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Food a fact of life
CRYOGENIC GRINDING
Presented by:
NINGTHOUJAM MANDA DEVI
M.Tech ( 2nd Year )
Reg. no: J4-01245-2013
Processing and Food
Engineering Department
Food a fact of life
What is Grinding
Grinding is a process of reducing the size of solid materials by
mechanical action, dividing them into smaller particles.
Perhaps the most extensive application of grinding in the food
industry is in the milling of grains to make flour, but it is
used in many other processes.
The grinding of corn for manufacture of corn starch, the
grinding of sugar and the milling of dried foods, such as
vegetables
Extension
Grinding process
Grinding size reduction is achieved by fracturing the materials
The material is stressed by the action of mechanical moving
parts
Time also plays a part in the fracturing process and it appears that
material will fracture at lower stress concentrations if these can
be maintained for longer periods of time.
The energy required depends upon the hardness of the
material and also upon the tendency of the material to crack its friability
Food a fact of life
GRINDING EQUIPMENT
Size reduction equipment can be divided into two classes
Crushers : The major action is compressive, breaking large pieces of
solid material into small lumps.
Grinders: Grinders combine shear and impact with compressive forces,
reduce crushed feed to powder form.
Force for reduce the size of food
a)Compression forces
b)Impact forces
c)Shearing(or attrition) forces
-Both the magnitude of the force and the time of application affect the extent
of grinding achieved.
- For efficient grinding, the energy applied to the material should exceed,
by as small a margin as possible, the minimum energy needed to rupture the
material.
Food a fact of life
Crushing head
Stationary jaw
reciprocating jaw
Fig. 2: Gyratory
crusher
Circular plates
Axis of rotation
CRYOGENIC GRINDING
INTRODUCTION
The word CRYOGENICS originates from the Greek word
cryo, which means creation (or) production by means of cold.
It deals with low temperatures as low as below 150 C or 123 K
to absolute zero.
Cryogenics is the study of low temperatures and behavior of
materials under these low temperatures.
A person who studies elements that have been subjected to
extremely cold temperatures is called a CRYOGENICIST.
Cryogens
The extremely low temperature are produced by using substances
called cryogens such as liquid nitrogen and liquid helium.
All cryogenic liquids are gases at normal temperatures and
pressures. So, these gases must be cooled below room
temperature to liquefy them.
They have boiling points below -150C. (Carbon dioxide and
nitrous oxide, which have slightly higher boiling points are
sometimes included in this category).
Cryogens
There are several cryogenic liquids such as Nitrogen, helium,
neon, argon, krypton, hydrogen, methane and liquefied natural
gas etc..
Liquid Nitrogen are the most commonly used.
Cryogens are stored in vessels called as Dewar flask which
provides good insulation
Different cryogens become liquids under different conditions of
temperature and pressure, but all have two properties in common:
they are extremely cold, and small amounts of liquid can expand
into very large volumes of gas
Food a fact of life
Liquid Nitrogen
Nitrogen gas makes up the major portion of the atmosphere
(78.03% by volume).
Inert, colourless, odourless, non-corrosive, non-flammable liquid
Extremely cold (boiling point -195.8C, 77K).
Similar appearance to water.
Volume of expansion liquid to gas (at 15C, 1 atm.) is 682 , i.e. 1
litre of liquid nitrogen evaporated to form 682 litres of nitrogen gas.
CRYOGENIC GRINDING
Also known as freezer milling/ freezer grinding / cryomilling.
is the act of cooling/chilling a material and then reducing it to
smaller particle size
Also a method of powdering herbs at sub-zero temperatures
ranging from 0 to -70F
All materials embrittle when exposed to low temperature
Utilizes the cooling effect of liquid nitrogen to embrittle materials
prior to and or during the grinding process
Food a fact of life
CRYOGENIC GRINDING
Normal grinding processes which do not use a cooling system can
reach up to 200F.
These high temperatures can reduce volatile components and
heat-sensitive constituents in herbs.
But cryogenic grinding process does not damage or alter the
chemical composition of the plant in any way.
Materials which are elastic in nature, having low melting points,
low combustion temperatures , sensitive to oxygen can be
ideally machined by cryogenic grinding process
Food a fact of life
GENERAL APPLICATIONS OF
CRYOGENIC GRINDING
Cryogrinding of steel:
The large amount of heat is generated during
machining/grinding at high speed and feed rate raises the
temperature at the cutting zones excessively.
to overcome this problem liquid nitrogen is fed to the grinding
spot.
Thermoplastics and thermo sets:
To which nylon, PVC, polyethylene, synthetic rubber are
commonly used in powder form, but not limited to, a variety of
applications such as adhesives, powdered coatings, fillers and
plastic sintering and moulding.
Food a fact of life
SPICES
Spices are the most important constituents of Indian food, not only in
household purposes but also in hotels, restaurants, food processing industries
etc.
Spices like Pepper, cinnamon, chilly, Ginger, Cumin seed, Nutmeg, clove
etc., have a characteristic taste and aroma and medicinal values.
These characteristic qualities are essential in them to have their value as
spice.
These qualities exist in them due to the presence of etheric oils within it.
(boiling points ranging down to 50oC)
The heat is developed inside the grinding Temperature below 0oC inside the grinding
mill
mill
The heat, which is developed during Negligible loss of volatile component
grinding, leads on one hand to
evaporation of the essential oil and on
the other hand, heat sensitive fats are
melted.
This in turn can lead to the grinding Not in Cryogenic process
elements become greasy (oily) and even
harms the machine by blocking it.
High energy consumption
High capacity motors are required to Low capacity motors are required to
grind the material
grind the material
No
control on particle size
Food a fact of life
Cryogenic
Grinded
essential oil
content
(ml. Per am.)
Standard
Grounded
essential oil
content
(ml. Per qm.)
5.5
100
5.5
100
3.5
64
Coriander
0.6
100
0.6
100
0.4
67
Black Pepper
2.9
100
2.9
100
1.5
52
Cumin Garam
3.5
100
3.5
100
1.6
46
Garam Masala
4.6
100
4.6
100
2.0
43
Spices
Ungrounded
essential oil
content
(ml. Per gm.)
Turmeric
http://www.cryofoods.com/what-is-cryogenic.asp,
accessed
Food a fact of life
Parameters
Whole Wheat
Cryogenically Ground
Flour
Report Result
Report Result
Energy
364 K cal.
100%
364 K cal.
100%
Protein
11.77 Gm
100%
11.77Gm
100%
Carbohydrates
75.17 Gm
100%
75.17 Gm
100%
Fat
1.83 Gm
100%
1.83 Gm
100%
Saturated fat
0.36 Gm
100%
0.36 Gm
100%
Sodium
25.63 mg/kg
100%
25.63 mg/kg
100%
Cholesterol
0 Gm
100%
0 Gm
100%
Dietary fiber
12.48 Gm
100%
12.48 Gm
100%
http://www.cryofoods.com/what-is-cryogenic.asp,
accessed
Food a fact of life
ADVANTAGES OF CRYOGENIC
GRINDING
Smaller particles size
More uniform particle size distribution
Process cooling/temperature control
Increased throughput
Reduced power consumption
Minimal loss of volatile components
Improves the aroma by minimizing the loss of essential oils when
compared with grinding at normal temperature
Food a fact of life
DISADVANTAGES OF CRYOGENIC
GRINDING
Cryo-grinding do have distinctive advantages over the conventional
cooling processes, but
The application of cryogen in moist atmosphere may cause
formation of ice around the delivery nozzle and the piping
system carrying the cryogen. This may cause a possible blockage
in the delivery system of liquid nitrogen.
Econonomic considerations should be solved.
PRECAUTIONS
1) Be familiar with hazards associated with cryogen use.
2) Work in an open, well-ventilated location.
3) Always wear safety goggles and/or face shield and appropriate
cryogen gloves.
4) Examine containers and pressure relief valves for signs of defect.
5) Ensure that all equipment and containers are free of oil, grease,
dirt, or other materials which may lead to flammability hazard
upon contact with liquid oxygen.
CONCLUSION
As prices for energy and raw materials rise and concern for the
environment makes safe waste disposal difficult and Costly,
resource recovery becomes a vital matter for today's business.
Cryogenic grinding technology can efficiently grind most tough
materials and can also facilitate Cryogenic recycling of tough
composite materials.
It employs a cryogenic process to embrittle and grind materials to
achieve consistent particle size for a wide range of products.
The cryogenic process also has a unique capability for recycling
difficult to separate composite materials.
Food a fact of life
REFERENCES
1. http://en.wikipedia.org/wiki/Cryogenics, accessed on 28 November 2014.
2. http://www.cryofoods.com/what-is-cryogenic.asp, accessed on 28-11-14
3. http://www.nzifst.org.nz/unitoperations/sizereduction1.htm, accessed on 2212-14
4. http://www.angrau.ac.in/media/10829/fden223fpequii.pdf, accessed on 2212-14.
5. ICAR. 2014. Studies on Cryogenic Grinding for Retention of Flavour and
Medicinal Properties of Some Important Indian Spices. Final Report of NAIP
component-4 Sub-Project on Basic and Strategic Research in Frontier Areas of
Agricultural Sciences. 2009-2014. CIPHET, Ludhiana. 60p.
6. http://en.wikipedia.org/wiki/Cryogenic_grinding, accessed on 27-12-14.
7.
8.
9.
10. K.K. Singh and T.K. Goswami (1999) Design of a cryogenic grinding
system for spices, Journal of Food Engineering ,39 (359-368).