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FOREWORD
The efficiency of the exchange of matter between the phases, in particular
between gas and liquid, is strictly tied with the contact area. The devices that
bring about the contact are based essentially on three types of liquid/gas
dispersion:
- dispersion of the gas in the liquid (continuous stage) in the form of bubbles
or foam; this is the case of plate columns or bubble towers;
- dispersion of the liquid in the gas (continuous phase) in the form of drops
as in spray towers or in plate towers operating in spray conditions;
- dispersion of the liquid in the form of a film submerged in the gas; this is
what happens in packed columns where packing is employed to create a
support for the film: in these circumstances, both phases are continuous.
In this manual we shall examine packed columns that are widely used in
industry, both in absorption and stripping operations and for distillation
purposes.
PACKING
The packing calls for the following characteristics:
B) Low load losses to permit the passage of great fluid flow-rates per unit of
section of the column without flooding.
This required a high degree of vacuum for the packing.
c) Resistance to chemical corrosion.
e) Low cost.
Fig. 2.4.0 shows some of the most common types of packing elements used
haphazardly. Rashig rings, very widely used in the past, are made of
- ceramic - glass
- stoneware - graphite
- metal - sundry plastic materials
Berl and Intalox saddles are generally made of ceramic, but can also be
produced in any material suitable for moulding.
Unlike Rashig rings, saddles only hace an "external" surface. The external
surface is generally more active than the "internal" one, the latter often not
being reached very well by the liquid and sometimes even containing "traps"
of non-renovated liquid.
Pall rings have recently found widespread application on account of their
excellent capacity and efficiency characteristics. Built of plastic materials or
metal, in sizes from 16 to 100 mm, they have proved particularly suited and
practical in operations under pressure and especially under vacuum.
The special shape of the notches and tongues is designed to carry the liquid
from the inner wall to the outer wall and viceversa.
Furthermore, the liquid film should cover the widest possible packing surface.
The upper limit of the operating range in correct fluids dynamic conditions lies
in the “flooding” of the column, a phenomenon which is characterized, as in
plate columns, by the whole or partial saturation of the column with liquid and
the resulting sudden increase in load losses.
In flooding conditions, the gas is forced to bubble in the liquid and thus
becomes a dispersed phase; the liquid may come out from the head pipe of
the gas in the form of foam or entrained drops.
Fig. 2.6.0a show the typical fluids dynamic behaviour of packing elementls
arranged in haphazard manner, in terms of
- load losses per unit of height of the packing ∆