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ABSTRACT
1. INTRODUCTION
Among the metal forming processes, cold metal forming processes are the most
advantageous one due to low scrap, high production rates, and increased yield
strength of cold formed products after forming operation. In general, the customer of
these products needs the new increased yield strength distribution for design
calculations. However, the products are not appropriate for standard material testing
experiments such as simple tension, simple compression or simple torsion. Thus,
usually either simplified analytic computations or finite element models are used to
predict the new increased yield strength distribution. Alternatively, the local flow stress
is determined by means of hardness measurements, which are converted to the
respective flow stress at the point of measurement.
Hardness tests have for a long time been a standard method for material
characterization as they provide an easy, inexpensive, non-destructive, and objective
method of evaluating basic properties from small volume of materials. As well as
resistance to plastic deformation; stiffness, strength of thin coatings, residual stresses
near the surface, and the fracture toughness of the material are some basic properties
that can be measured by the hardness tests.
In the literature, Vickers hardness number (HV) has been the most popular in
investigation of the relationship between hardness and the flow stress of the material
because of two reasons. Firstly, its superior resolution as compared to spherical
indenters. And secondly, the Vickers indenter is self-similar, through which the
hardness is ideally independent of the indentation load and indentation depth.
Therefore, in this study, Vickers indentation will be the main concern.
2. PREVIOUS STUDIES
A basic review of the first results is covered by Tabor. [1,2]. Tabor has shown that the
mean contact pressure, Pm, (or hardness) can be related to the yield stress of the
material, Y, by an expression based on the theory of indentation of rigid perfectly-
plastic solid.
3.20
Ratio Vickers Hardness to Yield
Stress (in kg/mm2)
3.00
2.80
M ild S t e e l
A n n e a le d C o p p e r
2.60
0.00 0.10 0.20 0.30
E q u i v a l e n t P l a sti c S tr a i n ϕ
Figure 1: Experimentally determined Vickers Hardness Number and Yield Stress ratios for
various amounts of initial plastic strain, Tabor [1,2]. (yield stresses are evaluated for an
engineering representative strain of 0.08)
Figure 1 shows that the comparison of Tabors formula with his own experimental
results. In this plot, ϕ designates the equivalent true plastic strain, which the specimen
experienced before indentation. It can be observed that the agreement is rather good
for mild steel, whereas the annealed cupper a scatter of about %15 is present. It
should be emphasized that Tabor’s formula is given at various places with slightly
varying coefficients and representative strain values as compared with the values
given in Eqn.3.
4.5
Ratio Vickers Hardness to
Yield Stress (in kg/mm 2)
4.0
3.5
2.5
0 0.4 0.8 1.2 1.6
Equivalent Plastic Strain ϕ
Figure 2: Ratio of Vickers Hardness number and yield stress by Dannenmann and Wilhelm. [3]
The relationship between Vickers hardness number and yield stress as related to
metal forming is investigated by Dannenmann, Wilhelm et al. [3]. The experimental
results can be seen in Figure 2. In their original work, no use of Tabor’s model as
explained above was made, so that an interpretation of their experimental results
utilizing Tabor’s model is also given in this figure. However, even this improved curve
indicates a conversion error of 20%.
Figure 3 shows a typical finite element mesh used for the analyses, which has been
conducted with the commercial code MARC. Axisymmetrical linear four node elements
have been used in the computation and no re-meshing has been applied.
Simulations have been conducted for five different materials, for which the normalized
flow curves are given in Figure 4. The materials have been selected such that the
strain-hardening exponents (n) cover the wide range. The Vickers hardness for each
material has been computed in the annealed state and four strain-hardened states
corresponding to the equivalent plastic strain of 0.04, 0.10, 0.24, and 0.40. In this
range of plastic strain the assumed Ludwik type of flow curve representation (Y=K⋅ϕn)
is at least moderately accurate.
2400 2400
Materials:
C10, C15, C35, St38, CuZn40
2000 2000
ness HV in MPa
ess HV in MPa
Prediction Interval
1600 1600
99% Confidence
1200 99% Confidence 1200 Interval
Interval Prediction Interval
Figure 5: Vickers hardness number v.s. Figure 6: Vickers hardness number v.s. the
initial yield stress of material. yield stress of the material computed at an
optimum offset equivalent plastic strain of
0.112.
Figure 5 and Figure 6 exhibit the Vickers hardness numbers (in MPa) versus the initial
yield stress and yield stress at an offset equivalent plastic strain of 0.112, respectively.
In the first plot, it can be concluded that the scatter is unacceptably large with the large
prediction interval. However, the second gives the better accuracy. Here, the offset
strain at which the flow stress is computed has been varied systematically until the
scatter in various hardness-flow stress pairs were minimized. The resulting value of
the equivalent plastic strain was 0.112. The slope of the regression line shown in the
figure corresponds to the coefficient in Tabor’s original formula as given in Eqn.3.
Hence, the modified Tabor’s equation can be given as:
After the numerical analysis, the Vickers indentation test experiments of new five
different materials in various strain-hardened states has been done to check the
correlation obtained from the finite element simulations. Before the tests, these
materials have exposed to the upsetting test to obtain their flow curves up to the large
plastic strains. The list of these materials and the coefficients of Ludwik equation
representing their flow curves are given in Table 1.
Table 1: List of the experimental materials and their material constants for Ludwik equation.
Cold direct-extrusion metal forming process has been chosen to get strain-harden the
materials. Since the process is very suitable for this purpose and gives the exact
equivalent plastic strain at the center of the extruded product. Therefore, the hardness
measurements have been done around the center of the experimental specimens.
(See in Figure 7.)
Figure 7: Extruded specimens in various strain-harden states and the picture of the center
cross-section of the specimen.
The results of the Vickers hardness measurements (in kg/mm2) for the experimental
materials can be seen in Table 2.
Table 2: Experimental results of HV for five different strain-harden states. (Vickers hardness
2
numbers in kg/mm )
300 30
25.9
Proposed Relation
Vickers Hardness HV
17.3
17.3
200 20
16.3
15.5
15.3
14.8
14.7
16
14.6
15
150
10
100
Classical Relation
Tabor's Relation 5
2.2
1.7
-3.3
50
-1.3
-3.4
Proposed Relation
Experiment 0
0 0.02 0.52 0.92 1.21 1.60
0.02 0.52 0.92 1.21 1.60 -5
Equivalent Plastic Strain
Equivalent Plastic Strain
Figure 8: Comparison of Predicted and Measured Hardness Numbers for material 20MoCr4.
Modified relation (eqn.4) gives the best accuracy in the material 20MoCr4 for which the
hardness comparisons and error plots are given in the Figure 8. However, it is
observed that the errors for the other materials are about 5-10%. To increase the
accuracy and verify the proposed relation or to predict a new relation, some additional
works such as new simulations and experiments are required.
As additional analysis, the ten different materials, which are mentioned so far, have
been simulated with the same mesh in Figure 3 to obtain the hardness numbers in the
larger strain-hardened states. And all results are shown in Table 3.
Table 3: Finite element simulation results for Vickers hardness numbers (in MPa) of analyzed
materials.
In Figure 9., the plot of the hardness numbers versus corresponding yield stress
values (in MPa) can be seen.
3000
Vickers Hardness Number (MPa)
2500
2000
16MnCr5
20MoCr4
1500 AlMgSi05
AlMgSi1
C10
1000 C35
Cf53
Ck15
500 CuZn40
St38
0
0 200 400 600 800 1000 1200
Figure 9: Plot of Vickers hardness numbers versus yield stress values of simulated materials
(in MPa).
Among these results given in Table 3, the hardness values for non-hardened case
(this can be thought as the hardness measurement values at the head side of the
specimens.) have been analyzed separately. Since these data have a disagreements
with the results of the relations fitted for all hardening case. Therefore, a new relation
that is given in equation 5 is obtained. And the percentage error values between the
Vickers hardness values calculated from the equation 5 and the hardness
measurement values at the head side of the experimental materials can be seen in
Table 4.
Table 4. Comparison of the modified relation (eqn.5) for the non-hardening case with the
experimental results.
Linear approximation analysis for the rest results obtained from the strain-hardened
cases have been done by using different offset strains. Unlike the modified Tabor
relation (eqn. 4), maximum regression is obtained with the offset strain of 0.120 and
the new relation is observed as following:
HV = 2.528 ⋅ Y (at an offset strain 0.130) for 0.00 < ϕ < 0.50
(7)
HV = 2.520 ⋅ Y (at an offset strain 0.230) for ϕ ≥ 0.50
Another work has been done to analyze the influences of the strain-hardening
exponent (n) in the Ludwik type representation of the flow curves. In this work, three
relations were found for the given interval of n as followings:
HV = 2.50 ⋅ Y (at an offset strain 0.118) for 0.00 < n < 0.10
HV = 2.52 ⋅ Y (at an offset strain 0.116) for 0.10 ≤ n < 0.20 (8)
HV = 2.54 ⋅ Y (at an offset strain 0.135) for n ≥ 0.20
Same analysis has been performed for the material constant K in the Ludwik’s formula
(Y=K⋅ϕn) as following :
HV = 2.51 ⋅ Y (at an offset strain 0.140) for K < 800 ⋅ MPa
(9)
HV = 2.51 ⋅ Y (at an offset strain 0.130) for K ≥ 800 ⋅ MPa
The comparisons between the predicted hardness numbers of material 20MoCr4 and
the numerical values of its hardness numbers obtained from the Vickers indentation
experiments are shown in Table 5.
Table 5. Comparison of the new modified relations with the experimental results of material
2
20MoCr4. (All hardness results are in kg/mm )
ACKNOWLEDGMENTS
• This study was a AFP Research Project : AFP-98-03-02-03
• Research assistantship of Bülent Yavuz is supported by the METU Graduate
School of Natural and Applied Science.
REFERENCES
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Roy. Society Series A., 192, pp 247-274
2. Tabor, D. (1951), The Hardness and Strength of Metals, Oxford Clarendon
Press
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Kaltumformvorgangen”, Bander Bleche Rohre, pp 368-394
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