ANAND ENGINEERING COLLEGE, AGRA

Deptt. Of Electronics & Instrumentation

TEACHING PLAN Faculty Name : Priyanka Parashar Subject Name : Analytical Instrumentation
S.No. UNIT 1 2 3 I 4 5 6 7 8 9 Topics of Lecture Introduction: Introduction and Scope of the subject UV Visible Spectroscopy: Introduction, Electromagnetic Radiation, and Spectrum, Interaction of Radiation with Matter, Lambert Law, Beer Law, Bear Lambert Law,. . Absorption Instruments, Radiation Sources, Optical Filters, Monochromator : Prism, Diffraction Gratings, Holographic Gratings, Materials of Optical Components Detectors: Photovoltaic, High Vacuum PhotoEmission Cells, Photomultiplier Tubes, Silicon Diode Detectors, Photo Diode Arrays, Sample Holders UV Visible Spectrophotometers; Calorimeters, , Double Beam spectrophotometer(Optical Diagram & Block Diagram); Microprocessor based Spectrophotometer (Block Diagram) Infrared Spectroscopy: Introduction, Near Middle Far IR range of Spectrum; Basic Components of IR Spectrophotometers Type of Infrared Spectrophotometers Sample Handling Techniques Flame Photometers (FP): Principle of Flame Photometry, Essential Parts of FP, Block Diagram for Flame Photometers, types of flame photometers clinical flame photometers, accessories for flame photometer expression for concentration, interferences in flame photometry, procedure for determinations. Atomic Absorption Spectrometers: Introduction Atomic Absorption Spectroscopy Atomic Absorption Instrumentation Sources of interferences, meter scale.

Class & Section: IVth yr(A+B) Subject Code:EIC-033

Remarks

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II

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Mass Spectrometers (MS): Basic of Mass Spectrometer(MS): Principle of operation Type of MS : Magnetic Deflection MS, Time of Flight MS, Radio Frequency MS,Quadruple Mass Spectrometer. components of Mass Spectrometers inductively coupled plasma-mass spectrometer, trapped ion analyzers, ion cyclotron resonance (ICR) mass spectrometer, quadruple ion trap mass spectrometer, applications of mass spectrometry, gas chromatograph-mass spectrometer, Liquid chromatograph-mass spectrometer, tandem mass spectrometry (MS/MS). Nuclear Magnetic Resonance (NMR): Introduction, Nuclear Magnetic Resonance (NMR) Spectroscopy Principle of NMR, types of NMR spectrometers, constructional details of NMR spectrometer, variation T-60A NMR spectrometer Sensitivity enhancement for analytical NMR-spectroscopy, Fourier transform NMR spectroscopy.

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Text Book(s) :(i) Hand book of analytical instrumentation ,R.S.Khandpur,TMH 2nd Eddition Reference Books: (i) 2. Instrumental Methods of Analysis: Willard, Merritt, Dean and Settle,
Seventh Edition, CBS Publishers.