JABATAN KEJURUT N TERAAN K KIMIA & PR ROSES, FAKULT KEJURU TI UTERAAN & ALAM B BINA, UNIVE ERSITI KEB

BANGSAAN MALAYS N SIA

IN NTEGRA ATED PR ROJECT FOR K T KKKR203 KKK 34, KR2454, KKKR232 KKK K 24, KR2364 A AND KKK KB2424 (CHEM MICAL & BIOCH HEMICA ENGINEERIN AL NG)

SEMESTE 2, 20 ER 011/2012 2

COU URSE LECT TURERS:

KKK KR2364: KKK KR2454: KKK KR2324: KKK KR2034: KKK KB2424:

NAL ISMAI (KK) IL DR. MAN DR. MOHD SHAHBU D UDIN MASD DAR (KB) PROF. IR DR. ZAHIRA YAAK R KOB (KK) ASSOC. PROF. IR DR. MAST . TURAH MA ARKOM DR. DAR RMAN NOR RDIN ASSOC. PROF. DR MEOR ZA R. AINAL ME EOR TALIB B DR. MA ASLI IRWA ROSLI AN ASSOC. PROF. DR JAMALIA MD JAH R. AH HIM (KB)

INTEGRATED PROJECT (KKKR2034, KKKR2454, KKKR2324, KKKR2364 & KKKB2424) Semester II, 2011-2012 Based on the product assigned for your group, prepare a report on the following: Task No. 1 Common Literature studies on the product usage, demand vs supply, future marketing potential and sources of raw materials, waste generation, any environmental issues such as discharge limit and relevant environmental act and safety precaution taken during the production process. Material Safety Data Sheet (MSDS) must be included in the Appendix. Prepare a process flow diagram (PFD) using standard engineering drawing symbols. Implement the usage of engineering design softwares such as autocad or visio. Describe the process flow stream by stream from the Input to the Output Based on the PFD, perform a heat and a mass balance on the reactor unit. Use the figure obtained from the demand vs supply profile to determine the feed throughput (mass flow rate) Compare your results with Superpro and/or ICON simulation. 4 KKKR2364 KK & KB Describe the transport phenomena of the heat and mass transfer in the reactor OR bioreactor. Support your descriptions by stating the appropriate equations and data related to the heat and mass transfer properties, parameters and the type of geometry employed: i) Heat Transfer in a reactor OR bioreactor Describe the heat conduction and convection transfer (and radiation if applicable only) processes involved. Some schematic diagrams with appropriate heat transfer profile in 2D (x-y) or 3D (x-y-z) of the process description should be presented. Identify the factors influencing the heat transfer rate in your process. Conduct some calculations if necessary to determine the heat flux/heat transfer rate, heat transfer coefficients and other important supporting parameters (dimensionless numbers, etc). ii) Mass Transfer in a reactor OR bioreactor: Describe the mass transfer processes by molecular diffusion or convective mass transfer (as well as Non-Fickian diffusion if applicable only). Some schematic diagrams with appropriate mass transfer profile in 2D (x-y) or 3D (x-y-z) of the process description should be presented. Identify the factors influencing the mass transfer rates in your process. Conduct some calculations if necessary to determine the mass flux, diffusion coefficients and other important supporting parameters (dimensionless numbers, etc). Week 12 Course Assignment Submission week Week 12

Common

Week 9 SUBMIT 4 COPIES Week 9 SUBMIT 4 COPIES

Common

KKKR2454/ KKKB2424 KK/KB

Design a suitable reactor/bioreactor unit for the particular process and state the reasons for your choice. Derive the general mole balance or mass balance equation for the reactor/bioreactor system and include the kinetic rate expression whenever necessary. If this particular process requires the use of a catalyst/biocatalyst, please justify your catalyst/biocatalyst choice. Specify any byproduct of the process. Suggest the separation method of the main product from its impurities and indicate a way of stabilizing these products in the final stream. Design a separation unit or units (distillation, absorption/stripping or liquid-liquid extraction) to treat a stream which produces vapour/gas-liquid or liquid-liquid products and justify its usage. For a selected separation unit, choose a column type (tray or packed) and describe the separation mechanism involved. Then determine the number of degrees of freedom and variables specification for that particular separation unit. You are also required to determine the process design in terms of temperature, pressure, flow rates, compositions and heat duty (for column, heating, cooling). Do the mass balance (component and total) on the unit and compare your results with Superpro and/or ICON simulation. Finally, determine the structural design such as the tray/packing type and design, number of stages/transfer units, column diameter and height.

Week 12

KKKR2324 KK & KB

Week 12

KKKR2034 KK & KB

Write computer codes using MATLAB software in order to create a mass balance calculation program for one of these three options: (1) reactor unit, (2) bioreactor unit or (3) main separation unit in your process. The program should be able to determine the outputs of the unit should a user enters the required inputs. Use your creativity to produce the outputs which may be in the form of tables of data or/and graphs or etc.

Week 12

Your report should include these following sections: 1. Cover of the report 2. Abstract 3. Table of Content 4. List of Figures and Tables 5. Glossary and Nomenclature /Notations 6. Introduction 7. Economic Analysis 8. Environmental issues 9. PFD of the process 10. Mass and Heat Balances 11. Heat and Mass Transfer 12. Reactor I / Bioreactor I 13. Separation Process I 14. Chemical Engineering Computation I 15. Summary of the work 16. References 17. Appendix = MSDS sheet, solution for mass and heat balance calculations, and code of the MATLAB solutions 18. A CD contains the softcopy of the MATLAB program

The report must be presented according to the Panduan Penulisan Tesis Gaya UKM (2009) format.

Each KK and KB group has to submit 4 copies of preliminary reports assigned to each of the course lecturers to Pejabat Am JKKP on Wednesday, 25 April 2012, Week 9, no later than 5 pm. Then, the lecturers will return the reports along with the feedbacks and comments to the students in Week 10.

The complete first draft (4 copies for KK and 4 copies for KB) integrated project report is to be submitted on Wednesday, 16 May 2012, Week 12. The report should contain no more than 50 pages excluding the Appendices.

Project Planning

Table 1: Integrated Project Planning Semester II Academic Session 2011-2012

Week

Task

Week 5

Project dissemination through SPIN

Week 9

Process Flow Diagram(PFD) submission: Wednesday 25 April 2012

Week 10

Course Lecturers returning the PFD with comments The whole report compilation and execution. Submission of complete draft : Wednesday , 16 May 2012

Week 10-12

Week 13

Project group presentation: Tuesday, 22 May 2012

Table 2: KK Groups For The Integrated Project Semester II Academic Session 2011-2012 Group Members QURRATU'ANIBINTIINCHEM.ZULFIKRI NORAZIFAHBINTIGHAZALI MUHAMADSHUKRIBINAHMADSHABRI EDNATANAILIN CHIONGSIEWCHIN MUHAMADFARISBINHASMUNI NURULNADIABINTINGAH AHMADRAFDIAHMADZIKRILEH NURFARAYUBINTISUHAIMI ONGBOONCHONG NORILHAMBINMOHAMEDNORIN TANCHINGYEE ADRIANHOIKLIANG MUHAMMADASHRAFB.MOHDAMIRRUZAN MAZNIBINTIJAMALUDIN JANANIA/PVELAYUDHAN FATHIYYAHBINTIMOHDZAINUDIN PANGKWONGYUEN CHANKHANNYE NOORZAIYANBINTIMISYAN KOKILAWANIA/PKRISHNAN AHMADZUHAIRIBINABDULGHAFAR TANCHUNGCHUAN Project Title

Production of propylene glycol

Production of isobutylene

Production of Polybutylene Terephthalate

Production of Isopropyl Alcohol

Production of Benzoic Acid

Production of Dimethyl Ether

Table 3: KB Groups For The Integrated Project Semester II Academic Session 2011-2012 Group Members AINHETIEQABINTIHAMDAN TANYIVON RAFIZIBINSALIHUDDIN Project Title

Production of polyhydroxybutyrate

NORZIELABINTIMAHADIN CHUNGKENVUI Production of Ethanol ERNAERVINANURZIANYBINTIZALANI LOWBEECHAN WONGMEIFANG SONIADILIPPATELA/PDILIPKUMAR MUHAMMADKHAIRILAZIMBINABDULLAH ZURAIFAHBINTIMINHAT MUHAMMADSAFARUDDINB.ABDULRAZAK

Production of Citric Acid

JUDYLOHEAEA FATINATIKAHBINTIKASSIM CHINLEENEE LEONGMANJIET NORASILABINTIKASIM RAJESWARIA/PJAYARAMAN SAWGEOKHOOI

Production of Biodiesel from Algae

Production of Hydrogen from microbe

MUHAMADAZRIBINMDDANIAL JAMILAHBINTIAHMAD Production of LIMKAHHUAY Aspartame TEEZHAOKANG

Evaluation and Assessment of Integrated Project (25 %)

Peer Assessment (20%)

Group Assessment (80%)

Final Report (70%)

Oral Presentation (30%)

Team working Technical Life Long Learning Current Issues Writing Communication

Communications

Style (10%)

Contents (90%)