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WHAT TO DO
Before Lab: Read this experiment and read Gilbert, Chapter 17-8, pages 868-878.
Set up your lab notebook appropriately for this experiment including a title bar, a
summary table, and the Reagent Table with the following reagents:
Nickel(II) nitrate, Ni(NO3)2•6H2O
Copper(II) sulfate, CuSO4 •5H2O
Cobalt(II) chloride, CoCl2 •6H2O
Sodium glycinate, Na+NH2CH2CO2-
Potassium oxalate, K2C2O4
Pyridine, C5H5N
1,2-diaminoethane, H2NCH2CH2NH2
sodium ethylenediaminetetraacetate, (Na+)4[(-O2CCH2)2NCH2CH2N(CH2CO2-)2]
ammonia, NH3
BE SURE TO NOTE THE DISPOSAL PROCEDURES IN YOUR TABLE.
Prepare the following table in your notebook before coming to lab. This table
should be one full page, landscape-format, in your notebook.
Table 1: Summary of data for the Transition Metal complexes of ___________
Ligand H2O NH2CH2CO2- C2O42- NH3 C5H5N EDTA H2NCH2CH2NH2
Color of TM complex
Wavelength(s) λ, nm
Energy, cm-1
Δo
f factor
During the Lab: Carry out the procedure as written. Enter all relevant
observations and data directly into your laboratory notebook. Complete your
calculations and provide at least one set of sample calculations. Clearly and
completely answer each question.
Complete the class data table and prepare for the lab discussion.
To be Turned In To Your Lecture Professor on Monday, May 3, 2010: All the
copy pages associated with this lab including at least the completed summary table, a
sample set of calculations, observations, and the complete answers to the questions.