Setup tab, the Print dialog box
appears (Figure 4-8). Make sure a printer is connected to the PC or avail-
able through a network before printing these settings. Click OK to print a
hard copy of the current analyzer configuration parameters.
Figure 4-8.
Print dialog box (Print
button).
When you click the Refresh button from the Setup tab, the latest Calibra-
tion or Configuration changes made in the Configurator Software are
updated in the analyzer.
After changing any of the parameters or their values from any Setup
dialog box, click OK to exit the dialog box and return to the Setup tab (see
Figure 4-6). Then, click the Apply button at the bottom of the M933
Properties dialog box (under the Setup tab). The software will then
prompt “Would you like to save the settings to EEPROM?”. Click YES to
send the new value(s) to the analyzer and save them to EEPROM.
The Gas Calibration dialog box (Figure 4-9) contains gas species informa-
tion and sampling system control parameters.
Figure 4-9.
Gas Calibration dialog
box.
Species
Displays the names of available, factory-set gas species/output set-
tings.
Span Conc
This is the concentration of the component (typically PPM) in the
calibration gas mixture. The concentration value must be entered
before initiating a calibrations sequence. The concentration is entered
in decimal notation. The maximum concentration which can be
entered is 999 999. If a calibration gas is not used, this value must be
set to zero. Concentrations are typically in PPM, but can be custom-
ized (refer to “Custom Output (Custom Setup),” later in this chapter.
SFactor
The Span (calibration) Factor for the calculated result (component
concentration) for each configured gas species. The analyzer’s Span
Factor is adjusted automatically whenever the analyzer is Spanned.
ZDriftSpec
At the end of every Auto-Zero or manual zero, the zero drift from the
previous Auto-Zero or manual zero result is calculated and displayed.
A “Warning Zero Drift” error message is displayed if the zero drift of
any species exceeds its Zero Drift Specification.
The analyzer gas flow control can operate in one of six “sampling”
modes. For normal operations, the analyzer is in the Auto mode.
Zero button
This button permits a manual zeroing of the analyzer. The analyzer
zero is adjusted automatically based on the average reading during
the Calibration Integration time period. The zero gas must be intro-
duced manually (see Chapter 5), using the Flow Control command
(Zero).
The Modbus dialog (Figure 4-10) box contains operational parameters for
the Customer Data Acquisition port.
Figure 4-10.
Modbus dialog box.
Address
Enter the Modbus network address assigned to the analyzer.
Baud Rate
Select the baud rate of the Modbus network.
Stop Bits
Select the number of stop bits of the Modbus network.
Parity
Select the parity of the Modbus network.
Figure 4-11.
Temperature Control
dialog box.
Bench
The measure range (°C) for the Optical Bench. For more information,
refer to “Optical Bench” following these descriptions.
Cell
The measure range (°C) for the Measuring Cell. For more information,
refer to “Measuring Cell” following these descriptions.
Column
The parameters for the Column Block. For more information, refer to
“Column Block” following these descriptions.
Range
The measure range (°C) for each temperature zone.
Setpoint (°C)
The control setpoint (°C) for each temperature-controlled zone.
Because the Model 933 Analyzer only monitors (it does not control)
the temperature of the Measuring Cell, the Measuring Cell setpoint
should be set to zero (0).
Kp (band)
The proportional term of the PI temperature control algorithm for
each zone.
Start-up (%)
The duty cycle used on start-up for each temperature-controlled zone.
Optical Bench
A (default) 2-3 31 °C to 47 °C
B 1-2 45 °C to 62 °C
A (default) 1-2 -3 °C to 66 °C
B 3-4 60 °C to 131 °C
C 5-6 121 °C to 194 °C
D 7-8 186 °C to 261 °C
Column Block
The Output Setup dialog box (Figure 4-12) contains Current and Voltage
output assignments plus concentration alarms and setting parameters.
Figure 4-12.
Output Setup dialog
box.
In addition to the usual capability of zeroing and spanning the V/I and
Voltage Outputs, you can also set them to a mid-scale level for diagnostic
purposes. The low end of each analog output range can be a nonzero
value.
Iout
Iout Assignment
Current output assignment with and without Track and Hold
(T&H).
Vout
Vout Assignment
Voltage output assignment with and without Track and Hold
(T&H).
Vout Zero
The measured voltage output when the analog output is set to
zero during the calibration procedure for a voltage output.
Vout Span
The measured voltage output when the analog output is set to
full-scale during the calibration procedure for a voltage output.
Normal button
Once analog output calibration is complete, this button will allow the
outputs to go back to normal operation.
Mid-Scale button
Places the outputs to mid scale.
Toggling between Alarm Disable and Alarm Enable will clear the
latched alarms.
NOTE
Conc. Assn.
Concentration alarm assignments.
Conc. On
This alarm will activate when the output value exceeds the Con-
centration On setpoint.
Conc. Off
This alarm will deactivate when the output value falls below the
Concentration Off setpoint.
Conc. Delay
The alarm activation will be delayed by the amount of time en-
tered in the Concentration Delay text field after the concentration
output has exceeded the Conc. On setpoint.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.
The Info dialog box (Figure 4-13) contains Microcontroller and Host
Controller information.
Figure 4-13.
Information dialog
box.
Host Version
Host Controller version number.
Micro Version
Microcontroller version number.
Serial #
Analyzer serial number.
EEPROM Writes
This indicates the number of times that data has been saved on the
EEPROM. The maximum number of saves that an EEPROM will allow
is 20,000. After this point, the EEPROM will need to be replaced (refer
to “EEPROM Replacement” in Chapter 6).
Reset M933
Resets the analyzer’s Host Controller board.
The Optical Bench dialog box (Figure 4-14) allows optical bench control
and data acquisition parameters to be viewed and modified.
Figure 4-14.
Optical Bench dialog
box.
Base (mV)
The minimum operating current control setpoint for each source lamp.
FltrPulse (mV)
Filter Pulse is the source lamp pulse current control signal for each
filter. The normal operating range is between base setting and Lamp
Max, with the control signal for the key filter being Lamp Max. If the
filter position is not used, the Filter Pulse value must be set to a
negative number. The recommended value is negative base setpoint.
Tzero
Transmittance Zero is the PMT signal transmittance value of the filters
with zero gas in the sampling system. It is adjusted automatically
whenever the analyzer is zeroed.
Bench Type
The bench type code defines the Optical Bench orientation and the
filter positions assigned to each source lamp. The code is the decimal
equivalent of an 8 bit binary number. The definition for each bit is
shown below under “Bench Orientation,” “Filter Position Assign-
ment,” and “Standard Bench-Type Code.”
Bench Orientation
B0 Measure PMT Reference PMT
0 PMT 1 PMT 2
1 PMT 2 PMT 1
0 0 0 1 3 5 4 6 2
0 0 1 3 5 4 6 1 2
0 1 0 1 3 4 5 6 2
0 1 1 1 3 2 Motorless
1 0 0 1 3 5 4 6 1
* B7, B6, B5, and B4 are reserved for future use.
8 1 0 0 0
* Values in brackets beside number is its decimal weighting.
Samples
This indicates the number of times the PMT signal is measured while a
filter is completely within the light path.
Delay
The time interval between when the filter becomes completely within
the light path and the first PMT signal measurement. The interval is
shown as multiples of 1.6 microseconds (µs).
MaxT90 (sec)
Maximum T90 is the time (default is 60 seconds) required for the
output signal to reach 90 percent of the final value after a step change
in the concentration. Larger values reduce the noise level on the
output signal but, at the same time, increase the response time. Ad-
justing from default is not recommended.
Key Filter
Key Filter is the position of the filter which gives the weakest signal
for a given source lamp current.
Auto-Setup button
The Automatic-Setup function optimizes the PMT gains and source
lamp currents. This function combines automatic signal adjustment
with manual jumper positioning and should be executed after any
lamps, filters, or PMTs have been installed or replaced. The process
requires approximately three minutes. To determine when an Auto-
Setup is needed, refer to Chapter 6.
The Matrix dialog box (Figure 4-15) contains information that is respon-
sible for partially calculating the concentration output and negating the
effects of cross talk by interfering gas species.
Figure 4-15.
Matrix dialog box.
Species
This designates which gas species are currently configured.
Row/Filter
The value in each row (Row 1–6) and each column (Filter 1–6) in the
calculation matrix.
The Column Timing dialog box (Figure 4-16) contains column operational
parameters.
Figure 4-16.
Column Timing dialog
box.
Species
These are the gas species that are currently configured for the ana-
lyzer.
Figure 4-17.
Compensations dialog
box.
Abs Offset
The absorbance offset vector for each filter location.
Compressibility
In addition to pressure and temperature compensations of the concen-
trations according to the ideal gas law, it is possible to enter an addi-
tional parameter, Z to account for the compressibility factor of the
sample gas. One value of Z is used for all species. The default value for
this parameter is 1, but can be any value between 0.5 and 1.5. The
correction is applied to the concentrations in the following manner:
<Conc>corr. = <Conc>uncorr. / Z
Default
The default absolute pressure for the Measuring Cell (mmHg or
"Hg). This value is used in place of the measured Measuring Cell
pressure when active pressure compensation is disabled.
LowScale
The pressure transducer low value (mmHg or "Hg) corresponding
to 0.0 VDC. See “Cell Pressure JP301 and JP302 Customer I/O
Board” below.
HighScale
The pressure transducer high value (mmHg or "Hg) corresponding
to 5.0 VDC. See “Cell Pressure JP301 and JP302 Customer I/O
Board” below.
Figure 4-18.
Advanced Options
dialog box.
At recheck interval minutes from the start of the first Auto-Zero, another
Auto-Zero is performed and the drift-over-time value for each species
is computed. If one of the drift-over-time values is above its allowable
specified value, the Startup Auto-Zero ReCheck process is repeated
for up to four more times.
The Custom Output dialog box (Figure 4-19) contains units information
and configuration parameters for custom setup.
Figure 4-19.
Custom Output dialog
box.
Conversion Factors
These are the units of measurement used for gas species concentra-
tions (PPMV is equal to 1). The analyzer always computes the concen-
tration in PPMV. To have the analyzer output concentration values in
other units, a conversion factor is required. See “Conversion Factors in
Custom Setup.”
H2S: 1.416581 mg/Nm^3 per ppm H2S: 0.705925 ppm per mg/Nm^3
COS: 2.49747 mg/Nm^3 per ppm COS: 0.400405 ppm per mg/Nm^3
MeSH: 1.999695 mg/Nm^3 per ppm MeSH: 0.500076 ppm per mg/Nm^3
Custom Results
Custom Result is the weighted sum of the first four species. A multipli-
cation factor is applied to each concentration before it is summed with
the next concentration.
Figure 4-20.
Status tab.
Status
This will indicate the communication status between the Configurator
and the Model 933 Analyzer (i.e., Online or DEMO).
Error Condition
There are two categories of alarm errors, Warning and Fault. Active
Warning and Fault errors are annunciated in the Error Condition list.
Fault errors indicate that a fault has occurred and the analyzer data
are not valid. Fault errors are also indicated by the Fault relay being
de-energized.
See Chapter 6 for a listing of the various warnings and faults and the
corrective actions.
Host Runtime
This indicates the amount of time the Host Controller has been opera-
tional.
Micro Runtime
This indicates the amount of time the Microcontroller has been opera-
tional.
Micro State
This displays messages that indicate which step of the Auto-Setup
function is currently being performed:
Host State
This displays messages that indicate the current operational status of
the analyzer:
Start-up shut-in/off The analyzer has shut off the flow of sample
gas through the sampling system during its
start-up sequence.
Start-up time delay This delay period, activated at analyzer
power-up or reset, allows time for the
analyzer to stabilize prior to operation. This
parameter is not user-adjustable.
Operational The analyzer is operating normally (sam-
pling gas).
Alarm clearing The analyzer is clearing an alarm after the
alarm has been corrected.
Calculated Results
The gas species, or parameters, calculated by the analyzer are dis-
played. The name of the result and its value will be displayed and
updated at one-second intervals. The custom parameter is a combina-
tion of calculated results (refer to “Custom Output (Custom Setup),”
earlier in this chapter).
Figure 4-21.
Optical Bench Data
tab.
Transmittance
Displays the transmittance for each filter location.
Absorbance
The absorbance for each filter location.
Figure 4-22.
Analyzer Data tab.
Concentration
This designates which gas species are currently configured and their
current values.
Analog Output Concentration Values
V-Output
The concentration value at each analog voltage output channel.
I-Output
The concentration value at each analog current output channel.
Timing
Next Auto-Zero (min)
The amount of time until the next Auto-Zero starts. Minus 1 (-1)
indicates timed Auto-Zero disabled.
Cal Ends (sec)
The amount of time left in the Calibration Integration Timer (see
Cal Int Time). Minus 1 (-1) indicates no gas calibration in progress.
Next Col Switch (sec)
The amount of time left until the regenerating column and absorb-
ing columns switch. Minus 1 (-1) indicates column switching
deactivated.
Temperature Zone
Temperature (°C)
The real time operating temperature for each temperature-con-
trolled zone (Bench/Cell/Column).
Duty Cycle (%)
The real time duty cycle of each temperature-controlled zone
(Bench/Cell/Column).
Solenoid
This will indicate which solenoid (Zero, Column A, Column B) is
currently energized, if any.
Alarm
This will indicate which, if any alarms are currently active.
Once the file is opened, click on the Standard Toolbar to start data
scanning.
Display Modes
• Meter Mode
Meter-type format. Alarms can be displayed to view current reading
relative to high- and low-alarm limits.
• Annunciator Mode
Track whether a measured parameter is within acceptable user-de-
fined limits using a simple color/text indication.
• Trend Mode
View trends of measured parameters.
• Tabular Mode
View information in a textual, table-type format.
• Custom Mode
Create custom setups to include a single mode display window or
multiple mode display windows.
Right-click on the display window for the device you have selected
(Figure 4-23) and then click Scan from the context menu. The Trend
Properties dialog box appears with the Scan tab active (Figure 4-24).
For Trend and Tabular modes, you must first select a channel before
you can define scan settings.
NOTE
Figure 4-23.
Mode context menu.
Figure 4-24.
Scan tab.
Data Source
Select the device from which to scan or temporarily disable the scan-
ning device.
Disabled
Select this option to disable the display of the selected channel.
Device
Select this option and use its list box to select the device from
which to scan.
1. Select the display window that will receive the linked data
from another data source.
2. Right-click over the display window and then click Scan from
the context menu that appears.
3. From the Data Source group, select the Link from button.
4. Select the data source to link from using the Link from list box.
Starting a Scan
To start a scan, click or select Scan from the Control menu. The
message “Scanning” and the scanning progress will appear in the Status
Bar at the bottom of the window (if it has been enabled).
If you have scheduled scans at timed intervals and the system has fin-
ished a scan and is waiting to start the next scan, the time remaining
before the start of the next scan is displayed.
“Idle” is displayed in the Status Bar when the system is not scanning.
Stopping a Scan
Click or select Scan from the Control menu to toggle off the scan.
Figure 4-25.
Schedule scans dialog
box.
1. Select the display window or windows for which data will be saved.
• Hold down the shift key and click on each window to be included
when selecting multiple display windows.
2. From the File menu, select Save Data or click on the Data File
Toolbar to view the Save As dialog box (Figure 4-26). From here, you
can specify data file attributes.
Figure 4-26.
Save As dialog box.
3. Once the attributes are set, enter a name for the data file in the File
name text field and save it in a folder using standard Windows tech-
niques. Select the following (as required):
4. To stop saving data, select Stop Saving from the File menu or click
1. From the File menu, select Open Data or click on the Data File
Toolbar.
3. Select Open. The data file appears on the screen. From here it can
either be viewed or printed.
1. From the File menu, select Convert Data File and select one or more
data files.
2. Click Convert to convert and save the file with a CSV extension.
Printing Data
The Configurator Software will print scanning information in a format
similar to how it is displayed on the screen using the display parameters
created for that mode. You can view a preview of what will be printed by
selecting Print Preview from the File menu.
In Custom mode, the system prints the currently selected display win-
dow. If you do not select a display window, the system prints information
for each display window using the required number of pages.
To print data:
4. If you select Print from the File menu, a standard Windows Print
dialog box appears. Set the additional print information.
Figure 5-1.
Gas Calibration dialog
box.
Calibration | 5-1
To perform a span gas calibration follow these steps:
2. Once the Auto Zero process is completed, turn off the zero gas.
3. Remove the Swagelok plug from the span gas connection inlet and
connect the span gas. See Figure 5-2.
PROCESS INSTRUMENTS
CAUTION:
RISK OF ELECTRIC SHOCK
ATTENTION:
CONSULT USER MANUAL
0344
PROCESS INSTRUMENTS II 2 G
Caution
Do not open when an explosive gas atmosphere is present.
Figure 5-2.
Span gas and zero
gas inlet locations
(Europe).
5. From the Flow Control list, select “Zero.” Click OK on the Gas Cali-
bration dialog box and then click Apply on the Setup tab. Click NO
when prompted to save parameters to EEPROM.
6. Adjust the span gas regulator so the pressure regulator on the Model
933 reads 80 PSI.
8. View the Analyzer Data tab (Figure 5-3) and observe the concentra-
tion readings.
Figure 5-3.
Analyzer Data tab.
10. Bleed down the calibration gas and disconnect it from the span gas
connection point.
11. Connect the Swagelok plug to the span gas connection point.
12. Turn on the zero gas and confirm that the pressure is at 80 PSIG.
13. From the Flow Control list, select “Auto.” Click OK on the Gas Cali-
bration dialog box and then click Apply on the Setup tab. Click YES
when prompted to save the parameters to EEPROM.
Calibration | 5-3
Analog Output Calibration
Figure 5-4.
Output Setup dialog
box.
Current Calibration
The current outputs are calibrated at the factory. If a current output
module is replaced or added, then that output should be calibrated.
Calibration of a current output is performed by entering the measured
zero and full-scale (span) signals for each output (see Figure 5-4). These
values are used to offset the output to the correct values.
To calibrate the output (1, 2, 3, or 4), connect a current meter to the output
of interest (see J109 on the Customer I/O board, Figure 5-5) and then:
4. Once all desired output channels have been measured and data
entered, click Span Cal.
6. Type the value into the applicable Span (mA) text field.
7. Once all desired output channels have been measured and data
entered, click OK and then click Apply. Click YES when prompted to
save the parameters to EEPROM.
Figure 5-5.
Customer I/O board
(Part No. 100-1758).
Calibration | 5-5
Voltage Calibration
The voltage outputs are calibrated at the factory. Most users will probably
use current outputs rather than the non-isolated voltage outputs. If the
I/O board is replaced, then the voltage outputs should be calibrated if
they are used for data acquisition. This is done from the Output Setup
dialog box (Figure 5-4). Calibration of a voltage output is performed by
entering the measured zero and full-scale (span) signals for each output.
These values are used to offset the output to the correct values.
To calibrate the output (1, 2, 3, or 4), connect a voltage meter to the output
of interest (see J108, Figure 5-5) and then:
3. Type the value into the applicable Zero (V) text field.
4. Once all desired output channels have been measured and data
entered, click Span Cal.
6. Type the value into the applicable Span (V) text field.
7. Once all desired output channels have been measured and data
entered, click OK and then click Apply. Click YES when prompted to
save the parameters to EEPROM.
Safety Considerations
To prevent an explosion, test the area around the analyzer for hazard-
! ous gases and proceed with maintenance only when the area is found
WARNING to be safe (nonhazardous).
Clean the Measuring Cell and the rest of the analyzer’s sampling
system. This schedule is a minimum requirement. If other
conditions are found to be present, as outlined under the section
titled “Cleaning the Measuring Cell and Replacing O-Rings,”
cleaning may be required more frequently.
Replace the flow restrictors (one in each of the three filter stages)
and clean the assembly before reassembling it.
* In natural gas streams that are extremely dirty, the flow restrictor
in the first filter stage may need to be changed more often
because it removes most of the liquids and particulate from the
gas.
Replace the o-rings and the filter elements in the Column Block
Assembly. At the same time, observe the check valves for wear
and replace them if necessary. Clean the Column Assembly cavity
before reassembling the Column Block.
If the sample response time is longer than normal, it is most likely due to
plugging somewhere in the sampling system. The next step is to locate
and remove the plug. The portion of the sampling system with the high-
est risk of plugging is the sample inlet and the section of the sample inlet
most prone to plugging is the Sample Probe Valve. One way to confirm
that a plug is in the sample inlet is to cap the Vent Line (or, optionally,
close the Vent Valve’s isolation valve) and Zero the analyzer.
After confirming that the plug is somewhere in the sample inlet, take
all appropriate safety precautions and dismantle the sample system,
NOTE starting at the Sample Probe.
Plugs in the sample outlet (or vent side) of the sample system are rare. If
an aspirator is used to transport the sample gas (i.e., part of a Heated
Sample Gas Probe, if used), a plug in the vent system can cause the aspira-
tor drive air to flow back into the Measuring Cell and, essentially, simulate
a Zero Gas Flow or Backpurge condition.
To do this, click the Gas Calibration button from the Setup tab to view
the Gas Calibration dialog box. From the Flow Control list, select
“Zero.”
3. Close the isolation valve on the Sample Probe Valve. Observe the flow
on the rotameter. If the flow reduces to a stop, a large plug has oc-
curred somewhere in the sampling system.
5. After locating the cause of the restriction or plug (and after cleaning or
replacing the part or line), leak test the fittings or connections that
were loosened or replaced. To do this, follow the procedures under
“Sampling System Leak Check” in Chapter 3.
6. Return the isolation valve on the Vent Valve to the open position (or
remove the NPT plug and reconnect the Vent Pipe to the Vent port on
the Measuring Cell). Both isolation valves should be open.
To do this, click the Gas Calibration button from the Setup tab to view
the Gas Calibration dialog box. From the Flow Control list, select
“Auto.”
8. Check the sample response time. Record the response time. The
recorded value can be used later as a reference while testing response
time.
If your application uses a Measuring Cell other than the two men-
tioned in this manual, refer to the Supplemental Information tab of
NOTE this manual, or the Documentation Package shipped with the analyzer
for the appropriate assembly drawing.
The o-rings in the Measuring Cell should be replaced every year to avoid
a leak in the sampling system. While the Measuring Cell is disassembled,
clean its chambers and parts, including the windows.
Refer to Figures 6-1, 6-2a, and 6-2b for assistance in locating and identify-
ing the parts that make up the Measuring Cell.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.
Start the Configurator Software and from the Edit menu, click Device
Properties, view the Setup tab, and then click the Gas Calibration
button. Refer to “Establishing Communications With the Analyzer
Using a Laptop Computer,” in Chapter 3.
From the Flow Control list, select “Zero”. Click OK and then click
Apply. Click NO when prompted to save parameters to EEPROM.
Close the sample inlet valve. Allow the analyzer sampling system to
backpurge with Zero gas for 2–3 minutes.
3. Return to the Gas Calibration dialog box and select “Shut-In” from
the Flow Control list. Click OK and then click Apply.
6. STANDARD RANGE
Remove the three M4 x 35 mm screws that secure the Measuring Cell to
the Window Cover. Grasp the edge of the window and carefully re-
move it. Remove the o-ring (P/N 300-9060).
LOW RANGE
Remove the three M4 x 35 mm screws that secure the Measuring Cell
to the Window Cover. Remove the three M4 x 8 mm screws that
secure the aperture plate to the Measuring Cell. Grasp the edge of the
window/mirror combination and carefully remove it. Remove both
o-rings (P/N 300-9060).
7. STANDARD RANGE
Hold the Measuring Cell vertically so that the Reflector Block is on top
and remove the three screws that secure the Reflector Block to the
Measuring Cell. Remove the Reflector Block.
Grasp the edge of the window and carefully remove it. Remove the
two o-rings (P/N 300-9060). Inspect all the o-rings for flexibility and for
any signs of wear or contamination.
LOW RANGE
Hold the Measuring Cell vertically so that the Reflector Block is on top
and remove the three screws that secure the Reflector Block to the
Measuring Cell. Remove the Reflector Block. Remove the o-ring
(P/N 300-9060).
9. Inspect the interior of the Measuring Cell for foreign material. If you
need to clean the interior, use a nonabrasive detergent and water
solution, isopropanol, or reagent-grade acetone followed by a rinse
with pharmaceutical-grade distilled water.
1. STANDARD RANGE
Hold the Measuring Cell vertically with the Reflector Block end up and
install two new o-rings (P/N 300-9060) and the window.
LOW RANGE
Install a new o-ring (P/N 300-9060) in the end of the Measuring Cell
that connects to the window holder. Install one new o-ring
(P/N 300-9060) in the window holder. Replace the window in the
window holder. Place the window mounting plate on the window
holder and secure it using the three M3 x 10 mm screws.
Hold the Measuring Cell vertically with the Reflector Block end up.
Connect the Reflector Block and window holder to the Measuring Cell
using the three screws removed earlier.
Using the three screws removed earlier, secure the Reflector Block to
the Measuring Cell. Tighten the screws evenly.
3. STANDARD RANGE
Invert the Measuring Cell and install a new o-ring (P/N 300-9060) and
the window.
LOW RANGE
Invert the Measuring Cell and install a new o-ring (P/N 300-9060) and
the window/mirror combination. Orient the window/mirror combination
so that the mirror side is not in contact with the sample gas. Install a new
o-ring (P/N 300-9060) on the aperture plate. Orient the aperture plate so
that the outside countersink hole is aligned with the sample fitting.
Secure the aperture plate to the Measuring Cell using the three
M4 x 8 mm screws removed earlier. Tighten the screws evenly.
LOW RANGE
Hold the Measuring Cell so that the sample fitting near the aperture
plate is up. Use the three screws removed earlier to secure the Measur-
ing Cell to the window cover. Tighten the screws evenly.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not power up the analyzer or laptop computer if there is a hazard-
ous gas atmosphere present.
8. Open the valves isolating the analyzer from the sampling stream
and/or remove the cap from the Vent Line outlet.
9. Allow the analyzer to warm up then click Gas Calibration from the
Setup tab. Select “Zero” from the Flow Control list. Click OK and then
click Apply. When prompted to save parameters to EEPROM, answer
click NO.
10. Click Optical Bench from the Setup tab and perform an Auto-Setup
function by clicking Auto-Setup.
12. When the zero calibration is complete, return the Flow Control setting
in the Gas Calibration dialog box to “Auto”. Click OK, and then click
Apply. Click YES when prompted to save the parameters to EEPROM.
The mating surfaces of the Column Block Assembly housing and cover
! is a flamepath.
CAUTION
Take care to avoid damaging this flamepath when disassembling and
reassembling the Column Block.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
• In the Check Valve if the parts are found to be damaged while per-
forming an unscheduled maintenance, or
• If the Measuring Cell was inspected and white particulate was re-
moved from it.
• The system flow rates have decreased. Typical flow on the rotameter
should be approximately 2 litres/min with 80 PSIG (550 KPAG) supply
pressure.
The spare parts for this assembly can be found under “Recommended
Spare Parts” in Chapter 7.
The parts that are removed and replaced in this procedure correspond
with Item #s in Figure 6-3.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.
1. Connect your laptop computer to the Model 933 Analyzer via the
Explosion-Proof Digital Communications Port on the front of the
Lower Enclosure.
Start the Configurator Software and from the Edit menu, click Device
Properties, view the Setup tab, and then click the Gas Calibration
button.
From the Flow Control list, select “Zero”. Click OK and then click
Apply. Click NO when prompted to save parameters to EEPROM.
2. Close the sample inlet valve. Allow the analyzer sampling system to
backpurge with Zero gas for 2–3 minutes.
5. Disconnect the tubing from the Column Block and follow the remain-
ing procedures.
6. Remove the three M6 X 12 mm screws (Item 28) that secure the Col-
umn Block valve cover (Item 27) to the Column Block (Item 25).
7. Remove the check valves (Item 26) from the Column Block with a pair
of needle nose pliers. Remove the o-ring (Item 29). Inspect the check
valves and o-ring for any signs of wear. Install a new o-ring. Replace
the check valves or install new check valves, if necessary.
8. With the check valves and o-ring in place, replace the Column Block
valve cover in the Column Block and tighten the three M6 X 12 mm
screws.
10. Inspect the o-ring (Item 9) on each column assembly and replace if
necessary.
11. Remove the M6 nut (Item 8) from the filter spool assembly (Item 4).
Remove the seal washer (Item 11), o-rings (Items 5 and 7), and filter
(Item 6).
12. Inspect filter for signs of saturation (yellowing) and replace if neces-
sary. If there is particulate on either black filter spool, clean it with
isopropanol or distilled water.
Figure 6-3.
Column Block assembly.
1. Reassemble the filter spool assembly (Item 4) and tighten the M6 nut
(Item 8) by hand.
2. For each column assembly (Item 10), replace new o-rings (Items 5
and 7) and filter element (Item 6) on the filter spool and then replace
the column assembly in the Column Block (Item 25).
3. Remove the ten M6 X 20 mm screws (Item 17) that secure the Column
Block flange (Item 20) to the Column Block and remove the two flow
restrictors (Item 23).
4. Inspect the flow restrictors for signs of plugging from column material
particulate and replace them with new ones if necessary.
5. Install the flow restrictors using new o-rings (Item 24). The o-rings are
rolled over the threads onto the flow restrictor.
6. Replace the ten M6 X 20 mm screws (Item 17) that secure the Column
Block flange (Item 20) to the Column Block (Item 25).
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not power up the analyzer or laptop computer if there is a hazard-
ous gas atmosphere present.
10. Open the valves isolating the analyzer from the sampling stream
and/or remove the cap from the Vent Line outlet.
11. Allow the analyzer to warm up then click Gas Calibration from the
Setup tab. Select “Zero” from the Flow Control list. Perform a manual
zero calibration by clicking the Zero button.
12. When the zero calibration is complete, return the Flow Control setting
to “Auto”. Click OK, and then click Apply. Click YES when prompted
to save the parameters to EEPROM.
The typical life span of the source lamps is approximately 9–12 months of
continuous operation. However, a source lamp can exhibit signs of degra-
dation after 5 to 6 months.
Figure 6-4.
Optical Bench Data
tab.
Figure 6-5.
Error Condition on
Status tab.
• The cathode of the source lamp must be centered on the optical axis of
the beam splitter for optimal operation of the analyzer. The cathode
and the outer envelope of the lamp are not necessarily concentric or
consistent from lamp to lamp.
Refer to Figure 6-1 for assistance in locating and identifying the hardware
components encountered while replacing the source lamps.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
2. After the area has been tested for hazardous gases (and found to be
safe), remove the 24 M10 screws from the EEx d Upper Enclosure door
and open it.
4. Loosen the Lamp Retaining Screw on the bottom of the lamp socket
and rotate the Lamp Adjustment Plate 90 degrees. Remove the Lamp
Socket Assembly.
Do not rotate or pull on the base of the source lamp because this may
! cause it to separate from the glass envelope. Grasp the glass envelope
CAUTION when rotating or pulling the source lamp.
6. Install the new lamps. Make sure that the narrow end of each lamp is
pushed completely into the holder. Do not touch the (flat) window at
the end of the lamp.
Before proceeding, test the area around the analyzer for hazardous
gases and proceed only when the area is found to be safe.
9. After the area has been tested for hazardous gases (and found to be
safe), restore power to the analyzer. Allow the analyzer to warm up
before continuing.
a. From the Setup tab, click Output to view the Output Setup dialog
box. Click Alarm Disable and then OK.
c. From the Setup tab, click the Gas Calibration button to view the
Gas Calibration dialog box (Figure 6-6).
From the Flow Control list, select “Zero”. Click OK and then click
Apply from the Setup tab. When prompted to save the parameters
to EEPROM, click NO. Allow the zero gas to flow for 2–3 minutes.
Figure 6-6.
Gas Calibration dialog
box.
11. Return to the Output Setup dialog box and click Alarm Enable and
then OK.
Return to the Gas Calibration dialog box and change the Flow Con-
trol setting back to “Auto”.
Click OK and then click Apply from the Setup tab. Click NO when
prompted to save parameters to EEPROM.
Figure 6-7.
Optical Bench dialog
box.
Figure 6-8.
Configurator screen
after opening
LampSetup.dyc.
To change the Y-axis voltage scale, move the mouse pointer to the
graph and right-click. Click Display and change the Upper and
NOTE Lower Limits.
15. Align the Source Lamps (described under “Source Lamp Alignment,”
later in this chapter) to ensure optimal operation and then perform
another Auto-Setup. Return to these procedures after the Auto-Setup
is complete.
16. After the lamp replacement and alignment process is complete, the
analyzer is ready to operate.
17. Using a soft, nonabrasive cloth, gently clean the mating areas
(flamepath) of the Upper Enclosure and its door and replace the 24
M10 screws. Tighten the M10 screws to 9.0 Nm, ±1.0 Nm (80 in.-lb,
±9 in.-lb).
When the Auto-Setup is initialized, the Automatic Lamp Control (Alc On)
function is automatically turned on. To view the current status of this
function, press the Optical Bench button from the Setup tab. The Alc On
check box will be checked when this function is on.
PMT Level and PMT Balance are adjusted only during the Auto-Setup
sequence. The range of operation for both these parameters is 0–10 VDC.
Normal values for both, after a successful Auto-Setup, is from 2.5–7.5
VDC. The analyzer will function with values outside this range, but it is a
sign that a change has likely occurred in the transmission of light within
the Optical Bench.
At the end of every Auto-Setup, always check the PMT Level and PMT
Balance. Take note of severe changes in PMT Level and PMT Balance
because they are as important as the absolute value.
The PMT Level signal adjusts the gain of both PMTs simultaneously in
the same direction. PMT Balance adjusts the gain of the two PMTs in
opposite directions by controlling a virtual ground circuit on the Optical
Bench Service Electronics Board.
If the PMT signals are outside their normal range of operation after the
Auto-Setup function is complete, check for the following:
• Was the Auto-Setup done with zero gas flowing through the sampling
system?
• Are the PMTs in their original sockets (i.e., is the higher gain PMT in
the Measure path)?
• Do the source lamps need replacement? If not, are the source lamps
aligned?
• Have there been any leaks from the Measuring Cell? If so, check the
condition of the optical filters, beamsplitter, mirrors, windows, lenses,
and o-rings in the Optical Bench and in the Measuring Cell (including
Reflector Block). Contact AMETEK for procedures not discussed in
this manual.
To perform an Auto-Setup:
1. From the Setup tab, click the Gas Calibration button to view the Gas
Calibration dialog box.
From the Flow Control list, select “Zero.” Click OK and then click
Apply from the Setup tab. When prompted to save the parameters to
EEPROM, click NO. Allow the zero gas to flow for 1–3 minutes.
2. From the Setup tab, click Output to view the Output Setup dialog box.
Click Alarm Disable and then OK.
3. From the Setup tab, click the Optical Bench button to view the Opti-
cal Bench dialog box.
5. From the Status tab, observe the status of the Micro State. The follow-
ing messages are displayed to indicate which step of the Auto-Setup
process is being performed:
7. From the Optical Bench dialog box, check the PMT Level and PMT
Balance again. The voltage should be between 2.5 and 9.84 VDC.
Cancel Auto-Setup
There are six jumper positions (four in P300 and two in P301) that can
accommodate one jumper each. At least one jumper is required in P300
and P301 at all times. Adding jumpers increases the supply voltage avail-
able to the Reference path PMT. This increases the PMT Balance and, to a
small degree, decreases the PMT Level. The opposite occurs if jumpers are
removed.
Figure 6-9 describes the effect on the PMT Balance and PMT Gain in
relation to different jumper positions.
2. After an acceptable PMT Balance and PMT Level has been achieved,
initiate a zero function.
To do this, click Gas Calibration from the Setup tab to view the Gas
Calibration dialog box. Click the Zero button to initiate a zero calibra-
tion and then click OK.
Click the Status tab and observe the Host State status to determine
the current operation being performed.
4. From the Setup tab, click Output. Click Alarm Enable and then OK.
4. Loosen the Locking Screw located between the two source lamps.
5. To obtain the maximum signal from the Measure PMT voltage, adjust
the Lamp Adjusting Screw for the lamp that is being adjusted.
7. Tighten the Locking Screw located between the two source lamps.
8. Tighten the Lamp Clamping Screw to secure the lamps. Do not over-
tighten; the spring should not be collapsed.
9. Tighten the Lamp Retaining Screw to secure the lamp socket. Do not
overtighten; the spring should not be collapsed.
Click the Zero button to initiate the zero calibration and then click OK.
Click the Status tab and observe the Host State status for a message
indicating the completion of the zero calibration.
Allow the analyzer to operate for 2–3 minutes with the zero gas still
flowing.
13. When the zero calibration is complete, return to the Output Setup
dialog box and click Alarm Enable and then OK.
Return to the Gas Calibration dialog box and change the Flow Con-
trol setting back to “Auto” (to return the analyzer to Analyzer Control
Mode). Click OK and then click Apply from the Setup tab. Click YES
when prompted to save parameters to EEPROM.
The lamp replacement and alignment process is complete and the ana-
lyzer is ready to operate.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.
2. From the Edit menu, click Device Properties to view the Model 933
Properties screen.
3. From the General tab, click Save Configuration to save the current
Model 933 Analyzer configuration parameter values to a file on the
PC.
Record the location and name of this file; it will be necessary to use
this file to restore the analyzer configuration parameter values after
replacing the EEPROM.
6. Properly orient the new EEPROM and place it on the IC socket. Make
sure all of the pins are seated in their pin sockets before pushing the
EEPROM gently and completely into the socket.
Close the Lower Enclosure door and replace the 24 M10 screws.
Tighten the M10 screws to 9.0 Nm, ±1.0 Nm (80 in.-lb, ±9 in.-lb).
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
9. From the Edit menu, click Device Properties to view the Model 933
Properties screen.
10. From the General tab, click Restore Configuration. Locate and open
the file saved in Step 3.
11. Click YES when prompted to save the parameters to EEPROM. The
software will transfer saved Model 933 Analyzer configuration param-
eter values to the new EEPROM. The EEPROM replacement process is
now complete.
The Model 933 Analyzer is designed with flamepaths that will prevent
flame propagation from within the analyzer’s EEx d Electronics Enclo-
sures to the outside, should an internal explosion occur.
• All separable joints in the Heated Column Block Assembly. These parts
include the mating surfaces of the Column Block Assembly housing
and its cover, and the connecting tube to the analyzer.
If at any time the enclosure door is open and service personnel are not
working on the EEx d Upper/Lower Enclosure, close the door and
secure it with at least one screw. This will reduce the risk of inadvert-
ently scratching or damaging the flamepath.
Before closing the door, gently clean the flamepath with a soft, non-
abrasive cloth and make sure the surfaces are free of debris.
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure and do not power up
the laptop computer if there is a hazardous gas atmosphere present.
The Model 933 Analyzer has a built-in error detection system that con-
tinuously monitors the operation of key parameters. An error can be
detected by either the Host Controller or the Microcontroller and can be
of two types: Fault and Warning. An error is annunciated by the Fault
Status relay or the Warning Status relay. If the analyzer is communicating
with the Configurator Software, the particular condition that causes an
error and the type of error are shown in the Error Condition display box
under the Status tab (Figure 6-11).
Figure 6-11.
Analyzer Status tab.
The Warning Status relay returns to the normal energized state automati-
cally when the offending error condition is corrected and/or the analyzer
completes one of the above operations.
A Fault indicates that a failure has been detected and the analyzer data is
invalid. Under the Fault situation, the analyzer de-energizes the Fault
Status relay and switches the sampling system into the shut-in mode, if
the Flow Control setting is “Auto.” If the Fault Status relay is configured as
non-latching, the relay returns to its normal energized state and the
sampling system is switched back to sampling state when the offending
error condition is corrected. However, if the Fault Status relay is config-
ured as latching, the operator must unlatch the relay in one of the follow-
ing ways:
Figure 6-12.
Host Controller error
conditions/diagnostics.
Figure 6-12.
Host Controller error
conditions/diagnostics.
Figure 6-12.
Host Controller error
conditions/diagnostics.
Figure 6-12.
Host Controller error
conditions/diagnostics.
Figure 6-12.
Host Controller error
conditions/diagnostics.
Figure 6-12.
Host Controller error
conditions/diagnostics.
Figure 6-15.
Upper enclosure
Overtemp switch
(thermo-switch)
location.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
Figure 6-16.
Microcontroller error
conditions/diagnostics.
If this doesn’t correct the error, click Info from the Setup tab to view the
Analyzer Information dialog box and click the Reset M933 button.
If this still doesn’t correct the error, open the Electronics Enclosure covers
and:
• Reset the Host Controller board (SW100, Lower Enclosure – see Figure
6-10).
The Service & Parts chapter discusses what to do if you need technical
support from AMETEK, or if you are returning parts for service. This
chapter also lists the recommended spare parts to have on hand to ensure
all consumable and replaceable parts are replaced according to the “Pre-
ventive Maintenance Schedule” included in Chapter 6.
Technical Support
AMETEK Western Research is committed to providing you the best
technical support in the industry. If you need service or application
assistance, contact your local or nearest AMETEK Service Centre or the
AMETEK factory AMETEK at (403) 235-8400 or 1-800-661-9198, or contact
your local AMETEK Western Research representative.
• AMETEK part number for the specific component you are enquiring
about, if known.
PROCESS INSTRUMENTS
Canada: 1-800-661-9198 U.S.A.: 1-800-537-6044
Optical Bench Service Electronics Board (100-1662) – Recommended Fuses to Have On-Site
120 V 240 V
Description (Location*) Part No. Fuse Type Part No. Fuse Type
Main Board (F200) 300-8778 125 mA 300-8777 63 mA
Photomultiplier Tube (F300) 300-3214 0.2 A 300-3214 0.2 A
Lamp (F201) 300-9524 32 mA 300-9524 32 mA
* These fuses are located on the Optical Bench Service Electronics PWB in the Upper Enclosure.
Follow the steps below to select one or more input channels to display on
your screen.
1. Select a mode in which to display the parameters that you will ob-
serve.
3. Select your device by clicking Device and choosing a device from the
list box.
4. From the Input Channel list box, select the species or parameter that
you want to display in the selected area on your mode display win-
dow by clicking on it.
5. Click OK. The species or parameter that you have selected now
appears on your mode display screen. You can repeat this procedure
up to the number of times defined by the display mode, or create a
custom mode display that contains a greater number of parameters to
be monitored. Figure A-1 list the parameters that can be monitored.
Any display or scan parameters that you define for a mode will not be
transferred to a new mode when you switch modes. However, the system
will continue to scan when you change modes.
Meter Mode
Meter mode allows you to view information in a meter-type format
(Figure A-2). You can assign the parameters in Figure A-1 to any one of 12
meters. Alarms can be set up and displayed on the meter to view the
current reading in relation to the High and Low alarm limits defined. You
can also define unique scan, display, and alarm output settings.
• Each meter has a bar representing a measured value. Text under the
meter displays the numeric value of the measured parameter.
• Each meter can be set to display alarm limits. As long as the measured
value is within the high and low alarm limits, the meter bar appears in
green.
• Any other actions associated with alarms are activated if the limit is
exceeded (e.g., running an information file, or setting off a digital or
analog output).
1. Select Meter from the Mode menu or select the icon from the
Standard Toolbar.
3. Right-click the active meter and define the Scan, Display, and/or
Alarm settings for the meter.
Figure A-2.
Meter mode display.
• For each channel, a green display indicates the value is within accept-
able limits.
• Before changing the display properties, you must select the display by
clicking on it. The display will be highlighted with a yellow border
when selected.
3. Right-click the active display and define the Scan, Display, and/or
Alarm settings for the display.
Figure A-3.
Annunciator mode
display.
• You can view the exact value of a trend line by holding down the left
mouse button in the trend graphical display area. Display the Data
File Toolbar to view the time of each data point.
1. Select Trend from the Mode menu or select the icon from the
Standard Toolbar.
3. Right-click the graph and define the Scan, Display, and/or Alarm
settings for the graph.
Figure A-4.
Trend mode (graph)
display.
• You can copy any of the columns from a Tabular display window to
the clipboard. For more information, see also “Copying Magnitudes”
and “Copying Channels” under “About Dynamic Data Exchange
(DDE),” later in this Appendix.
• Before changing the display properties, you must select the display by
clicking on it. The display will be highlighted with a yellow border
when selected.
1. Select Tabular from the Mode menu or select the icon from the
Standard Toolbar.
3. Right-click the active display and define the Scan, Display, and/or
Alarm settings for the display.
Figure A-5.
Tabular mode display.
For example, you can customize the window to show one Meter mode
display window, one Trend mode window, and two Annunciator win-
dows. Or, you could set up two Trend mode display windows, or two
Tabular mode windows.
Three default custom mode setups are included with the Configurator
Software and more can be added as needed. For each display window
added in Custom mode, the scanning, displays, and alarm output options
are set as if in that mode.
For example, if adding a Meter mode window within the Custom mode,
all settings for that window are defined as if in Meter mode.
Figure A-6.
Set Custom Mode
Menu dialog box.
2. From the Edit menu, select Add Display and select the type of display
you want to add from the list of standard mode types. Or, use the
Custom mode icons on the Custom Mode Toolbar to add different
displays.
3. Specify the data source. Select the applicable source of data from the
Data Source group by clicking Device and then selecting the device
you want to enable.
5. From the File menu, select Save As to save the Custom mode. Or
6. To retrieve the Custom mode file at a later time, select Open Configu-
ration from the File menu. If you used one of the predefined icons,
double-click one of the files to retrieve it.
• To move the window, press and hold down the mouse button (just an
outline of the window is visible) while moving the display window,
then release the mouse button.
1. From the Edit menu, select Add Display. Choose the type of display
window to add.
2. From the Edit menu, select Delete Display, press the Del key on the
1. From the File menu, select Save As. You can save the Custom mode
setup under a new name or use one of the predefined icons.
3. By default, the system places these files in the folder where the
Configurator Software is installed and gives the file a .dyc extension.
If you save a Custom mode file in the install folder with the name
“startup.dyc” it will automatically be opened when the program starts.
1. From the Mode menu, select Set Menu to view the Set Custom Mode
Menu dialog box (Figure A-6). You can associate a Custom mode file to
appear at the bottom of the Mode menu.
You can also provide a menu/button name to appear instead of the file
name at the bottom of the menu.
2. Navigate to the location of the Custom mode file using the Browse
button.
3. To enter a name that will appear at the bottom of the Mode menu,
enter a name in the Menu/Button Name text field.
Figure A-7.
Preferences dialog
box.
• Trend Colors
Set the default trend channel colors.
You can copy any of the columns from a Tabular display window to
the clipboard.
Copying Magnitudes
You can copy any of the columns from a Tabular display window to the
clipboard.
3. From the Edit menu, select Paste Special (or Paste Link, depending on
the version of Windows running) to create the DDE link and continu-
ously update the data in real time.
Copying Channels
2. Right-click and select Copy Channels. This places the name of the
channel onto the clipboard.
3. From the Edit menu, select Paste Special (or Paste Link, depending on
the version of Windows running) to create the DDE link and continu-
ously update the channel names in real time.
If you are importing data into Microsoft Excel, select Preference from
the Edit menu. To place the numbers into separate columns, select
NOTE Return from the DDE Item Separator group. To place the numbers
in rows, select Tab.
Figure A-8.
Defining Display
Parameters screen.
Title
Type the title for the display window. It will then appear in the title
bar for that window and in other areas of the software to identify the
display window.
Lower limit
Applies to Trend and Meter modes only. This value is used only when
the Autoscale check box is not checked. If the Logarithmic check box
is selected, use this text field to enter the number of logarithmic
decades to display on the Y-axis using the upper limit as the top of the
display range. If the Logarithmic is not checked, enter a value into this
text box for the lower limit.
Units
This is the value in which your results will be displayed.
• In the Units text field, type in the units on which you want the
scanned information displayed.
• Precision
Defines the number of digits after the decimal point to be shown.
For example, if the precision is set to 2, a reading might be 5.22.
Channel name
Applies to Trend and Tabular modes only. Names the displayed
channel. See Figure A-9. Select one of the Channels buttons and enter
a name for it in the Channel name text field.
Figure A-9.
Trend Mode Display
Parameters screen.
Minutes
Applies to Trend mode only. Defines the time interval to include on
the display.
Display Values
If checked, displays channel values in Trend mode.
Figure A-10.
Alarm setup.
For Trend and Tabular modes, first select the channel as the source of the
alarms before you define the alarm values. Setting alarms includes defin-
ing alarm limits and defining the actions that should be taken when an
alarm limit is reached. Alarm limits also appear on the main display for
the current mode. High and Low limit alarms appear in red; High and
Low warning alarms appear in yellow.
Name Enter a name for the alarm that will be used to identify
the alarm to the system.
Value Enter the high (upper) limit value for the alarm.
High Warning
When checked, enables the High Warning alarm.
Name Enter a name for the alarm that will be used to identify
the alarm to the system.
Value Enter the high (upper) limit value for the alarm. Must
be lower than the high alarm value.
Low Limit
When checked, enables the Low Limit alarm.
Name Enter a name for the alarm that will be used to identify
the alarm to the system.
Name Enter a name for the alarm that will be used to identify
the alarm to the system.
Value Enter the low limit value for the alarm. Must be higher
than the low alarm value. For analog mode, any mass
values that fall below this limit are counted even if they
are from the same scan.
Action button
Choose the Action button to view the Alarm Action dialog box (Fig-
ure A-11), where you can specify what action the system should take
when the specified alarm is set. This can be used for all four alarms.
Figure A-11.
Alarm Action dialog
box.
Info File Enter the name and path of a help file or use the
Browse button to navigate to the location of a help
file and select the file.
Sound
Enter the name and path of a sound file or use the Browse button to
navigate to the location of the sound files and select a file. This allows
you to include warning sound (in addition to text instructions) to alert
the operator when the alarm is set.
Digital Output
Define how to send the alarm information to a digital output. Select
the device to which you want to send the digital output by using the
Device list box. Select the digital output module using the Module list
box.
Figure A-12.
Alarm message dialog
box.
• Natural gas produced from formations that are rich in heavy hydro-
carbons is usually processed. The processing reduces the hydrocarbon
dew point temperature to the required pipeline specifications. At these
installations, process upsets can result in high dew point temperatures
and hydrocarbon liquids in the gas.
Options | B-1
When accurate and reliable operation is needed for instruments such as
gas chromatographs, lead acetate tape or UV H2S analyzers, dew point
analyzers, some BTU analyzers, and intermittently-operated equipment
such as the manual dew point testers, the requirement of a liquid and
particulate-free sample is more critical. You will significantly reduce
maintenance of this instrumentation by using the appropriate filtration in
the sampling system.
Filtration Stages
1. The first filtration stage is a coarse membrane filter. A membrane filter
is a thin membrane with small holes of a controlled size. Gases will
pass through the pores in the membrane with only a small pressure
drop. Liquid droplets will stay on the upstream side because their
surface tension is too high to allow them to pass through the pores.
This filter removes particulate and high surface-tension liquids such as
water, alcohols, glycols, and some amines. Most of the low-surface
tension liquids such as hydrocarbons will also be eliminated. Since this
membrane has a low surface area and volume, the filter will not
absorb volatile liquids. In contrast to the membrane filter, a single-
stage, coalescing filter can have problems, because during upset
conditions, these single stage filters become saturated with volatile
liquids and these liquids can only be evaporated slowly over time.
2. The second filtration stage is another membrane filter. This filter has
smaller pores than the first stage. In this stage, small quantities of low
surface tension liquids, such as hydrocarbons, that are not extracted
by the first filter are removed. Most of the pressure drop through the
entire Filterblock assembly occurs across the second filter stage.
3. The third and final filtration stage is a small coalescing filter. This filter
will remove trace quantities of liquid aerosols as small as 0.1 microns.
Should the membranes in the first two stages become ruptured, this
stage will temporarily act as the main particulate and liquid filter.
• Total flow from the drain flow restrictors will increase by about 50
SCCM (0.05 l/min or 0.1 SCHF) for each 30 PSI (210 KPA) increase in
the inlet pressure. Typical values for this combined drain flow are:
- 0.165 l/min (0.35 SCHF) at 100 PSIG (690 KPAG) inlet pressure.
- 0.825 l/min (1.75 SCHF) at 500 PSIG (3450 KPAG) inlet pressure.
When depressurizing the system for any reason, always bleed off the
! pressure on the downstream side of the filter. If the pressure is dropped
CAUTION on the inlet side first, damage to the membrane filter elements may
result. Should the outlet pressure be higher than the inlet pressure by
as little as 210 KPA (30 PSI or 2 BAR), the membranes will rupture.
When one or both membranes have ruptured, replace them as soon as
possible.
Options | B-3
Natural Gas Filter Maintenance
The parts that are removed and replaced in these procedures correspond
with Item #s in Figure B-1.
4. Visually inspect both membrane filters (Items 12 & 14) for damage,
particulate, and liquid films before removing the filters. Remove the
two small o-rings (Item 5) from the flat faces of the housings.
6. Remove the M6 nut (Item 23), washer (Item 22), o-ring (Item 21), and
then the coalescing filter element (Item 20).
8. Clean all the metal parts in the assembly by immersing them in a clean
solvent. The solvent should not attack aluminum or stainless steel.
Remove the parts from the solvent and allow them to fully dry before
replacing. Isopropanol or acetone are both acceptable solvents for this
purpose.
Figure B-1.
Filterblock Assembly.
Options | B-5
9. If the previous sample gas flow rates through the sampling system
suggest possible plugging of the internal flow restrictors (Item 3), the
restrictors should be replaced with new ones. If there was an excessive
amount of liquid in the first membrane filter stage, then the first drain
flow restrictor should be replaced.
10. Carefully install new o-rings (Item 4) on the internal flow restrictors.
Roll the o-rings over the threads making sure not to crack or scratch
the o-rings. In the bottom hole of each housing section, install a new
flow restrictor. Hand-tighten the restrictor using a 2.5 mm ball driver
or hex wrench.
The parts that are removed and replaced in these procedures correspond
with Item #s in Figure B-1.
1. Reinstall the flow restrictor fittings (Item 3) into the bottom of each
housing section. Use Teflon tape on the NPT threads.
2. Install two new small o-rings (Item 5) on the flat faces of the housing
sections.
3. Install a new o-ring (Item 19) in the Filterblock Core (Item 16). Do not
use any lubricants on the o-rings.
4. Install a new coalescing filter cartridge (Item 20). Secure the filter
cartridge with the washer (Item 22) and M6 nut (Item 23). Use a new
o-ring (Item 21), in the washer. Lightly tighten the M6 nut. Place the
coalescing filter assembly into its housing. You might have to rotate
the filter assembly as you push it into the housing (Item 24). Tighten
the M6 X 20 mm screws (Item 17) with a 5 mm ball driver or an hex
wrench until the Filterblock Core sits on the housing.
5. Place the Back Filterblock (Item 24) on a flat surface with the mem-
brane side facing up. Install one sintered stainless steel disk (Item 15)
into its recess.
8. If the membrane and o-ring are separate, then carefully centre the
membrane over the sintered disk. Use one finger to hold the mem-
brane in place. Place the o-ring over the membrane. Carefully push
the o-ring halfway into its groove in one location. Likewise, press the
rest of the o-ring to half its depth, beginning with the section across
from the first location. The membrane should now be tightly
stretched.
9. Place the Center Filterblock (Item 13) on a flat surface with the mem-
brane side facing up. Install the sintered disk (Item 15). Retrieve a new
high-flow membrane (membrane color white) and o-ring (Item 12)
from the clear plastic bag. Since the o-ring is usually bonded to the
High-Flow membrane, review Step 7 for instructions on installing it.
10. In all the housing sections, ensure that the o-rings are still in place.
Stack the three housings together by aligning the screw holes. Install
the M6 X 50 mm screws (Item 11). Tighten the screws in a cross-
pattern.
11. Install the Filterblock Assembly on the mounting screws. Attach and
tighten all tubing connections.
12. Open the valve at the inlet of the sampling system. With a suitable
leak detection liquid, leak check the Filterblock Assembly and fittings.
Options | B-7
Filterblock Assembly Spare Parts
The recommended spare parts list for the Filterblock Assembly are listed
below.
• Use a 1/8” NPT female thread connector on the inlet flame arrestors.
• Use stainless steel fittings and tubing to connect clean and dry air or
nitrogen to both inlet flame arrestors at a pressure of between 1 and 10
PSIG (6.9 and 69 KPAG).
• The purge gas should have a water dew point temperature of less
than -30 °C and be contaminant free.
Options | B-9
UPPER ENCLOSURE
Figure B-2.
Inlet and vent flame
arrestor locations for
Environmental Purge
Option. LOWER ENCLOSURE
Before proceeding, test the area around the analyzer for hazardous
! gases and proceed only when the area is found to be safe.
WARNING
3. From the M933 Properties dialog box, click the Setup tab and then
click Compensations to view the Compensations dialog box (Figure
B-3).
Figure B-3.
Compensations tab
using the Pressure
Compensation option.
Options | B-11
4. Click Measured under Cell Pressure and then enter the LowScale and
HighScale values to activate the measurement (refer to Chapter 4 for
more information).
Jumpers on the Customer I/O Board are set up for a default pressure
measurement range of 3413.19–5171.49 mm Hg absolute (66–100
NOTE
PSIA).
Diagnostics Feature
• The user must supply an external power supply (15–30 VDC) capable
of supplying 25 mA per loop.
Options | B-13
Low Range (White Cell) Measuring Cell (Field Upgradeable)
The standard analyzer is equipped with a 2-pass measuring cell with a
total path length of 40 cm. The Low Range (White) Cell and path length
combination is suitable for hydrogen sulfide minimum full-scale concen-
tration ranges of 0–25 PPM. As an option, the 40 cm cell can be replaced
with a 4-pass Measuring Cell with 81.2 cm path length. This longer, Low
Range measuring cell is suitable for hydrogen sulfide minimum full-scale
concentration ranges as low as 0–5 PPM.
• Extra gas runs are performed at the factory to minimize the interfer-
ence of hydrogen sulfide and methyl mercaptan on the carbonyl
sulfide reading. These additional calibration tests ensure that the
carbonyl sulfide output meets the accuracy specifications as stated in
Chapter 2. These accuracy specifications also depend on whether the
analyzer is equipped with a Standard or Low Range (White Cell)
Measuring Cell.
• The wiring connections for the extra current output are shown in the
Customer Connections Wiring Schematic in Chapter 3.
Options | B-15
Calibrated Methyl Mercaptan Output (Factory Upgradeable Only)
The standard analyzer comes with one self-powered current (V/I) output
configured for hydrogen sulfide concentration. The standard analyzer
measures carbonyl sulfide (COS) and methyl mercaptan (MeSH) concen-
trations and compensates the hydrogen sulfide (H2S) reading for their
presence. The hydrogen sulfide output from the analyzer is tested and
calibrated at the factory so that the interference of the other two species is
minimized.
• Extra gas runs are performed at the factory to minimize the interfer-
ence of hydrogen sulfide and carbonyl sulfide on the methyl mercap-
tan reading. These additional calibration tests ensure that the methyl
mercaptan output meets the accuracy specifications as stated in
Chapter 2. These accuracy specifications also depend on whether the
analyzer is equipped with a Standard or Low Range (White Cell)
Measuring Cell.
• The wiring connections for the extra current output are shown in the
Customer Connections Wiring Schematic in Chapter 3.
Overview
This Appendix (Model 933 Analyzer Customer Modbus Communication
Interface, Revision 1.3, November 17, 2003) describes the customer serial
communication interface on the Model 933 Analyzer. The communication
protocol implemented is Modicon Modbus as defined in “Modicon Modbus
Protocol Reference Guide” (PI-MBUS-300 Rev. C). The Modbus protocol
transmission mode implemented is Remote Terminal Unit (RTU) with the
analyzer operating as a slave device.
Modbus Address
The analyzer needs to be assigned a Modbus slave address, which can be
a number from 0–247 with ‘0’ disabling the analyzer Modbus interface
altogether.
Communication Parameters
While the number of data bits is always 8, the baud rate, number of stop
bits and parity of the analyzer Modbus serial communication port are
selectable. The default communication parameter settings are 9600 baud,
1 stop bit and no parity.
• As for the loop-back test function, only one diagnostic code, Return
Query Data (00), is supported by the Model 933 Analyzer for verifica-
tion of correct communication connection. Illegal function exception
code is returned for unsupported loop-back test diagnostic codes.
0 Reserved —
1 Auto-Zero r,w
2–7 Reserved —
8 Manual Zero r,w
9 Manual Span r,w
10–22 Reserved —
23 Concentration Alarm Soft Enable (0 = disable; 1 = enable) r,w
24 Fault Relay (0 = fault; 1 = normal) r
25 Warning Relay (0 = warning; 1 = normal) r
26 Concentration Alarm Invalid Relay (0 = invalid; 1 = valid) r
27 Concentration Alarm1 (0 = off; 1 = on) r
If the Modbus master initiates the same action before that action is
completed, the message is acknowledged but the action does not
restart. Since only one calibration action can be active at any given
time, if function code 15 is used to request more than one action, the
lowest action bit in the request takes precedence.
Holding Registers
RAM space on the Model 933 Analyzer is limited and not every
customer’s data acquisition system supports Modbus floating point value
transfer. These floating point values, accessed on a Model 933 Analyzer,
are scaled up and converted into integer values to load into Modbus
registers for transmission. The register values must be scaled back at the
receiving end to yield the actual values. The size of a Modbus holding
register is 16-bit. It can assume a value from -32768 to +32767 in two’s
complement. The holding register definitions, units of measurement and
scaling factors are listed in the following pages.
The references to ‘*’, ‘**’, ‘***’, and ‘#’ in the Holding Register Defini-
tions are:
The unit of measurement for concentration result is PPMV when the Unit Conversion
Factor is the default value of 1.0. However, the concentration result unit can be
changed, for example to mg/Nm3 or lb/mmscf, using a different Unit Conversion
Factor. See “Custom Output” in Chapter 4.
7–9 Reserved – – –
10–19 Track & Hold Results of Registers 0 to 9 Reg0 to Reg9 Reg0 to Reg9 Reg0 to Reg9
Holding registers #0 to #29 are the primary registers the Modbus master
should monitor regularly. Their values are updated once a second.
• Registers #0 to #19 are concentration results calculated by the ana-
lyzer.
• Registers #20 to #25 are analog inputs measured by the analyzer.
• Registers #26 to #29 are analyzer status codes.
Holding registers #134 to #153 are used for customizing analyzer concen-
tration result outputs. They are normally set up at the factory and do not
require modification by the customer. They are accessed as floating point
values and are included here for completeness.
Registers #154 to #159 are used for programming the scaling factors of
analyzer concentration result-related values.
5–15 Reserved
5 Lamp Failure
6–15 Reserved
0 EEPROM Full
6–15 Reserved
5–15 Reserved
Drawings | D-1
Backpan Dimensions
PROCESS INSTRUMENTS
CAUTION:
RIS K OF ELECTRIC SHOCK
ATTENTION:
CONSULT USER MANUAL
0344
II 2 G
PROCESS INSTRUMENTS
Caution
Do not open when an explosive gas atmosphere is present.
LOOSE CLAMPED
Drawings | D-3
Lower Enclosure
PROCESS INSTRUMENTS
Drawings | D-5
Backpan Component Layout (Europe)
PROCESS INSTRUMENTS
CAUTION:
RISK OF ELECTRIC SHOCK
ATTENTION:
CONSULT USER MANUAL
0344
PROCESS INSTRUMENTS II 2 G
Caution
Do not open when an explosive gas atmosphere is present.
1. Internal Tooth 3 mm SS Washer (300-0642) – 4 places 15. Column Block Mounting Tube (300-9123)
2. Ground Terminal (300-0511) 16. Mounting Tube Locknut (300-9135) – 2 places
3. Ground Wire (300-8306) 17. M6 x 20 Socket HD SS Hex Screw (300-4492) – 10 places
4. Filter Spool (300-9149) 18. M3 x 6 Button HD SS Hex Screw (300-4865) – 6 places
5. O-Ring, Aflas, #113 (300-9147) 19. Warning Label (300-9169)
6. Coalescing Filter Element (300-6217) 20. Column Block Flange (300-9159)
7. O-Ring, Viton, #010 (300-2375) 21. 1/8" O-Ring Seal Fitting (300-9139) – 3 places
8. M6 Nut (300-0263) 22. Cartridge Heater 120 VAC (300-9038)
9. O-Ring, Viton, #121 (300-8719) 240 VAC (300-9039)
10. Column Assembly 23. Flow Restrictor (100-1794) – 2 places
2-Turn Column Assembly (100-1789) 24. O-Ring, Aflas, #008 (300-6241) – 2 places
4-Turn Column Assembly (100-1857) 25. Column Block (300-9156)
11. Seal Washer (300-6151) 26. Check Valve (100-1788) – 2 places
12. RTD (300-4924) 27. Column Block Valve Cover (300-9160)
13. Overtemp Switch (300-9062) 28. M6 x 12 Socket HD SS Hex Screw (300-4496) – 3 places
14. Overtemp Switch Mounting Hardware 29. O-Ring, HSN, #125 (300-9060)
Drawings | D-7
AC Distribution PWB (P/N 100-1771)
Drawings | D-9
Host Controller Board (P/N 100-1757)
Drawings | D-11
Micro-Interface Board (P/N 100-1759)
Drawings | D-13
Customer Connections Wiring Schematic (North America)
Drawings | D-15
Conduit Entries and AC Power Connection Locations (North
America)
LOWER ENCLOSURE
DETAIL A
LOWER ENCLOSURE
DETAIL A
Drawings | D-17
RS-232 Cable Communications Connections
Drawings | D-19
Natural Gas Filterblock Assembly – Optional (P/N 100-1782)
Drawings | D-21
Solenoid Block (Europe)
Drawings | D-23
Low Range (White) Measuring Cell (100-1780)
UPPER ENCLOSURE
LOWER ENCLOSURE
Drawings | D-25
PMT Buffer Board P/N 100-0140
Drawings | D-27
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Conversion Factors
PARAMETER TO CONVERT FROM: TO: MULTIPLY BY:
AMOUNT of SUBSTANCE lb mol kmol 0.453 592 4
g mol kmol 0.001
(for Ideal gas) m of gas (0 °C, 101.325 kPa)
3
kmol 0.044 615 8
m3 of gas (15 °C, 101.325 kPa) kmol 0.042 493 2
ft3 of gas (60 °F, 1.0 atm) kmol 0.001 195 30
LENGTH ft m 0.304 8
in mm 25.4
yd m 0.914 40