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Hach Company, 2001, 2002, 2004. All rights reserved. Printed in the U.S.A. ce/dk 04 February 2005 Edition 4
Table of Contents
Safety Precautions .................................................................................................................................................... 4 Specifications ............................................................................................................................................................ 5
Installation ........................................................................................................................................................... 11 Section 2 Installation......................................................................................................................................... 13 2.1 Selecting a Location for the APA 6000 Analyzer ............................................................................................... 13 2.2 Mounting ........................................................................................................................................................... 13 2.2.1 Bench Mount ........................................................................................................................................... 14 2.2.2 Wall Mount............................................................................................................................................... 14 2.3 Electrical Connections ...................................................................................................................................... 15 2.3.1 Power Connections at the Analyzer......................................................................................................... 16 2.3.2 Alarm Relay Connections ........................................................................................................................ 20 2.3.3 Recorder Output Connections ................................................................................................................. 21 2.4 Plumbing Installation ......................................................................................................................................... 22 2.4.1 Sample Line Installation .......................................................................................................................... 23 2.4.1.1 Sample Conditioning................................................................................................................... 24 2.4.2 Drain Line Connection ............................................................................................................................. 25 2.4.2.1 Waste Disposal ........................................................................................................................... 26 2.5 Air Purge ........................................................................................................................................................... 26 Startup .................................................................................................................................................................. 27 Section 3 Startup ............................................................................................................................................... 29 3.1 Introduction ....................................................................................................................................................... 29 3.2 Preparing Sample Conditioning and Starting Sample Flow .............................................................................. 29 3.3 Installing Reagents and Standards ................................................................................................................... 29 3.3.1 Supplying Power ...................................................................................................................................... 30 3.3.2 Priming the Analyzer ............................................................................................................................... 31 Section 4 Instrument Menus ........................................................................................................................... 33 4.1 The AquaTrend Interface................................................................................................................................... 33 4.1.1 The AquaTrend Interface Keypad ............................................................................................................ 33 4.1.2 The AquaTrend Interface Display ............................................................................................................ 34 4.2 Menu Functions................................................................................................................................................. 37 4.2.1 Alarm Log ................................................................................................................................................ 37 4.2.2 AquaTrend Menu ..................................................................................................................................... 37 4.2.2.1 Display Setup.............................................................................................................................. 37 4.2.2.2 Language .................................................................................................................................... 40 4.2.2.3 Edit Name ................................................................................................................................... 40 4.2.2.4 Set Time/Date ............................................................................................................................. 41 4.2.2.5 Security Setup ............................................................................................................................ 42 4.2.3 Sensor Menu ........................................................................................................................................... 44 4.2.3.1 Calibration................................................................................................................................... 44 4.2.3.2 Alarm Setup ................................................................................................................................ 47 4.2.3.3 Recorder Setup........................................................................................................................... 48 4.2.3.4 Measurement Options ................................................................................................................ 50
Page 2 Table of Contents
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Table of Contents
4.2.3.5 Enabling Solution Level Monitoring ............................................................................................ 51 4.2.3.6 Setting Solution Levels ............................................................................................................... 51 4.2.3.7 Solutions & Cleaning Options ..................................................................................................... 52 4.2.3.8 Sensor Diagnostics ..................................................................................................................... 52 4.3 Other Device Menu and Network Menu ............................................................................................................ 55 4.4 Data Display...................................................................................................................................................... 55 4.4.1 Numerical Display.................................................................................................................................... 55
Maintenance ........................................................................................................................................................ 57 Section 5 Maintenance and Troubleshooting ............................................................................................. 59 5.1 Maintenance ..................................................................................................................................................... 59 5.1.1 Shutting the Analyzer Down (Off or Standby).......................................................................................... 59 5.1.2 Scheduled Maintenance .......................................................................................................................... 59 5.1.2.1 Cleaning the Instrument.............................................................................................................. 60 5.1.2.2 Sample Conditioning................................................................................................................... 60 5.1.2.3 Changing Modules ...................................................................................................................... 62 5.1.2.4 Changing Tubing ........................................................................................................................ 63 5.1.2.5 Rotary Valve Module .................................................................................................................. 65 5.1.2.6 Maintaining the Autoburette Module ........................................................................................... 68 5.1.2.7 Greasing the Lead Screw in the Autoburette Module ................................................................. 70 5.1.3 Unscheduled Maintenance ...................................................................................................................... 71 5.1.3.1 Fuse Replacement...................................................................................................................... 71 5.1.3.2 Cleaning the Mixer Module Chamber ......................................................................................... 74 5.2 Troubleshooting................................................................................................................................................. 75 5.2.1 General Troubleshooting Procedure ........................................................................................................ 75 5.2.1.1 Check Alarm Log ........................................................................................................................ 75 5.2.1.2 Check Solutions .......................................................................................................................... 75 5.2.2 Examine the Rotary Valve ....................................................................................................................... 76 5.2.3 Examine the Autoburette ......................................................................................................................... 76 5.2.4 Examine the Tubing and Fittings ............................................................................................................. 76 5.2.5 Back Pressure Gauge ............................................................................................................................. 76 5.3 Specific Alarm/Warning Messages ................................................................................................................... 77 Appendix A Network Connections....................................................................................................................... 81
Network Connections in the APA 6000 Analyzer.......................................................................................... 81
General Information........................................................................................................................................... 93
Replacement Parts and Accessories ...................................................................................................................... 94 How to Order........................................................................................................................................................... 96 Repair Service ........................................................................................................................................................ 97 Limited Warranty ..................................................................................................................................................... 98 Certification ............................................................................................................................................................. 99
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Safety Precautions
Section 2.3 Electrical Connections on page 15 Section 2.3.1 Power Connections at the Analyzer on page 16 Section 2.3.2 Alarm Relay Connections on page 20 Section 2.3.3 Recorder Output Connections on page 21 Section 2.4 Plumbing Installation on page 22 Section 3.3 Installing Reagents and Standards on page 29 Section 5.1.2.3 Changing Modules on page 62 Section 5.1.2.4 Changing Tubing on page 63 Section 5.1.2.6 Maintaining the Autoburette Module on page 68 Section 5.1.3.1 Fuse Replacement on page 71
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Specifications
Specifications are subject to change without notice. Specifications for range, accuracy, repeatability, response time, cycle time, detection limit, and other parameter specific items are listed in the parameter-specific manual.
Performance
Recorder Outputs: Two isolated, 420 mA outputs standard. Output span programmable over any portion of the range (500 V isolation from earth ground). Alarms: 14 programmable internal alarms Relays: Two SPDT relays with a maximum contact rating of 5 A resistive load at 240 V ac. Additional relays available through optional Signal Output Module. Power Requirements: 95240 V ac, 50 or 60 2 Hz, 150 VA Installation Category: II Sample Inputs: Two sample streams (with optional hardware) Maximum Operating Temperature Range: 5 to 50 C (41 to 122 F) Relative Humidity: 5 to 95% relative humidity, non-condensing Network Interface: LonWorks FTT-10 twisted-pair free topology Maximum Node-to-node Distance: 400 meters (1320 feet)
Features
Instrument Enclosure: NEMA 4X (Indoor) and IEC 529 (IP 66) with provision for air purge Instrument Installation Category: II Reagent Enclosure: Fully enclosed latch cases with protected ducting for instrument drain; additional plumbing connections for instrument case and reagent enclosure overflow drains.
Sample Requirements
Sample Filtration: 0.5 m or smaller. Sample Pressure: 0.5 to 30 psig (0.035 to 2 bar) maximum at sample inlet block Sample Temperature: 5 to 50 C (41 to 122 F) Sample Flow: 1000 to 2000 mL/min.
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Page 5 Specifications
Section 1
Introduction
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Page 7 Introduction
Section 1
1.2.1 Components
The AquaTrend Interface The APA 6000 Process Analyzer has an AquaTrend Interface built into the instrument door. It provides a numerical or graphical display and a keypad for user input. The AquaTrend Interface displays, graphs, and logs sensor readings, and is used for operator control and sensor setup. Autoburette Module The analyzer uses a positive-displacement autoburette to measure fluids through the various analytical components in the instrument. The autoburette module consists of a clear acrylic block which houses a ceramic piston, a double seal for the piston, a linear actuator, a two-way solenoid valve, and control circuitry. Detector Module Samples are measured in a temperature controlled flow cell detector. All detector modules contain a holding coil. The holding coil acts as a storage area for fluids as they are drawn into the instrument before being directed to the appropriate module for mixing or sensor readings. The detector module for some instruments also contains a reaction coil. The reaction coil optimizes the dispersion utilized in some analysis methods. Valve Module The valve module directs fluids to various components in the instrument. Mixer Module The mixer module mixes reagents with the sample or standards. The mixing action also removes excess air from the sample.
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Section 1
Step One The burette draws sample into the Holding Coil. 10-Port Rotary Valve Reaction Coil
Detector
Holding Coil
Mixer Drain
Filtered Sample IN Reagent IN 10-Port Rotary Valve Mixing Chamber Reaction Coil Waste
Step Two The burette draws reagent into the Holding Coil.
Detector
Holding Coil
Mixer Drain
Filtered Sample IN Reagent IN Step Three The burette moves sample and reagent into the Mixing Chamber. 10-Port Rotary Valve Mixing Chamber Reaction Coil Waste
Detector
Holding Coil
Mixer Drain
Filtered Sample IN Reagent IN Step Four The burette draws the sample/reagent mixture into the Holding Coil. 10-Port Rotary Valve Mixing Chamber Reaction Coil Waste
Detector
Holding Coil
Mixer Drain
Filtered Sample IN Reagent IN Step Five The burette moves the sample/reagent mixture through the Reaction Coil and the Detector and measures the response of the Detector. Mixing Chamber Waste
Reaction Coil
Detector
Holding Coil
Mixer Drain
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Installation
DANGER
Some of the following manual sections contain information in the form of warnings, cautions and notes that require special attention. Read and follow these instructions carefully to avoid personal injury and damage to the instrument. Only personnel qualified to do so, should conduct the installation/maintenance tasks described in this portion of the manual.
DANGER
Certains des chapitres suivants de ce mode demploi contiennent des informations sous la forme davertissements, messages de prudence et notes qui demandent une attention particulire. Lire et suivre ces instructions attentivement pour viter les risques de blessures des personnes et de dtrioration de lappareil. Les tches dinstallation et dentretien dcrites dans cette partie du mode demploi doivent tre seulement effectues par le personnel qualifi pour le faire.
PELIGRO
Algunos de los captulos del manual que presentamos contienen informacin muy importante en forma de alertas, notas y precauciones a tomar. Lea y siga cuidadosamente estas instrucciones a fin de evitar accidentes personales y daos al instrumento. Las tareas de instalacin y mantenimiento descritas en la presente seccin debern ser efectuadas nicamente por personas debidamente cualificadas.
GEFAHR
Einige der folgenden Abschnitte dieses Handbuchs enthalten Informationen in Form von Warnungen, Vorsichtsmanahmen oder Anmerkungen, die besonders beachtet werden mssen. Lesen und befolgen Sie diese Instruktionen aufmerksam, um Verletzungen von Personen oder Schden am Gert zu vermeiden. In diesem Abschnitt beschriebene Installations- und Wartungsaufgaben drfen nur von qualifiziertem Personal durchgefhrt werden.
PERICOLO
Alcune parti di questo manuale contengono informazioni sotto forma davvertimenti, di precauzioni e di osservazioni le quali richiedono una particolare attenzione. La preghiamo di leggere attentivamente e di rispettare quelle istruzioni per evitare ogni ferita corporale e danneggiamento della macchina. Solo gli operatori qualificati per luso di questa macchina sono autorizzati ad effettuare le operazioni di manutenzione descritte in questa parte del manuale.
Page 11 Installation
Section 2
Installation
2.2 Mounting
An installation kit (Cat. No. 51040-00) is supplied with the instrument. The kit includes: Grab sample kit (Cat. No. 62037-00) Four 0.5 micron filters (Cat. No. 62011-00) 20 ft. of -in. poly tubing (Cat. No. 47438-00)
Page 13 Installation
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Section 2
2.2.1 Bench Mount
Important Note: The analyzer must be bolted to the bench.
Secure the rear of the instrument to the bench or table with two -20 UNC screws through the holes in the metal frame on the back of the instrument (see Figure 3). This will prevent the instrument from tipping while the module panel is open.
Page 14 Mounting
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Section 2
2.3 Electrical Connections
DANGER All electrical connections should be made by a qualified technician to assure compliance to all applicable electrical codes. DANGER Tous les branchements lectriques doivent tre effectus par un technicien qualifi pour assurer la conformit toutes les normes lectriques applicables. PERIGO Todas las conexiones elctricas deben ser ubstaladas por personal tcbico cualificado a fin de asegurar su conformidad con las normas elctricas vigentes. GEFAHR Alle elektischen Anschlsse mssen van qualifizierten Techniekem durchgefhrt werden, damit die bereinstimmung mit allen elektrischen Anschlussdaten gewrhrleistet ist. PERICOLO Tutte le connessioni elettriche devono essere fatte da un tecnico qualificato.
To access electrical connections in the APA 6000 instrument, remove the two hold-down fasteners in the upper corners of the module panel. Slowly pull the panel forward until it is fully supported by the steel restraining cable (see Figure 4 and Figure 5). Four access holes for electrical connections are provided along the back of the instrument enclosure (see Figure 6). Remove the cover seals by loosening the wing nuts from inside the instrument. This product is designed to meet NEMA 4X (INDOOR) and IEC 529 IP 66 enclosure requirement when the front door is securely latched. Achieving these protection levels, however, depends on the use of proper hardware in the installation of this product. Standard off-the-shelf NEMA-approved conduit hardware is required for proper installation of all electrical connections. For process or industrial applications, the national electrical codes of most countries require that ac service feeds be hard-wired and contained in conduit systems. The APA 6000 Analyzer has been designed to conform to this requirement. Hach recommends conduit for two reasons: 1. It is generally required by most local electrical codes, and 2. use of metal conduit can improve immunity to lightning surges and ac power transients. In hard-wired electrical applications, the power and safety ground service drops for the analyzer should be no longer than 6 meters (20 feet) unless metal conduit is used to shield the ac power wiring. In applications where power cords are allowed by local electrical codes and power surges and transients are not a great concern, an 18-gauge, 3-conductor power cord (including a safety ground wire) can be used, but its length must not exceed 3 meters (10 feet). The power cord or power cable is not supplied with the APA 6000 Analyzer and must be selected to meet applicable electrical codes for the installation site.
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Section 2
Hach recommends that care be taken with hook-up configurations other than shown in these illustrations. First, be sure your configuration satisfies local electrical codes and second, ensure that your configuration does not cause susceptibility to lightning, power surges, or transients upsets.
2.3.1
Note: Be sure the analyzer power switch is turned off. Dry operation may damage the analyzer.
Route the power leads through the access hole on the back of the enclosure. Line voltage connections are wired directly to the terminal strip J10 (see Figure 6 and Figure 7). Make the ground connection to the adjacent ground stud using an appropriate closed loop connector (see Table 1). Table 1 Wiring Color Codes
Connector hot line conductor 01 neutral conductor 02 ground conductor (#8 stud)
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Section 2
Figure 4 Looking Inside the APA 6000 Analyzer, with Hinged Module Panel Down
Figure 5
Looking Inside the APA 6000 Analyzer, Removing the Customer Access Cover
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Section 2
Figure 6 Looking Inside the APA 6000 Analyzer, Locating and Identifying the Customer Connections
Air Purge
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Section 2
Figure 7 Wiring Options
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Section 2
2.3.2 Alarm Relay Connections
DANGER La zone de raccordement des relais est conue pour des connexions soit tout en basse tension (<30 V) soit tout en haute tension (>30 V). Un risque dlectrocution existe si des connexions basse et haute tension sont faites dans la zone de raccordement des relais. PELIGRO El rea de conexin de los rels esta diseada para conexiones que sean todas de baja tensin (inferior a 30V o bien todas de alta tensin (superior a 30V). Existe riesgo de descargas si se combinan conexiones de alto y bajo voltaje en el rea de conexin de los rels. GEFAHR Die Ralaisanschlsse sind entweder fr Niederspannung (< 30V) oder fr Hochspannung (>30 V) vorgesehen. Wenn sowohl Nieder-als auch Hochspannung an die Relais angeschlossen wird, kann es zu einem Stromschlag kommen. PERICOLO La zona riservata ai contatti di allarme disegnata per bassi voltaggi (<30 V) e alti voltaggi (> 30V). Assolutamente non confondersi nell'utilizzo dei bassi e degli alti voltaggi. Note: Limit current to the relay contacts to 5 amps. This can be accomplished with an external switch and a 5-amp fuse or with a switched 5-amp circuit breaker. You must be able to remove power from the relays locally in case of an emergency or for servicing of the product.
DANGER The relay connection area is designed for either all low voltage (<30 V) or all high voltage (>30 V) connections. A shock hazard exists if low and high voltage connections occur simultaneously in the relay connection area.
The analyzer contains two alarm relays designed for use with either high voltage (greater than 30 V-RMS and 42.2 V-PEAK or 60 V dc) or low voltage (less than 30 V-RMS and 42.2 V-PEAK, or less than 60 V dc), but not a combination of both high and low voltage. Wire alarm relays to the connectors labeled Alarm A or Alarm B on the back electrical panel (see Figure 8). For terminal strip and strain relief locations see Figure 6. SPDT relay contacts are unpowered and rated to carry up to 5 amperes at 240 V ac with a resistive load. If high-current or inductive-load devices are to be controlled by analyzer alarms, use a heavy-duty slave relay actuated by the alarm relay. Both normally open and normally closed contacts are available. The connector will accept 22- to 12-gauge wire, insulated as appropriate for the voltage. Size the wires according to the load and local electrical code regulations. If more relays are desired, supplement your system with the AquaTrend Signal Output Module (SOM) (Cat. No. 51250-00). Each SOM provides two additional relays.
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Section 2
Figure 8 Alarm Relay Connections
2.3.3
DANGER Facility power systems may have ground potentials if poor grounding techniques have been used. To reduce the chance of shock hazards, care must be taken when connecting equipment grounded at different locations (potentials). Carefully follow the instructions given in this section.
The analyzer contains two isolated 420 mA analog outputs which can drive a recorder or control a process (see Figure 9). Recommended output impedance is 3.6 to 500 ohms. Route 22-to 12-gauge recorder wires through the access hole below the terminal strip and connect them to the terminal
Page 21 Electrical Connections
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Section 2
strip J8, labelled Recorder (see Figure 6). Use shielded, twisted-pair cable to connect the analyzer to the recorder. Tie the shield to earth ground only at the analyzer end to avoid ground loops. To ensure the analyzer meets NEMA 4X and IP 66 enclosure ratings, use only NEMA-style enclosure strain relief fittings. If more analog outputs are desired, you can supplement your system with the AquaTrend Signal Output Module (SOM). Each SOM provides two additional analog outputs. Figure 9 APA to Recorder Connections
2.4
Plumbing Installation
The nature of tasks described in this section requires individuals to understand the associated dangers. Please read all caution statements in the left-hand column of this section before installing the instrument. Burns, shock, eye injury, fire, and chemical exposure may occur. Hach Company assumes individuals performing these tasks are qualified and aware of proper safety procedures.
CAUTION This instrument is not intended for use with flammable samples or those containing hydrocarbons.
PRUDENCE Cet instrument nest pas conu pour une utilisation avec des chantillons inflammables ou des chantillons contenant des hydrocarbures. CUIDADO Este instrumento no est destinado para uso con muestras inflamables o que contengan hidrocarburos. VORSICHT Dieses Gert darf nicht fr Tests mit brennbaren Proben oder Proben, die Kohlenwasserstoffe enthalten, benutzt werden. ATTENZIONE Questo strumento non utilizzabile con campioni infiammabili o contenenti idrocarburi.
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Section 2
DANGER This instrument should be installed by qualified technical personnel to ensure adherence to all applicable electrical and plumbing codes. DANGER Cet appareil doit tre install par du personnel technique qualifi, afin dassurer le respect de toutes les normes applicables dlectricit et de plomberie. PELIGRO Este instrumento debe ser instalado por personal tcnico capacitado para assegurar el cumplimiento con todos los cdigos elctricos y de plomera aplicables. GEFAHR Um zu gewhrleisten, da alle elektrischen und sanitrinstallationstechnischen VDE-Vorschriften und gegebenefalls die Zusatzvorschriften der zustndigen Elektrizitts- und Wasserwerke erfllt werden, darf dieses Gert nur von geschultem Fachpersonal installiert werden. PERICOLO La strumentazione deve essere installata da personale qualificato, sia per le connessioni elettriche sia per quelle idrauliche.
Run sample lines with small diameter tubing to the analyzer to minimize lag time (the time required for sample to flow from sample point to the analyzer). Route the tubing as directly as possible between the sampling point and the analyzer. Long sample lines and low flow rates result in significant lag time between actual process line conditions and the sampling point of the instrument. Install sample line taps into larger process pipes to minimize the chances of ingesting sediment from the pipe line bottom or air bubbles from the top. A tap projecting into the center of the pipe is ideal (see Figure 10).
Poor
Poor
Good
Best
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Section 2
New tubing, valves and other sample conditioning equipment may be contaminated with substances (oils, dust, etc.) which may contribute to low or high readings on initial startup. Flush the sample line with sample for 12 hours before calibration. For faster cleaning, plumb the sample line to a container of 14 liters of a dilute caustic solution such as 1 N (5%) sodium hydroxide solution and cycle it through to clean sample system components. When the solution is depleted, connect the sample line to the sample source and run the analyzer for an hour to purge the sodium hydroxide solution.
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Section 2
Figure 11 Location of the Sample Conditioning Block
Vent
Drain
Unfiltered Sample In Remove these two screws to take off the Sample Conditioning Block. Filtered sample into instrument.
The analyzer is connected to a drain system through a -inch hose barb fitting on a drain block on the right side of the analyzer case (see Figure 12). After analysis, the waste exits the instrument through the manifold at the bottom of the instrument and into the drain block. This block connects to a -inch ID hose and provides a vented vacuum break at this point. A vent is located on the top of the drain block. Also see section 2.4.2.1. Route instrument waste through a -in. ID hose to a PVC pipe assembly, which must be located one foot below the level of the instrument drain block. The catastrophic drain is located in the middle of the tubing manifold and is sized to accommodate a 1-in. ID hose. This drain is used if an upset inside the instrument results in a significant leak. The supplied hose from this drain port must be connected and run to a drain which is one foot below the bottom of the instrument. The reagent enclosures each have an overflow fitting in the bottom of the case. Plumb these to the drain by punching out the knock-out in the fitting, attaching a 3/8-inch ID hose to each fitting and running it to a drain which is one foot lower in elevation than the bottom of the instrument.
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Section 2
Figure 12 Drain Line Connection
Drain Block
All drains must be at least one foot below the bottom of the instrument.
Drain from Instrument Drain Block (Customer supplied 3/4 inch tubing.) From Catastrophic Drain
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Startup
DANGER
Handling chemical samples, standards, and reagents can be dangerous. Review the necessary Material Safety Data Sheets and become familiar with all safety procedures before handling any chemicals.
DANGER
La manipulation des chantillons chimiques, talons et ractifs peut tre dangereuse. Lire les Fiches de Donnes de Scurit des Produits (FDSP) et se familiariser avec toutes les procdures de scurit avant de manipuler tous les produits chimiques.
PELIGRO
La manipulacin de muestras qumicas, estndares y reactivos puede ser peligrosa. Revise las fichas de seguridad de materiales y familiarcese con los procedimientos de seguridad antes de manipular productos qumicos.
GEFAHR
Das Arbeiten mit chemischen Proben, Standards und Reagenzien ist mit Gefahren verbunden. Es wird dem Benutzer dieser Produkte empfohlen, sich vor der Arbeit mit sicheren Verfahrensweisen und dem richtigen Gebrauch der Chemikalien vertraut zu machen und alle entsprechenden Materialsicherheitsdatenbltter aufmerksam zu lesen.
PERICOLO
La manipolazione di campioni, standard e reattivi chimici pu essere pericolosa. La preghiamo di prendere conoscenza delle Schede Techniche necessarie legate alla Sicurezza dei Materiali e di abituarsi con tutte le procedure di sicurezza prima di manipolare ogni prodotto chimico.
Page 27 Startup
Section 3
3.1 Introduction
Startup
It is assumed that the analyzer has already been plumbed to the sample source and a drain, as well as wired to a power source and any other electrical wiring associated with 420 mA connections, relay connections, and network connections by the installation technician as outlined in Section 2. This section presents the steps, in sequence, an operator should take to begin operation. This section will: describe how to prepare the sample conditioning describe the steps to install the reagents and standards list the steps required to prime the sample lines and reagents.
3.3
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Page 29 Startup
Section 3
5. Place the new bottle in the reagent compartment. Hach recommends changing all the solutions at the same time and does not recommend adding fresh reagent to fill a partially full bottle.
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Section 3
3.3.2 Priming the Analyzer
Note: Do not allow the instrument to run before installing reagents and standards and providing sample.
After internal checks, the analyzer will begin operation. It is important to prime the analyzer because operating without fluid may damage components. Priming the analyzer ensures that the standards and/or reagents fill the tubing going to the valve module. To prime the analyzer, complete the following steps: 1. Press the MENU key to start from the MAIN MENU. 2. Select SENSOR MENU and press ENTER. 3. Select the sensor by name (default is #1 APA6000) and press ENTER. 4. Select SOLUTIONS & CLEANING and press ENTER. 5. Select PRIMING and press ENTER. 6. Select PRIME ENTIRE SYSTEM NOW. This will prime all the lines from the solution bottles and sample lines. The system prime will take approximately 715 minutes. The analyzer will display various messages about the progress of the cycle. 7. A pop-up window will indicate that priming will begin after the current operation cycle. When priming starts, a pop-up window will indicate the time remaining to complete the prime cycle. 8. When priming is complete, the analyzer will automatically begin measuring sample. The analyzer will require 36 hours for readings to stabilize. During this time, the analyzer will establish temperature control. After readings stabilize, a calibration is required to obtain accurate values. See section 4.2.3.1 on page 44.
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Section 4
Instrument Menus
MENU
ENTER
Section 4
The arrow icons and their positions in the arrow field in the top right corner of the display (item 7 on Figure 16) indicates the active arrow keys. For example, if three arrow icons are present in the arrow field, pointing up, down, and right, then the up, down, and right arrow keys can be used while viewing that screen. Figure 15 shows examples of the screen categories and Table 3 contains summaries of the arrow key functions for each screen category. Figure 15 AquaTrend Interface Screen Categories
1. Menu Screen
1. Menu Screen
Section 4
When viewing data in graph mode, you can see a history of readings over the last 2 hours, 8 hours, 30 hours, 7 days, or 30 days. The AquaTrend Interface, however, displays data for only one measurement channel at a time in the graphic mode. For details on selecting the preferred graph time and scale, see section 4.2.2.1 on page 37. Figure 16 AquaTrend Interface Menu and Numeric Data Display Fields
Section 4
Figure 17 AquaTrend Interface Graph Fields
1 16
AquaTrend
15 14 13
5 12 6 11 7
Alarms
10
Time or date value of data at cursor position Current time (latest data).
Retrieves value of data at cursor position Graph of 60 minutes, 8 hours, 24 hours, 7 days, or 30 days of data. These settings are selectable in the DISPLAY SETUP menu (see section 4.2.2.1). Depending on the sensor type and configuration, the display shows measurement name or the sensor location, or a combination of both. Units and chemical form of the measurement on the channel Direction of these arrow icons correspond to enabled arrow keys for each screens. Most recent measurement (same as numeric display)
Section 4
4.2 Menu Functions
The first level of menu functions is comprised of Alarm Log, Aquatrend Menu, Sensor Menu, Other Device Menu, and Network Menu. Each level of menus will be discussed in detail below.
The most recent alarm/warning is listed first. A bell icon to the left of the warning indicates the alarm/warning is active. Selecting a specific alarm/warning and pressing ENTER provides more detailed information about that alarm/warning (i.e., time, date, value).
Section 4
Flash On Alarm: Controls whether or not the display will flash when an alarm has been detected. Contrast Level: Controls the level of contrast in the display.
Measurement to Channel
APA 6000 Analyzers can measure from 1 or 2 sample streams, requiring assignment of a measurement channel for each parameter on a stream. For example, parameter options could be called 1Hardness and 2Hardness. In addition, each sample stream may report up to five different parameters. To assign a measurement to a channel, use the MEASUREMENT TO CHANNEL function.
Section 4
Channel Graph Settings
To optimize the graphical display, establish the minimum and maximum values to be displayed. For example, if the expected range is 07 ppm, assign 0 as the measurement minimum and 7 as the measurement maximum. 1. Press the MENU key to access the Main Menu. 2. Select AquaTrend Menu and press ENTER. 3. Select DISPLAY SETUP and press ENTER. 4. Select CHANNEL GRAPH SETTINGS from the Display Setup Menu and press ENTER. A list of available channels will appear. 5. Select the channel of interest and press ENTER. 6. Select YMAX and press ENTER. 7. Use the arrow keys to change the displayed values. Press ENTER to accept the value or EXIT to cancel. 8. Repeat step 6 and step 7 to change the YMIN: displayed value. Enter negative numbers by changing the first character to a negative sign with the arrow keys. Setting the Graph Time (x-axis): 1. Press the DISPLAY key until a graph is displayed. 2. Press the up or down arrow keys to select the channel of interest. 3. Press the right or left arrow key to change the time base. The time base will cycle through 2 hours, 8 hours, 30 hours, 7 days, and 30 days. The time scale is shown below the X-axis.
Flash on Alarm
When an alarm is active, the display can flash to bring attention to the alarm condition. Enable/Disable the Flash on Alarm as follows: 1. Press the MENU key to access the Main Menu. 2. Select AquaTrend Menu and press ENTER. 3. Select Display Setup and press ENTER. 4. Move the pointer to Flash On Alarms. YES or NO will be displayed to the right of that line. If the displayed option is correct, press the EXIT key to return to the previous menu level. If the displayed option is not correct, press ENTER. A pop-up window will appear. Use the arrow keys to move the pointer to the desired option and press the ENTER key to accept it. Press the EXIT key to return to the previous menu level.
Section 4
Adjusting the Display Contrast
Adjusting the contrast level setting of the AquaTrend Interface allows the operator to choose the most readable display for the lighting conditions. 1. Press MENU to start from the Main Menu. 2. Select AquaTrend Menu and press ENTER. 3. Select Display Setup and press ENTER. 4. Select Contrast Level. 5. A pop-up window provides a choice of settings between 0 and 24 (0 being the lowest setting). Use the up and down arrow keys to adjust the contrast. Press ENTER to accept the displayed contrast level.
4.2.2.2 Language
English is the default language of the APA 6000 Analyzer. To display another language follow the instructions below: 1. Press the MENU key to start from the Main Menu. 2. Select AquaTrend Menu and press ENTER. 3. Select Language and press ENTER. 4. Use the up or down arrow key to select the appropriate language and press ENTER. All screens will be displayed in this language.
Section 4
4.2.2.4 Set Time/Date
The current time and date have been factory set on the AquaTrend Interface, but the time may need to be adjusted to your time zone. If it is necessary to reset the time and date, proceed as follows:
Section 4
Setting the Correct Day of the Week
Use this procedure to change the current day of the week: 1. Press the MENU key to start from the Main Menu. 2. Select AquaTrend Menu and press ENTER. 3. Select Set Time/Date and press ENTER. 4. Select Day and press ENTER. 5. A pop-up window will prompt for the correct day. Use the up or down arrow key to highlight the desired day. 6. Press ENTER to save the change or press EXIT to cancel. The day will change automatically. Check to be sure the clock is set at the correct time.
The default password is HACH. The default security level is NONE. This security level allows access to all functions. If the password is changed and then is lost or forgotten, contact your Hach representative for further instructions.
Section 4
Changing the System Password
1. Press MENU to start from the Main Menu. 2. Select AquaTrend Menu and press ENTER. 3. Select Security Setup and press ENTER. 4. Select Set Password and press ENTER. 5. Enter the current password for access to the AquaTrend Interface menus. Pressing the right and left arrow keys moves the cursor right and left; pressing the up and down arrow keys scrolls through the available characters. The default password is HACH. 6. Press ENTER to confirm or press EXIT to cancel. 7. Enter the new password by using the arrow keys as in step 5. 8. Re-enter the new password.
Setting the security level to NONE allows access, without a password, to any of the menus except SECURITY SETUP.
Section 4
Set the security level as follows:
1. Press the MENU key to start from the Main Menu. 2. Select AquaTrend Menu and press ENTER. 3. Select Security Setup and press ENTER. 4. Select Security Level: and press ENTER. 5. Enter the password (default is HACH). Use the left and right arrow keys to choose the character to change and use the up and down arrow keys to cycle through letters, numbers and symbols until you reach the character you want. 6. Use the arrow keys to select NONE, PARTIAL, or TOTAL. 7. Press ENTER to confirm or press EXIT to cancel.
* APA6000 Alkalinity and HR Hardness instruments defaults are each Monday at 4:00 a.m. APA6000 HR Hardness instrument default is each Monday at 4:00 a.m. Page 44 Menu Functions
Section 4
Reducing the frequency of the auto-calibration will reduce standard usage, but it may also reduce measurement accuracy. Hach recommends that the analyzer be calibrated when any reagent or standard is changed or as often as necessary to achieve acceptable results. Calibration should only be performed after the analyzer has been turned on for more than five hours. This allows the temperature inside the analyzer to stabilize.
Note: When auto-calibrate is set to 12 hours, the analyzer calibrates at the set auto-cal time and again 12 hours later.
Execute Calibration
To start a calibration manually, proceed as follows. The instrument will finish its current cycle, then perform the calibration. 1. Press the MENU key to start from the Main Menu. 2. Select Sensor Menu and press ENTER. 3. Select the sensor by name and press ENTER. 4. Select Calibration and press ENTER. 5. Select Execute Calibration and press ENTER. 6. The CALIBRATION PENDING message will appear.
Section 4
The analyzer will wait until any current measurement or priming cycle is complete before calibrating. Calibration typically takes 1 hours to complete.
Section 4
4.2.3.2 Alarm Setup
Each APA 6000 Analyzer provides 14 alarm signals for your system. Two of these, ALA and ALB, are permanently attached to the analyzers internal alarm outputs, labeled Relay A and Relay B. The remaining alarm signals, AL1 through AL12, can be attached to relays in optional Signal Output Modules (SOMs). SOMs can be purchased separately, and provide two relays and two analog outputs each. For information see the SOM Manual (Cat. No. 51250-18). Each of the alarm setup options provides a setting for measurement, enabling/disabling alarms, alarm type, and alarm set point. Alarms can be configured as one of six types: high, low, rate (in mg/L/hour units), sensor warning, sensor alarm, or unconfigured. Table 6 describes the parameters available on each alarm type. Parameters in bold print indicate default settings. Table 6 Parameters for Setting Alarms
Options TYPE MEASUREMENT SET POINT ENABLED MEAS FAILURE Set point Alarms High, Low, Rate, Unconfigured [Sensor measurement] [Legal value] Yes, No Off, On, Hold Sensor Warnings and Alarms Sensor Warning, Sensor Alarm, Unconfigured ----Yes, No ---
8. If High, Low or Rate was selected in step 7, the following setup options are available:
Section 4
Select Measurement to change the sample measurement that is monitored for alarm generation. Select Set Point to specify a numeric value for the alarm. Select Enabled to turn the alarm on or off. Select Meas Failure to set the alarms response when sample is not flowing to the analyzer or the analyzer experiences a fault that prevents it from providing the selected measurement. On and Off turn the alarm on or off; Hold leaves the alarm in the state it was in prior to the failure.
9. If you selected Sensor Warning or Sensor Alarm in step 7, select Enabled. Select Yes or No to turn the alarm on or off, respectively. 10. Press ENTER to save the alarm setting, or press EXIT to cancel.
Section 4
6. To change the type of output, select TYPE and press ENTER. 7. Select Recorder to send the analog output to a recorder 8. Press ENTER to confirm the setting or press EXIT to cancel. 9. To change the measurement that the recorder output will track, select Measurement: XXXX and press ENTER. 10. Select the desired measurement and press ENTER. 11. To change the minimum measurement value that corresponds to the minimum recorder output, select Min: XXXX and press ENTER. 12. Modify the minimum value by using the arrow keys and press ENTER when the value entry is complete. 13. To change the maximum measurement value that corresponds to the maximum recorder output, select Max: XXXX and press ENTER. 14. Modify the maximum value by using the arrow keys and press ENTER when the value entry is complete. 15. To enable or disable the recorder output, select Enabled and press ENTER. 16. Select Yes or No to indicate that the recorder output is enabled or disabled, respectively, and press ENTER. 17. To change the recorder output action when the analyzer is unable to perform measurements in the selected measurement range, select MEAS Failure: XXXX and press ENTER. 18. Select Hold, Go Max, or GO Min to indicate what the output action should be when the analyzer cannot perform a selected measurement. Go Max sets the output to 20 mA, Go Min sets the output to 4 mA, and HOLD keeps the output at the current value. Press ENTER. 19. To complete the recorder setup for RCA or RCB see the following section. To complete the recorder setup for RC112 see Analog Output Settings in the SOM Manual.
Section 4
To adjust (trim) the milliamp output range for the internal recorder/controller outputs (RCA or RCB) or to change the range: 1. Select Output A Setup or Output B Setup. Press ENTER. 2. To adjust the mA output at the bottom of the scale: a. Select Zero Scale Trim and press ENTER. b. Use the up/down arrow to select Fine or Coarse Adjustment. Press ENTER. The new trim mA value will appear. c. Select Accept New Value when done and press ENTER. 3. To adjust the mA output at the top of the scale: a. Select Full Scale Trim and press ENTER. b. Use the up/down arrow to select Fine or Coarse Adjustment. Press ENTER. The new trim mA value will appear. c. Select Accept New Value when done and press ENTER 4. To select either 020 mA or 420 mA as the output range, select Output Range and press ENTER.
1. Press the MENU key to start from the Main Menu. 2. Select Sensor Menu and press ENTER. 3. Select the sensor by name and press ENTER. 4. Select Measurement Options and press ENTER. a. Select Chemical Form and press ENTER. Select the desired chemical form and press ENTER. b. Select Sample Sequence and press ENTER. Assign a sample sequence and press ENTER. c. Select Display and assign the reading to the appropriate DDM if desired. Press ENTER. d. Select Units and press ENTER. Select Hold Outputs and press ENTER. Select the units you want to use and press ENTER, or press EXIT to cancel.
Note: When units are changed, the display shows new units with the next measurement.
Section 4
4.2.3.5 Enabling Solution Level Monitoring
Solution level monitoring by default is set to Off. The display will show Level Monitor: On/Off. When On is chosen (solution monitoring enabled), solution levels will be displayed as 0 to 100% full. To turn Solution Level Monitoring on or off proceed as follows: 1. Press the MENU key to start from the Main Menu. 2. Select Sensor Menu and press ENTER. 3. Select the sensor by name and press ENTER. 4. Select Solutions and Cleaning and press ENTER. 5. Select Level Monitor: On/Off and press ENTER. a. If monitoring is off the display will show: Turn on Level Monitor Levels Will Start @ 100% b. Select Yes and press ENTER to enable monitoring or select No to exit. c. If monitoring is on, the display will show: Turn off Level Monitor. Select Yes and press ENTER to disable or select No to exit.
Section 4
4.2.3.7 Solutions & Cleaning Options
There are two cleaning options, Clean System Now and Auto-Clean. Clean System Now will start the clean cycle as soon as the current operation finishes. The Auto-Clean option allows the user to change the frequency of the cleaning cycle. 1. Press the MENU key to start from the Main Menu. 2. Select Sensor Menu and press ENTER. 3. Select the sensor by name and press ENTER. 4. Select Solutions & Cleaning and press ENTER. 5. Select Instrument Clean and press ENTER. 6. Select Auto-Clean and press ENTER. Select the Automatic Clean Frequency and press ENTER.
Note: Using the default settings is strongly recommended by the manufacturer and should only be changed if sample components cause measurement problems. If cleaning frequency is decreased, verify that the cleanliness and operation of the analyzer is not degraded. Changing the cleaning frequency may interfere with the autocalibration.
Hold Outputs
Holds all outputs at the current level for 30 minutes, until this function is manually cancelled or until power is cycled off/on. 1. Press the MENU key to start from the Main Menu. 2. Select Sensor Menu and press ENTER. 3. Select the sensor by name and press ENTER. 4. Select Sensor Diagnostics and press ENTER. 5. Select Hold Outputs and press ENTER. 6. Select Hold Outputs for 30 Min or Abort Output Hold and press ENTER.
Section 4
4. Select Sensor Diagnostics and press ENTER. 5. Select Internal Relay Test and press ENTER. 6. Select A or B and press ENTER. 7. Select Test Open Relay or Test Closed Relay and press ENTER.
Default Calibration
Restores the factory default calibration curve. 1. Press the MENU key to start from the Main Menu. 2. Select Sensor Menu and press ENTER. 3. Select the sensor by name and press ENTER. 4. Select Sensor Diagnostics and press ENTER. 5. Select Default Calibration and press ENTER.
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Section 4
6. A pop-up window will appear. 7. Select Yes or No and press ENTER.
Sample Streams
This option allows the user to add or delete a second sample stream to the analyzer. 1. Press the MENU key to start from the Main Menu. 2. Select Sensor Menu and press ENTER. 3. Select the sensor by name and press ENTER. 4. Select Sensor Diagnostics and press ENTER. 5. Select Sample Streams and press ENTER. 6. A pop-up window will appear. 7. Select One or Two and Press ENTER.
Section 4
Note: Note the selections under SIO1 SETUP and SIO2 SETUP are the same. Up to two SIOs can be connected to the APA 6000. If installing a second SIO or the analyzer is connected to the second SIO on the network, select SIO2 SETUP.
If Computer format is selected and Output is set to Auto, the readings, alarms, and warnings will be sent out as they occur. If Output is set to Queried, the information is sent only when a query command is sent from the computer. The Time/Date will be sent with readings if Yes is selected and can be turned off by setting to No. If Printer Format is selected, the Output and Time/Date options are ignored and not shown in the menu. See Appendix B on page 85 for more information on printer and computer formats.
Sensor Status
The sensor status function indicates if the APA 6000 is in Standby or Online. The analyzer will go into Standby on a system Alarm condition. This menu also contains a Restart function. When this function is used, the sensor status reverts to Online when the restart procedure is complete.
Maintenance
DANGER
Handling chemical samples, standards, and reagents can be dangerous. Review the necessary Material Safety Data Sheets and become familiar with all safety procedures before handling any chemicals.
DANGER
La manipulation des chantillons chimiques, talons et ractifs peut tre dangereuse. Lire les Fiches de Donnes de Scurit des Produits (FDSP) et se familiariser avec toutes les procdures de scurit avant de manipuler tous les produits chimiques.
PELIGRO
La manipulacin de muestras qumicas, estndares y reactivos puede ser peligrosa. Revise las fichas de seguridad de materiales y familiarcese con los procedimientos de seguridad antes de manipular productos qumicos.
GEFAHR
Das Arbeiten mit chemischen Proben, Standards und Reagenzien ist mit Gefahren verbunden. Es wird dem Benutzer dieser Produkte empfohlen, sich vor der Arbeit mit sicheren Verfahrensweisen und dem richtigen Gebrauch der Chemikalien vertraut zu machen und alle entsprechenden Materialsicherheitsdatenbltter aufmerksam zu lesen.
PERICOLO
La manipolazione di campioni, standard e reattivi chimici pu essere pericolosa. La preghiamo di prendere conoscenza delle Schede Techniche necessarie legate alla Sicurezza dei Materiali e di abituarsi con tutte le procedure di sicurezza prima di manipolare ogni prodotto chimico.
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Section 5
5.1 Maintenance
1. Press the MENU key. 2. Select Sensor Menu, then press ENTER. 3. In the Select Sensor Menu, select the sensor name and press ENTER. 4. Select Sensor Status and press ENTER. A pop-up window will appear. Use the arrow keys to select Standby or Restart. Press ENTER If the analyzer will be shut down for an extended period of time, all reagents, standards, and samples should be flushed out of the system. This is accomplished by supplying deionized water in place of all reagents, standards, and samples and performing a Prime Entire System function.
* Check/replace filter and fill cleaning solution every two weeks in typical municipal wastewater applications.
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Table 9 Three-Month Maintenance
Item Autoburette module Valve module Maintenance Required Replace piston seals and O-rings. Replace valve rotor and inspect condition of stator (dry the stator before inspection); if scored, replace stator. Check for leaks. Replace as needed.
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Filtered sample is aspirated through the filter as needed. The instrument is not affected by how fast the sample is flowing through the block as long as the flow is between 1000 and 2000 mL per minute. If the filter becomes plugged, replace it with one of the spare filters supplied with the unit (Cat. No. 62011-00). To remove the filter from the sample conditioning block: 1. Turn off the sample flow and place the analyzer in standby mode.
Note: Sample will drain from the block when the filter holder is removed. Be prepared to dispose of this appropriately.
2. Remove the filter holder from the block by unscrewing the large knurled nut on the bottom of the block (see Figure 18). 3. Remove the quad-ring at the top of the filter assembly (see Figure 19). 4. Slide the filter off the top of the assembly. 5. Install a new filter. 6. After the new filter is in place, replace the quad-ring and screw the filter assembly into the sample conditioning block. 7. Turn sample flow on and restart the analyzer.
Note: The manufacturer does not recommend cleaning and reusing clogged filters.
Depending on your sample, the filter may quickly become plugged. The APA 6000 Micro Filter System (Cat. No. 51339-00, 115 V or Cat. No. 51339-01, 230 V) may be purchased to provide longer periods of operation between maintenance intervals. Figure 18 Removing the Sample Conditioning Block
Unfiltered sample IN
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Figure 19 Removing the Filter
5.1.2.3
Changing Modules
Refer to Figure 20 and follow the instructions below to replace a module:
Note: Chemicals are present in the pump, valve, and reagent tubing. Before doing any maintenance, review all MSDSs, and use recommended safety measures to prevent exposure to potential chemical hazards.
1. Put the analyzer in standby (see section 5.1.1 on page 59). This will extend the piston in the autoburette body and put the valve in a known position. Turn off power to the instrument by toggling the on/off switch at the top center of the module panel to off (O). 2. Break the siphon of any reagent/cleaning tubing that is connected to the module by removing the tubing from the bottles (see section 3.3 on page 29). Shut off the sample stream to the analyzer. 3. Remove all fittings from the module. 4. Loosen the two captive screws that secure the module to the instrument panel with a Phillips screwdriver. 5. Pull the module straight out to remove. 6. Reverse the process to reinstall the module.
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Figure 20 Part Identification for Module Removal
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Tubing replacement will be required if a tube becomes crimped or kinked and is interfering with fluid flow or the tubing becomes fouled due to sample conditioning upset (or improper sample conditioning).
5. If the tube is an external tube, slide the rubber grommet onto the tubing and insert into the appropriate position in the manifold on the inside bottom of the instrument case. 6. Route the tubing to its appropriate place on the outside and inside of the instrument (refer to Plumbing Diagram in the parameter-specific manual). 7. Install the fitting onto the tubing, as shown in Figure 21 or Figure 22. 8. Tighten fittings in the ports.
Warning: DO NOT over-tighten the fittings. Fittings should be firmly finger tightened. Loose fittings will result in air or liquid leaks and poor analyzer performance. In some case, a tool may be required to sufficiently tighten a fitting.
#10-32 Nut
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Figure 22 -28 Fitting Assembly
Tubing
Chamfered End
Flat End
Chamfered End of Locking Ring Flattened End of Locking Ring
Detail A
4. Before removing the valve head, remove tubing to ports 4, 7, and 10 for wrench clearance (see Figure 24). There is no need to drain sample line 3 as the sample was turned off in step 2. The line to port 7 is the waste line.
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5. Using a 7/64-in. Allen wrench, loosen the three recessed socket head cap screws in the valve stator (valve head). Do not completely remove the screws, but back them out far enough to remove the head. These screws will help hold a ring spacer that lies under the valve head or stator. Be careful not to lose this spacer. Pull the valve head away from the valve module and inspect surfaces of the rotor and stator.
Note: Do not the scratch the surfaces of the rotor and stator. Note: A small amount of fluid may drain from the stator. If the volume is large, be sure the siphon to the reagent bottles was broken.
6. Inspect the slot in the rotor for any plastic shavings or sample debris. If these are visible, remove the rotor from its holder for cleaning. Carefully clean this slot with a small stylus, or a soft bottle brush, taking care not to scratch the valve surface. 7. Dry and then inspect the valve surface of the valve head/stator. If this surface is scored, replace the valve head along with the rotor. Figure 23 Valve Rotor Part Identification
Valve Stator
7
8
4
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Figure 24 Removing Screws From the Valve Stator
Reinstallation
1. Before reinstalling the rotary valve, dry all surfaces with paper toweling. Reposition the valve head with port 1 at 12 oclock (top center) on the valve body. Make sure the locating pins in the valve body engage the locating pin holes on the back side of the valve head/stator. 2. Hold the valve stator in place as you engage the three socket head cap screws. Take care to evenly tighten these three screws. You will feel an even resistance as the valve stator tightens down. This is because a spring washer will be compressed during the rotor/stator mating. Tighten these screws in even increments until tight (100 to 120 inch-ounces of torque or 0,7 to 1,4 Joules of torque). 3. Re-attach lines 4, 7, and 10 to the valve head/stator. If the valve stator is replaced, connect the remaining lines to the new stator.
Note: Do not over-tighten these valve fittings. These fitting are finger-tight fittings. Torque these fitting to no more that 18 inch-ounces (0.13 Joule).
4. Return the raised reagent lines of the reagent/standard bottles to their original positions. 5. Start the analyzer. Go to the Prime Menu and select the Prime Entire System option. Once readings stabilize, recalibrate the instrument.
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5.1.2.6 Maintaining the Autoburette Module
CAUTION To familiarize yourself with handling precautions, dangers and emergency procedures, always review the Material Safety Data Sheets prior to handling containers, reservoirs, and delivery systems that contain chemical reagents and standards. Protective eye wear is always recommended when contact with chemicals is possible. PRUDENCE Pour se familiariser avec les prcautions prendre lors de la manipulation, les dangers et les procdures d'urgence, toujours lire les Fiches de Donnes de Scurit des Produits avant de manipuler les rcipients, les rservoirs et les systmes de distribution contenant les ractifs chimiques et les solutions talons. Il est toujours recommand de porter des lunettes de protection lorsqu'un contact avec les produits chimiques est possible. CUIDADO Para familiarizarse con las precauciones de manipulacin, los peligros y los procedimientos de emergencia, siempre estudie las Hojas de Datos de Seguridad de los Materiales antes de manipular recipientes, depsitos y sistemas de entrega que contengan reactivos y patrones qumicos. Siempre se recomienda el uso de protectores oculares cuando sea posible el contacto con productos qumicos. VORISCHT Es wird dringend empfohlen, die Sicherheitsdatenbltter vor der Handhabung von Behltern, Tanks und Zufuhrsystemen, die chemische Reagenzien und Standardsubstanzen enthalten, aufmerksam durchzulesen, damit Sie sich mit den beim Umgang mit diesen Chemikalien notwendigen Vorsichtsmanahmen, Risiken und Notfallschutzmanahmen vertraut machen, Es wird empfohlen, in allen Situationen, in denen mit einem Kontakt mit Chemikalien zu rechnen ist, eine Schutzbrille zu tragen. ATTENZIONE Per familiarizzare con misure di precauzione di controllo manuale, con procedure pericolose e di emergenza, rileggere sempre le schede di sicurezza del materiale prima di maneggiare contenitori, imballaggi per spedizione che contengono reagenti chimici e standards. Si consiglia di indossare sempre gli occhiali protettivi quando possibile un contatto con agenti chimici.
Replace autoburette piston seals if: They have been in use longer than 3 months. Air leakage into the autoburette body through the seals is visible. There are signs of leakage on the back side of the autoburette module.
Important Note: Regular maintenance of the Autoburette Module is critical for correct analyzer function. Failure to perform the required regular maintenance will void the manufacturer warranty.
Use the following procedure, Figure 25, and Figure 26 to replace the autoburette seals: 1. Place the instrument in standby, then turn it off. The piston will be fully forward. 2. Break the siphon to the cleaning solution by disconnecting the reagent tubing from the reagent vent cap insert. Lift the reagent line until the bottom of the reagent line is above the liquid level in the bottle. 3. Remove the two tubes connected to the autoburette body. 4. Remove the knurled lock ring from the autoburette body; set it aside for reuse when reassembling the autoburette.
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5. Gently slide the autoburette body assembly off of the piston by pulling it away from the module base. Be careful not to bend the piston and lead screw assembly during removal. 6. Use a -inch open-end wrench to loosen the ceramic piston guide from the Autoburette Body assembly. Unscrew the piston guide and set it aside. Figure 25 Autoburette Module
7. Remove the two piston seals from the seal retaining ring and discard. Take care not to damage the seal retaining ring. 8. Remove the O-ring that is seated within the assembly. Do not use a sharp tool for O-ring removal, damage to the auto-burette body could result. 9. Install a new O-ring; make sure it is fully seated in the groove. 10. Install the two new piston seals onto the seal retaining ring. Place one seal flanged-side up and press the seal retaining ring onto it. Repeat for the opposite side. Ensure both rings are fully engaged and that the resulting edge is flat. 11. Drop the assembled piece into the autoburette body so it is resting on the O-ring. 12. Install the ceramic piston guide and tighten just until resistance is felt. 13. Fully insert the stainless steel alignment tool. 14. Securely hand-tighten the ceramic piece into the Autoburette Body.
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Note: The adequacy of sealing is not determined by the tightness of the piston guide. Overtightening of the piston guide will lead to premature failure.
15. Slide the alignment tool out of the assembled Autoburette Body.
Note: If the alignment tool does not slide out easily, the ceramic piece is too tight. Loosen the ceramic piece slightly and remove the alignment tool.
16. Lubricate the outer circumference of the ceramic piston guide with the pump lubricant (Cat. No. 62044-00). Do not allow the lubricant to touch the piston. 17. Slide the assembled unit onto the Autoburette Piston with the weep hole oriented at the bottom. 18. Reinstall the knurled lock ring and hand-tighten it to complete the installation.
Note: There should NOT be any movement of the autoburette body once the lock ring is fully in place.
19. Reinstall the two tubing connections. 20. Replumb the instrument; refer to the plumbing diagram in the parameterspecific manual supplied with your instrument. 21. Restart and prime the instrument. Figure 26 Autoburette Body Assembly
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4. Locate the lead screw in the recessed area at the top of the module. 5. Apply a thin bead of grease the length of the exposed screw.
Note: Do not apply grease to the portion of the screw protruding from the back of the module. Grease the part of the screw that is exposed in the recessed area on the top of the module only.
6. Slide the module back into the instrument, retighten the screws and turn the power back on.
Important Note: Failure to preform monthly maintenance on the autoburette module will void the warranty.
5.1.3.1
Fuse Replacement
DANGER Couper l'alimentation lectrique de l'appareil pour retirer ou installer un fusible. PELIGRO Apagar la electricidad del instrumento al quitar o instalar fusibles. GEFAHR Beim Entfernen oder Einsetzen der Sicherung muss die Stromzufuhr zum Gert unterbrochen werden. PERICOLO Staccare lo strumento dall'alimentazione a rete prima di togliere o inserire un fusibile.
DANGER Remove power from the instrument when removing or installing a fuse.
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The analyzer contains two ac line (5mm x 20 mm) fuses (Cat. No. 52083-00). These are located on the power supply board in the back of the instrument. They protrude through the power supply cover on the lower right side and are labeled F1 and F2 (see Figure 28). It is not necessary to remove the power supply cover to replace the fuses. Replace the fuses as follows: 1. Disconnect all ac power to the analyzer. 2. Turn the fuse carrier turn counterclockwise to remove it from the fuse holder. 3. Replace the fuse (T1.6 A. 250 V, Cat. No. 52083-00) inside the carrier. 4. Turn the fuse carrier turn clockwise to reinstall it in the fuse holder. 5. Reconnect ac power to the analyzer.
DANGER For continued protection against fire hazard, replace the fuse only with a fuse of the same type and rating. DANGER Pour assurer la protection contre les risques d'incendies, remplacez les fusibles uniquement par des fusibles du mme type et pour la mme intensit. PELIGRO Para una continua proteccin contra incendios, reemplace los fusibles nicamente por los del tipo y capacidad recomendados. GEFAHR Zur Wahrung des kontinuierlichen Brandschutzes drfen die Sicherungen nur mit Sicherungen des gleichen Typs und mit gleichen Stromkennwerten verwendet werden. PERICOLO Per evitare ogni pericolo di incendio, sostituire ogni fusibile solamente con uno dello stesso tipo ed amperaggio.
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Figure 28 APA 6000 Analyzer Electrical Terminals and Fuse Location
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Section 5
5.1.3.2 Cleaning the Mixer Module Chamber
It may become necessary to clean the mixer module chamber and the surface where the stir bar rests. This is usually indicated when the module chamber becomes discolored by biogrowth, staining, or sediment. 1. For safety reasons, run a CLEAN cycle before disassembling the mixer module. 2. Put the instrument in standby. 3. Notice the mixer housing is split. Use a Phillips screwdriver to loosed the two captive screws that secure the module to the instrument panel. 4. Hold the part of the housing next to the block while pulling the top of the housing out from the block. The part of the housing that holds the stir bar should stay attached to the instrument. Let the top part of the housing hang from the attached tubing. 5. Use a cotton swab soaked with a 10% household bleach solution to clean the mixing chamber and the module housing top. Rinse well with deionized water. See Figure 29. Figure 29 Mixer Module Parts
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6. If necessary, use a cotton swab soaked with a 10% household bleach solution to clean the surface the stir bar rests on and the stir bar. Rinse with deionized water. 7. Reassemble the housing, making sure the o-ring and stir bar are in place. See Figure 29. 8. Tighten the Phillips screws that hold the top of the housing to the block. 9. Restart the instrument.
5.2 Troubleshooting
5.2.1 General Troubleshooting Procedure
This section provides general procedures to solve problems that affect the analyzers performance. The first sign of a problem may be an alarm or warning, but erroneous or erratic readings may not always cause an alarm or warning. Being familiar with the steps in this section will help to quickly solve operational problems.
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Page 75 Troubleshooting
Section 5
5.2.2 Examine the Rotary Valve
Watch the rotary valve movement during a cycle. If fluid is moving from the common port to more than one outlet port, cross-leakage in the rotary valve is occurring. Inspect the rotary valve per section 5.1.2.5 on page 65. It is likely that stator will need to be replaced. Verify fluid is aspirated in when the autoburette is aspirating. If air is pulled into the tubing connected to the center port, and there is fluid at the selected port, the selected port may be clogged. Inspect and clean the rotary valve per section 5.1.2.5 on page 65. If reagent or standard is not delivered, disassemble and inspect the valve rotor and stator for blockage or buildup. Also inspect the reagent and standard port tubing.
Important Note: Do not shorten the tubing lengths for the holding coil.
Examine the fittings for leakage and tighten if necessary. The fittings should be firmly finger tight. If tubing was recently replaced, check the tubing lengths against the table presented in the parameter-specific manual.
Page 76 Troubleshooting
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autoburette dispenses fluid through the detector line. Following dispensation, the pressure may drop 34 psi and then should remain approximately constant. The gauge can indicate possible problems in the following ways: If the back pressure never reaches 20 psi and fluctuates as the autoburette is dispensing fluid, this may indicate leaking seals in the autoburette. If the back pressure reaches 20 psi as the autoburette dispenses, but then drops below 5 psi after the burette has stopped, this may indicate a leak in the valve which may also indicate the beginning of wear that can result in leakage between valve ports and poor performance. Finally, if the gauge reads above 25 psi, it is likely that the back pressure device or detector line has buildup and needs to be replaced.
None.
None.
None.
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Section 5
Table 12 APA 6000 System Alarms
Alarm/Warning A/D FAILURE Cause Detector module main analog to digital converter has failed. RAM on APA main circuit board has malfunctioned. Chemistry dipswitch is set to an illegal location. Valve module is not communicating with controller. Burette module is not communicating with controller. Mixer module is not communicating with controller. Detector module is not communicating with controller. Internal communication problem. Valve was unable to find its home signal. Valves home signal is always on. Valve was unable to move to the desired port. Analyzer Action Analyzer shuts down. Corrective Action Restart the analyzer. Replace detector module if problem persists. Restart the analyzer. Replace main board if problem persists. Verify dipswitch setting is correct. If the problem persists, replace the main board. Check to ensure all cable connections are secure. Replace module if problem persists. Replace the burette module. Replace the mixer module. Replace the detector module. Replace the main circuit board. Replace module if problem persists. Replace the valve module. Replace module if problem persists. Check for clogged lines or incorrect plumbing in the analyzer. Rebuild the pump. If problem persists, replace autoburette. Check for clogged lines or incorrect plumbing in the analyzer. Rebuild the pump. If problem persists, replace autoburette. Check for clogged lines or incorrect plumbing in the analyzer. Rebuild the pump. If problem persists, replace autoburette. Check for clogged lines or incorrect plumbing in the analyzer. Rebuild the pump. If problem persists, replace autoburette. Service the Sample Conditioning Unit or restore the sample flow.
Analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down. An alarm is logged and the analyzer shuts down.
INVALID DIPSWITCH
BURETTE1 COMM FAIL MIXER COMM FAIL DETECTOR COMM FAIL INTERNAL COMM FAIL VALVE NO HOME VLV HOME SIG ON VLV MOVE ERR
The Home location for Burette 1 has drifted outside of its limit from the last Home check.
The cumulative offset drift from Home has exceeded the acceptable limits.
BURETTE1 NO HOME
BURETTE1 HOME ON
SAMPLEx OUT
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Table 13 System Warnings
Alarm/Warning POWER FAILURE Cause Power was turned off or lost. Analyzer Action A warning message is logged. Analyzer continues to operate. A warning message is logged. Analyzer continues to operate using the average of the cal readings. A warning message is logged. Analyzer continues to operate using the previous calibration. Corrective Action None.
Typically a mechanical failure. Follow trouble shooting guidelines for modules. Typically a mechanical failure, also may be out of reagents and/or standards.
Standard xs readings are outside acceptable calibration limits and are not repeatable.
Check fluid level in each bottle. If fluid level is almost empty, replace the bottle and reset the Analyzer continues to operate fluid level. If the fluid level is not near empty, reset the fluid level to reflect the correct level. A warning message is logged. Analyzer continues to operate using the previous calibration. A warning message is logged. Analyzer continues to operate. Analyzer continues to operate. Analyzer continues to operate. Reagent or standard problem. Replace reagents and/or standards.
Light is leaking into the colorimeter. Colorimeter LED light output is too low. Colorimeter LED light output is too high.
Replace detector module. Replace detector module if problem persists. Replace detector module if problem persists.
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Appendix A
Network Connections
The connections described below use the following parts: Shielded, two-conductor cable (Cat. No. 52157-00) Cable Termination Kit (Cat. No. 52156-00) - includes: Strain Relief (2) (Cat. No. 52025-00) Sealing Washer (2) (Cat. No. 10338-14) Locknut (2) (Cat. No. 10596-12) Insulated Quick Connects (6) (Cat. No. 52143-00) Heat Shrink Tubing (1 foot) (Cat. No. 40825-00)
The Cable Termination Kit is supplied with the SIO, SOM, or PS1201 Modules. If connecting the APA 6000 to another APA 6000, order this kit and cable along with the additional APA 6000. 1. Make sure there is no power supplied to the APA 6000. 2. Open the APA 6000 door and remove the screws on the hinged panel holding the modules to access the electrical connections at the back of the instrument. Refer to Figure 30. 3. Remove the two lower wing nuts on the lower back panel, then remove the lower terminal strip cover. Refer to Figure 31. Figure 30 Electrical Connections
Appendix A
Figure 31 Removing the Customer Access Cover
4. Remove the wire access plug below the network terminal strip where the network cable will be routed into the APA 6000. Refer to Figure 32. 5. Take one end of the network cable and strip 15 cm (6 in.) of outer insulation from the cable. 6. Put the strain relief and sealing washer (supplied with the cable) over the cable and slide the strain relief and sealing washer 7 inches down from the end of the cable. Tighten the strain relief nut until the cable does not slip through the strain relief.
Note: Connect shield at one end of cable only. If connecting to another analyzer, then connect shield in only one of the analyzers. Insulate the non-connected end with tape or heat-shrink tubing.
7. Remove inch of insulation from the white and green wires. Either insulate the shield wire with appropriate length of heat shrink tubing or remove inch of insulation from the shield wire. Pull the cable through the APA 6000 wire access opening until the strain relief/sealing washer is pulled flush with the opening. From inside the analyzer, screw the locknut onto the strain relief and tighten.
Appendix A
Figure 32 Access to the Network Terminal Strip
Air Purge
Appendix A
8. Connect the white wire to the APA 6000 position A on the Network terminal block. Connect the green wire to position B on the Network terminal block. If connecting the shield wire, connect the ground wire of the cable to the terminal stud near the network terminal block. 9. If the AquaTrend Interface in the analyzer will be the master AquaTrend Interface or if the analyzer is not connected to a network, connect network terminator by placing the jumper over pins 2 and 3 on the J11 connector (see Figure 33). If this is not the master AquaTrend Interface, place the jumper over pin 2. 10. Replace the lower terminal strip cover over the electrical connections and install the two wing nuts to secure the cover. 11. Close the hinged panel holding the modules and reinsert and tighten screws holding the module door shut. Figure 33 Network Terminator
J11 Connector 3 1
Jumper
J11 Disabled 3 1 1
J11 Enabled 3
Appendix B
First occurrence of any alarm or warning will be sent out. The time/date of the alarm or warning is printed followed by either ALRM or WARN to specify it is an alarm or warning. The specific alarm or warning is then printed on the next line. When the alarm or warning condition clears it will be sent preceded by END: to indicate the condition is cleared. Some alarms and warnings provide information only and do not have an end (i.e. a fail to calibrate message is printed out only when the condition occurs). If a alarm or warning condition is active, then a *A for alarm or a *W for warning is appended to the measurement readings. Computer Format When the SIO is setup to transmit to a computer, the format is similar to the printer format described above. In addition, the year is included in the date and the alarms and warnings are printed out on the same line as the time and date. When using PC format, the time/date stamp can be disabled and the readings can be queried instead of being sent out in real-time. If the SIO is in Queried mode, the readings are sent out only when the analyzer receives RMR command, alarms and warnings are sent only when receive RAR command (refer to Table 14 for more on RMR and RAR commands). Remote RS232 Commands Table 14 lists the commands that can be sent to the APA 6000 Analyzer for remote analyzer operation.The analyzer response to remote commands will be OK if changing instrument settings. Commands which query settings or values will be responded to with the current settings or readings. If the analyzer does not recognize the command then a BAD CMD message is returned. If the analyzer recognizes the command but the settings are invalid then BAD SETTINGS is returned. Messages to the analyzer must be terminated with a carriage return character to signify end of command. Linefeed characters and spaces are ignored. All incoming characters are converted to uppercase before evaluated. When sending commands through the SIO, the channel number must precede the command. For example, if the analyzer is connected to SIO channel 1 and you wish to restart the analyzer, 1SRT should be sent. The analyzer will reply with OK and the SIO inserts the channel assigned for the analyzer (i.e. [1]OK will be the response to the computer).
Appendix B
Table 14 APA 6000 Remote RS232 Commands
Description of Remote Command Restart system Put instrument in standby Perform a calibration Perform a clean cycle Prime entire system Prime reagents Prime standards Command SRT HLT CAL CLN PMA PMR PMS Description of Command/Settings Restarts the system. Puts the analyzer in standby. Performs a calibration at end of the current cycle. Performs a clean cycle at end of the current cycle. Primes all the reagent and sample lines now. Primes reagents lines at end of current cycle. Primes standard lines at end of current cycle. Sending just first three characters CTM will result in current auto-cal. settings to be returned. Add the equal sign and one of the characters listed in the Command column to the left to set new auto-calibration interval. Calibrate every 12 hours. x = 0 to 23 indicates time of day to calibrate (using a 24-hour clock). If x=22, the analyzer calibrates at 10:00 p.m. and a.m. Calibrate daily. x = 0 to 23 indicates time of day to calibrate (using a 24Hhour clock). Auto-Calibrate Weekly. x = 6 to 12 which signifies the day of week to calibrate where Monday=6 and Sunday=12. y = 0 to 23 to indicate time of day to calibrate (using 24-hour clock). Sending just first three characters recalls the calibration values from the last calibration. Adding =A will recall all calibrations stored (up to 7). Resets calibration curve to factory default values. Sending just first three characters results in current settings being returned. Adding =x will result in following settings where x =1=6 hours, x=2=12 hours and x=3=24 hours. Sending just first three characters results in current settings being returned. Adding =x will result in following settings: x =1=6 hours, x=2 =12 hours and x=3=24 hours. x=4 to 10 signifies clean weekly where the day of the week to clean is 4 for Monday to 10 for Sunday. Returns SEQUENCE=12...1 which represents the order in which the samples are measured. Can have up to 8 values in sequence. The numbers after the equal sign represent the order in which sample measurements are performed. Nitrate V1.0 C1.0, Copper V1.0C1.0, Ammonium V1.0 C1.0, Amm and Nitr V1.0 C1.0, Hardness V1.0 C1.0, Alkalinity V1.0 C1.0 Output up to last 10 alarms/warning messages since last RAR command. Only enabled if SIOx setup in Query mode. Output last measurement reading for all cycles (grab and normal measurement readings & calibrations). Only enabled if SIOx setup in Query mode. Resets all standards, reagents, and cleaning solutions to 100% Send just first three characters if requesting level The third character is the number of the reagent. Add = followed by reagent level in percent if setting to a new level. Allowed values are between 0 and 100%.
CTM
CTM=4,x
CTM=5,x
CTM=x,y
CLI=x
SEQ Get/Set sample sequence SEQ=12. Get instrument ID Output latest alarms/warnings RID RAR
RMR RFL
RG1=xxx
Appendix B
Table 14 APA 6000 Remote RS232 Commands (continued)
Description of Remote Command Command Description of Command/Settings Send just first three characters if requesting level The third character is the number of the standard. Add = followed by standard level in percent if setting to a new level. Allowed values are between 0 and 100%. Send just first three characters if requesting level Add = followed by fluid level in percent if setting to new level. Allowed values are between 0 and 100%. The percent sign is optional. Sends out all Instrument settings. Send first three characters to get instrument name. Default name is #1 APA 6000. Add equal sign plus text to set new name. Maximum length of name is 12 characters. Note: all letters will be converted to upper case. Set x = F or H or Z for output recorder full-scale, half-scale or zero respectively. Send just first three characters to stop test. Set x = F or H or Z for output recorder full-scale, half-scale or zero respectively. Send just first three characters to stop test. Set x = 0 or 1 for relay off or on. Send just first three characters to stop test. Set x = 0 or 1 for relay off or on. Send just first three characters to stop test. Get version numbers of instrument and its modules. For Hardness V1.0 C1.0, EXT NEURON: EXT0101, INT NEURON: INT0101, (and following if used:), VALVE MODULE: VLV0103 DETECT MODULE: DET0102, BURETTE1 MODULE: PMP0102, MIXER MODULE: PMP0102 Transmits all messages in current alarm log. Clears alarm logs.
SD1=xxx
Query/Set pump wash fluid level Request all instrument settings and information
WSH=xxx
ALL
RIN=xxx
Test internal recorder channel A Test internal recorder channel B. Test internal relay A. Test internal relay B.
RVN
TAL WAL
Appendix C
Sample Sequencing
Hach recommends using the Sample Sequencing Kit (Cat. No. 62009-00) to add a second sample stream to the analyzer in clean water applications. The Sample Sequencing Kit contains a vortex filter sample conditioning block, tubing, fittings, spare filters, and instructions. For wastewater applications Hach recommends using the APA 6000 Micro filter Kit (Cat. No. 51339-00 115 V or 51339-01 230 V).
Quality Control
A second sample stream may be used to verify the operation of the APA 6000 by reading a known sample at regular intervals. Hach recommends using the Quality Control Kit (Cat. No. 62032-00).This kit includes a carboy capable of holding a one month supply of a quality control standard, plus the tubing and fittings necessary to plumb the carboy to the analyzer.
Grab Sample
To occasionally check a second sample or verify operation by reading a known sample, use the Grab Sample Kit (Cat. No. 62037-00) which is supplied with the instrument.
Appendix C
Setting Up the Sample Sequence
For analyzers with two sample streams, the measurement sequence option allows the user to customize the sequence of sample stream measurements. The analyzer will measure the sample streams based on the step order the operator selects. The sample streams can be in any order; the analyzer will sequence up to eight sample cycles. For example: 1, 2, or 1, 2, 1, 1, 1, 2.
Note: The sequence will terminate at the first unused step. Subsequent steps will be cleared.
Appendix C
3. Use the sample sequencing function to control the frequency of the readings taken from the new sample stream.
Key Press 1. 2. MENU SENSOR ENTER SELECT SENSOR Select sensor by name 3. 4. 5. ENTER MEASUREMENT OPTIONS ENTER SAMPLE SEQUENCE ENTER STEP X Select the first unused step. 6. ENTER SAMPLE NUMBER Assign either sample stream 1 or 2 to the step 7. ENTER Menu Selection
For each STEP X (18) in Step 4, choose one of the measurement streams to sequence. The instrument will analyze in this sequence down to the first step left unused and will then repeat the sequence. For example, if you want the analyzer to alternate readings between the sample and the quality control standard, you would only program 1, 2. If you want the analyzer to read the quality control standard every fourth measurement, program 1, 1, 1, 2.
General Information
At Hach Company, customer service is an important part of every product we make. With that in mind, we have compiled the following information for your convenience.
AquaTrend Instrument................................................................................................................each.......... 51200-00 AquaTrend Instrument with SOM ...............................................................................................each.......... 51350-00 Cable Termination Kit .................................................................................................................each.......... 52156-00 Digital Display Module (DDM) ....................................................................................................each.......... 52400-00 Power Cord, UL/CSA, 115 V, w/ NEMA-style strain relief ..........................................................each.......... 46306-00 Power Cord, VDE, 230 V, w/ Continental-style plug and NEMA-style strain relief .....................each.......... 46308-00 PS2401 Power Supply, 115 V ....................................................................................................each.......... 54352-00 PS2401 Power Supply, 230 V ....................................................................................................each.......... 54353-00 Serial Input/Output Module (SIO)...............................................................................................each.......... 52074-00 Signal Output Module (SOM) .....................................................................................................each.......... 51250-00
Sample Conditioning
APA 6000 Micro Filter System, 115 V ........................................................................................each.......... 51339-00 APA 6000 Micro Filter System, 230 V ........................................................................................each.......... 51339-01 Sample Conditioning Block, -in fittings....................................................................................each.......... 62008-00 Sample Sequencing Kit..............................................................................................................each.......... 62009-00 Y-strainer Kit...............................................................................................................................each.......... 46618-00
Replacement Parts
AquaTrend Instrument Manual ...................................................................................................each.......... 51350-18 Binder, D-ring, for AquaTrend manual........................................................................................each.......... 52001-77 Autoburette Module ....................................................................................................................each.......... 57150-00 Back Pressure Regulator Assembly...........................................................................................each.......... 55226-00 Bulkhead Union, 0.25 OD tubing to tubing (for air purge bulkhead) ..........................................each.......... 51104-00 Cable, backplane .......................................................................................................................each.......... 51161-00 Cable, AquaTrend ......................................................................................................................each.......... 51164-00 Circuit Board, AquaTrend ...........................................................................................................each.......... 51092-00 Faceplate Assembly, APA 6000 (plastic bezel only, does not include circuit board) ..................each.......... 51022-00 Filter, Ceramic, for Filter assembly.............................................................................................each.......... 62011-00 Fitting, Ferrule, 0.062 OD...........................................................................................................each.......... 51130-00 Fitting, Ferrule, with ring, 0.062 OD ...........................................................................................each.......... 51132-00 Fitting, Union, Tefzel, -28 ........................................................................................................each.......... 51359-00 Flangeless Hex Nut Fitting, 0.062 OD........................................................................................each.......... 51129-00 Flangeless Nut Fitting, 0.062 OD ...............................................................................................each.......... 51131-00 Fuse, 1.6 A, 250 V, 5 mm x 20 mm, UL, CSA, VDE approved...................................................each.......... 52083-00 Grommet, manifold, APA 6000 (for tubing).................................................................................each.......... 51036-00 Plug, air purge, for -in. tubing..................................................................................................each.......... 51140-00 Plug, manifold, APA 6000...........................................................................................................each.......... 51224-00 Plug, flat bottom, Tefzal, -28....................................................................................................each.......... 51293-00 Power Switch, 4A, 250 VAC .......................................................................................................each.......... 51155-00 Reagent Bottle Vent Cap Assembly ...........................................................................................each.......... 51215-00 Reagent Housing Assembly.......................................................................................................each.......... 51048-00 Restraining Cable, steel, w/eyelets (for module panel) ..............................................................each.......... 51417-00 Rotary Valve, 10-port, with actuator...........................................................................................each.......... 51150-00 Rotary Valve, head only .............................................................................................................each.......... 51507-00 Seal, oil tight, 0.88-in. diameter .................................................................................................each.......... 42210-00 Stator, for 10-port valve..............................................................................................................each.......... 51347-00 Stir Bar, micro, 3 mm x 10 mm...................................................................................................each.......... 20549-59 Teflon Tubing, 0.170 ID x 0.250 OD ...................................................................................... per foot.......... 45462-00
Teflon Thread Tape, 0.25-in wide ...............................................................................................1 roll.......... 70608-24 Tubing, Tefzel, 0.030 ID x 0.062 OD, 2000 psi ...................................................................... per foot.......... 51178-00 Valve Body Replacement, 10-port valve ....................................................................................each.......... 51507-00 Valve Module Assembly, APA 6000............................................................................................each.......... 62050-00 Valve Plug, 10-32 .......................................................................................................................each.......... 51393-00
Kits
Installation Kit............................................................................................................................................... 51040-00 Filter, 0.5 micron ..................................................................................................................each.......... 62011-00 Grab Sample Kit ..................................................................................................................each.......... 62037-00 Poly Tubing, -in. OD......................................................................................................20 feet........... 47438-00 Tool Kit ......................................................................................................................................................... 51291-00 Alignment tool...................................................................................................................1 each.......... 57161-00 Allen Wrench, 7/64 in., long arm (1) ..................................................................................1 each.......... 51345-00 Fitting, Hex Nut, 0.062-in.OD tubing (4) ...........................................................................4 each.......... 51129-00 Fitting, Ferrule, 0.062 in. OD tubing (4) ............................................................................4 each.......... 51130-00 Fitting, Flangeless Nut, 0.062 in. OD tubing (10) ...........................................................10 each.......... 51131-00 Fitting, Ferrule w/ Ring, 0.062 in. OD tubing ((10) ..........................................................10 each.......... 51132-00 Nut Extender Tool, Flangeless (1) ....................................................................................1 each.......... 51174-00 Plug Fitting, Hex Nut Valve, 10-32 (3)...............................................................................3 each.......... 51393-00 Plug, Flat-bottom Tefzel, -28 (4) ....................................................................................4 each.......... 51293-00 Tefzel tubing, 0.030 ID x 0.062 in. OD, 2000 PSI ............................................................15 feet.......... 51178-00 Tubing cutter, for 1/16-in. Tubing (1) ..................................................................................1 each.......... 51356-00 Wrench, Valco Valve, -inch (1).......................................................................................1 each.......... 51357-00 Maintenance Kit ........................................................................................................................................... 62028-00 Auto burette piston seals .................................................................................................8 each.......... 57163-00 Grease, Lead Screw ......................................................................................................... 1 tube.......... 62044-00 O-ring, fluorocarbon..........................................................................................................4 each.......... 62014-00 Valve Rotor .............................................................................................................................2 each.......... 51348-00
How to Order
U.S.A. Customers
By Telephone: 6:30 a.m. to 5:00 p.m. MST Monday through Friday (800) 227-HACH (800-227-4224) By Fax: (970) 669-2932 By Mail: Hach Company P.O. Box 389 Loveland, Colorado 80539-0389 U.S.A.
Information Required
Hach account number (if available) Your name and phone number Purchase order number Brief description or model number billing address Shipping address Catalog number Quantity
International Customers
Hach maintains a worldwide network of dealers and distributors. To locate the representative nearest you, send e-mail to intl@hach.com or contact: Hach Company World Headquarters; Loveland, Colorado, U.S.A. Telephone: (970) 669-3050; Fax: (970) 669-2932
Repair Service
Authorization must be obtained from Hach Company before sending any items for repair. Please contact the Hach Service Center serving your location. In the United States: Hach Company Ames Service 100 Dayton Avenue Ames, Iowa 50010 (800) 227-4224 (U.S.A. only) FAX: (515) 232-3835
In Canada: Hach Sales & Service Canada Ltd. 1313 Border Street, Unit 34 Winnipeg, Manitoba R3H 0X4 (800) 665-7635 (Canada only) Telephone: (204) 632-5598 FAX: (204) 694-5134 E-mail: canada@hach.com In Latin America, the Caribbean, the Far East, the Indian Subcontinent, Africa, Europe, or the Middle East: Hach Company World Headquarters, P.O. Box 389 Loveland, Colorado, 80539-0389 U.S.A. Telephone: (970) 669-3050 FAX: (970) 669-2932 E-mail: intl@hach.com
Limited Warranty
Hach Company warrants this product against any defects that are due to faulty material or workmanship for a period of one year from the date of purchase. In the event that a defect is discovered during the warranty period, Hach Company agrees that, at its option, it will repair or replace the defective product or refund the purchase price of the defective product less any charges for shipping and handling. This warranty does not apply to: (i) damage caused by Act of God; (ii) damage caused by misuse, neglect, accident or improper application or installation; (iii) damage caused by any repair or attempted repair not authorized by Hach Company; (iv) any product not used in accordance with the instructions furnished by Hach Company. Any product repaired or replaced under this warranty will itself be warranted only for the remainder of the warranty period of the original product being repair or replaced. This warranty does not apply to short-life or consumable components of a product, such as, without limitation, light bulbs and chemical reagents.
Limitation of Remedies
The remedies of repair, replacement or refund of purchase price as stated above are the exclusive remedies for the breach of this warranty. In no event shall Hach Company be liable for any incidental or consequential damages of any kind for breach of warranty, negligence, on the basis of strict Liability or under any other legal theory.
Geographical Limitation
This warranty is extended only to products purchased, delivered and used in the 50 United States.
Certification
Hach Company certifies this instrument was tested thoroughly, inspected and found to meet its published specifications when it was shipped from the factory. The APA 6000 Analyzer has been tested and is certified as indicated to the following instrumentation standards:
Product Safety
UL 3101-1 (ETL Listing # H0492805390) CSA C22.2 No. 1010.1 (ETLc Certification # H0492805390) Certified by Hach to EN 61010-1 (IEC1010-1) per 73/23/EEC, supporting test records by Intertek Testing Services.
Immunity
EN 61326 (EMC Requirements for Electrical Equipment for Measurement, Control and Laboratory Use) per 89/336/EEC EMC: Supporting test records by Hach Company, certified compliance by Hach Company. Standards include: IEC 1000-4-2:1995 (EN 61000-4-2:1995) Electro-Static Discharge Immunity
IEC 1000-4-3:1995 (EN 61000-4-3:1996) Radiated RF Electro-Magnetic Field Immunity IEC 1000-4-4:1995 (EN 61000-4-4:1995) Electrical Fast Transients/Burst IEC 1000-4-5:1995 (EN 61000-4-5:1995) Surge IEC 1000-4-6:1996 (EN 61000-4-6:1996) Conducted Disturbances Induced by RF Fields IEC 1000-4-11:1994 (EN 61000-4-11:1994) Voltage Dip/Short Interruptions
Additional immunity Standard/s include: ENV 50204:1996 Radiated Electro-Magnetic Field from Digital Telephones
Emissions
Per 89/336/EEC EMC: EN 61326:1998 (Electrical Equipment for measurement, control and laboratory use-EMC requirements) Class "A" emission limits. Supporting test records by Criterion Technology O.A.T.S. (NVLAP #0369), certified compliance by Hach Company. Standards include: EN 61000-3-2 Harmonic Disturbances Caused by Electrical Equipment
EN 61000-3-3 Voltage Fluctuation (Flicker) Disturbances Caused by Electrical Equipment
Canadian Interference-causing Equipment Regulation, IECS-003, Class A: Supporting test records by Criterion Technology O.A.T.S. (NVLAP #0369), certified compliance by Hach Company.
This Class A digital apparatus meets all requirements of the Canadian Interference- Causing Equipment Regulations. Cet appareil numrique de la classe A respecte toutes les exigences du Rglement sur le matriel brouilleur du Canada.
Page 99 Certification
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Certification
FCC PART 15, CLASS A LIMITS: Supporting test records by Criterion Technology O.A.T.S. (NVLAP #0369), certified compliance by Hach Company. This device complies with Part 15 of the FCC Rules. Operation is subject to the following two conditions: (1) this device may not cause harmful interference, and (2) this device must accept any interference received, including interference that may cause undesired operation. Changes or modifications to this unit not expressly approved by the party responsible for compliance could void the user's authority to operate the equipment. This equipment has been tested and found to comply with the limits for a Class A digital device, pursuant to Part 15 of the FCC Rules. These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment. This equipment generates, uses, and can radiate radio frequency energy and, if not installed and used in accordance with the instruction manual, may cause harmful interference to radio communications. Operation of this equipment in a residential area is likely to cause harmful interference, in which case the user will be required to correct the interference at his own expense.
The following techniques of reducing the interference problems are applied easily. 1. Disconnect the APA 6000 Analyzer from its power source to verify that it is or is not the source of the interference. 2. If the APA 6000 Analyzer is connected into the same outlet as the device with which it is interfering, try another outlet. 3. Move the APA 6000 Analyzer away from the device receiving the interference. 4. Reposition the receiving antenna for the device receiving the interference. 5. Try combinations of the above.
6200518 Certification.fm