Beruflich Dokumente
Kultur Dokumente
Column
Done by:
Amal Jamal Eddin 1050893
Sara Alhallaq 1051713
Zaina AlDhaheri 1046702
Saniha Aysha Ajith 1051470
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Introduction
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Absorption - Selected components are removed
from a gas mixture depending on their relative
solubility in a specific liquid.
Two types
Physical Chemical
Absorption Absorption
Examples: Absorption
Example: Removal of
of carbon dioxide using
ammonia, sulfur dioxide,
sodium carbonate
carbon dioxide or acetone
solution and Scrubbing
from a mixture with air
ammonia from gas
using water
stream using acid solution
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Packed bed columns
• Hollow columns filled with
small packing pieces
• Liquid stream is introduced
at the top and a gas stream
at the bottom
• Absorbed component
leaves at bottom while he
unabsorbed components
from top.
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• Packing inside the column: available in
different shapes and types of material
• Increase the surface area to provide better
transfer
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Theory
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Loading point – lowest gas flow where surface is wetted and gas
impedes the liquid.
Flooding point – Point where gas will force liquid out of top of
the column.
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𝐾𝑖𝑠𝑡𝑒𝑟𝑠 𝐶𝑜𝑟𝑟𝑒𝑙𝑎𝑡𝑖𝑜𝑛:
∆𝑃𝑓𝑙𝑜𝑜𝑑𝑖𝑛𝑔 = 0.115 𝐹𝑃0.7
𝐸𝑐𝑘𝑒𝑟𝑡 𝑃𝑙𝑜𝑡
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𝐺𝑦2 𝐹𝑝 𝜇0.1 F=
𝐺𝑥 𝜌𝑦
Capacity factor, ψ = 𝐺𝑦 𝜌𝑥 − 𝜌𝑦
𝜌𝑥 − 𝜌𝑦 𝜌𝑦
𝐺𝑦2 𝜇0.1
Transport property factor, φ =
(𝜌𝑥 − 𝜌𝑦 )𝜌𝑦
1 1
Zena Correlation: 𝑉 + 𝑄 = 𝐶𝑜𝑛𝑠𝑡𝑎𝑛𝑡
3 2
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Main constituents of a packed bed
column
• Glass Raschig rings
• A water storage tank
• A centrifugal pump
• A centrifugal air blower
• Sensors
Electronic flow meter
Temperature Sensors
Electronic air flow sensor
Electronic pressure sensors
• An electric console box.
(pressure drop ,flow rates and temperatures
readings)
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Procedure
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• Switch on the water pump and set it to a flow rate of 2 L/min.
1 • Let the water completely wet the column and stabilize.
•Open the valve to let the air flow start and set it to 20 L/min
2 •Note down P1 and P2 (pressure differential).
•Continue increasing the air flow rates in equal intervals of 10 L/min , note down
3 P1 and P2 , and record both loading and flooding points.
•Repeat previous steps for the water flow of 5 L/min,6 L/min , 7 L/min, 8 L/min.
•For water floe rates of 7 and 8 L/min increase air flow rates in equal intervals of 5
5 L/min since loading and flooding points appear faster.
• Turn off the air line, decrease the water flow rate to 0 L/min, switch off the water
6 pump and finally close turn off the power supply.
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Safety
Considerations
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Wear appropriate PPEs including: Lab coats
Safety goggles
Hard covered shoes
Durable clothing and high-impact gloves.
Mechanical hazards: Explosion through the top of the packed bed column.
Solution: switch off the air supply into the column.
Physical hazards: The huge size of equipment Solution: It should be handled with
care.
Loud noise Solution: wear ear protection gear if necessary.
Electrical hazards: Using the electrical console and wiring with wet hands
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Data Collected
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Water flow rate of 2 (L/min)
Gas Flow Pressure
T1 T2 P1 P2
rate Differential P1+ Remarks
(L/min)
(oC) (oC) (mbar) (mbar)
P2 (mbar)
20.0 19.6 20.0 0.0 0.0 0.0
30.0 19.6 20.0 0.2 0.1 0.3
40.0 19.6 20.0 0.4 0.3 0.7
No loading or
50.0 19.5 20.0 0.6 0.5 1.1
flooding points
60.0 19.6 20.1 0.8 0.7 1.5
70.0 19.6 20.1 1.3 1.0 2.3
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Results
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Water Gy 𝑷𝟏 + 𝑷𝟐 log Gy 𝑷𝟏 + 𝑷𝟐
flow rate 𝒌𝒈 𝐥𝐨𝐠
𝑳 𝑳
[L/min] [ 𝟐 ]
𝒎 .𝒔 𝒎𝒃𝒂𝒓
[ ]
𝒎𝒊𝒏
2 0.08 0.00 -1.09
0.12 0.21 -0.91 -0.67
0.16 0.50 -0.79 -0.30
0.20 0.79 -0.69 -0.10
0.24 1.07 -0.61 0.03
0.28 1.64 -0.55 0.22
Water Gy 𝑷𝟏 + 𝑷𝟐 log Gy 𝑷𝟏 + 𝑷𝟐
flow rate 𝒌𝒈 𝐥𝐨 𝐠
[ 𝟐 ] 𝑳 𝑳
𝒎 .𝒔
[L/min] 𝒎𝒃𝒂𝒓
[ ]
𝒎𝒊𝒏
5 0.08 0.29 -1.09 -0.54
0.12 0.93 -0.91 -0.03
0.16 1.86 -0.79 0.27
0.20 3.21 -0.69 0.51
0.24 5.21 -0.61 0.72
0.28 8.36 -0.55 0.92
Water Gy 𝑷𝟏 + 𝑷𝟐 log Gy 𝑷𝟏 + 𝑷𝟐
flow 𝒍𝒐𝒈 ( )
𝒌𝒈 𝑳 𝑳
rate [ ]
𝒎𝟐 . 𝒔 𝒎𝒃𝒂𝒓
[L/min] [ ]
𝒎𝒊𝒏
6 0.08 0.50 -1.09 -0.30
0.12 1.79 -0.91 0.25
0.16 4.29 -0.79 0.63
0.20 7.14 -0.69 0.85
0.24 15.50 -0.61 1.19
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Water Gy 𝑷𝟏 + 𝑷𝟐 log Gy 𝑷𝟏 + 𝑷𝟐
flow rate 𝒌𝒈
𝒍𝒐𝒈 ( )
[ 𝟐 ] 𝑳 𝑳
𝒎 .𝒔
[L/min] 𝒎𝒃𝒂𝒓
[ ]
𝒎𝒊𝒏
7 0.08 1.00 -1.09 0.00
0.10 3.57 -0.99 0.55
0.12 6.36 -0.91 0.80
0.14 8.57 -0.85 0.93
0.16 11.43 -0.79 1.06
0.18 19.50 -0.74 1.29
Water Gy 𝑷𝟏 + 𝑷𝟐 log Gy 𝑷𝟏 + 𝑷𝟐
flow 𝒌𝒈
( ) 𝒍𝒐𝒈 ( )
[𝒎𝟐 .𝒔] 𝑳 𝑳
rate
[L/min]
8 0.08 3.36 -1.09 0.53
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Log pressure losses gradient vs. log gas flow rate
2.00
1.50
0.50
0.00
-2.00 -1.80 -1.60 -1.40 -1.20 -1.00 -0.80 -0.60 -0.40 -0.20 0.00
-0.50
-1.00
Log Gy (kg/m2.s)
Water Flow Rate 2(L/min) Water Flow Rate 5(L/min) Water Flow Rate 6(L/min)
Water Flow Rate 7(L/min) Water Flow Rate 8(L/min)
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Pressure drop packing factor, Fp, using experimental pressure drop at
flooding
0.00350
0.00250
0.00200
0.00150
0.00100
0.00050
0.00000
0.00000 0.00001 0.00001 0.00002 0.00002 0.00003 0.00003 0.00004
Transport property factor (𝝋)
Slope of the plot = 123.73, which is equal to the pressure drop packing factor, Fp.
The error is equal to 81.78%.
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Experimental Eckert plot based on the experimental data:
Gx Capacity
Gy
Water Flow Air flow Flow factor factor
𝒌𝒈
[L/min] [ 𝟐 ] [L/min] 𝒌𝒈 [F]
𝒎 .𝒔 [ ]
𝒎𝟐 .𝒔 [Ψ]
20 0.08 2.86 0.0003
30 0.12 1.91 0.0007
40 0.16 1.43 0.0013
2 6.63
50 0.20 1.14 0.0021
60 0.24 0.95 0.0030
70 0.28 0.82 0.0040
20 0.08 7.15 0.0003
30 0.12 4.76 0.0007
40 0.16 3.57 0.0013
5 16.58
50 0.20 2.86 0.0021
60 0.24 2.38 0.0030
70 0.28 2.04 0.0040
20 0.08 8.58 0.0003
30 0.12 5.72 0.0007
6 19.89 40 0.16 4.29 0.0013
50 0.20 3.43 0.0021
60 0.24 2.86 0.0030
20 0.08 10.01 0.0003
25 0.10 8.00 0.0005
30 0.12 6.67 0.0007
7 23.21
35 0.14 5.72 0.0010
40 0.16 5.00 0.0013
45 0.18 4.45 0.0017
20 0.08 11.44 0.0003
25 0.10 9.15 0.0005 26
8 26.52
30 0.12 7.62 0.0007
Experimental Eckert Plot
0.0045
0.004
0.0035
0.0025
0.002
0.0015
0.001
0.0005
0
0 1 2 3 4 5 6 7 8 9 10 11 12 13
Flow Factor (F)
Water Flow Rate 2(L/min) Water Flow Rate 5(L/min) Water Flow Rate 6(L/min)
Water Flow Rate 7(L/min) Water Flow Rate 8(L/min)
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Calculations of pressure drop packing factor from the
experimental Eckert plot
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Zena Correlation:
Gx Gy
V Q
𝒌𝒈 𝒌𝒈 V1/3 + Q1/2
[ 𝟐 ] [ 𝟐 ] [ft3/ft2.min] [Gal/ft2.min]
𝒎 .𝒔 𝒎 .𝒔
16.58 0.28 45.69 24.41 8.52
19.89 0.24 39.16 29.29 8.81
23.21 0.18 29.37 34.18 8.93
26.52 0.14 22.84 39.06 9.09
Average 8.84
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Sample Calculations
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EP
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Conclusion
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Packed Bed Column experiment is important to
learn, observe and determine the flooding and
loading points.
It was recognized that the pressure drop increases
as the gas flow rate increases.
At higher water flow rates, the flooding and loading
points were observed faster.
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How to improve the experiment?
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Any Questions?
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• [1] E. Gomes and I. Zuburtikudis, Heat Exchanger Experiment. Abu Dhabi: Abu Dhabi
University, 2017.
• [2] "Experiment (5) Absorption with Chemical Reaction", 2017. [Online]. Available:
https://classes.engineering.wustl.edu/2009/fall/che473/handouts/PackedBed.pdf. [Accessed:
28- Oct- 2017].
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