Manufacturer:

~
Page 1/7
ArcelorMittal Tubular Products Roman S.A. MILL TEST CERTIFICATE B 19621/1
STEFAN CEL MARE STR, BL 15, SC. A, PARTER I according to EN 10204/3.1/2004
ROMAN, NEAMT ROMANIA - 19.05.2020 ArcelorMittal
Buyer: P.VAN LEEUWEN JR'S BUIZENHANDEL BV Total weight: Total Length: Pieces Bundles
SEAMLESS STEEL LINE PIPES 5.681 tons 77.13 meters
Lindtsedijk 100, PO BOX 1 NL 3330 AA, 7 -
Zwijndrecht, Netherlands - lbs - feets
Standard: API 5L ed. 46-2018-PSL2; ASTM A 333/A 333M-2018; ASME SA 333/SA 333M-2017; EN 10216-3-2014; ASTM A 106/A I06M-2019; ASME
SA 106/SA l06M-2017; ASME B16.25-2017; Specif.no.15206E-Rev 009.1/10.03.2017 with deviations as per T.O. AMR offer 29/31.03.2017;
ASME Sect.II, Part. D Table Y-1; NACE MR0175/ISO 15156-1&2-2015; ANSI/NACE MR 0103/ISO 17945-2015
Buyer's
reference
PO NO. : 3519975/08.04.2020
Contract 50004602
Dimensions: 323.90 x 9.50 mm
-
I
Schedule: - Length: 10.00 - 11.80 m
-
-
-
Item I Item Client Hydro Test: I Bar I PSI I MPa I Time(sec) Steel Grade: X52N/6/C/P355NL2TC 1 - PSL2
1 I 177402 I 180 I - I 18.0 I 5 -
Chemical Analysis(%)
C Mn Si s p Cr Ni Cu Al Mo V Nb Ti B N
Bulletin Product !Max 0.18 1.06 0.45 0.005 0.025 0.30 0.30 0.30 - 0.08 0.080 0.020 0.040 0.0010 0.0200
Heat
No. Req. !Min - 0.90 0.10 - - - - - 0.020 - - - - - -
458070 Heat analysis 0.13 1.25 0.22 0.004 0.012 0.14 0.11 0.12 0.026 0.03 0.070 0.002 0.002 0.0001 0.0090
66640 Heat analysis 0.15 1.22 0.22 0.003 0.010 0.09 0.11 0.18 0.035 0.02 0.062 0.001 0.001 0.0003 0.0056
66641 Heat analysis 0.14 1.30 0.19 0.004 0.013 0.09 0.11 0.17 0.031 0.02 0.062 0.001 0.001 0.0002 0.0061
458070 20-301 Product analysis 0.13 1.25 0.21 0.002 0.009 0.14 0.09 0.16 0.021 0.03 0.066 0.002 0.002 0.0000 0.0096
458070 20-301 Product analysis 0.13 1.24 0.21 0.003 0.009 0.14 0.09 0.15 0.021 0.03 0.066 0.002 0.002 0.0000 0.0094
66640 20-351 Product analysis 0.15 1.23 0.21 0.003 0.009 0.09 0.10 0.17 0.033 0.02 0.063 0.002 0.001 0.0002 0.0066
66640 20-351 Product analysis 0.15 1.22 0.21 0.003 0.009 0.08 0.10 0.17 0.034 0.02 0.063 0.002 0.001 0.0002 0.0063
66641 20-301 Product analysis 0.13 1.21 0.20 0.003 0.010 0.15 0.09 0.15 0.021 O.oJ 0.064 0.002 0.002 0.0001 0.0065
66641 20-301 Product analysis 0.13 1.23 0.20 0.002 0.009 0.15 0.09 0.15 0.021 O.oJ 0.064 0.002 0.002 0.0000 0.0065

®
We state on our sole responsibility that the delivered products are in conformity with the order Quality Control Representative
requirements.

Formular 12A, rev.9

Manufacturer:
-
~
Page 2/7
ArcelorMittal Tubular Products Roman S.A. MILL TEST CERTIFICATE B 19621/1
STEFAN CEL MARE STR, BL 15, SC. A, PARTER I according to EN 10204/3.1/2004
ROMAN, NEAMT ROMANIA - 19.05.2020 ArcelorMittal
Buyer: P.VAN LEEUWEN JR'S BUIZENHANDEL BV Total weight Total Length: Pieces Bundles
SEAMLESS STEEL LINE PIPES 5.681 tons 77.13 meters
Lindtsedijk I 00, PO BOX I NL 3330 AA, 7 -
Zwijndrecht, Netherlands - lbs - feets
Standard: API 5L ed. 46-2018-PSL2; ASTM A 333/A 333M-2018; ASME SA 333/SA 333M-2017; EN 10216-3-2014; ASTM A 106/A 106M-2019; ASME
SA 106/SA 106M-2017; ASME 816.25-2017; Specif.no.15206E-Rev 009.1/10.03.2017 with deviations as per T.O. AMR offer 29/31.03.2017;
Buyer's
reference
PO NO.: 3519975/08.04.2020
Contract 50004602
Dimensions: 323.90 x 9.50 mm
-
I
ASME Sect.II, Part. D Table Y-1; NACE MR 0175/ISO 15156-1&2-2015; ANSI/NACE MR 0103/ISO 17945-2015
Schedule: - Length: 10.00 - 11.80 m
-
-
-
Item I Item Client Hydro Test: I Bar I PSI I MPa I Time(sec) Steel Grade: X52N/6/C/P355NL2TC 1 - PSL2
1 I 177402 I 180 I - I 18.0 I 5 -
Chemical Analysis(%)
Nb+Ti+V Cr+Mo+ Ni +Cu+ V CE IIW

Heat
Bulletin Product IMax 0.120 1.000 0.42
No. Reg. !Min - - -
458070 Heat analysis 0.074 0.470 0.40
66640 Heat analysis 0.064 0.462 0.41
66641 Heat analysis 0.064 0.452 0.41
458070 20-301 Product analysis 0.070 0.486 0.40
458070 20-301 Product analysis 0.070 0.476 0.40
66640 20-351 Product analysis 0.066 0.443 0.41
66640 20-351 Product analysis 0.066 0.433 0.40
66641 20-301 Product analysis 0.068 0.484 0.40
66641 20-301 Product analysis 0.068 0.484 0.40
CEpcm = C+Si/30+Mn/20+Cu/20+Ni/60+cr/20+Mo/l 5+V/10+5B CE_S = C+Mn/6 CE11w = C+Mn/6+(Cr+Mo+V)/5+(Ni+Cu)/I 5

We state on our sole responsibility that the delivered products are in conformity with the order Quality Control Representative
requirements.

Formular 12A, rev.9

Manufacturer:
~
Page 3/7
ArcelorMittal Tubular Products Roman S.A. MILL TEST CERTIFICATE B 19621/1
STEPAN CEL MARE STR, BL 15, SC. A, PARTER I according to EN 10204/3.1/2004
ROMAN, NEAMT ROMANIA - 19.05.2020 ArcelorMittal
Buyer: P.VAN LEEUWEN JR'S BUIZENHANDEL BY Total weight: Total Length: Pieces Bundles
SEAMLESS STEEL LINE PIPES 5.681 tons 77 .13 meters
Lindtsedijk 100, PO BOX 1 NL 3330 AA, 7 -
Zwijndrecht, Netherlands - lbs - feets
Standard: API 5L ed. 46-2018-PSL2; ASTM A 333/A 333M-2018; ASME SA 333/SA 333M-2017; EN 10216-3-2014; ASTM A 106/A l06M-2019; ASME
SA 106/SA l06M-2017; ASME Bl 6.25-2017; Specif.no.15206E-Rev 009.1/10.03.2017 with deviations as per T.O. AMR offer 29/31.03.2017;
Buyer's ASME Sect.II, Part. D Table Y-1; NACE MR 0175/ISO 15156-1&2-2015; ANSI/ NACE MR 0103/ISO 17945-2015
PO NO. : 3519975/08.04.2020 Length:
reference Dimensions: 323.90 x 9.50 mm !Schedule: - 10.00 - 11.80 m -
Contract 50004602 - - -
Item I Item Client Hydro Test: I Bar I PSI I MPa I Time(sec) Steel Grade: X52N/6/C/P355NL2TC1 - PSL2
1 I 177402 I 180 I - I 18.0 I 5 -
Tensile Test
Length Width/Diameter Thickness Section Mechanical test YS YS UTS UTS E YS/UTS
Heat Orientation
mm inch mm inch mm inch mm2 inch2 Bulletin No. MPa (PSI:1000) MPa (PSI:1000) % max:-
458070 Longitudinal Flat 50.8 - 40.00 - 10.30 - 412.0 - 20-1491 426.00 - 525.00 - 39.40 0.81
458070 Longitudinal Flat 50.8 - 40.00 - 10.10 - 404.0 - 20-1491 422.00 - 530.00 - 40.10 0.80
458070 Longitudinal Flat - - 20.00 - 10.00 - 200.0 - 20-907 425.00 - 520.00 - 33.90 0.82
458070 Longitudinal Flat 50.8 - 40.00 - 10.20 - 408.0 - 20-1049 428.00 - 573.00 - 40.80 0.75
458070 Longitudinal Flat 50.8 - 40.00 - 10.10 - 404.0 - 20-1049 414.00 - 557.00 - 42.20 0.74
458070 Longitudinal Flat - - 20.00 - 9.80 - 196.0 - 20-610 423.50 - 540.80 - 34.40 0.78
66640 Longitudinal Flat 50.8 - 40.00 - 9.90 - 396.0 - 20-1491 418.00 - 532.00 - 39.60 0.79
66640 Longitudinal Flat - - 20.00 - 10.50 - 210.0 - 20-907 423.80 - 519.00 - 34.30 0.82
66641 Longitudinal Flat 50.8 - 40.00 - 10.50 - 420.0 - 20-1491 432.00 - 529.00 - 40.60 0.82
66641 Longitudinal Flat 50.8 - 40.00 - 10.30 - 412.0 - 20-1491 430.00 - 536.00 - 41.30 0.80
66641 Longitudinal Flat - - 20.00 - 10.20 - 204.0 - 20-907 426.50 - 514.70 - 33.80 0.83

We state on our sole responsibility that the delivered products are in conformity with the order Quality Control Representative
requirements.

Formular 12A, rev.9

Manufacturer:
~
Page 4/7
ArcelorMittal Tubular Products Roman S.A. MILL TEST CERTIFICATE B 19621/1
STEFAN CEL MARE STR, BL 15, SC. A, PARTER I according to EN 10204/3.1/2004
ROMAN, NEAMT ROMANIA - 19.05.2020 ArcelorMittal
Buyer: P .VAN LEEUWEN JR'S BUIZENHANDEL BV Total weight: Total Length: Pieces Bundles
SEAMLESS STEEL LINE PIPES 5.681 tons 77 .13 meters
Lindtsedijk 100, PO BOX I NL 3330 AA,
- lbs - feets
7 -
Zwijndrecht, Netherlands
Standard: API SL ed. 46-2018-PSL2; ASTM A 333/A 333M-2018; ASME SA 333/SA 333M-2017; EN 10216-3-2014; ASTM A 106/A 106M-2019; ASME
SA 106/SA l06M-2017; ASME Bl 6.25-2017; Specif.no.15206E-Rev 009.1/10.03.2017 with deviations as per T.O. AMR offer 29/31.03.2017;
Buyer's ASME Sect.II, Part. D Table Y-1; NACE MR0175/ISO 15156-1&2-2015; ANSI/NACE MR 0103/ISO 17945-2015
reference
PO NO.: 3519975/08.04.2020
Dimensions: 323.90 x 9.50 mm I
Schedule: - Length: 10.00 - 11.80 m -
Contract 50004602 - - -
Item I Item Client Hydro Test: I Bar I PSI I MPa I Time(sec) Steel Grade: X52N/6/C/P355NL2TC1 - PSL2
1 I 177402 I 180 I - I 18.0 I 5 -
Impact Test
Impact Test Temp. Reg.KV Req.Avr. A vr. fracture Shear Area
Heat Orientation Size (mm) KV values (J) KCU min:-J/cm 2 T:°C Lateral Expansion min. mm
Bulletin No. (oC) (min. J) (min. J) energy (J) min.%

458070 20-1901 Transversal 10x7.5x55 -50 14.0 133 141 119 20.0 131 - - - 95 95 90 1.16 1.24 1.04
458070 20-1902 Longitudinal 10x7.5x55 -50 21.0 154 166 137 30.0 152 - - - 95 95 95 1.35 1.45 1.20
458070 20-1713 Longitudinal 10x7.5x55 -50 21.0 129 93 133 30.0 118 - - - 90 85 90 1.22 0.75 1.10
458070 20-1714 Transversal 10x7.5x55 -50 14.0 106 88 115 20.0 103 - - - 90 85 90 0.88 0.70 0.93
66640 20-1901 Transversal 10x7.5x55 -50 14.0 123 109 136 20.0 123 - - - 90 90 95 1.08 0.95 1.19
66640 20-1902 Longitudinal 10x7.5x55 -50 21.0 145 159 171 30.0 158 - - - 95 95 95 1.29 1.41 1.51
66641 20-1901 Transversal 10x7.5x55 -50 14.0 127 143 120 20.0 130 - - - 90 95 90 1.11 1.25 1.04
66641 20-1902 Longitudinal 10x7.5x55 -50 21.0 165 139 153 30.0 152 - - - 95 95 95 1.46 1.24 1.36

Hardness Test
Hardness Test HV IO max.- HRCmax.22
Heat HBmax.- HV 10 max.-
Bulletin No. OD Midwall ID End A EndB
458070 20-1174 - - - - - - - <20
458070 20-844 - - - - - - - <20
66640 20-1174 - - - - - - - <20
66641 20-1174 - - - - - - - <20

We state on our sole responsibility that the delivered products are in conformity with the order Quality Control Representative
requirements.

Formular 12A, rev.9

Manufacturer:
~
Page 5/7
ArcelorMittal Tubular Products Roman S.A. MILL TEST CERTIFICATE B 19621/1
STEFAN CEL MARE STR, BL 15, SC. A, PARTER I according to EN 10204/3.1/2004
ROMAN, NEAMT ROMANIA - 19.05.2020 ArcelorMittal
Buyer: P.VANLEEUWEN JR'S BUIZENHANDELBV Total weight: Total Length: Pieces Bundles
SEAMLESS STEEL LINE PIPES 5.681 tons 77.13 meters
Lindtsedijk 100, PO BOX 1 NL 3330 AA, 7 -
Zwijndrecht, Netherlands - lbs - feets
Standard: API 5L ed. 46-2018-PSL2; ASTM A 333/A 333M-2018; ASME SA 333/SA 333M-2017; EN 10216-3-2014; ASTM A 106/A 106M-2019; ASME
SA 106/SA 106M-2017; ASME B16.25-2017; Specif.no.15206E-Rev 009.1/10.03.2017 with deviations as per T.O. AMR offer 29/31.03.2017;
ASME Sect.II, Part. D Table Y-1; NACE MR0175/ISO 15156-1&2-2015; ANSI/NACE MR 0103/ISO 17945-2015
Buyer's
reference
PO NO. : 3519975/08.04.2020
Contract 50004602
Dimensions: 323.90 x 9.50 mm
-
I
Schedule: - Length: 10.00 - 11.80 m
-
-
-
Item I Item Client Hydro Test: I Bar I PSI I MPa I Time(sec) Steel Grade: X52N/6/C/P355NL2TCI - PSL2
1 I 177402 I 180 I - I 18.0 I 5 -
Yield Strength Test
Yield Strength T 0C YS
Heat YS (MPa)
Bulletin No. (PSI):1000
458070 20-440 300 326.90 -
458070 20-427 300 298.00 -
66640 20-427 300 310.10 -
66641 20-427 300 317.90 -
Technological/Microstructure Test
Flattening Test Flattening Microstructure Inclusion level Size grain
Heat Heat
Bulletin No. Test Bulletin No. max. "z" ferritic min. "z"
458070 20-1305 OK 458070 20-280 0 10

458070 20-1305 OK 458070 20-307 0 10

458070 20-977 OK 66640 20-206 0 10

458070 20-977 OK 66641 20-206 0 9

66640 20-1305 OK

66641 20-1305 OK

66641 20-1305 OK

We state on our sole responsibility that the delivered products are in conformity with the order Quality Control Representative
requirements.

Formular 12A, rev.9

Manufacturer:
~
Page 6/7
ArcelorMittal Tubular Products Roman S.A. MILL TEST CERTIFICATE B 19621/1
STEFAN CEL MARE STR, BL 15, SC. A, PARTER I according to EN 10204/3.1/2004
ROMAN, NEAMT ROMANIA - 19.05.2020 ArcelorMittal
Buyer: P.VAN LEEUWEN JR'S BUIZENHANDEL BV Total weight: Total Length: Pieces Bundles
SEAMLESS STEEL LINE PIPES 5.681 tons 77.13 meters
Lindtsedijk I 00, PO BOX 1 NL 3330 AA,
- lbs - feets
7 -
Zwijndrecht, Netherlands
Standard: API 5L ed. 46-2018-PSL2; ASTM A 333/A 333M-2018; ASME SA 333/SA 333M-2017; EN 10216-3-2014; ASTM A 106/A 106M-2019; ASME
SA 106/SA I06M-2017; ASME Bl6.25-2017; Specif.no.15206E-Rev 009.1/10.03 .2017 with deviations as per T.O. AMR offer 29/31.03.2017;
Buyer's ASME Sect.II, Part. D Table Y-1; NACE MR 0175/ISO 15156-1&2-2015; ANSI/NACE MR 0103/ISO 17945-2015
reference
PO NO.: 3519975/08.04.2020
Contract 50004602
Dimensions: 323.90 x 9.50 mm I
Schedule: - Length: 10.00 - 11.80 m -
- - -
Item I Item Client Hydro Test: I Bar I PSI I MPa I Time(sec) Steel Grade: X52N/6/C/P355NL2TC1 - PSL2
l I 177402 I 180 I - I 18.0 I 5 -

Heat
Heat Pieces Length (m) Weight (kg)
458070 4 - -
66640 1 - -
66641 2 - -

We state on our sole responsibility that the delivered products are in conformity with the order Quality Control Representative
requirements.

Formular 12A, rev.9

Manufacturer:
~
Page 7/7
ArcelorMittal Tubular Products Roman S.A. MILL TEST CERTIFICATE B 19621/1
STEFAN CEL MARE STR, BL 15, SC. A, PARTER I according to EN 10204/3.1/2004
ROMAN, NEAMT ROMANIA - 19.05.2020 ArcelorMittal
Buyer: P. VAN LEEUWEN JR'S BUIZENHANDEL BV Total weight: Total Length: Pieces Bundles
SEAMLESS STEEL LINE PIPES 5.681 tons 77.13 meters
Lindtsedijk 100, PO BOX I NL 3330 AA, 7 -
Zwijndrecht, Netherlands - lbs - feets
Standard: API SL ed. 46-2018-PSL2; ASTM A 333/A 333M-2018; ASME SA 333/SA 333M-2017; EN 10216-3-2014; ASTM A 106/A 106M-2019; ASME
SA 106/SA I06M-2017; ASME B 16.25-2017; Specif.no.15206E-Rev 009.1/10.03.2017 with deviations as per T.O. AMR offer 29/31.03.2017;
ASME Sect.II, Part. D Table Y-1; NACE MR 0175/ISO 15156-1&2-2015; ANSI/NACE MR 0103/ISO 17945-2015
Buyer's
reference
PO NO. : 35 l 9975/08.04.2020
Contract 50004602
Dimensions: 323.90 x 9.50 mm
-
I
Schedule: - Length: 10.00 - 11.80 m
-
-
-
Item I Item Client Hydro Test: I Bar I PSI I MPa I Time(sec) Steel Grade: X52N/6/C/P355NL2TC l - PSL2
1 I 177402 I I180 - I I 518.0 -
Remarks PIPES IN COMPLIANCE WITH PED: 2014-68-EU/15.05.2014, ANNEX 1, SECTION 4.3.
Manufacturing process - hot rolling.
Hot finished, steel is fully killed, fine grained practice and produced by electric furnace, source 0300007; GOOOI08.
Heat treatment: normalizing at temperature 890-940°C, time soaking 11 min.
Visual inspection and dimensional check without objection.
Electromagnetic testing: Le+Li (12.5 % from W.T.)- satisfactory.
Wet magnetical particles testing on the pipe ends - satisfactory.
Magnetism residual max.30 Gauss.
Hydrostatic test hold for 5 sec. no leakage noticed.
For each reduction of0.01 % below the specified carbon maximum,on increase of0.05% manganese above the specified maximum will be pemitted up
to a maximum of 1.35 %.
Marking by die stamping with round nose tool :Heat no .. ; ARCELORMITTAL TUBULAR PRODUCTS ROMAN;A/SA 333 Gr.6 LT-50;A/SA
I06C/API 5L X52N PSL2 ;EN 10216-3 P355NL2 TCl ;SMLS-323,90-9,50-180bar- month/year.
Marking by painting : Heat no .. ; ARCELORMITTAL TUBULAR PRODUCTS ROMAN -API Spec.SL-0231-<APl>month/year-ASTM A
333/A333M/ASME SA333/SA333M/ASTM Al06/AI06M/ASME SA 106/SAI06M/EN I0216-3-323,90-9,50-L360N/X52N/grade 6/C/P355NL2
TCl-PSL 2-SMLS- Heat no ... ;serial no .. ;Length (m)- Weigth(kg)-180 bar/NDE-HF-LT-50C+PO 3519975+Article no.177402+"Van Leeuwen" +Made
in Romania+ blue ring and green ring at each end of pipe.
The products was manufactured, sampled, tested, marked and inspected in accordance with the Standards, the supplementary requirements, and any
other requirements designated in the purchase order, and has been found to meet such requirements.

We state on our sole responsibility that the delivered products are in conformity with the order Quality Control Representative
requirements. Digitally signed by Deina
Deina Nistor
Date: 2020.06.29 12:26:59
+03:00
Formular 12A, rev.9 Nistor Reason: Aprobat,
Location: Roman