GENERAL TECHNICAL ‘STDI0006.PRO.001 el F DOCUMENTS Leeann PHYSICAL AND CHEMICAL TREATMENT Rev: 0 __Date : 940901 ‘OF HYDROSTATIC TEST WATER Pages tof 8 Treatment method No.1 Type of water: UTILITY WATER SALT WATER AND SEAWATER Equipment concemed: All Materials: Carbon steel Ja Trestment purposes: bactericidal, to neutratize the flora of sulphate-reducing bacteria, 2. Trenenent eh Furetion 1 eompoat fon Minimum dose Bacterick Gturarataenyae 250 ppm of active canponent ‘3._Speciel trestment conditions No corment. 4. pret cine Unneceesary from the corrosion standpoint. If the equipnent is purged and then placed on hold, all the low points shalt be opened, the equipment shall be rinsed with fresh or potable water, then dried or placed under nitrogen athosphere. AIL the inets shell be sealed off. 5 Discharge of tluids The fluid discharge procedure shall be submitted to the Onner tor approval before the operation, 6. Monitoring eeguineg Inspection of bacterial activity on water samples taken on completion of equipment filling, by test kits for sulphate-reducing bocteria. Oxygen scavenging treatnent is not specified, because any corrosion (by Loss of wetal) resulting fram this onygen will renain moderate. However, this corrosion can generate @ quantity of rust-coloured ferric oxide deposit. If this deposit is unwanted, or If the fluld Is presumed to renain in the equipment for nore then one week, this treatment shalt be replaced by treatment NO.4.GENERAL TECHNICAL ‘STDI 0005.PRO.001 el F DOCUMENTS Laem PHYSICAL AND CHEMICAL TREATMENT Rev. : 0 __Date : 940801 OF HYDROSTATIC TEST WATER Page 2 of 8 Treatment method No.2 ‘Type of water: UTILITY WATER SALT WATER AND SEAWATER Equipment concemad: Vessels Process pipework Materials: Carbon steel! Ireatment purposes: bactericidal, to neutralize the becterial flora 2. Trentmene chemicels Function Chemteat conpositfon Minimum dose Bactericide | Sodium hypochlorite See NOTE NOTE 10 mg/L chlorine = 65 mg/l of sodium hypochlorite at 48° chlorineter, ‘._Soncial_treatment conditions The dose of product shall be sufficient to ehtain a free chlorine content of at Least 5 pm, after Pesetion with the organic matter in the water used. 4, Draining and rinsing The equipment shalt be purged within 48 h after filling. This purge shalt ne carried cut at att the Low points. | The equipment shall then be cinsed with potable water. If the equipment ia kept on hald before use for more than one week, 1t shall be dried er placed under nitrogen ateosphere, ALL the inlets shall be sealed off, Ss _Honi toring requires Free chlorine content at the end of f1lLing. Do not delay sampling and measurement because the free chlorine is consuned progressively by corrosion, 2. Observations This treatment is ideal for snl l-volune equipment (2 few m), for operations in which the water is kept in the equipment for a short tine interval.| GENERAL TECHNICAL ‘STD1.0005.PRO.001 DOCUMENTS elf 2 PHYSICAL AND CHEMICAL TREATMENT Date: 940001 Fev. 0 (OF HYDROSTATIC TEST WATER Page: 3 oof 8 Treatment method No.3 Type of water; POTABLE WATER UTILITY WATER Equipment concerned: Procass circuits and vessels in which the service temperature is > 60°C Materials: Stainless steels La Treatment purposes: avotd the fFects of chloride ions after resumption of operat ions. 2. Treatment chemicals: no chenicate. Function ‘chemical composition Minimum dose 3. Specinl teestment conditions The chloride concentration shalt be less than 10 ma/t. The diasolved iron concentration shall be less than 1 mg/l. The ater shatt not contein ferric particles (total iron < 2 mg/l). 4. Draining end ringing Drainage of the hydrostatic test water is to be done within one week after completion of the test. The raining shall be carried out at ail the Lov potnte. Rineing with type A de-ionized water until the ehleride concentration is the same as in the rinse water. All the low points shail be rinsed. 5. Discharge of tHuids $.tonltering reavired Sefore filling: dissotved iron and total iren concentration in the hydrotest water, Chloride ion concentration, Before rinsing: check the chloride content of the de-ionized ‘ater: During rinsing: ehteride ien concentration in discharged water 1. Observations The drainage and rinsing phases can be avoided by using type A water directly for the test. The need for NghLy de-fonized water (type A) applies to installations operating in anhydrous conditions, hence a risk of chloride concentration at the holdup points. Instaltatians operating with water present can tolerate test waters with higher chloride contente, fo a maximum of 100 mg/l.GENERAL TECHNICAL $TDI 0005.PRO.001 el F DOCUMENTS a PHYSICAL AND CHEMICAL TREATMENT Fev. 0 OF HYDROSTATIC TEST WATER Page: 4 of Treatment method No.& Type of water: UTILITY WATER ‘SALT WATER AND SEAWATER Equipment concerned: Pipelines Materials: Carbon stee! ‘oxygen renoval and bacterfetdat. a nical Funetton Chemical composition intmum dose ‘xveen ‘Sulphite or Bieulphite ‘ecording to Gate Sheet scavenger + baccerietae Stutaratconyde 250 pom of active compound wulti-purpose | Suiphite or Bisulphite + quaternary | 1000 to 1500 ppa depending on product vont ‘Lx Spacial treatment conditions ‘Tho oxygen scavenger shall be mixed with the fluid at the ‘Last ainute! to avoid re-aeration of the ueter. The dissolved oxygen content (test described in Section 6 below) shall be lees than 50 ppb, The votune of water to be injected shall be about 110% of the total volune of the pipe, to allow for vests at the Pipe inlet cand see Section 6). 4. Drainage and ringing Unnecessary. Sx Discharge of fiuids The fiuld discharge procedure shal be sumitted to the Ouner for approval . &: Monitoring required At the injection eoint During fitting with test water: oxygen concentration of the water entering the pipe, downatrenm of the Ereatnent point after the injection of 10% and 90K of the volume to be injected. A reaction time of at lease $0 21s necessary between injection and sampling point At pipe qutiee During fYlLing with test water: oxygen concentration of the test water and teat of bacterial activity, on samples taken after injectien setueen 102 and 10B% of the volume of the pipe.GENERAL TECHNICAL ‘STD! 0008.PRO.001 el F DOCUMENTS ec PHYSICAL AND CHEMICAL TREATMENT Fev. 0 Date ; 940901 OF HYDROSTATIC TEST WATER Page: 5 of 5 onths) fm the equipment without any signi of iron oxide depostes feant risk of corrosion. It also helps to avoid the formation