Beruflich Dokumente
Kultur Dokumente
Date of experiment
Researcher
Technician
Safety Officer
Data Analyst
Introduction
Objective
In this experiment, you will investigate two titration curves for the acid-base
reaction outlined in Part A and B. Using the titration curves obtained, you are
going to determine the concentration of acids and also confirm the weak acid
used in Part B is acetic acid. .
Hypothesis
…………………………………………………………………………………………..
…………………………………………………………………………………………..
…………………………………………………………………………………………..
…………………………………………………………………………………………..
…………………………………………………………………………………………..
…………………………………………………………………………………………..
…………………………………………………………………………………………..
Reference :…………………………………………………………………………….
…………………………………………………………………………………………..
Experimental Procedure
Take great care of the electrode – It is damaged by caustic alkalis. Wash the
electrode system immediately after each titration and allow to stand in a
beaker of deionised water.
Safety Precaution:
Please refer to MSDS of the following chemicals for the risk/hazard
identification. Specify precautions.
Chemical Risk/Hazard Precaution
HNO3
CH3COOH
NaOH
Data
0.00 88.00
5.00 89.00
10.00 90.00
15.00 91.00
20.00 92.00
25.00 93.00
30.00 94.00
35.00 95.00
40.00 96.00
45.00 97.00
50.00 98.00
55.00 99.00
60.00 100.00
65.00 105.00
70.00 110.00
75.00 115.00
77.00 120.00
79.00 125.00
81.00 130.00
83.00 135.00
85.00 140.00
86.00 145.00
87.00 150.00
A. Weak acid-Strong Base Titration: Titration of acetic acid with the
standardised sodium hydroxide.
1) From your graphs, estimate the equivalence point from the region
where pH changes rapidly with titre (show on the graph)
a. HNO3 solution
b. HAc solution
3) From titration curve obtained in Part B, find the pK a value of acetic acid.
Compare this value with the pKa of acetic acid in data book.
Discussion
Design an experiment:
Devise a plan using similar apparatus and reagent provided in this experiment
to determine the pKa of phosphoric acid in coca-cola beverage.
Apparatus& Reagents Required