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1
Chapter 1
GENERAL
DESCRIPTION
2
1.1 IMPORTANCE OF THE LEAK TEST
In this leaflet, the term “leakage” defines the leakage of gas or fluid from a product, which will
affect the overall quality of the product.
The problem of leakage includes a variety of meanings, depending upon the industrial fields
where the term is used. For example, with fuel handling products, leakage can introduce a danger
of a fire, explosion, runaway, etc., while with other products it refers to low performance and
economic loss. In the food and drug industries it can cause a change in properties and/or shade, or
even rot in case of food. A small leak can grow into an unexpected size then creates product
liability problems, which at times, can become a crucial damage to a company.
3
1.3 A VARIETY OF LEAK TEST METHODS
Table 1.3 Leak Testing Methods
4
1.4.2 Factors Influencing Flow State
When considering the flow in a large pipe, the flow velocity of fluid at the wall of the pipe is 0
because the flow stays with the wall due to the viscosity of the fluid.
The velocity increases as the position of the flow is measured away from the wall because the
influence of viscosity reduces and the flow becomes dominated by inertia.
The layer which is influenced by both viscosity and inertia is called a boundary layer and the
layer becomes thin when the flow velocity of fluid is high or the viscosity of fluid is low. The
flow state which is dominated by inertia is turbulent flow.
By contrast, when considering the flow in a small pipe, a boundary flow develops near the wall of
the pipe due to viscosity and it merges at the center area of the pipe. The flow has a velocity
distribution with a parabolic shape and this flow state which is dominated by viscosity is viscous
flow (or laminar flow).
The Reynolds number (Re) indicates the boundary of the 2 types of flows.
Re = U・D/ν
U: Mean Flow Velocity within Pipe
D: Inner Diameter of Pipe
ν: Kinematic Viscosity Coefficient
When the Reynolds number is larger then 2200 (Re>2200), the flow is turbulent flow, when the
number is smaller than 1200 (Re<1200), the flow is viscous flow, and when the number lies
between the 2 values, the flow is intermediate flow in which viscosity and inertia influence each
other. If the diameter of the pipe decreases further, the flow can be described as follows. Viscosity
represents a state in which the molecules of fluid collide with each other and influence each other,
but the flow within a pipe becomes independent of its viscosity when the diameter of the pipe is
smaller than the distances of the collision of molecules (mean free path).
This state is molecular flow and the Knudsen number (Kn), a dimensionless number, determines
the state of flow.
Kn = λ/D
λ: Mean Free Path of Gas
D: Inner Diameter of Pipe
In this leaflet, differences in the state of a pipe are considered because leak flow is being
considered. However, laminar flow or molecular flow will occur even in a large pipe when the
pressure in a pipe is reduced, because it causes a smaller kinematic viscosity coefficient or a
longer mean free path.
5
1.4.3 Leakage of Gas or Fluid (Turbulent Flow)
Calculation Equation of Leak Volume
P2+0.1
P1+0.1 ≦0.5 then the flow is chocked flow.
293
Q=120×S(P1+0.1)
273+t
P2+0.1
>0.5 then the flow is subsonic flow.
P1+0.1
293
Q=240×S (P2+0.1)
(P1−P2)
273+t
Q: Air Flow Volume (L)
S: Effective Sectional Area (mm2)
P1: Upstream Pressure (MPa)
P2: Downstream Pressure (MPa)
t: Temperature (℃)
Leakage is a phenomenon which occurs when a fluid such as air, water, or oil passes through an
unintended opening such as a small hole. A resultant leak volume differs according to the
difference of pressure across the opening; and relates with the ease of fluid flow through the
opening; conductance.
This can be expressed by the following equation.
Q = C (P1 – P2 ) ---------------------------------------------------(1.1)
Where Q is leak volume, P1 – P2 represents the difference between two pressures, and C is
conductance.
When leakage is the subjective problem, the ease of fluid flow (C) depends on a variety of factors,
including the configuration of the opening, length, etc. It is therefore difficult to apply one type of
equation to all cases. In this section, an explanation is given using general application equations.
Where Qa is the volumetric flow of outlet side pressure (atmospheric pressure) converted from
compressible fluid such as air.
However, if P1 is negative, the leak volume is expressed in terms of the state of atmospheric
pressure. The P2 in the denominator in equation 1.2 is replaced with P1 .
With a volumetric flow rate QW representing non-compressive fluid such as water, oil, etc. the
following equation is applied;
pR 4 (P1 − P2 )
QW = -----------------------------------------(1.3)
8? W l
6
Qa : Volumetric flow rate of compressive fluid (air) under pressure P2
Q W : Volumetric flow rate of non-compressive fluid
P1: Primary (test) pressure
Pin-hole of Radius
(when negative pressure, atmospheric pressure) R
P2: Secondary (test) pressure
(when negative pressure, test pressure) P1
R: Radius of the opening
l : Length of the opening
? P2
? a : Viscosity of compressive fluid
? w : Viscosity of non-compressive fluid
Fig. 1.2 Theoretic Model of Leakage
The relationship of volumetric flow rate influenced by the difference between gaseous fluid
and liquid, and between two pressures with the same test piece is shown in Table 1.2. Refer to
equations 1.1 and 1.2.
Table 1.2 Relationship between Leak Volume vs. Test Pressure and Viscosity
Condition Relative Equation
Q ?
=
The ratio of leak volume to the fixed test ax ay
Gas
pressures towards different gases. Q ?
ay ax
Q wx ? wy
Fluid
The ratio of leak volume to the fixed test
=
pressure towards different liquids. Q wy ? wx
Q wx ? wy P1x − P2x
The ratio of leak volume to the different = ×
test pressure s towards different liquids. Qwy ? wx P1y − P2 y
(P x − P2 x )
The ratio of leak volume to the different 2 2
Qax ?
test pressures towards different gas es and = wy × 1
liquids. Qwy 2? a x P2x (P1y − P2y )
Gas/ Liquid
The ratio of leak volume to the fixed test Qax ? (P + P2 )
pressure towards different gases and = wy × 1
liquids. Qwy 2? a x P2
7
Viscosity (Viscosity Coefficient) η
Viscosity is one of the important factors when handling fluid. Different units are used in
different fields. Here are some examples;
Table 1.3 Viscosity Coefficient of
1P = 1 dyne・sec・cm-2 = 1gr・sec-1 ・cm-1
Gases and Liquids
= 10-1 N・sec・m-2 Fluid Temperatur
Temperature Viscosity
= 10-1 Pa・sec = 1.02×10-6 kgf・sec・cm-2 0℃ 1.71 × 10 P
-4
-2
sec 70℃ 0.40×10 -2 P
Pa: Pascal 20 ℃ 26×10 -2P
Brake -2
Also, to represent kinematical viscosity of the fluid, use the Oil
50℃ 10× 10 P
-2
equation; 70℃ 7×10 P
Gasoline 20 ℃ 6×10 -3 P
?= ?/?
But ?is the density of the fluid.
Some examples of the viscosity coefficients for air, water, brake oil and gasoline are shown in
Table 1.3.
d
R 4 P1 + P2 P1 − P2
Q (cc/ sec) = 3.879 × 105 × ×
l?a 2 P2
Note: R: Radius of Pipe, l : Length of Pipe ,? a: Viscosity of Fluid ,
P 1 : Primary Absolute Pressure, P2 : Secondary Absolute Pressure
8
(2) Calculation of Leak Rate in Non-Compressive Fluid
Using equation 1.3, volumetric flow rates of non-compressive fluid based on a variety of
calculation units are summarized in Table 1.5
a R4 −1
Q(m /sec) = 3.925 ×10
3
× (P1 − P2 )
l?w
b R4
Q(ml/sec) = 3.925 ×10 −1 × (P1 − P2 )
l?w
c R4
Q(ml/sec) = 3.925 ×10 −1 × (P1 − P2 )
l?w
1
R: (cm); l : (cm); ? a: (P = kg sec/cm 2 ) ; P1 , P2 : (kg/cm2 )
9.80665 × 10
5
d
R4
Q(ml/sec) = 3.849 × 105 × (P1 − P2 )
l?w
9
1.4.5 Molecular Flow
When the mean free path ? of gas is larger than the inner diameter D of a pipe, the molecules of
gas only collide with the wall of the pipe and rarely collide with each other.
○ ○ ○
○
○ ○ λ
λ
○
○ ○ D ○
○ D
○ ○
○ ○
○ ○
Fig. 1.4 State in the Pipe Fig. 1.5 State in the Pipe
(with Large Diameter) (with Small Diameter)
Molecules often collide with each other in the flow. Molecules rarely collide with each other in the flow.
In this state, the interaction among molecules (viscosity) is weak and the flow becomes molecule
flow in which collisions of the molecules and the wall are dominant. By defining the Knudsen
number (Kn), a dimensionless number, as Kn = λ/D, the state of flow can be classified as
follows.
・Kn<0.01 Re<1200 Viscous Flow
・Kn>1 Molecular Flow
When gas at normal temperature flows in a straight circular pipe it is called molecular flow, it
can be expressed by the following equation.
0.523a3
Q = ×(P 1−P2)
M1/2・L
Q: Flow Rate, Pa・m 3/sec
a: Radius of Pipe, cm
L:Length of Pipe, cm
M:Molecular Weight of Gas
P1: Inlet Pressure, Pa
P2: Outlet Pressure, Pa
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MEMO
11
Chapter 2
LEAK TEST
12
2.1 DIFFERENTIAL PRESSURE TYPE LEAK TEST
2.1.1 Operating Principle
In the field of medicine the use of a balancing scale is often used as a precise method for
calculating arbitrarily small amounts of substance. The instrument is used to precisely measure a
weight close to the balancing weight (a reference value) by increasing the weight value on the
opposite side (Fig.2.1).
The FUKUDA Air Leak Testers use the same principle as the balancing scale. The same air
pressure is charged to both the work to be tested and the master work and the change in pressure
balance within a fixed time is checked for the presence of a leak. If there is no leakage, the
charged air pressure shows no change and the balanced status is sustained for a long time (Fig.
2.2). However, if leakage occurs, the pressure in the tested work decreases with time and this
leads to an unbalanced status (Fig. 2.3). The leak rate (ml/sec) determines how fast the
unbalanced status occurs.
Fig. 2.1 Precise Weight Measurement Fig. 2.2 Charge Same Pressure and Fig. 2.3 If Leakage Occurs, the
of Medicine with Balancing Scale Check for Pressure Balance Balance will be lost
Pressure Source
* The master work should be the same as the tested
work without leakage
Fig. 2.5 shows the basic pneumatic circuit actually installed in the FUKUDA Air Leak Testers.
The solenoid valves SV1 , SV2 , and SV3 are opened to charge air into both the tested work and the
master work at a certain pressure. Then SV2 and SV3 are closed. If the tested work has a leakage,
the inside pressure of it gradually decreases according to its leak rate and a pressure difference
against that in the master work occurs. This differential pressure is detected by the differential
pressure sensor. The sensor converts the pressure into an electrical signal and it is displayed on
the tester. The FUKUDA Air Leak Testers utilize the differential pressure value measured after a
preset elapsed time to make an OK/NG judgment automatically.
13
Solenoid Valve, SV2
3 Way Valve, SV1
Calibrator
Pressure Gauge Valve, V1
Air Pressure
Source Differential Pressure
Sensor
Valve, V2
Filter
Fig. 2.5 Basic Pneumatic Circuit of Differential Pressure Type Air Leak Tester
The FUKUDA Air Leak Testers perform the following 4 processes sequentially and makes an
existence/nonexistence judgment of the leakage.
圧力計 圧力計
電磁弁 電磁弁
SV1 SV2 Meter SV1
SV2 Meter
◎ * * * Pa ◎ ***Pa
Pressure Pressure
減圧弁
Reducing 電磁弁
Valve Differential
差圧センサー Pressure Sensor
メーター 減圧弁 電磁弁 Differential
差圧 センサー Pressure
メーター Sensor
Reducing Valve
SV1 SV1
電磁弁
SV3 Master
マスター SV3
電磁弁 Master
マスター
SV3
SV3
14
Leak
リーク
ワーク
ワーク 圧力計
圧力計
SV2 Work SV1 電磁弁
SV2 Work
SV1 電磁弁
SV2 SV2
◎ *** Pa
◎ 500Pa
Pressure Pressure
減圧弁 差圧 センサー メ ーSensor
ター
減圧弁 電磁弁 Differential
差 圧セ ンPressure Sensor
サ ー メーター 電磁弁 Differential Pressure
Reducing Valve Reducing Valve
SV1 SV1
電磁弁
SV3 電磁弁
SV3 Master
マスター
マスター
SV3 SV3
Fig. 2.8 Detection Process Fig. 2.9 Exhaust Process
The differential pressure sensor which converts a pressure value into an electrical signal is the
heart of the FUKUDA Air Leak Testers. Therefore, FUKUDA doesn’t rely on other manufacturers
for this sensor, and has originally developed and manufactures it by ourselves.
15
2.1.4 Applied Measuring Method
(1)Leak Side Measurement
This method is applied when the measurement becomes unstable due to the substance within
the tested work.
Work
Chamber
Work
Tank
Examples: Semiconductor, Camera, Crystal, SAW Filter, Chemical Bag, Food Package, and Molded Parts.
Fig. 2.11 Basic Circuit of Sealed Work Measurement with Pressurized Tank
16
2.1.5 For Performance Enhancement
(1) Mastering Measurement and Fitting Measurement
In a leak test the gas in the work generates heat due to adiabatic compression during
pressurization of the work and this causes a momentary temperature rise in the gas within the
work. Therefore, a temperature difference between the gas inside the work and the outside air
occurs and the heat of the inside gas dissipates through the wall of the work over a long time. The
heat dissipation continues until the temperature inside the work becomes equal to the ambient
temperature. The time required for the heat dissipation depends on the material and shape of the
work, the equipment used for clamp sealing, etc.
For example, in cases of aluminum work and an iron work with a same shape, the aluminum work
dissipates its heat quickly, because the heat conductivity of aluminum is higher than that of iron.
Since the heat conduc tivity of metals is higher than that of air, the work with internal structure
and larger internal surface area dissipates its heat quickly.
However, the heat remains inside and it dissipates slowly when the outside structure of the work
and its internal structure have no contact. For example, a sintered metal filter has small metal
contact area between its case and the sintered metal part. The speed of heat dissipation depends on
works like this. In a leak test, a leak is detected according to the pressure change in the work
which is pressurized at a test pressure. Therefore, it is difficult to perform accurate leak detection
when the state of the gas within the work changes due to its heat dissipation.
The master- less method and the fitting method that are the measuring methods employed in our
leak tester enable measurements with correction for the influence of the heat.
Work with many contact points of the Work with a few contact
Hollow Work internal structure points of the internal structure
17
(1)-1 Mastering Measurement (PAT. No.: 3461973, 3502687)
Same Angle
Leak (equals to leak volume)
2sec
Pa
θ
Actual Measured Data Mastering Data (Noise)
Subtract the leak area from
the measured data area and
Time sec store the resultant value as the
DET
mastering data.
M.DET
Fig. 2.12 Mastering Measurement
When the normal measurement is used with the work to which the mastering process is performed:
Resulting Differential Pressure
Leak
Pa
θ
Actual Measured Data Mastering Data
Time sec
DET
Fig. 2.13 Normal Measurement
Characteristics
・ Reduced pressurization time and detection time when compared to the existing leak test
methods. (A detection time less than 5 sec can be set)
・ Repeatability of measurements depends on the mastering data
Leak
Pa
θ′
Actual Measured Data Mastering Data
Time sec
DET
18
(1)-2 Fitting Measuring (PAT. PEND.)
The heat dissipation of the work is realized as follows.
Differential Pressure
Pressurization
Leak Detection Port
(Work Port) Leak from Work ; a
Curve without Leak
Inside Temperature c
of Work b1
Ambient Temperature of Work b2 b
b1, b2, and b: Constants of pressure
converted from temperature
Detection Process Time
Fig. 2.15 Temperature Inside of Work Fig. 2.16 Leak Characteristic Curve
In Fig. 2.15, the temperature within the work increases when the work is pressurized to the test
pressure through the work port. Then the pressurization valve is closed and the pressure change
within the work is detected using the differential pressure sensor. This differential pressure at the
start of the detection process becomes b1 (a pressure at a different temperature from b2). After
that the internal temperature of the work approaches the ambient temperature at the heat
dissipation rate which is determined by the heat conductivity, C, of the work and the inside
temperature of the work becomes equal to the ambient temperature (b2) over a long time.
The pressure b which is the convergent point of the differential pressure due to heat dissipation
is obtained by the equation; b = |b1 – b2|. The heat dissipation curves are as shown in Fig. 2.17
when the value b varies in actual use environments.
The curves are also as shown in Fig. 2.18 when the heat conductivity varies in actual use
environments.
Differential Pressure
Differential Pressure
Fig. 2.17 When Resultant Differential Pressure Varies Fig. 2.18 When Heat Conductivity Varies
Due to Heat Dissipation
In fitting measurement, these 2 kinds of pressure variation can be corrected at the same time.
These corrections are made using a calculation method to determine constants (a, b, c) by fitting
the pressure curve to the equation of heat dissipation characteristic.
y = ax + b( 1-ecx ) ・・・・・・・・・・・・・・(2.2)
The constants a, b and c are calculated from the differential data at 0.1 second intervals in the
detection process, thus they approximate equation 2.2 with the least error.
The calculated value (of a leak) is displayed as the measurement result. (FittingSet4)
In some cases, however, the error due to the approximation calculation may become large when
the measurement condition is unstable and these 2 kinds of pressure variations are small. In such
cases, measure the values of b and c with a long detection time and obtain their accurate values.
The performance will be improved by substituting them into the equation 2.2 as constants and
calculating the value with approximation in the OK/NG measurement of an actual work.
(FittingSet1)
The FittingSet1 is a correction function similar to that in the master-less measurement.
It is also conceivable that the perfo rmance will be improved by only fixing the heat conductivity
C of the work in some environments.
It enhances the following ability to environmental variation. (FittingSet0)
19
FittingSet2 is a measuring mode in which fixed corrections of leak values are added to FittinSet1.
FittingSet3 is similar to the existing leak testers, such as the work- master comparison method, and
corresponds to the measuring method which generates the heat dissipation characteristics on both
sides of the differential pressure sensor, the tested work and the master work, and counterbalances
them with each other.
Lead Pressure
Pressure Change Due to
Internal Temperature
Pressure/Temperature
Pressure/Temperature
Stable Zone
Stable Zone
Test Pressure
Internal Temperature Change
20
(4) Exhaust Bypass
The exhaust bypass unit is used when a foreign material such as water, oil or swarf attaches to
or mixes into the works. The foreign material may contaminate the inside of the air leak tester
because the pressurized air passes through the tester when the air is exhausted. If the foreign
material mixes into the inside of the air leak tester, it may cause the malfunction of the internal
solenoid valve or the failure of the differential pressure sensor. Therefore, these troubles shall be
prevented by letting the pressurized air within the works exhaust through the exhaust bypass,
without passing through the inside of the tester.
・ The use of the exhaust bypass is recommended when foreign materials attach to or mixes
into the works.
・ By the use of the exhaust bypass unit, the causes which may lead to the failure of the air
leak tester will be reduced and stable measurement results can be obtained.
(6) LPU-300
This is the air leak tester dedicated for the works with a small internal volume (30 ml or less). It
has high detection sensitivity because its capacity is very small (0.7 ml).
21
2. 2 DIRECT PRESSURE DETECTION AIR LEAK TEST
2.2.1 Operating Principle
In this test method, the test pressure is charged only to the tested work and a leak is detected by
measuring the pressure drop (or increase) in the work after a given time. This method is suitable
for the measurement of a large leak but is not suitable for a trace leak, because the influences of
temperature, deformation, etc. directly result in a pressure change.
SV1 SV2
Work
start
OK
NG
22
2.3 HYDROGEN GAS DETECTION LEAK TEST
2.3.1 Operating Principle
In this test method, hydrogen molecules which infiltrate through a ceramic filter are detected
using a semiconductor concentration sensor. Hydrogen molecules will diffuse from high to low
concentration. By taking advantage of this nature of hydrogen molecules, the leaked hydrogen
molecules which diffuse within the sensor are measured.
The advantages of using hydrogen gas
・ Cheap gas price
・ Easy to leak due to low viscosity and less persistent
・ The lightest molecule.
・ Easy on the environment (no pollution)
・ Nonflammable and safe because the gas is used as a mixed gas of 5% hydrogen and 95%
nitrogen.
・ Non-corrosive inert gas (harmless to humans)
・ Low background level in the atmosphere (0.5ppm)
As described above, there are many advantages when hydrogen is used.
The deposition time can be reduced in two ways. That is, to increase the test pressure or to
decrease the chamber internal volume. For example, if the charging pressure is tripled, the
deposition time is reduced to one tenth. This is effective for the leak of a viscous gas and most
gases have some viscosity.
The deposit time when the hydrogen concentration of the sample gas reaches 5ppm is shown in Table 2.1.
The values in the table are reduced by half if the alarm level is set to 2.5ppm.
23
Table 2.1 Deposit Time
Leak Volume
-2 -3
10 10 10-4 10-5 10-6
atm ml/sec atm ml/sec atm ml/sec atm ml/sec atm ml/sec
Work Volume 1ml 0sec 0.1sec 1sec 10sec 100sec
10ml 0.1sec 1sec 10sec 100sec 16min
100ml 1sec 10sec 100sec 16min 2.8h
1L 10sec 100sec 16min 2.8h 28h
10L 100sec 16min 2.8h 28h 278h
φLeak
C=Ctrancer
Vchamber
24
Example:
If the units of Fleak and Fsample are the same, other units can be used.
When the mixed gas is 5% hydrogen and the sample flow rate is 1 atm ml/sec, the equation
above is expressed as follows.
C = 5000 Fleak
Assume that a normal sample flow rate is 1atm ml/sec
The suction probe used is the AP-55.
Chamber or Hood
25
3-3 On Decompression Chamber Method (An Evolved Version of Decomposition Methods)
The sensor of ‘Sensistor Technologies’ leak detector which uses a mixed gas of 5% hydrogen
and 95% nitrogen as a tracer gas is necessary to conduct this measurement at atmospheric
pressure. In automatic leak tests, some works can not be tested in practice because the space
within the chamber has large influences on the detection capability and cycle time. In this method,
the apparent space can be reduced and the pressure at the sampling position of the automatic
probe can be set to atmospheric pressure by reducing the pressure within the camber to 1 kPaabs
and by sucking in a certain amount of air and exhausting the same amount. As a result of this, the
detection capability can be enhanced and the cycle time can also be shortened.
Chamber
Decompression Pump
Exhaust Air
Sampling Hose
Detector
Automatic Probe
Charging and Exhaust
System of Tracer Gas
26
2.4 Helium Gas Detection Leak Test
2.4.1 Operating Principle
In this method, a trace amount of helium gas
which is leaked from the tested work is Light ion
removed and placed in a detector (mass
spectrometer), to detect the gas. Helium ion
The helium gas is ionized by the electron beam
from the filament within the ion chamber of the Collector
Slit
analyzing tube. The ions are accelerated and Molecule Heavy ion
move out through a slit and then pass through ○
the magnetic field generated by the analyzer. × A
Since the circular trajectories of the ions
depend on their mass, the collector can catch
the helium ions.
Analyzer
There are several types of analyzer. The typical (generates magnetic field)
types include the magnetic field modification
type (magnetic sector), omegatron type, and
quadrupole type. Fig. 2.25 Principle of Helium Gas Detection Leak Test
H eディテクター H eディテクター
He Detector He Detector
Work Work
He He
ボンベ ボンベ
He Gas Cylinder He Gas Cylinder
V V
P P
Fig. 2.26 Pressurization with Helium Gas Fig. 2.27 Detection with Helium Detector
H eディテクター
He Detector
Work
He
He Gas Cylinder
ボンベ
V
P
27
(2) Vacuum Vessel Method (Bell Jar Method)
2-1 Depressurize the work and chamber. (Fig. 2.29)
Depressurize the work so that the concentration of helium gas is not decreased by atmospheric
pressure.
2-2 Pressurize with helium gas. (Fig. 2.30)
Discharge the pressurized helium gas into the work.
2-3 Conduct a leak test. (Fig. 2.31)
Detect and calculate with the detector.
2-4 Clean the helium gas with nitrogen gas. (Fig. 2.32)
Exhaust the gases with the vacuum pump.
2-5 Open the work and chamber to atmospheric pressure. (Fig. 2.33)
N2 Gas
N
2 N2 NGas
2
Cylinder
ボンベ V Cylinder
ボンベ V
P P
He Detector He Detector
He He
Gas HeHeGas
ボンベ ボンベ
Cylinder Cylinder
V V
P P
Fig. 2.29 Depressurization of Work Fig. 2.30 Pressurization with Helium Gas
N2 Gas
N
2
N2 NGas
2
Cylinder
ボンベ V Cylinder
ボンベ V
P P
He Detector He Detector
He He
Gas HeHeGas
ボンベ
Cylinder ボンベ
Cylinder
V V
P P
N2 Gas
N
2
Cylinder
ボンベ V
P
Work H e ディテクター
He HeGas
He Detector
ボンベ
Cylinder
V
P
28
2.4.3 Calculation Equation of Leak Volume
Measurement of Detection Sensitivity
(a) While opening the valve for the calibration leak, record the elapsed time and the meter reading
of the helium leak detector, and take the reading when it is stabilized as X2 . In this step, the
reading can be obtained from either the chart of the recorder or the time history of the reading.
(b) Close the valve of the calibration leak and take the reading when it is stabilized as X1 . If the
background level varies, measure the maximum value (X1max) and minimum value (X1min ) and
take their average as the background X1 .
(X1max+X1min )
X1 =
2
(c) Calculate the detection sensitivity (S) using the equation below.
(X2−X1)
S= [1/(Pa・m3/sec)]
Qc
Qc : Leak volume from the calibration leak after compensated for the temperature at
(Pa・m3 /sec)
X1 : Reading of the helium leak detector with the background level. (Output)
X2 : Reading of the helium leak detector for the calibration leak. (Output)
(d) Calculate the minimum detectable leak volume (L) using the equation below.
2 2Qc(X1max−X1min )
L= (X1max−X1min ) = (Pa・m3/sec)
S X2−X1
(e) Measurement of time constant
X2-X1
Output
τ
37% of (X2-X1)
X2
X1
29
(XP−X1)
QT =
S
Xp : Value of the helium leak detector at the test
X1 : Value of the helium leak detector with the background level (Output)
S : Detection sensitivity
Open
Discharge the helium gas within the work and open the vacuum vessel (bell jar) to the atmosphere.
Post-processing
Perform the necessary post-processing.
Judgment
Judge the result according to the inspection standard or specification. Use 1 x 10-7 Pa・m3 /sec unless other
wise noted.
By combining the differential pressure detection leak test and the helium gas detection leak test,
an ideal measurement environment can be configured.
30
2.5 FLOW RATE LEAK TEST
2.5.1 Operating Principle
There are two major flow meter types for air (gas), a volume flow meter and mass flow meter.
The volume flow meter includes a differential pressure flow meter (laminar flow meter), variable
area flow meter, and volumetric flow meter, and the mass flow meter includes a thermal mass
flow meter (mass flow meter) and vortex flow meter.
The volume flow rate is expressed by volumetric displacement per unit time (l/min) and the
mass flow rate is expressed by mass displacement per unit time (g/min). However, they are
generally expressed by a volume flow rate unit at a certain condition where reference pressure and
temperature are specified in pursuant to typical flow rate measurements nowadays.
Among volume flow meters, the laminar flow meter has a characteristic that the pressure loss
⊿P is proportional to the flow rate Q when the flow in the pipe is a laminar flow.
128µL 32µL
⊿P= Q= U
4
pd d2
⊿P : Pressure Difference L
µ : Viscosity Coefficient
L : Length of Pipe
d : Diameter of Pipe
Q : Flow Rate
U : Average Flow Velocity of Fluid Pressure Difference ⊿P
Fig. 2.36 Principle of Differential Pressure Flow meter
A laminar element has a structure such that many capillary tubes are bundled along a flow path,
and fluid passes through each capillary tube. Since the d of it is small, the Reynolds number is
extremely small.
The pressure difference ⊿P (pressure drop) of an actual laminar element is expressed as the sum
of the pressure drops, ⊿P1 and ⊿P2 , when the flow in it is assumed as a Poiseuille flow over the
entire length.
32µL V2
⊿P=⊿P1+⊿P2= U+Kr ⊿P1 ⊿P2
d2 2g
Capillary Tube
Kr: Loss Coefficient at the End of Capillary Tube
In order to keep the linearity of the pressure difference
⊿P against the flow rate, the value of the following
⊿P
equation must be small enough.
Fig. 2.37 Principle of Laminar Flow meter
⊿P1 k d
= Re =
⊿P2 64 L
The FUKUDA Laminar Flow meter is designed to keep the linearity up to twice the rated flow.
The typical flow rate sensor used in a mass flow meter is a thermal mass flow rate sensor.
On the capillary tubes that work as a sensor, resistive
elements with a high resistance temperature coefficient
are attached at the upstream (Rus) and downstream
(Rds) of the tube. When electric currents are applied to
the elements, they generate heats. The temperatures of Rus Rds
these elements are same when there is no flow in the
pipe. If the fluid begins to flow in the pipe under this Flow
condition, the upstream element is deprived of heat by
the fluid and the down stream element receives the heat.
A temperature difference ⊿T occurs between the
upstream element and downstream element, and the Fig. 2.38 Principle of Thermal Mass Flow meter
temperature difference ⊿T has a functional relationship
with the mass flow rate of the fluid. Therefore, the mass flow rate is measured by the changes of
the resistances of electric signals, and then by amplifying and correcting them.
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2.5.2 Basic Operation
(1) Flow meter (at Atmospheric Pressure)
In the atmospheric pressure method, the
work is positioned at the air pressure
source side and the laminar at the
atmospheric pressure side.
Work The test pressure is supplied to the work
and the leaked air passes through the
laminar and it is exhausted into the
atmosphere.
The flow rate can be obtained by
multiplying the pressure difference at the
laminar by the laminar coefficient.The
Fig. 2.39 Mass Flow meter at Atmospheric Pressure same laminar coefficient can be used
when the test pressure is changed.
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2.5.4 Applied Measurement Method
The basic methods of gas flow rate have been described in the BASIC OPERATION section
above, the methods to improve the measurement performance are stated here.
When a flow rate measurement is conducted using a volume flow meter (laminar flow meter, *
hereinafter referred to as laminar) or mass flow meter, the flow velocity in the pipe is extremely
low if the estimated effective sectional area is extremely small. In such a case, it is necessary to
take a substantially long measurement time to perform a proper flow rate measurement, because
the flow velocity in the pipe is extremely low.
There is a method to improve the measurement performance by using a pressurization bypass to
reduce the measurement time as short as possible.
Work
As shown in Fig. 2.41, by using a method to achieve the specified pressure in the work with
holes whose flow rate is very low by the use of a circuit without the work, the area with a slow
flow rate is practically limited to the holes of the work and this leads to the reduction of
measurement time.
When a flow rate is measured with a laminar flow meter or mass flow meter, a regulator is used
to adjust a pressure to the specified pressure. Since the regulator adjusts the pressure while
supplying a flow to compensate the pressure loss of the work in the secondary side, a normal
regulator can not maintain the specified pressure because of its structure.
When the specified pressure can not be maintained, this causes the failure to obtain stable flow
rate measurement results.
In such a case, the above mentioned problem can be solved by the use of an electropneumatic
regulator (we call this an APU) which always supplies the specified pressure even if the pressure
loss of the work varies. (The APU theory will be explained in Chapter 3.)
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Chapter 3
Peripheral Equipment
34
3.1 EXHAUST BYPASS UNIT
OUTLINE
The exhaust bypass unit is used when foreign materials such as water, oil, or swarf attaches to
or mixes into the works. Since the pressurized air charged FE-20
within the pass through the air leak tester (here after referred
to as ALT) when it is exhausted, these materials may enter
into the inside of the ALT. If they enter into the inside of the
ALT, it may cause the malfunction of the internal solenoid
valve or the failure of the differential pressure sensor.
Therefore, these troubles shall be prevented by using the
exhaust bypass as it lets the pressurized air within the work
directly exhaust through it, without passing through the
inside of the ALT.
・ The use of the exhaust bypass is recommended when foreign materials attach to or mix
within the works.
・ By using the exhaust bypass unit, the causes which may lead to the failure of the ALT will
be reduced and stable measurement results can be obtained.
There is also the pressurization & exhaust bypass unit which has the pressurizing bypass function
in addition to the exhaust bypass function.
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3.3 FLOW MASTER
OUTLINE
The flow master is a flow rate device which can maintain FFM-100
a constant flow rate by applying a specified pressure. It has a
glass capillary tube in the body. It generates a constant flow
rate at a specified pressure by adjusting the length and
diameter of the glass capillary tube.
By using the flow master, the daily checks of the ALT’s
function and accuracy with actual leaks can be conducted
easily. The OK/NG judgment condition for leak testing can
be set by using the flo w master in combination with a work
as a leak master. It is also capable of measuring the internal volume of a work when used with a
differential pressure type ALT.
3.4 CALIBRATOR
OUTLINE
The calibrator changes its internal volume when the scale
dial is rotated.
By using it in combination with a differential pressure type
ALT, the sensitivity check of ALTs and the internal volume
measurement of works can be conducted by measuring the
resultant pressure difference due to a volume change.
36
3.5 SUPER ELECTROPNEUMATIC REGULATOR (APU)
OUTLINE
37
Chapter 4
Information about
Equipment
38
4.1 MANAGEMET OF WATER, OIL AND FOREIGN MATERIALS
When using the air leak testers, it is most important to correctly manage the water, oil and
foreign materials mixed into the air used for testing. This is because they may have various
harmful effects and cause a failure, if they enter into the inside of air leak testers.
Fig. 4.1 Failure Causes Fig. 4.2 Details of the Source of Foreign
As shown in Fig. 4.1, 66% of the failures caused are due to foreign materials. According to the
survey on the detail of the main cause, 74% of mix is due to primary pressure and 26% due to
works as shown in Fig. 4.2. Installation of a filter set (air filter and mist separator) just before an
air leak tester is recommended to prevent the mix of foreign materials from the primary pressure.
Capacity of Filter Set to be Installed (Flow rate shall be selected according to the product)
39
One of the failure causes of the products is the suction of foreign materials from the work
during exhaust. Installing an external exhaust unit (charge external exhaust unit) is recommended
to prevent the suction of foreign materials.
Table 4.2 Primary Pressure Management Range for Each Measurement Range
Measurement
Range Control Range Primary Pressure
V -5 - -90kPa Direct supply from vacuum pump
UL 0 - 20kPa 50kPa
L 10 – 99kPa 100 – 200kPa
M 50 – 700kPa 100 – 900kPa
H 300 – 990MPa Set Pressure + 30%
H1 0.5 - 2.0MPa Set Pressure + 30%
H2 1.0 - 4.0MPa Set Pressure + 30%
40
4.3 CLAMPING AND SEALING JIG
Clamping and sealing are the absolute requirements for leak testing. Since shape and test
pressure depend on each work, appropriate clamping pressure and seal method are required for
the work.
4.3.1 Clamping
Clamping pressure is expressed as follows: Cylinder diameter x Air (Oil) pressure = (Seal area x
test pressure + Crush force of rubber seal) x Factor for stabilization.
The factor for the stabilization of clamping depends on the seal conditions such as surface
roughness, rubber hardness, etc (the normal ratio of maximum value to minimum is 2).
O-ring Sealing
There is almost no
Work Work volume change due to a
metal contact condition
between the work and
sealing jig.
O-ring ゙
O-ring Sealing Jig Sealing Jig
* The O-ring may come away during unclamping, so take an appropriate preventive measure such as dovetail groove.
Fig. 4.5 Seal Method (O-ring Sealing)
Sealing Jig
Sealing Jig Urethane Rubber
Urethane Rubber
* By covering the side surface of the rubber, the deformation during sealing can be reduced.
41
Urethane Rubber Seal with Core Cylinder Since the deformation of the
seal is restrained and the
change of internal volume
decreases, the measurement
accuracy is improved.
Core Cylinder
Core Cylinder
Urethane Rubber
Urethane Rubber Sealing Jig Sealing Jig
Fig. 4.7 Seal Method (Urethane Rubber Sealing with Core Cylinder)
1) Utilization of core
Core
2) Selection of piping
In leak testing, the volume of the piping is added to the volume of a work. Therefore, use piping
as short as possible and increase the detection sensitivity.
42
4.4 CHANGE IN TEMPERATURE
When the temperature change of the sealed work occurs, the pressure of it also changes and the
measurement becomes unstable.
Sources of heat
・ Solenoid valves
・ Change of ambient temperature (air conditioning etc.)
Measures
・ Use pneumatic valves instead of solenoid valves.
・ Enclose the test equipment with a acrylic box
・ Wrap the piping with spiral tubes etc.
43