Tnshumntal malhods of Analynis P7olT

Uoit-
Inatumuntokon_o Ga Chromalgrabhy. (for9) Dr. Parjanya Shukla

Dtectovs - Dr. M. P. Singh Clases

x The ohulad soluts poiclus olong wih Ke coriAT gas

exit rom column and entor +ke datector.

Ke datocors Ken produu aluchical signals proporkonal to

Comunhahion 6oluta.
The ignals 07 omplijiad and sucorded as peaks at
intarv &ls on chromadograph.
(a) ThaTma Cmduchivity DetactorA (T¢D):-
Ako callud Dilunha Thurmal Conduchivihy Detacbor (D7Co) .

Th prinuipb d Ki dutacor is hat

keat Joss fhom o didaman and uistanu d, o

wiTs tKrough wh'ch o' Cumant is looing is dibonda
upon tksKermal conduchvity dtKi àas in which
i immThRd.
www. Amplifier and
recorder

Whan only Comier gas Jows

hal Jon to meta block ts Attenuator

Convtont ilomand temp. amains w

R
Bartery (Direct
curTent sOurce)
MA
CmAtanf Wheatstone

brndge
arraingcnient Bridge
voltage

whun an onalyts speie low and ww-

N

Reference
N control Sensing
Cavily
filament Voltmeter cavity
filament

pas lomint
hevmal cmduchvity chong which Metal block

s Aanaad by wheat ston bidae

- Reference gas

aYTangement. C - Eluent

By-Dr.0Mahndio Pratab Sing

x Tha imbalanu brtw un uurenu R) and
AphAing (S) ouments ov ilomnt tembavotwre Dr.
Paanya
&
Shukla

Dr. M. P. Singh Classe

smuasurs d and o signa is uord1d.

Advantoqes
i m b l t and inexpensive
Durablu and has long Ufa.
hoviclus ocuraks uula.
Non- Asluchve s0 known a univeYAal detetom.
Disadvontaqes
Adw Semitivity.
Aechad by
by uebuahon in temparakurs and low
Hate.

(b) Elckon Captura Dakachora-(e cD)

Th elhcbon affinity o diftunt Aubstan u can bs usud
as R
K basis or an oni2ahom detecor

known as Ki ehchon captura delechor

(4 ponds to ony hoss Compounds whos.a moliculis have
an
oflinih or aucrons 2.9. chlorinakad combounds, alky!
Juud eh.)
A oi mads osHadioochve Cakodu-)
meal bku Ni 6 or htanium
ihide isplaud insidu o lon Rodioachivu
doil.
talon Coatod ull Coaing
* contain a cahods and an
gnodu o1 luchon movamont

By-DY.Mohndyo haBab Sing Anods C)

Tnlt d Column elllunt

The aluchons emiHad om Modioochve souu hov
Auia'an onergy to exut ofoms of Dr. Parjanya Shukla
&
"CoTTiAY Dr. M.P. 8ingh Classes

#Rdlps in ioniging alutad samble

Th men prodaud as asusult o lonizahan d aluka
o ucoTds d in tKi om o peak

s kulhs to
idankfy R compounds
C)fJoms Tonizakion Detachor (C1D):-
xWhn 07gonit combounds oYA inhoduud into o hydrogan-02
o7
ydrogan ar. lom
Kuy ge ionigad Ku pro duu caman
((orir gas produu Jow vsl d unant or no urant)

o tk unan! þroduud rom &ombls ionizabon is daached.

Ra cordur

Amplitier

PJoinum Tah (+)- Echaust

Colador plab (t)-

D Pows
Hydrogen lona Supbly

Oxidont
Hydroqen

Eunt rom column