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This certificate verifies that part number K23050, Salt in Crude Analyzer, was
manufactured in conformance with the applicable standards set forth in this
certification.
This unit is tested before it leaves the factory, to ensure total functionality and
compliance to the above specifications and ASTM standards. Test and inspection
records are on file for verification.
Jesse Kelly
Application Engineer
Koehler Instrument Company
K23050 Salt in Crude Analyzer
Operation and Instruction Manual
Table of Contents
1 Introduction .................................................................................................................. 4
1.1 Koehler’s Commitment to Our Customers................................................................................................. 4
1.2 Recommended Resources and Publications ............................................................................................ 4
1.3 Instrument Specifications .......................................................................................................................... 4
1.4 Software Specifications ............................................................................................................................. 4
2 Safety Information and Warnings............................................................................... 5
3 Getting Started ............................................................................................................. 5
3.1 Packing List ............................................................................................................................................... 5
3.2 Unpacking .................................................................................................................................................. 5
3.3 Setup ......................................................................................................................................................... 5
3.4 Software Installation .................................................................................................................................. 6
3.5 Software Operation.................................................................................................................................... 6
4 Instrument Description ............................................................................................... 8
4.1 General Description ................................................................................................................................... 8
4.2 Microprocessor Control ............................................................................................................................. 8
4.3 Display ....................................................................................................................................................... 8
4.4 Keypad ...................................................................................................................................................... 8
4.5 Power Requirements ................................................................................................................................. 8
4.6 pH Input ..................................................................................................................................................... 8
5 Operation...................................................................................................................... 9
5.1 Measurements ........................................................................................................................................... 9
5.1.1 Conductance .................................................................................................................................. 9
5.1.2 Temperature .................................................................................................................................. 9
5.1.3 pH .................................................................................................................................................. 9
5.2 Operation and Control ............................................................................................................................... 9
5.2.1 ON/RESET Key ............................................................................................................................. 9
5.2.2 SELECT Key ............................................................................................................................... 10
5.2.3 Display Selected Parameters ...................................................................................................... 10
6 Calibration .................................................................................................................. 10
6.1 Calibrate Conductance ............................................................................................................................ 10
6.1.1 Zero Conductance ....................................................................................................................... 11
6.1.2 Span Conductance ...................................................................................................................... 11
6.2 Calibrate Temperature............................................................................................................................. 11
6.2.1 Zero Temperature ........................................................................................................................ 11
6.2.2 Span Temperature ....................................................................................................................... 12
6.3 Calibrate pH ............................................................................................................................................. 12
6.3.1 pH Zero ........................................................................................................................................ 12
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Operation and Instruction Manual
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Operation and Instruction Manual
19 Warranty ..................................................................................................................... 22
20 Returned Goods Policy ............................................................................................. 22
Notes .................................................................................................................................. 23
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Operation and Instruction Manual
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Operation and Instruction Manual
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Operation and Instruction Manual
NOTE: When first installed, the software is in 2. Main Screen. The Next Screen will be the Main
demo mode, it must be registered in order for Screen of the Salt-In-Crude Software. See
the software to work with the unit. Figure 3 below:
2. Registration. Start the program and then go
to >> Help >> Register. A registration screen
will appear with a registration number (Refer
to Figure 1, below). E-mail Koehler at
software@koehlerinstrument.com or call with
the registration number for the unlock code.
Once the software has been registered, it
must be restarted before tests are run.
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K23050 Salt in Crude Analyzer
Operation and Instruction Manual
The “Port Open” indicator light will turn red if the procedure. To use this function, the Salt in
command is successful. The Comm. port tab is Crude Unit must also be in “Upload” mode. The
illustrated in Figure 3 above. user must then click the “Get Calibration Table”
button and the Salt vs. Conductance Calibration
4. Timer Tab. This tab features a basic timing Table will be sent to the “Text Received” box.
function. This screen allows the user to choose
the duration of the timer in minutes, then by 9. Database. This function can be used to store
simply clicking on the “Start Timer” button the data. The Database screen is shown in Figure 6
timer will begin and be displayed as Time below. To access this screen click on the “View”
Elapsed. The Timer Tab also features a text box pull down tab. Then click “Database”. Click on
where the user can take additional notes. The the “Get Data” to display the Data from the
Timer Tab is illustrated in Figure 4 below. “Main” screen to the “Database” screen. Once
the desired Data is displayed here the user can
use a variety of commands available in the
“Database” screen.
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Operation and Instruction Manual
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Operation and Instruction Manual
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Operation and Instruction Manual
be utilized to escape from a calibration menu shown and the instrument will revert to the "Main
entered in error. Menu". The code number to be entered is the
device serial number. It is written inside the battery
5.2.2 SELECT Key compartment on the bottom of the unit. The
number is entered by pressing the "up" or "down"
When the K23050 instrument is first activated it arrow keys until the proper number is displayed.
will begin monitoring the various system channels The "ENTER" key is then pressed and the
and displaying the selected parameters. Pressing instrument will evaluate the entry.
the SELECT key brings up a Command list or
menu. An "X" at the end of a line indicates which This security feature may be selectively turned on
command is active. The selection "X" is moved or off through the "Access ON/OFF" menu.
from command to command by use of the arrow "Access ON/OFF" is listed in the main menu and
keys. Pressing the 'down' arrow moves the when selected the user will be prompted to enter
selection cursor down. Pressing the 'up' arrow the "access code number". This will always be the
moves the "X" up a line. When the cursor moves case in order to restrict unauthorized operators
to the bottom or top of the display the command from controlling access to the "Calibration Menu".
list will scroll in the appropriate direction revealing Once the proper code number is entered the user
the next command. When the last available is presented with:
command has been viewed the command list will
roll around to the starting command. Security Check
The available commands are: Use the arrow keys to position the "X" at the
desired setting and then press the "ENTER" key;
a. Main Screen the security setting will be stored in non-volatile
b. Calibration memory and the instrument will return to the main
c. Data Logging menu. The security feature will operate as
d. Display Parameters selected from here on.
e. Logging Parameters
f. Set Date/Time The 'Calibrate' function gives the user the ability to
g. Auto shutoff calibrate any of the measurement channels
h. Power Off (conductance, temperature, pH, pH milliVolts, daily
i. Upload Data blank, salt curve, internal battery, and external
j. Decimal Places battery). It is not recommended that the user
k. Access On/Off calibrate the internal or external battery channels.
If, this is done improperly it can cause improper
5.2.3 Display Selected Parameters operation of the power management module and
subsequent battery failure.
The 'Display Selected Parameters' function directs
the instrument to begin real time display of the When the 'Calibrate' function is selected from the
selected parameters. Activate this function by command menu a 'Calibration' submenu is
placing the cursor on this line with the arrow keys presented. Here a list of the available parameters
and pressing the 'ENTER' key. is shown. The user moves the highlighting cursor
(selection "X") to the desired parameter by means
6 Calibration of the arrow keys, pressing the 'ENTER.' key to
begin calibration of the designated parameter.
The K23050, Salt in Crude Analyzer is equipped
with a security feature designed to restrict access 6.1 Calibrate Conductance
to the Calibration Menu. If the security check is
turned on the user will be prompted to enter a Conductance calibration involves establishing the
code number before access is granted to the zero and span points of the system. This is
"Calibrate Menu". If the code number is improperly accomplished by using a dry sensor for "zero" and
entered the message "Access Denied" will be
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Operation and Instruction Manual
connecting a standard resistor for the conductance Use the arrow keys to adjust the displayed
span value. conductivity value to the desired 1.0000S. Once
this is done press the 'ENTER' key. The unit will
When conductance has been selected for measure the conductance, establish the new slope
calibration the K23050will display: and store the data in non-volatile memory. It will
then revert to the 'Conduct. Cal' menu. If the
Conduct. Cal calibration procedure has been completed, choose
Zero _X 'Exit' and press the 'ENTER' key. This will
Span____ command the K23050 instrument back to the main
Exit ____ function menu.
Make certain that 0 S is set as the calibration Temperature must be calibrated at two points
value and press the 'ENTER' key to establish the along its scale. One point will be a low value or
zero offset point and store the new data in 'Zero' point and the other an upscale value or
non-volatile memory. Once this has been done the 'Span' point. The 'Zero' point should be near 0.00
K23050 will revert to the 'Conduct. Cal' menu. °C and the 'Span' value is pre-set at 50°C. When
Here the 'Span' or 'Quit' function can be selected. establishing the zero and span points the
temperature sensor (the 1/4" stainless steel tube
next to the conductivity electrodes) must be placed
6.1.2 Span Conductance in a solution that is at the desired temperature. It
should be noted that only the lower end of the
temperature tube below the tip jacks can be
When conductivity span or slope is to be adjusted immersed in the liquid.
clip the conductance calibration jacks between the
two conductivity electrodes. Select "Span" on the
unit and press "ENTER". The unit will retrieve the
6.2.1 Zero Temperature
last conductivity span value that was used for
calibration. This will be shown on the system
display: When temperature is to be calibrated for zero
offset the unit will retrieve the last temperature
Cal Conductance 'zero' value used and display:
Adjust w/ Arrows
Then Press Enter Temp 0.000 C <-- Last cal. temp.
1.0000 S
Adjust w/ Arrows
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Operation and Instruction Manual
Use a laboratory thermometer to measure the Note: The K23050 uses a high impedance,
temperature of the span solution. With the arrow differential amplifier in the pH/ion circuit. In order
keys, adjust the displayed temperature to the to keep the sensor's signal in the common mode
desired point of calibration. Press the 'ENTER' key range of the amplifier the solution must be kept at
and the unit will establish the slope of the or near the potential of the instrument's circuit
temperature sensor, store the data in non-volatile common. This is accomplished by placing the
memory and revert to the 'Temperature Cal' menu pH/ion ground electrode in the solution. The
where the user may continue calibration or choose pH/ion electrode is connected to the readout unit
'Exit' to return to the main menu. via the ground connector on the bottom of the
module.
6.3 Calibrate pH
The pH/ion ground electrode must be in the
solution at all times when pH or ion readings are
When pH is selected for calibration the K23050
being taken. This includes calibration as well as
will display:
analytical measurements.
pH Temperature
6.3.1 pH Zero
Auto_____X
Man._____
The pH sensor is placed in the appropriate buffer
At this point the device is asking the user to and allowed to equilibrate. The pH zero offset
indicate how it will determine the pH buffer adjustment is intended to establish the isopotential
solution temperature during calibration. This is an point of the sensor. This is done by placing the
sensor in a buffer 7.00 solution. pH buffers are
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Operation and Instruction Manual
readily available and are usually accompanied by the new cal data in non-volatile memory. The unit
a chart that gives the buffer value for various will then return to the 'pH Calibration' menu for
temperatures. Refer to this chart when entering further cal selections or exit to the main menu.
the buffer value.
6.4 Calibrate pH Millivolts
When 'pH Zero' is selected the display will show:
The pH millivolt channel is a second display mode
pH 07.010 for the pH input channel. It utilizes separately
stored calibration data and is intended for
Adjust w/ Arrrows displaying the millivolt output from a sensor
Then press Enter connected to the pH input, BNC connector. This
sensor may be a pH, specific ion, or ORP sensor.
The unit recalls the last pH zero cal point from The displayed value is not temperature
non-volatile memory and that is displayed. compensated.
The operator now uses the arrow keys to adjust To calibrate this channel a voltage standard must
the pH buffer 7 value to the appropriate setting for be connected to the pH input. A 'Zero' offset
the temperature of the solution. When this is adjustment is performed with the voltage standard
accomplished press the 'ENTER' key and the unit set near 0.0000 volts. The 'span' adjustment is
will derive the offset data, store the information in then done with the standard set to a value
non-volatile memory and revert to the 'pH between 0.5000 volt and 0.7500 volt. During
Calibration' menu. calibration the pH/ion ground electrode must be
connected to the negative terminal of the
calibration voltage source.
6.3.2 pH Span
When 'Calibrate pH Millivolts' is selected the
instrument will display:
The pH electrode and ground electrode are placed
in the appropriate buffer solution and allowed to pH Millivolt
equilibrate. The pH span point can be any buffer
solution sufficiently far away from the zero point Zero_____X
(7.00) to allow accurate slope derivation. This is Span_____
typically a buffer 4.00 or 10.00. Exit______
The pH sensor should be thoroughly rinsed in Use the 'ARROW' keys to choose the desired
distilled water and dried prior to insertion in the function, then press the 'ENTER' key to proceed to
buffer solution. This will prevent contamination of that task.
the buffer solution. Allow several minutes for the
sensor to equilibrate before proceeding.
(Displaying pH or pH mV when the sensor is 6.4.1 Zero pH Millivolt
placed in the buffer will give an indication when
the sensor has come to its final value.)
When the pH millivolt channel is selected for zero
offset calibration the pH input should be either
When pH Span is selected the display will show:
shorted (connecting the center pin of the BNC
connector to the outer shell) or have a voltage
pH 04.000
standard connected and set to near 0.0000 volts
DC.
Adjust w/ Arrows
Then Press Enter
The unit will display:
The unit recalls the last pH span value from
mV 0.0000 VDC
non-volatile memory and presents it for display.
The arrow keys are used to adjust the pH span
ADJUST W/ARROWS
value to the desired point. Once this is done the
THEN PRESS ENTER
user presses the 'ENTER' key and the instrument
will make the appropriate calculations and store
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Operation and Instruction Manual
Use the arrow keys to adjust the displayed voltage 6.6 Calibrate Salt
to the value set into the voltage standard or
0.0000 if the input is shorted. Press the 'ENTER' The Salt Calibration menu is the point where the
key when this has been done. instrument establishes its relationship between
conductivity and salt concentration. Before
The unit will establish the zero offset value, store entering this menu the instrument's temperature
the calibration data and return to the pH Millivolt reading should have been verified and conductivity
Cal menu. "zero" and "span" set. In addition the "salt"
standards should have been prepared per ASTM
D3230.
6.4.2 Span pH Millivolt
When this menu is selected the K23050 prompts
Set the voltage standard connected to the pH the user with:
input to a value between 0.5000 and 0.7500 volt.
When 'Span pH Millivolt' is selected the instrument Salt Calibration
will display: Erase Old Cals?
The Daily Blank feature offers a means of Once a Salt Calibration has been performed the
adjusting the salt calibration information for slight operator may view the calibration data via the
variations in system offset. This is accomplished serial communication port. If it is determined that a
by introducing the conductivity/temperature sensor calibration point was overlooked or improperly
to the Blank standard prepared per ASTM D3230. performed the user may chose to NOT erase old
When the sensor has stabilized and the 'Enter' key calibration data and re-enter the calibration point
pressed the instrument will determine the in question.
conductance of the solution; calculate the
difference from the last Blank reading and adjust Once the "Salt Calibration Menu" is started a list of
all of the Salt calibration data accordingly. standard salt values is presented to the user. They
are:
NOTE: In this step as with any of the salt Blank, 1 ptb, 3 ptb, 5 ptb, 10 ptb, 15 ptb, 20 ptb,
calibration procedures the volume of standard 25 ptb, 30 ptb, 40 ptb, 50 ptb, 65 ptb, 75 ptb, 85
solution used must be kept constant. ptb, 100 ptb, 150 ptb, and Exit
Approximately 90 ml of solution is recommended
(just enough to cover the electrodes in their The calibration procedure is to be systematic:
sample beaker). This volume should be measured
precisely as it effects the conductivity 1) Rinse the sensor electrodes in alcohol and dry.
measurement.
2) Place the electrodes in a selected and precisely
measured salt standard solution.
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Operation and Instruction Manual
3) Select that standard from the list via the arrow battery condition. When this mode is selected the
keys and press "ENTER". unit will display:
The instrument will store the salt value and Select the desired function with the 'SELECT' key
conductance reading in a table of calibration then press the 'ENTER' key to execute the
values. command.
Not all of the remaining standard values Press the 'ENTER' key and the unit will establish
are required to be entered. However, the the zero point on the internal battery voltage
instrument establishes a linear slope channel, store the data in non-volatile memory and
between each standard value used. return to the 'Calibrate Internal Battery' menu.
Therefore, a much more accurate salt
reading will be calculated if the maximum 6.7.2 Span Internal Battery
number of salt standards are entered.
To set the span point of the internal battery
The instrument will not calculate a salt channel the battery that was removed during the
value if it encounters a conductivity
'zero' process must be reinstalled. Activate the
measurement higher or lower than that instrument and monitor the battery voltage with a
obtained during salt calibration. In these digital volt meter.
instances it will display 999999 ptb as the
measured salt value. For this reason it is
The display will show:
advisable to utilize a salt standard well
above those that will normally be Int Bat 5.50 V
measured, thus, avoiding ambiguous
readings. Adjust w/ Arrows
Then Press Enter
6.7 Calibrate Internal Battery
Use the arrow keys to adjust the displayed
Note: This is typically a factory procedure. battery reading to the appropriate value. Press
the 'ENTER' key to establish the calibration of
The internal battery voltage is monitored by the this channel. After this is accomplished the
CPU in order to alert the user of a pending low
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Operation and Instruction Manual
unit will revert to the 'Calibrate Internal Battery’ 'ENTER' key to establish the calibration of this
menu. channel. After this is accomplished the unit will
revert to the 'Calibrate External Battery’ menu.
6.8 Calibrate External Battery
7 Data Logging
Note: This is typically a factory procedure.
The "Data Logging" menu offers the user control
The external battery voltage is monitored by the over the various logging parameters and functions.
CPU in order to alert the user of a pending low It allows the user to select which parameters will
battery condition. be stored when a data scan is logged; select
either manual or automatic modes; set logging ID
When this mode is selected the unit will display: number and increment value; enable or disable
the logging feature.
Ext. Bat. Cal
When the Data Logging function is selected the
Zero___X display will show:
Span___
Exit ___ Enable/Disable
Select the desired function with the 'ARROW' keys Auto/Manual ____X
then press the 'ENTER' key to execute the ID Number_______
command. Exit_____________
6.8.1 Zero External Battery The user moves the selection character (X) to the
desired function by pressing the "ARROW" keys.
To set the zero offset adjustment value for the Once the desired function is marked press the
external battery the unit should be operating from "ENTER" key to perform that operation.
the internal battery. Disconnect the external
battery from the readout. The display will show:
7.1 Enable/Disable Data Logging
Ext Bat 0.00 V
The Enable/Disable menu shows the following
Adjust w/ Arrows display:
Then Press Enter
Logging
Press the 'ENTER' key and the unit will establish
the zero point on the external battery voltage Disabled____X
channel, store the data in non-volatile memory and Enabled_____
return to the 'Calibrate External Battery' menu.
This menu assumes that the set up procedures
6.8.2 Span External Battery have been performed; the auto/manual entry has
been made and any desired ID number and
To set the span point of the external battery increment value entered.
channel, activate the instrument and monitor the
external battery voltage with a digital volt meter. Enabling logging, if in the manual mode, will
periodically display 'Manual Logging Enabled' in
The display will show: the real time display mode. This tells the user that
Logging is Enabled and pressing the 'ENTER' key
Ext Bat 6.45 V will cause the selected parameters to be stored as
a data scan. The parameters will be stored along
Adjust w/ Arrows with the date, time and logging ID number.
Then Press Enter
If automatic logging has been selected when
Use the arrow keys to adjust the displayed battery logging is enabled the K23050 will prompt the user
reading to the appropriate value. Press the for the starting date, time, and interval between
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Operation and Instruction Manual
data scans. Also, the unit will periodically display The logging ID number consists of up to a five digit
'Auto Logging Enabled while in the 'display integer that will be stored with the other logging
parameters' mode. information if it is selected. In this menu the
display will show:
7.2 Auto/Manual Data Logging
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Operation and Instruction Manual
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Operation and Instruction Manual
Set Time Use the arrow keys to select Yes or No and press
the "ENTER" key. If "Yes" is selected then
Hour_____X instrument will power down. If, "No" is selected it
Minute____ will return to the main command menu.
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Operation and Instruction Manual
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WARNING: Disconnect power to the unit before The charge state of either battery can be checked
servicing to avoid exposure to high voltages by displaying the battery voltages on the unit
and/or temperatures which may result in personal system display. The internal battery back should
injury or death. The Koehler Salt-in-Crude measure 5.4 volts or higher when at full charge
Analyzer requires very little maintenance for (without the charger on). The external battery will
proper operation. If you have any questions about measure 6.8 volts at full charge without its charger
maintaining your equipment, then please do not plugged in).
hesitate to contact the Koehler technical service
department.
16.2 Routine Maintenance
16.1 Battery Charging
The K23050 Salt in Crude Analyzer requires little
The K23050 contains an internal battery pack routine maintenance to provide many years of
comprised of four AA size, NICAD batteries. When continuous service. However, over the course of
fully charged these can provide approximately time, some instrument parts may need to be
eight hours of continuous operation. The unit replaced. When ordering replacement part(s),
comes with an external AC adapter, which can be please provide the model number, serial number,
used to power the instrument directly or to charge and product shipment date of your equipment so
the internal battery pack. To power the K23050 that we can ensure you will receive the proper
from the AC adapter plug the adapter connector replacement part(s).
into the jack labeled "Power". The instrument may
be run continuously in this manner. If the 16.3 Replacement Parts and Accessories
instrument is primarily operated from AC power
the user should periodically monitor the internal
battery voltage and recharge when the battery falls Part Number Description
below 4.9 volts. It is not intended for the unit to be
K23050-1 Electrode Cap Assembly
secured by simply unplugging the AC power
adapter. The instrument should be turned off by K23050-2 Serial Cable Assembly
means of the "POWER OFF" procedure in the Temperature Probe and
main menu. K23050-3
Wire Assembly
To charge the internal batteries plug the adapter Power Adapter, Dual
K23050-4
Voltage 115/230V
connector into the jack labeled "Power". The unit
has a build in battery charging circuit that will K23050-5 Ground Electrode
recharge the internal batteries in 14 - 16 hours. K23050-6 Calibration Resistor
This is assuming the unit is not activated. If it is
External Battery with
operating a very limited amount of charging K23050-7
Stand
current will be available for the batteries.
K23050-8 Table Top Stand
The unit system offers an optional external, sealed K23000-CASE Salt in Crude Case
Nickel Metal Hydride (NiMh) battery and external
charger. This is a recommended option if the K88615 Serial to USB Adapter
K23050 is going to be used on extensive field 332-002-017 100 mL Beaker
studies or when long time data logging is to be
performed. Since data will be lost if the instrument Data Acquisition
K23050-SW
is turned off or loses power while storing Software CD
information, the larger capacity external battery is
a good safeguard. 17 Service
When fully charged the external battery can Under normal operating conditions and with
operate the K23050 for approximately 130 hours. routine maintenance, the K23050 Salt in Crude
To charge the external battery, simply plug the Analyzer should not require service. Any service
external battery charger, power adapter into a
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Operation and Instruction Manual
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Notes
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Operation and Instruction Manual
Notes
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