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Field service training 18.

October 2010

Radiation-based process instrumentation

Agenda
Why nucleonic measurement? The nucleonic measuring principle Typical industries and markets Application examples Don't be afraid of gamma radiation PROTRAC: typically VEGA plics the idea with a future Configuration and parameter adjustment Source container shipping

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Reliable measurement technology for extreme process conditions


Why nucleonic measurement?
Suitable for extreme conditions Measuring principle works without contact to process medium High reliability of the measuring principle Some application areas still allow no other alternative to nucleonic measurement

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The nucleonic measuring principle


A familiar measuring principle
The principle is based on the radiation emitted by radioactive isotopes Isotopes are mounted into a source holder The radiation is damped when penetrating material A detector mounted to the tank receives the radiation and converts it into an electrical signal The detector calculates the level, density or concentration of the measured product from the received (attenuated) radiation

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Nucleonic measurement technology


Application areas
1

Level switching (1) Continuous level (2) Density and concentration as well as flow measurement of liquids (3) Interface measurement (4)

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Typical industries and markets


Special application areas
Chemical industry Petrochemical industry Metal processing Oil and gas Pulp and paper Energy production Aggregates and mining Cement industry

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Application example density


Flue gas desulfurization
Emission protection through flue gas desulfurization in coal power stations Lime milk suspension binds sulphur dioxide Concentration measurement of the lime milk by means of density measurement Lime milk is very abrasive

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Application example density


Flue gas desulfurization
Emission protection through flue gas desulfurization in coal power stations Lime milk suspension binds sulphur dioxide Concentration measurement of the lime milk by means of density measurement Lime milk is very abrasive

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Application example point level


Cellulose production
In cellulose production, wood chips are broken down chemically with the help of a cooking liquor In a special reactor, the cooking liquor is regenerated so that it can be used again Temperature 160 C, pressure 10 bar Aggressive process conditions The maximum level in the reactor must be monitored

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Application example point level


Cellulose production
In cellulose production, wood chips are broken down chemically with the help of a cooking liquor In a special reactor, the cooking liquor is regenerated so that it can be used again Temperature 160 C, pressure 10 bar Aggressive process conditions The maximum level in the reactor must be monitored

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Application example level


Polyester melt reactor
Its almost impossible to imagine our lives without polyester This versatile plastic is created in a polyester melt reactor Process temperature 220 C The vessel is enclosed in a heating jacket Rotation of the container Nucleonic measurement has proven itself worldwide in this application

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Application example level


Polyester melt reactor
Its almost impossible to imagine our lives without polyester This versatile plastic is created in a polyester melt reactor Process temperature 220 C The vessel is enclosed in a heating jacket Rotation of the container Nucleonic measurement has proven itself worldwide in this application

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Application examples point switch


Measurement in cyclones in cement applications
In the lower part of the cyclone, buildup often occurs which results in blockage To avoid downtimes, the cyclone must be monitored for buildup and possible clogging Compressed air can prevent clogging, however, over a longer period can damage the refractory lining The thickness of the buildup must be monitored, to activate removal with compressed air, if necessary

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Application examples point switch


Measurement in cyclones in cement applications
In the lower part of the cyclone, buildup often occurs which results in blockage To avoid downtimes, the cyclone must be monitored for buildup and possible clogging Compressed air can prevent clogging, however, over a longer period can damage the refractory lining The thickness of the buildup must be monitored, to activate removal with compressed air, if necessary

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Don't be afraid of gamma radiation


Highest sensitivity
Detectors of the PROTRAC series are extremely sensitive Conventional Geiger-Mueller counters do not even respond here Remarkable measuring precision and quick response times Advantage
Reduction of source activity

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PROTRAC: typically VEGA!


A high degree of safety
Integrated safety functions Self monitoring and diagnosis Asset Management System Developed acc. to IEC 61508 Qualified up to SIL2 NEW
VEGA is the first supplier to offer level, point level and density instruments with SIL

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plics The idea with a future


Simpler is better
plics makes everything simpler From selection to ordering to setup The modular system can be exactly adapted to the measuring task plics allows unrestricted selection and combination of sensors, process fitting, electronics and housings Advantage:
Simple planning, short delivery time, uncomplicated connection, fast setup and commissioning

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plics Electronics

Anzeige- und Bedienmodul

4 20 mA HART Features

Profibus PA

Foundation Fieldbus

 Relay output  Analogue and digital inputs  Serial multi-gauge communication bus  Qualified up to SIL2  Simple electronics exchange

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plics Housing

Aluminium

Stainless steel

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plics Indicating and adjustment module

PLICSCOM

VEGACONNECT

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Configuration and parameter adjustment


One module for all plics instruments
Simple adjustment via four compact membrane keys Measured value indication with unit Clear text with graphical elements Lighting (optional) Device information Diagnostics messages

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PLICSCOM Easy and informative


Display
Measured value indication with unit Plain text with graphic elements Multilingual menu Lighting

Simple navigation
Clear menu structures Tree structures Unambiguous terms

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plics Sensor system

NEW

PVT scintillator

Flexible plastic scintillator

NaI crystal

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Source container VEGASOURCE

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Design of the source container VEGASOURCE


Benchmarking data
Small space requirement and simple mounting Safe and easy source replacement Padlock for fixing the function settings Pneumatic switch-ON / switch-OFF Collimation angle 5, 20 and 40 Fire-proof version 821C / 30 min. (according ISO 7205, IEC 60405, AERB/SS/2, ANS N538)

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Design of the source container VEGASOURCE


Benchmarking data
Small space requirement and simple mounting Safe and easy source replacement Padlock for fixing the function settings Pneumatic switch-ON / switch-OFF Collimation angle 5, 20 and 40 Fire-proof version 821C / 30 min. (according ISO 7205, IEC 60405, AERB/SS/2, ANS N538)

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Design of the source container VEGASOURCE


Benchmarking data
Small space requirement and simple mounting Safe and easy source replacement Padlock for fixing the function settings Pneumatic switch-ON / switch-OFF Collimation angle 5, 20 and 40 Fire-proof version 821C / 30 min. (according ISO 7205, IEC 60405, AERB/SS/2, ANS N538)

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Design of the source container VEGASOURCE


Engineering design
Model A (Standard)

Figure: VEGASOURCE 35
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Figure: VEGASOURCE 31

Design of the source container VEGASOURCE


Benchmarking data
Weight with manual ON/OFF: SE31 app. 40 kg SE35 app. 87 kg Weight with pneumatic ON/OFF: SE31 app. 50 kg SE35 app. 97 kg Max. Cs-137 loading: SE31: 600 mCi /22,2 GBq SE35: 3.000 mCi / 111 GBq Max. Co-60 loading: SE31: 20 mCi / 740 MBq SE35: 100 mCi / 3,7 GBq Montingflange: DN100 PN16 Ambient temperature: -40 C ... +200 C
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Design of the source container VEGASOURCE


Altitude 12,500 m 5.0 8,848 m 1.0

Equivalent dose
The equivalent dose defines the energy dose taken in by the body through ionising radiation Measurement unit for the dose rate is the microsievert/hour (Sv/h) The sievert (Sv) unit is a measure of the biological effects of radiation The largest exposure results from a medical x-ray examination The dose rate a radiation source generates depends on the activity and the distance

Mount Everest

Scintillation detector

1.0

Zugspitze

2,962 m 0.1 0m 0.01 Dose rate in Sv/h

Venice

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Mounting instructions

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Mounting instructions
Mounting position for cont. level
The source container must be mounted at the height of, or slightly above, the max. level The radiation must be aligned exactly with the detector The source container and detector should be mounted as close as possible to the vessel to avoid control zones An gap between source container and vessel must be blocked off and marked. In general two or more source containers are used for large measuring ranges

Radiation-based process instrumentation Page 32 31 August 2011 Roland Bonath

Mounting instructions
Mounting position for cont. level
The source container must be mounted at the height of, or slightly above, the max. level The radiation must be aligned exactly with the detector The source container and detector should be mounted as close as possible to the vessel to avoid control zones An gap between source container and vessel must be blocked off and marked. In general two or more source containers are used for large measuring ranges

Radiation-based process instrumentation Page 33 31 August 2011 Roland Bonath

Mounting instructions
Mounting position for cont. level
The source container must be mounted at the height of, or slightly above, the max. level The radiation must be aligned exactly with the detector The source container and detector should be mounted as close as possible to the vessel to avoid control zones An gap between source container and vessel must be blocked off and marked. In general two or more source containers are used for large measuring ranges

Radiation-based process instrumentation Page 34 31 August 2011 Roland Bonath

Mounting instructions
Mounting position for point level
The source container version with an collimation angle = 5 is recommended for point level If larger collimation angle (20 or 40) are used, ensure that the ray is horizontal For this purpose, mount the radiation source container in such a way that the eyelet is positioned horizontally.

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Mounting instructions
Mounting position for density
The most constant conditions for density measurement in pipes are achieved if the unit is mounted on vertical pipes If only horizontal pipes are accessible, the path of the ray should also be arranged horizontally to reduce the influence of air bubbles and build-up. In order to achieve a longer path of the radiation through the medium and thus a larger measuring effect

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Pipe mounting bracket KV31

Figure: Pipe mounting bracket KV31 - vertical detector mounting


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Pipe mounting bracket KV31

Figure: Pipe mounting bracket KV31 - horizontal detector mounting


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Pipe mounting bracket KV31

Figure: 30 pipe mounting bracket KV31 with diagonal beam


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Mounting accessoires

Figure: L-bracket PTB3 for FIBERTRAC and MINITRAC


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Setup / Adjustment

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Configuration and parameter adjustment


Communication with all systems
PLS/SPS

Standard communication protocols are available for adjustment and connection in process automation
4 20 mA /HART Profibus PA and Foundation Fieldbus

VEGAMET

All settings can be made with one adjustment software (DTM or EDD) Simple setup is also possible via the indicating and adjustment unit PLICSCOM

AMS/ PDM DTM


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EDD

EDD

Service and diagnosis Asset Management


Asset management functions
Failure Maintenance

Function control

Standardized status messages acc. to NE 107 or VDI/VDE 2650 Detailed diagnosis in the instrument with cleartext display Digital transmission via HART, Profibus and Foundation Fieldbus

Out of specification

Preventive maintenance
Early recognition of malfunctions Diagnosis evaluation with PACTware 4.0 Simplified servicing

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Configuration and parameter adjustment


Background calibration
80

The background calibration is necessary in order to register the natural background radiation The pulse rate of this background radiation is automatically subtracted from any other measured pulse rate

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Configuration and parameter adjustment


Full calibration
185

The radiation is switched on Most of the Gammaphotones will be blocked by the liquid The pulse rate is low Background pulse rate of the background radiation is automatically subtracted

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Configuration and parameter adjustment


Empty calibration
3891

The radiation is switched on Within the measuring range, the vessel is emptied as far as possible Ideally: 0%, maximum 40% Background pulse rate of the background radiation is automatically subtracted

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Configuration and parameter adjustment


Measuring mode
1941

The amount of pulse rate depends on the filling level An low number of pulses means an high filling level of the vessel The measured pulse rate is inverse proportional to the filling level An detailed relation between filling level and pulse rates is defined by the Linearization curve

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Configuration and parameter adjustment


Density measurement
For density and concentration measurements the MINITRAC needs the two parameters:
899

The absorption coefficient of the measured material The reference pulse rate Io

sample 1

For many applications an one-point calibration is sufficient This calibration point should be located as near as possible to the operating point If high accuracy is required over the complete measuring range two or more calibration points should be applied.
sample 1

DTM
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Configuration and parameter adjustment


Density measurement
The calibration points for an multiple point calibration should be located as far from each other as possible The calibration points should be uniformly distributed over the measuring range

1491

sample 2

sample 2

DTM
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Configuration and parameter adjustment


Density measurement
After the calibration points have been entered, the MINITRAC automatically calculates the linearization curve For recalibration (e.g. buildups in the pipe) the parameter real value correction can used The absorption coefficient is kept unchanged from the original calibration

1491

sample 1

sample 2

I = 10 * e - * roh * d
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Configuration and parameter adjustment


DTM Device Type Manager
Device DTM Driver for field devices and Remote I/O Communication DTM Driver for communication protocols such as Profibus, Foundation Fieldbus Provides all instrument-specific data and functions Runs in different frame applications such as PACTware, ABB, etc.

LIVE Demo

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Configuration and parameter adjustment


Electrical connection
Two connection chambers are available Depending on the instrument version the signal output is either in the primary or in the secondary chamber
Primary terminal connections

Secondary terminal connections


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Configuration and parameter adjustment


Primary terminal connections 1. 2. 3. 4. 5.
Primary terminal connections

Power supply Power supply 4 20 mA active output (only explosion protected devices) 4 20 mA passive output (only explosion protected devices) 4 20 mA input Switching input open collector Switching input relay contact Switching output (NPN transistor Multisensor communication bus 2x address switches for MGC

6. 7. 8. 9. 10.

Secondary terminal connections 1. 2. 3.


Secondary terminal connections
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4 20 mA output option (IS safe devices) PLICSCOM connection Connections for external indication (VEGADIS) Ground connection

4.

Configuration and parameter adjustment


Density calibration example
Density calibration One point calibration Min. process value: 1,5 kg/m Max. process value: 3,0 kg/m Pipe diameter 200 mm Pulse rate for density 3,0 kg/m: 1000 ct/s Pulse rate for density 1,0 kg/m: 3000 ct/s

Lesson:
Setup the gauge Build an linearization curve

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Source container shipping

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Source container shipping


Source loading
Eckert & Ziegler load the VEGASOURCE container Eckert & Ziegler labels the type plate Eckert & Ziegler ship the source container direct to the end user

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Source container shipping

1. Serial number VEGASOURCE container 2. Order code 3. Document ID 4. Radiation angle 5. Local dose rate at a defined distance from the surface

6. Wording "Hochradioaktive Strahlenquelle" (highly radioactive source), depending on activity 7. Isotope (Cs-137 or Co-60) 8. Serial number of the source capsule 9. Source activity in Bq and mCi 10. Manufacturing date of the source capsule

Radiation-based process instrumentation Page 57 August 31, 2011 Roland Bonath

Editorial
Field service training radiation-based process instrumentation Version: EN 18 October 2010

VEGA Grieshaber KG Am Hohenstein 113 77761 Schiltach Germany Phone +49 7836 50-0 Fax +49 7836 50-201 E-mail info@de.vega.com www.vega.com

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