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CHEMICAL ENGINEERING
DEFINITIO
N
Detector
X-Ray
Source
Powdered
sample
Presentation Title
Your company information
FUNCTIO
N
How it work
Take a tenth of the weight of sample (pure
is better)
Grind sample in powder form. Size less
than ~ 10 m or 200-mesh preferred
Put the sample holder
Must be considered in order to get a flat
surface and get a random distribution of
orientations lattice
SAFETY
x-rays produced by the diffractometer pose a very real danger. Human
tissue can be severely damaged if exposed to the x-rays used in x-ray
diffraction. Long-term, chronic exposures at moderate levels can directly
cause a variety of skin disorders, and chronic relatively low- level
exposures may be a factor resulting in increased cancer risk in exposed
personnel. Although modern XRD equipment includes safeguards
designed to minimize or eliminate radiation in the work environment, an
awareness of the dangers of radiation exposure and associated safety
issues is required for anyone using the x-ray diffractometer.
LITERATURE SITES
http://faculty.olin.edu/~jstolk/matsci/Operating
%20Instructions/Shimadzu%20XRD%20operating
%20instructions.pdf [06 Maret 2015]
http://www.leeds.ac.uk/heritage/Astbury/X_ray_diffractio
n/ [06 Maret 2015]
http://en.wikipedia.org/wiki/Diffractometer [06 Maret
2015]